#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/72/2237206.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237206_Fobs loop_ _publ_author_name 'Traore, Bocar' 'Boye, Mouhamadou Sembene' 'Sidibe, Mamadou' 'Diop, Libasse' 'Guionneau, Philippe' _publ_section_title ; Benzyltriphenylphosphonium dichloridotriphenylstannate(IV) ; _journal_coeditor_code PK2448 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m42 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.042 _cell_angle_gamma 90.000 _cell_length_a 10.0222 _cell_length_b 17.1480 _cell_length_c 21.2925 _exptl_crystal_F_000 1576.00 _reflns_d_resolution_high 0.7417 _[local]_cod_data_source_file pk2448Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bt060f-1 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1234.08 1242.57 44.19 o 3 0 0 4924.29 4705.46 262.81 o 4 0 0 7181.88 7877.86 216.88 o 5 0 0 15.09 40.60 21.01 o 6 0 0 3099.62 2969.90 103.87 o 7 0 0 217.42 256.63 66.44 o 8 0 0 1230.75 1136.69 65.34 o 9 0 0 693.67 684.14 44.64 o 10 0 0 1544.47 1517.82 72.39 o 11 0 0 1365.74 1583.13 109.27 o 12 0 0 94.95 134.35 65.09 o 13 0 0 35.62 -44.29 103.35 o 1 1 0 459.20 524.47 36.93 o 2 1 0 47931.16 46446.70 1708.18 o 3 1 0 10733.59 10379.70 232.81 o 4 1 0 20397.09 19399.27 441.01 o 5 1 0 15504.93 15414.79 289.41 o 6 1 0 565.49 431.48 23.69 o 7 1 0 2799.64 2641.96 93.17 o 8 1 0 19.58 -20.01 25.59 o 9 1 0 11.29 -18.17 27.04 o 10 1 0 475.54 412.13 47.47 o 11 1 0 1053.38 1059.69 55.41 o 12 1 0 566.10 659.27 73.52 o 13 1 0 1038.09 1030.05 99.19 o 0 2 0 39138.93 40051.66 967.73 o 1 2 0 16348.17 15633.22 546.31 o 2 2 0 5483.45 5626.30 269.10 o 3 2 0 19782.95 19345.57 493.67 o 4 2 0 3499.87 3185.55 87.30 o 5 2 0 2822.80 2735.10 136.12 o 6 2 0 306.03 303.88 30.61 o 7 2 0 2136.12 2030.32 97.67 o 8 2 0 1803.95 1676.38 80.07 o 9 2 0 1855.83 1976.66 74.69 o 10 2 0 688.70 698.03 68.20 o 11 2 0 353.93 325.29 38.51 o 12 2 0 0.25 5.74 60.73 o 13 2 0 37.27 15.90 67.26 o 1 3 0 74.33 70.42 7.96 o 2 3 0 611.74 595.84 29.19 o 3 3 0 1212.76 1347.00 62.04 o 4 3 0 1234.52 1089.15 56.14 o 5 3 0 4310.80 4358.05 113.71 o 6 3 0 6501.61 6280.37 174.70 o 7 3 0 266.54 264.58 36.04 o 8 3 0 53.98 33.32 27.70 o 9 3 0 11.13 -31.02 61.80 o 10 3 0 212.00 191.23 56.27 o 11 3 0 426.68 539.50 45.72 o 12 3 0 346.65 254.19 63.85 o 13 3 0 97.12 157.38 65.09 o 0 4 0 55100.51 57389.42 997.94 o 1 4 0 9770.27 9862.34 168.56 o 2 4 0 807.08 824.83 27.32 o 3 4 0 695.30 911.57 115.83 o 4 4 0 3119.19 2760.12 228.28 o 5 4 0 86.84 78.26 13.72 o 6 4 0 835.73 675.24 34.97 o 7 4 0 805.56 729.06 37.47 o 8 4 0 110.06 158.06 27.01 o 9 4 0 52.62 19.71 29.47 o 10 4 0 103.43 101.36 33.03 o 11 4 0 9.05 -25.66 25.66 o 12 4 0 5.70 67.37 34.41 o 13 4 0 2.39 25.57 56.72 o 1 5 0 4243.78 4420.63 78.17 o 2 5 0 2719.85 2504.87 60.03 o 3 5 0 608.01 573.30 36.64 o 4 5 0 5232.97 5287.29 462.10 o 5 5 0 4106.01 3966.74 205.02 o 6 5 0 916.96 914.11 50.09 o 7 5 0 3504.22 3222.30 143.22 o 8 5 0 535.74 509.91 25.57 o 9 5 0 31.38 14.20 13.80 o 10 5 0 122.30 140.35 30.90 o 11 5 0 69.43 75.64 37.29 o 12 5 0 0.95 -46.11 46.11 o 13 5 0 94.14 114.83 69.17 o 0 6 0 9.82 22.15 15.66 o 1 6 0 7250.01 7286.79 117.61 o 2 6 0 18239.96 18208.33 782.71 o 3 6 0 2369.36 2093.72 79.98 o 4 6 0 425.69 416.12 52.08 o 5 6 0 1102.75 1069.65 44.87 o 6 6 0 2953.04 3047.26 241.18 o 7 6 0 1030.14 1001.39 56.19 o 8 6 0 2421.36 2375.69 152.61 o 9 6 0 3033.40 2986.98 185.24 o 10 6 0 14.35 -19.46 39.84 o 11 6 0 263.36 226.22 54.40 o 12 6 0 20.06 -44.99 54.62 o 13 6 0 26.96 -80.20 88.28 o 1 7 0 813.99 788.85 26.65 o 2 7 0 1505.09 1291.51 35.59 o 3 7 0 1607.25 1463.90 53.30 o 4 7 0 13990.57 13968.32 1003.05 o 5 7 0 6882.52 6740.67 574.22 o 6 7 0 5335.05 5270.65 343.13 o 7 7 0 4424.41 4533.92 146.39 o 8 7 0 73.08 141.54 48.58 o 9 7 0 18.94 20.92 46.69 o 10 7 0 171.51 189.28 91.59 o 11 7 0 584.72 605.27 70.85 o 12 7 0 132.60 155.66 59.86 o 0 8 0 18955.48 19007.75 392.96 o 1 8 0 18385.96 18495.29 260.80 o 2 8 0 18717.73 18904.79 286.29 o 3 8 0 2669.44 2598.63 132.23 o 4 8 0 6.63 32.57 28.56 o 5 8 0 121.21 120.79 18.39 o 6 8 0 215.42 215.62 23.90 o 7 8 0 1442.22 1553.17 65.09 o 8 8 0 1681.64 1730.36 73.52 o 9 8 0 2044.45 2035.84 132.92 o 10 8 0 689.86 715.94 72.72 o 11 8 0 298.75 316.42 60.95 o 12 8 0 205.22 281.00 114.70 o 1 9 0 3580.07 3552.92 65.64 o 2 9 0 5077.25 4859.24 139.18 o 3 9 0 16633.39 16547.41 612.13 o 4 9 0 4849.63 4920.80 157.90 o 5 9 0 5573.36 5660.70 376.74 o 6 9 0 2455.97 2424.64 131.83 o 7 9 0 105.83 133.65 27.34 o 8 9 0 7.75 -5.91 24.61 o 9 9 0 56.01 64.09 32.48 o 10 9 0 14.29 -20.35 34.41 o 11 9 0 247.12 204.73 50.48 o 12 9 0 562.32 533.44 124.03 o 0 10 0 18168.97 19625.85 409.79 o 1 10 0 16496.08 16392.11 260.39 o 2 10 0 1818.06 1524.38 41.19 o 3 10 0 3732.14 3861.24 80.89 o 4 10 0 872.17 829.70 75.67 o 5 10 0 517.79 557.51 37.94 o 6 10 0 13.93 8.83 22.96 o 7 10 0 506.31 482.27 26.22 o 8 10 0 864.53 967.58 93.88 o 9 10 0 302.64 378.98 50.09 o 10 10 0 565.20 660.30 58.61 o 11 10 0 69.13 32.88 113.42 o 12 10 0 88.72 58.20 109.97 o 1 11 0 0.66 45.95 17.89 o 2 11 0 67.96 37.73 16.30 o 3 11 0 3204.74 3182.30 120.50 o 4 11 0 1007.22 1009.56 86.32 o 5 11 0 419.16 530.89 43.65 o 6 11 0 925.07 912.64 42.11 o 7 11 0 40.89 29.53 13.92 o 8 11 0 482.89 458.00 35.93 o 9 11 0 154.00 116.70 26.31 o 10 11 0 198.95 178.93 59.57 o 11 11 0 164.81 208.04 113.42 o 0 12 0 108.51 173.28 33.63 o 1 12 0 609.79 594.91 31.22 o 2 12 0 2.08 -14.66 14.66 o 3 12 0 1561.22 1780.38 52.12 o 4 12 0 4065.11 3928.34 161.03 o 5 12 0 50.13 57.92 24.88 o 6 12 0 96.69 149.63 49.99 o 7 12 0 90.78 88.50 67.84 o 8 12 0 275.37 218.50 29.76 o 9 12 0 22.26 -17.86 32.33 o 10 12 0 9.41 29.32 76.51 o 11 12 0 13.88 91.54 92.11 o 1 13 0 104.30 120.70 22.40 o 2 13 0 403.89 331.67 44.75 o 3 13 0 32.42 74.76 32.24 o 4 13 0 45.29 59.99 31.17 o 5 13 0 1223.43 1304.07 59.00 o 6 13 0 39.37 104.65 29.27 o 7 13 0 153.51 133.60 34.97 o 8 13 0 7.62 3.33 20.09 o 9 13 0 86.48 109.41 34.35 o 10 13 0 19.30 19.46 67.49 o 11 13 0 4.15 -95.52 95.52 o 0 14 0 923.34 846.07 56.72 o 1 14 0 39.07 65.87 21.68 o 2 14 0 6.16 2.86 17.89 o 3 14 0 537.85 495.33 33.94 o 4 14 0 766.42 816.20 84.29 o 5 14 0 37.65 35.92 28.44 o 6 14 0 532.55 610.04 44.64 o 7 14 0 398.34 387.90 27.17 o 8 14 0 1230.36 1294.36 70.14 o 9 14 0 470.43 587.21 75.62 o 10 14 0 168.58 243.61 155.02 o 1 15 0 118.03 120.92 24.39 o 2 15 0 37.51 13.28 26.64 o 3 15 0 1257.59 1290.01 53.95 o 4 15 0 1932.26 2069.23 68.50 o 5 15 0 2392.84 2452.19 280.17 o 6 15 0 1684.68 1802.33 132.13 o 7 15 0 304.73 284.98 20.92 o 8 15 0 383.22 316.40 48.97 o 9 15 0 31.21 -76.77 132.87 o 10 15 0 85.00 -54.26 90.99 o 0 16 0 1270.93 1248.60 95.99 o 1 16 0 2235.83 2379.06 67.44 o 2 16 0 866.24 866.39 50.09 o 3 16 0 591.40 579.00 41.08 o 4 16 0 346.95 326.33 55.41 o 5 16 0 487.73 561.46 49.02 o 6 16 0 76.97 24.98 32.39 o 7 16 0 365.38 370.72 51.42 o 8 16 0 1168.10 1164.28 177.20 o 9 16 0 451.09 408.98 117.37 o 1 17 0 900.19 922.16 46.89 o 2 17 0 793.92 849.28 51.33 o 3 17 0 2399.33 2643.96 149.23 o 4 17 0 1048.03 1083.43 58.71 o 5 17 0 791.58 863.84 58.52 o 6 17 0 1040.95 1048.85 111.27 o 7 17 0 23.98 -48.49 48.49 o 8 17 0 230.41 250.99 98.77 o 9 17 0 0.11 12.65 91.23 o 0 18 0 527.06 642.42 92.28 o 1 18 0 2840.64 3022.77 90.71 o 2 18 0 824.05 759.65 48.83 o 3 18 0 235.21 208.77 43.22 o 4 18 0 7.32 -25.84 25.84 o 5 18 0 263.81 310.50 45.13 o 6 18 0 23.40 -36.91 62.75 o 7 18 0 317.14 346.29 111.67 o 8 18 0 158.38 133.08 93.52 o 1 19 0 6.28 -11.60 25.05 o 2 19 0 318.29 277.90 44.44 o 3 19 0 482.80 484.93 41.26 o 4 19 0 301.15 250.99 51.42 o 5 19 0 359.10 363.66 74.90 o 6 19 0 216.73 149.64 158.71 o 7 19 0 15.75 -55.77 118.11 o 0 20 0 131.21 98.57 44.14 o 1 20 0 49.28 44.07 36.23 o 2 20 0 113.96 126.12 35.10 o 3 20 0 285.59 347.34 43.69 o 4 20 0 86.58 92.76 55.89 o 5 20 0 1.59 87.00 64.53 o 6 20 0 20.20 50.65 75.55 o 1 21 0 87.97 156.55 33.49 o 2 21 0 0.09 1.01 36.23 o 3 21 0 57.51 68.05 48.56 o 4 21 0 3.19 -18.45 67.86 o 5 21 0 12.73 75.98 106.91 o 0 22 0 29.15 60.90 92.27 o 1 22 0 191.14 85.70 45.39 o 2 22 0 9.67 28.26 64.68 o 3 22 0 20.62 -81.13 104.38 o 4 22 0 0.53 62.13 121.80 o 1 23 0 40.81 10.20 68.93 o -13 1 1 39.86 55.52 58.51 o -12 1 1 23.80 31.35 35.62 o -11 1 1 0.15 7.70 18.21 o -10 1 1 132.63 102.66 28.00 o -9 1 1 527.52 557.92 41.17 o -8 1 1 385.84 381.88 36.07 o -7 1 1 2857.00 2663.30 70.37 o -6 1 1 183.81 221.69 17.65 o -5 1 1 1923.95 1923.20 56.74 o -4 1 1 7683.13 7665.36 141.77 o -3 1 1 927.99 968.98 51.88 o -2 1 1 2527.89 2358.95 57.39 o -1 1 1 3620.12 3042.00 155.63 o 1 1 1 11094.33 10839.66 457.19 o 2 1 1 303.64 289.25 18.12 o 3 1 1 5756.20 5510.96 127.48 o 4 1 1 1650.83 1531.48 49.02 o 5 1 1 294.35 332.43 22.17 o 6 1 1 1018.32 1117.70 39.75 o 7 1 1 5.74 -3.41 30.38 o 8 1 1 39.36 23.16 42.00 o 9 1 1 508.13 439.14 58.61 o 10 1 1 245.04 190.73 41.56 o 11 1 1 0.56 26.44 23.78 o 12 1 1 154.39 98.20 44.31 o 13 1 1 71.56 2.36 63.85 o -13 2 1 9.93 -47.70 67.26 o -12 2 1 791.01 879.12 74.72 o -11 2 1 699.61 722.98 48.21 o -10 2 1 1906.85 1856.14 77.84 o -9 2 1 1452.21 1385.33 66.70 o -8 2 1 4.16 -46.51 77.51 o -7 2 1 2153.75 2118.78 100.74 o -6 2 1 23.42 3.16 35.43 o -5 2 1 377.06 346.32 64.23 o -4 2 1 3162.06 3106.29 83.11 o -3 2 1 735.74 628.15 29.49 o -2 2 1 4782.58 4618.49 186.97 o -1 2 1 34534.01 33109.02 1311.91 o 0 2 1 14035.53 14104.20 286.11 o 1 2 1 4229.28 4361.98 228.60 o 2 2 1 229.14 302.90 18.94 o 3 2 1 1831.46 1828.21 60.97 o 4 2 1 10836.05 10939.25 256.22 o 5 2 1 3425.77 3224.62 84.83 o 6 2 1 4232.67 4103.72 101.11 o 7 2 1 934.15 839.69 39.43 o 8 2 1 4838.44 4619.82 121.44 o 9 2 1 1031.39 1023.38 58.88 o 10 2 1 354.90 311.51 44.75 o 11 2 1 399.90 403.52 37.00 o 12 2 1 3.80 43.48 46.49 o 13 2 1 21.81 53.15 61.42 o -13 3 1 228.60 269.77 67.86 o -12 3 1 83.69 91.04 54.62 o -11 3 1 13.07 51.08 34.10 o -10 3 1 281.62 305.06 34.33 o -9 3 1 524.81 570.57 90.98 o -8 3 1 2637.38 2493.84 90.06 o -7 3 1 8937.29 8510.81 565.98 o -6 3 1 6597.85 5938.26 196.84 o -5 3 1 25272.14 25539.55 748.03 o -4 3 1 19127.61 18991.35 518.95 o -3 3 1 22010.78 21475.35 828.44 o -2 3 1 6092.24 6193.92 148.17 o -1 3 1 13067.29 12521.05 173.76 o 0 3 1 1835.60 1588.51 28.51 o 1 3 1 31646.51 31952.90 885.85 o 2 3 1 7577.33 6965.72 526.32 o 3 3 1 7699.74 7467.13 605.50 o 4 3 1 6420.18 5840.16 245.76 o 5 3 1 227.61 209.04 39.43 o 6 3 1 3351.74 3485.78 84.24 o 7 3 1 63.72 25.96 27.70 o 8 3 1 218.29 230.03 29.32 o 9 3 1 1747.20 1530.25 65.25 o 10 3 1 2085.93 2127.00 88.76 o 11 3 1 754.31 827.77 51.52 o 12 3 1 821.34 907.56 83.65 o 13 3 1 320.44 289.55 67.33 o -13 4 1 22.59 -51.67 84.89 o -12 4 1 578.20 560.33 58.45 o -11 4 1 968.80 1081.44 51.62 o -10 4 1 2743.42 2901.01 102.03 o -9 4 1 3587.40 3689.95 111.95 o -8 4 1 2620.03 2436.08 188.35 o -7 4 1 4589.90 4251.47 146.41 o -6 4 1 88.75 59.52 27.37 o -5 4 1 6871.12 6565.75 263.76 o -4 4 1 8575.59 7990.05 474.55 o -3 4 1 19236.08 18606.42 728.81 o -2 4 1 7630.40 7554.49 310.39 o -1 4 1 7467.73 7282.96 183.12 o 0 4 1 14854.73 14017.69 199.51 o 1 4 1 14871.84 14741.80 401.42 o 2 4 1 8436.34 8260.04 643.92 o 3 4 1 2634.36 2852.49 219.58 o 4 4 1 82.07 51.67 31.32 o 5 4 1 4673.42 4362.54 96.29 o 6 4 1 13772.53 13371.94 472.74 o 7 4 1 8802.65 8799.86 175.06 o 8 4 1 12347.03 12582.23 261.75 o 9 4 1 2019.06 2225.09 110.20 o 10 4 1 1763.60 1863.42 108.71 o 11 4 1 362.07 376.89 76.83 o 12 4 1 45.49 54.13 54.52 o 13 4 1 2.30 -32.88 54.62 o -13 5 1 121.41 145.05 169.78 o -12 5 1 121.53 99.66 57.42 o -11 5 1 71.58 46.32 28.77 o -10 5 1 71.59 66.46 18.73 o -9 5 1 1493.77 1511.82 47.91 o -8 5 1 5219.10 5373.54 143.05 o -7 5 1 3273.84 3013.77 67.05 o -6 5 1 17581.89 16917.76 290.36 o -5 5 1 31966.64 32841.18 916.22 o -4 5 1 4586.36 4164.90 454.73 o -3 5 1 3314.60 3064.65 76.32 o -2 5 1 3247.19 3125.14 154.74 o -1 5 1 5.94 24.83 7.95 o 0 5 1 5.21 48.61 10.31 o 1 5 1 2519.45 2726.69 98.16 o 2 5 1 11167.41 11318.29 453.18 o 3 5 1 8392.08 8315.03 601.56 o 4 5 1 5865.77 6044.81 398.99 o 5 5 1 5108.95 5264.15 268.37 o 6 5 1 2871.13 2771.83 72.18 o 7 5 1 769.67 831.61 57.55 o 8 5 1 1526.18 1404.51 76.94 o 9 5 1 2133.37 2031.80 73.86 o 10 5 1 2407.92 2420.71 87.55 o 11 5 1 1281.37 1307.29 79.93 o 12 5 1 648.50 533.94 79.64 o 13 5 1 434.26 332.28 78.30 o -13 6 1 113.43 97.61 87.19 o -12 6 1 208.16 163.33 61.99 o -11 6 1 366.46 328.58 48.82 o -10 6 1 790.61 852.98 77.50 o -9 6 1 833.42 849.45 62.54 o -8 6 1 1621.85 1581.50 78.05 o -7 6 1 2325.19 2241.44 89.69 o -6 6 1 118.81 137.91 30.14 o -5 6 1 667.72 604.37 55.44 o -4 6 1 675.07 507.95 43.26 o -3 6 1 7560.85 7514.11 128.92 o -2 6 1 6654.27 6131.63 183.30 o -1 6 1 7422.89 7495.38 189.26 o 0 6 1 4177.13 3959.41 70.36 o 1 6 1 11641.01 11179.76 302.14 o 2 6 1 26.38 74.74 15.18 o 3 6 1 329.77 323.42 24.61 o 4 6 1 4241.40 4009.35 109.82 o 5 6 1 5433.45 5449.28 393.79 o 6 6 1 7430.81 7241.26 200.60 o 7 6 1 9145.63 9166.15 521.52 o 8 6 1 1728.13 1854.08 175.93 o 9 6 1 920.55 1086.98 90.10 o 10 6 1 759.98 743.78 68.42 o 11 6 1 158.14 129.58 47.92 o 12 6 1 15.54 58.23 69.17 o 13 6 1 14.48 91.60 361.71 o -12 7 1 1.83 -8.44 54.62 o -11 7 1 28.39 11.21 40.86 o -10 7 1 3.49 8.11 39.17 o -9 7 1 535.39 499.35 66.65 o -8 7 1 721.53 671.21 140.28 o -7 7 1 425.26 317.04 40.47 o -6 7 1 2939.25 2833.64 89.21 o -5 7 1 3983.28 3985.28 184.15 o -4 7 1 10549.93 10110.76 243.73 o -3 7 1 5476.09 5228.14 183.61 o -2 7 1 7770.30 7481.26 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