#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:48:13 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181293 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/71/2237168.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237168_Fobs loop_ _publ_author_name 'Praveen, A.S.' 'Jasinski, Jerry P.' 'Krauss, Shannon T.' 'Yathirajan, H. S.' 'Narayana, B.' _publ_section_title ; 6-(3-Chlorophenyl)imidazo[2,1-b][1,3,4]thiadiazole ; _journal_coeditor_code IM2414 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o66 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.269 _cell_angle_gamma 90.000 _cell_length_a 5.4380 _cell_length_b 12.4222 _cell_length_c 14.1684 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8083 _cod_data_source_file im2414Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 203.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 140.12 164.38 7.91 o 4 0 0 847.67 744.32 40.87 o 6 0 0 5.89 6.27 2.75 o 1 1 0 10.09 10.23 2.25 o 2 1 0 915.83 1024.83 15.80 o 3 1 0 1168.43 1092.49 29.40 o 4 1 0 3.19 2.99 1.54 o 5 1 0 610.19 569.34 18.85 o 6 1 0 66.04 74.07 5.42 o 0 2 0 344.16 388.15 8.45 o 1 2 0 1898.19 2187.44 103.22 o 2 2 0 280.86 320.44 8.47 o 3 2 0 4498.23 4162.15 314.21 o 4 2 0 28.52 36.49 5.90 o 5 2 0 143.74 137.56 10.09 o 6 2 0 0.70 2.39 2.13 o 1 3 0 152.34 178.60 5.01 o 2 3 0 26.13 16.71 1.92 o 3 3 0 123.14 119.01 6.63 o 4 3 0 231.25 189.91 13.57 o 5 3 0 0.53 -0.36 2.63 o 6 3 0 0.65 0.48 1.78 o 0 4 0 9288.63 9443.88 447.11 o 1 4 0 69.00 71.88 4.04 o 2 4 0 571.72 662.94 21.16 o 3 4 0 18.29 16.72 3.00 o 4 4 0 960.25 923.99 33.26 o 5 4 0 2.67 -0.85 2.64 o 6 4 0 0.50 0.95 1.52 o 1 5 0 142.51 174.89 7.18 o 2 5 0 8.91 16.97 2.29 o 3 5 0 28.44 20.25 3.17 o 4 5 0 68.15 60.93 7.60 o 5 5 0 63.99 62.55 12.11 o 6 5 0 229.29 250.83 9.04 o 0 6 0 2568.22 2556.87 60.39 o 1 6 0 425.95 425.01 16.60 o 2 6 0 19.33 12.32 2.20 o 3 6 0 465.91 463.35 17.27 o 4 6 0 18.19 10.69 3.66 o 5 6 0 50.24 54.37 7.46 o 6 6 0 17.96 20.94 3.35 o 1 7 0 109.73 89.63 5.71 o 2 7 0 408.21 408.58 25.02 o 3 7 0 1990.00 1936.06 166.49 o 4 7 0 98.52 107.08 8.81 o 5 7 0 268.43 308.31 14.30 o 0 8 0 3819.98 3270.30 113.11 o 1 8 0 41.85 49.46 5.68 o 2 8 0 59.87 61.52 5.89 o 3 8 0 74.40 86.43 6.59 o 4 8 0 607.69 620.58 20.21 o 5 8 0 78.32 95.90 8.26 o 1 9 0 4.88 4.24 2.09 o 2 9 0 221.30 206.67 7.70 o 3 9 0 71.56 76.06 6.32 o 4 9 0 90.42 93.40 8.07 o 5 9 0 33.10 27.03 3.54 o 0 10 0 73.16 59.28 6.34 o 1 10 0 269.14 261.63 10.29 o 2 10 0 6.42 6.45 2.28 o 3 10 0 348.97 346.66 15.62 o 4 10 0 183.32 209.69 14.25 o 1 11 0 609.44 571.88 25.08 o 2 11 0 41.66 38.00 4.50 o 3 11 0 283.39 281.34 13.57 o 4 11 0 60.65 61.88 6.40 o 0 12 0 373.48 319.02 18.59 o 1 12 0 575.15 555.11 21.72 o 2 12 0 31.36 29.34 4.60 o 3 12 0 34.79 37.13 4.36 o 4 12 0 0.52 -1.89 1.95 o 1 13 0 2.45 1.31 1.62 o 2 13 0 785.41 836.34 23.61 o 3 13 0 8.42 11.82 2.16 o 0 14 0 66.05 71.33 10.15 o 1 14 0 4.68 3.84 2.65 o 2 14 0 84.75 91.84 5.77 o 1 15 0 618.56 772.76 32.24 o -5 0 1 20.05 21.35 4.68 o -3 0 1 1342.79 1251.96 161.01 o -1 0 1 14557.00 13632.47 262.14 o 1 0 1 982.34 873.74 127.28 o 3 0 1 331.84 353.34 16.04 o 5 0 1 263.69 248.06 16.82 o -6 1 1 1065.45 1014.07 24.04 o -5 1 1 472.04 426.73 15.92 o -4 1 1 228.56 193.70 10.63 o -3 1 1 9.30 3.94 1.64 o -2 1 1 4160.35 3856.16 121.00 o -1 1 1 54.49 50.14 2.77 o 0 1 1 333.04 290.77 42.13 o 1 1 1 1199.66 1236.63 27.89 o 2 1 1 824.13 870.71 18.87 o 3 1 1 2143.30 2115.65 54.17 o 4 1 1 4.55 4.85 4.50 o 5 1 1 36.45 30.93 4.20 o 6 1 1 268.33 283.66 12.59 o -6 2 1 254.04 264.47 10.45 o -5 2 1 38.64 37.56 4.63 o -4 2 1 0.61 4.56 2.92 o -3 2 1 137.75 149.83 6.63 o -2 2 1 1.84 2.74 1.47 o -1 2 1 0.97 3.08 0.75 o 0 2 1 21.74 22.69 1.31 o 1 2 1 2279.20 2445.52 43.77 o 2 2 1 404.28 387.19 13.76 o 3 2 1 191.38 183.38 9.00 o 4 2 1 239.42 246.46 12.52 o 5 2 1 250.81 260.44 17.18 o 6 2 1 302.72 315.22 15.56 o -6 3 1 43.19 40.46 4.68 o -5 3 1 376.10 422.35 15.61 o -4 3 1 17.12 16.86 4.03 o -3 3 1 2145.11 2207.51 52.74 o -2 3 1 2603.84 2449.80 128.58 o -1 3 1 1457.32 1447.07 28.18 o 0 3 1 2460.74 2499.95 94.85 o 1 3 1 788.70 764.26 23.34 o 2 3 1 29.46 20.91 2.08 o 3 3 1 1551.30 1525.75 43.37 o 4 3 1 3.37 5.54 2.49 o 5 3 1 18.59 21.27 4.96 o 6 3 1 9.30 10.99 2.58 o -6 4 1 2.12 5.10 2.62 o -5 4 1 200.80 191.34 14.48 o -4 4 1 198.12 172.34 9.11 o -3 4 1 220.19 224.32 10.43 o -2 4 1 43.07 44.39 3.55 o -1 4 1 19.06 22.64 2.36 o 0 4 1 2504.28 2679.09 155.71 o 1 4 1 56.97 67.61 3.76 o 2 4 1 190.58 204.05 12.72 o 3 4 1 836.44 1047.94 31.95 o 4 4 1 147.44 127.20 11.20 o 5 4 1 181.81 190.42 30.64 o 6 4 1 31.10 38.06 4.05 o -6 5 1 816.36 874.96 20.40 o -5 5 1 21.76 30.25 5.84 o -4 5 1 7.76 7.90 3.42 o -3 5 1 3.79 9.74 2.39 o -2 5 1 3576.93 3914.51 69.71 o -1 5 1 574.49 571.91 13.79 o 0 5 1 768.29 703.30 28.42 o 1 5 1 838.58 839.55 22.39 o 2 5 1 988.90 1032.06 29.54 o 3 5 1 5.09 7.66 2.12 o 4 5 1 140.63 143.86 12.04 o 5 5 1 8.91 9.88 3.23 o 6 5 1 49.46 54.74 3.91 o -6 6 1 92.57 90.51 6.44 o -5 6 1 153.73 164.89 13.13 o -4 6 1 390.71 408.99 15.27 o -3 6 1 1544.89 1497.03 44.77 o -2 6 1 724.12 875.67 27.17 o -1 6 1 284.26 296.44 19.65 o 0 6 1 55.31 66.71 4.96 o 1 6 1 3063.58 3068.82 218.42 o 2 6 1 515.09 512.72 28.81 o 3 6 1 2.98 2.67 1.83 o 4 6 1 249.78 237.08 53.93 o 5 6 1 103.63 91.01 9.51 o 6 6 1 72.43 86.84 8.41 o -5 7 1 285.53 311.31 18.31 o -4 7 1 5.40 2.48 1.76 o -3 7 1 254.71 298.40 29.48 o -2 7 1 76.90 71.92 6.15 o -1 7 1 1288.46 1188.90 91.51 o 0 7 1 140.28 166.03 8.63 o 1 7 1 206.29 188.43 11.43 o 2 7 1 1142.26 1061.15 32.93 o 3 7 1 2697.59 2836.91 75.18 o 4 7 1 953.28 958.08 29.34 o 5 7 1 3.27 2.39 2.25 o -5 8 1 19.23 16.56 2.56 o -4 8 1 420.40 429.22 18.41 o -3 8 1 257.51 245.80 11.31 o -2 8 1 15.79 27.28 4.49 o -1 8 1 212.67 221.68 9.84 o 0 8 1 2094.36 1978.90 236.72 o 1 8 1 0.56 0.88 1.81 o 2 8 1 117.70 127.27 8.87 o 3 8 1 1365.66 1163.04 50.99 o 4 8 1 540.01 554.25 25.10 o 5 8 1 312.39 338.11 13.61 o -5 9 1 101.80 104.11 6.60 o -4 9 1 18.80 27.23 4.61 o -3 9 1 306.61 300.47 15.97 o -2 9 1 4033.27 3693.52 94.56 o -1 9 1 45.48 35.21 4.58 o 0 9 1 180.78 159.31 12.10 o 1 9 1 889.48 871.78 34.94 o 2 9 1 258.96 277.34 10.63 o 3 9 1 0.31 2.48 2.66 o 4 9 1 68.01 68.03 5.56 o 5 9 1 209.80 234.03 12.31 o -4 10 1 8.76 10.66 2.99 o -3 10 1 517.35 525.62 29.88 o -2 10 1 90.57 84.86 6.63 o -1 10 1 151.90 134.38 7.22 o 0 10 1 1258.35 1140.16 32.03 o 1 10 1 293.18 285.99 10.77 o 2 10 1 2.77 -0.93 2.62 o 3 10 1 163.18 162.47 10.67 o 4 10 1 14.76 14.79 4.10 o -4 11 1 34.07 34.94 4.86 o -3 11 1 56.09 63.41 6.39 o -2 11 1 67.78 68.09 5.88 o -1 11 1 77.79 75.53 6.05 o 0 11 1 22.60 18.81 3.97 o 1 11 1 369.83 354.81 12.35 o 2 11 1 46.60 51.43 5.95 o 3 11 1 233.92 249.94 12.57 o 4 11 1 82.74 91.87 12.67 o -4 12 1 170.63 194.41 13.35 o -3 12 1 525.00 579.12 23.35 o -2 12 1 147.07 139.15 9.80 o -1 12 1 94.64 90.71 6.56 o 0 12 1 16.31 17.95 2.90 o 1 12 1 318.30 296.71 13.39 o 2 12 1 13.72 12.61 3.18 o 3 12 1 53.18 61.36 5.42 o 4 12 1 161.61 156.25 10.88 o -3 13 1 43.20 48.29 7.85 o -2 13 1 105.59 119.31 9.44 o -1 13 1 3.51 3.20 2.70 o 0 13 1 113.24 88.57 7.28 o 1 13 1 0.67 1.63 2.01 o 2 13 1 122.11 141.92 8.36 o 3 13 1 36.35 45.52 4.91 o -2 14 1 63.71 61.62 4.34 o -1 14 1 41.05 40.10 4.35 o 0 14 1 152.60 163.41 10.89 o 1 14 1 4.32 4.13 1.40 o 2 14 1 7.80 7.91 2.36 o -1 15 1 51.96 57.78 6.78 o 0 15 1 109.90 102.79 6.79 o 1 15 1 120.39 123.01 10.52 o -6 0 2 2.69 2.28 2.96 o -4 0 2 3528.14 3182.73 109.62 o -2 0 2 7814.97 7253.29 206.40 o 0 0 2 396.03 398.57 16.71 o 2 0 2 843.34 1002.23 27.66 o 4 0 2 1226.10 1143.65 53.98 o 6 0 2 201.67 197.22 13.63 o -6 1 2 0.15 5.13 2.41 o -5 1 2 9.91 8.55 2.28 o -4 1 2 29.23 21.90 3.42 o -3 1 2 87.98 102.15 5.36 o -2 1 2 385.51 470.67 22.41 o -1 1 2 3201.31 3361.08 71.00 o 0 1 2 956.74 1044.62 19.22 o 1 1 2 7901.61 8191.31 162.80 o 2 1 2 31.75 40.14 2.70 o 3 1 2 405.81 408.16 17.77 o 4 1 2 987.17 967.74 34.16 o 5 1 2 198.51 187.99 15.01 o 6 1 2 83.33 89.00 6.46 o -6 2 2 52.30 46.69 4.26 o -5 2 2 148.08 124.01 8.14 o -4 2 2 64.12 69.55 6.15 o -3 2 2 2225.18 2095.99 53.44 o -2 2 2 305.68 363.86 16.71 o -1 2 2 201.09 181.33 4.97 o 0 2 2 2569.29 2913.04 54.75 o 1 2 2 41383.33 38998.32 660.80 o 2 2 2 120.75 132.10 8.25 o 3 2 2 835.52 925.77 29.40 o 4 2 2 95.83 90.86 5.85 o 5 2 2 98.82 95.76 9.68 o 6 2 2 25.94 22.81 3.41 o -6 3 2 197.82 180.21 11.62 o -5 3 2 97.17 110.32 7.59 o -4 3 2 69.72 57.45 5.72 o -3 3 2 108.15 100.40 10.62 o -2 3 2 458.46 476.30 15.63 o -1 3 2 88.58 94.05 3.77 o 0 3 2 2536.20 2559.14 95.33 o 1 3 2 25.77 35.49 2.27 o 2 3 2 213.49 241.62 11.76 o 3 3 2 492.39 577.52 23.12 o 4 3 2 410.66 410.38 21.13 o 5 3 2 61.82 54.65 7.92 o 6 3 2 44.17 41.20 3.75 o -6 4 2 264.54 295.56 15.78 o -5 4 2 8.66 5.93 2.58 o -4 4 2 326.96 344.93 35.02 o -3 4 2 225.23 269.74 11.52 o -2 4 2 932.72 915.71 34.17 o -1 4 2 1.71 1.52 0.76 o 0 4 2 4454.94 4452.65 107.82 o 1 4 2 1025.03 1094.81 23.94 o 2 4 2 4.24 0.76 1.40 o 3 4 2 32.32 23.28 4.24 o 4 4 2 1270.23 1208.28 41.10 o 5 4 2 5.89 -0.75 2.49 o 6 4 2 18.49 19.71 2.50 o -6 5 2 183.92 192.31 9.36 o -5 5 2 73.69 77.41 11.08 o -4 5 2 116.94 119.50 8.79 o -3 5 2 48.68 51.66 5.04 o -2 5 2 1435.21 1580.04 64.14 o -1 5 2 3.84 1.82 1.41 o 0 5 2 476.53 572.26 12.30 o 1 5 2 210.54 195.44 7.95 o 2 5 2 2.18 3.44 1.35 o 3 5 2 738.82 741.45 28.68 o 4 5 2 364.16 407.28 21.28 o 5 5 2 21.69 21.34 3.95 o 6 5 2 1.02 0.58 1.17 o -6 6 2 19.76 16.28 3.11 o -5 6 2 0.16 0.44 2.02 o -4 6 2 50.23 60.62 6.54 o -3 6 2 2027.00 2098.96 136.87 o -2 6 2 906.63 928.31 31.63 o -1 6 2 9.13 5.22 1.45 o 0 6 2 419.38 469.54 17.22 o 1 6 2 3493.81 3566.41 80.12 o 2 6 2 269.48 278.21 10.80 o 3 6 2 286.85 262.78 16.06 o 4 6 2 3.95 4.22 2.07 o 5 6 2 133.78 127.46 9.19 o -5 7 2 522.88 597.70 20.10 o -4 7 2 5.04 4.11 2.00 o -3 7 2 3.59 5.04 2.85 o -2 7 2 142.51 150.40 8.92 o -1 7 2 452.95 432.08 36.04 o 0 7 2 128.39 98.72 6.59 o 1 7 2 442.96 449.89 13.45 o 2 7 2 3.54 3.46 1.90 o 3 7 2 375.74 381.73 11.53 o 4 7 2 310.44 341.08 15.95 o 5 7 2 39.06 37.80 4.71 o -5 8 2 39.36 45.19 4.92 o -4 8 2 289.06 288.60 17.74 o -3 8 2 11.38 13.58 3.54 o -2 8 2 50.71 48.80 4.83 o -1 8 2 126.11 150.12 8.53 o 0 8 2 369.84 295.68 16.07 o 1 8 2 791.06 738.97 25.79 o 2 8 2 26.79 22.88 3.71 o 3 8 2 138.94 129.22 13.29 o 4 8 2 150.33 168.72 10.70 o 5 8 2 175.68 176.97 12.14 o -5 9 2 91.32 96.78 7.92 o -4 9 2 170.13 186.65 9.62 o -3 9 2 722.34 723.62 25.64 o -2 9 2 2578.34 2467.64 79.38 o -1 9 2 425.63 399.99 22.69 o 0 9 2 72.73 73.92 8.23 o 1 9 2 93.18 82.97 6.98 o 2 9 2 752.92 754.04 22.16 o 3 9 2 84.27 79.30 7.46 o 4 9 2 61.42 67.98 6.43 o 5 9 2 106.57 104.48 7.14 o -5 10 2 0.01 -1.04 1.68 o -4 10 2 80.51 84.89 6.13 o -3 10 2 247.72 240.63 13.90 o -2 10 2 0.97 3.13 1.95 o -1 10 2 157.01 161.62 12.89 o 0 10 2 245.90 213.04 8.39 o 1 10 2 596.16 598.25 20.11 o 2 10 2 121.53 112.68 12.23 o 3 10 2 109.93 109.49 10.49 o 4 10 2 16.53 14.83 2.71 o -4 11 2 2.44 4.32 2.45 o -3 11 2 3.71 5.31 3.26 o -2 11 2 17.57 14.56 3.21 o -1 11 2 314.36 307.06 21.22 o 0 11 2 563.15 561.50 19.26 o 1 11 2 390.07 367.01 15.13 o 2 11 2 106.67 98.53 10.79 o 3 11 2 435.63 435.27 20.90 o 4 11 2 7.81 8.37 2.57 o -4 12 2 196.73 256.42 15.72 o -3 12 2 1032.98 1069.42 31.41 o -2 12 2 1.28 1.28 2.02 o -1 12 2 0.10 -0.25 3.22 o 0 12 2 138.07 125.86 6.96 o 1 12 2 100.93 105.51 7.06 o 2 12 2 38.31 39.46 4.87 o 3 12 2 157.63 162.77 23.06 o -3 13 2 22.98 27.91 3.91 o -2 13 2 713.74 823.78 28.09 o -1 13 2 115.75 111.84 10.04 o 0 13 2 1027.15 1008.57 23.85 o 1 13 2 2.92 -0.89 1.83 o 2 13 2 221.14 225.54 10.57 o 3 13 2 93.32 112.00 7.50 o -2 14 2 35.58 34.70 3.53 o -1 14 2 17.94 21.90 3.39 o 0 14 2 109.23 107.88 8.52 o 1 14 2 33.34 32.67 9.27 o 2 14 2 114.63 102.36 13.81 o -1 15 2 541.30 448.32 20.74 o 0 15 2 15.26 17.72 2.95 o 1 15 2 8.73 4.58 1.84 o -5 0 3 49.36 44.85 17.73 o -3 0 3 164.98 216.16 12.52 o -1 0 3 782.42 871.72 20.40 o 1 0 3 1.61 3.45 1.23 o 3 0 3 2609.59 2553.51 90.01 o 5 0 3 63.33 69.57 8.44 o -6 1 3 6.50 7.70 1.97 o -5 1 3 669.52 629.92 19.56 o -4 1 3 198.83 175.84 11.43 o -3 1 3 223.82 259.94 8.80 o -2 1 3 3694.56 3324.43 59.80 o -1 1 3 2027.77 2087.31 38.85 o 0 1 3 2158.23 2275.58 30.55 o 1 1 3 26.08 33.67 2.03 o 2 1 3 891.20 935.71 34.63 o 3 1 3 55.98 68.21 7.38 o 4 1 3 685.36 637.01 21.83 o 5 1 3 0.16 1.74 2.50 o 6 1 3 60.81 54.76 4.66 o -6 2 3 27.01 22.26 4.54 o -5 2 3 96.12 109.93 8.83 o -4 2 3 63.55 53.19 5.44 o -3 2 3 89.26 117.46 6.83 o -2 2 3 50.51 54.14 3.25 o -1 2 3 58.35 52.98 1.95 o 0 2 3 10636.16 10665.25 289.19 o 1 2 3 12107.47 12633.44 166.18 o 2 2 3 1497.45 1693.73 80.49 o 3 2 3 30.45 32.80 4.09 o 4 2 3 418.49 363.09 19.91 o 5 2 3 60.36 60.51 6.52 o 6 2 3 284.48 295.90 17.17 o -6 3 3 82.88 97.15 8.62 o -5 3 3 3576.09 3568.02 99.62 o -4 3 3 301.91 276.71 12.98 o -3 3 3 6.83 10.37 2.33 o -2 3 3 10.70 3.09 1.10 o -1 3 3 4868.40 4972.79 53.97 o 0 3 3 344.55 330.13 16.75 o 1 3 3 5.74 10.40 1.34 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33.92 o 1 6 3 578.25 659.87 23.88 o 2 6 3 113.09 104.15 17.52 o 3 6 3 16.26 13.90 5.54 o 4 6 3 661.32 634.66 22.60 o 5 6 3 14.71 13.83 3.09 o -5 7 3 824.96 885.95 25.48 o -4 7 3 4.61 3.48 2.55 o -3 7 3 4.22 11.07 3.57 o -2 7 3 145.28 140.27 8.61 o -1 7 3 4435.12 4646.01 83.36 o 0 7 3 328.31 347.58 11.42 o 1 7 3 231.38 274.73 12.13 o 2 7 3 466.49 514.61 17.94 o 3 7 3 66.81 69.28 5.19 o 4 7 3 68.88 67.39 6.78 o 5 7 3 28.90 29.77 4.04 o -5 8 3 2.49 3.85 2.52 o -4 8 3 571.26 603.05 46.92 o -3 8 3 107.04 103.42 10.50 o -2 8 3 796.59 734.25 23.99 o -1 8 3 152.30 129.22 10.42 o 0 8 3 52.34 50.35 6.27 o 1 8 3 764.56 877.32 29.69 o 2 8 3 340.98 360.15 19.24 o 3 8 3 490.83 505.34 19.07 o 4 8 3 248.78 237.63 13.78 o 5 8 3 2.72 5.20 1.96 o -5 9 3 5.67 7.49 2.73 o -4 9 3 241.21 257.82 13.41 o -3 9 3 734.29 739.91 25.04 o -2 9 3 93.54 87.51 7.68 o -1 9 3 2.57 4.01 1.51 o 0 9 3 320.40 259.27 15.58 o 1 9 3 827.98 857.93 101.26 o 2 9 3 194.05 173.04 13.57 o 3 9 3 80.54 91.46 11.76 o 4 9 3 19.48 34.51 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