#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/72/2237213.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237213_Fobs loop_ _publ_author_name 'Jucov, Evgheni' 'Kornienko, Alexander' 'Masi, Marco' 'Evidente, Antonio' 'Antipin, Mikhail' _publ_section_title ; (2S,3R,4S,4aR)-2,3,4,7-Tetrahydroxy-3,4,4a,5-tetrahydro[1,3]dioxolo[4,5-j]phenanthridin-6(2H)-one hemihydrate ; _journal_coeditor_code RK2387 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o9 _journal_page_last o10 _journal_volume 69 _journal_year 2013 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.355 _cell_angle_gamma 90.000 _cell_length_a 10.9006 _cell_length_b 20.3736 _cell_length_c 11.8839 _exptl_crystal_F_000 1320.00 _reflns_d_resolution_high 0.8021 _[local]_cod_data_source_file rk2387Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 520.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 -21 0 69.72 53.75 5.41 o 0 -20 0 559.49 471.57 19.65 o 1 -20 0 465.11 440.28 23.28 o 2 -20 0 481.83 451.20 28.78 o 6 -20 0 77.11 72.75 7.24 o 7 -20 0 21.87 16.96 2.43 o 8 -20 0 154.98 127.25 6.99 o 1 -19 0 570.42 486.14 13.94 o 2 -19 0 147.89 129.87 5.83 o 3 -19 0 107.63 96.13 5.07 o 4 -19 0 583.88 559.29 15.94 o 7 -19 0 80.36 71.43 7.10 o 8 -19 0 61.93 52.49 3.49 o 0 -18 0 1333.62 1214.46 32.73 o 1 -18 0 7497.46 6630.20 89.09 o 2 -18 0 34.84 32.63 3.96 o 3 -18 0 530.88 441.61 11.36 o 4 -18 0 90.25 73.05 4.01 o 5 -18 0 32.60 27.34 2.52 o 6 -18 0 113.75 98.41 7.49 o 7 -18 0 813.05 658.39 15.93 o 8 -18 0 38.47 31.05 1.92 o 9 -18 0 427.87 370.83 8.45 o 1 -17 0 1223.09 1155.90 16.91 o 2 -17 0 2144.94 1988.12 30.58 o 3 -17 0 158.69 127.12 5.95 o 4 -17 0 319.04 290.84 9.48 o 5 -17 0 439.20 383.26 11.53 o 6 -17 0 571.06 520.46 10.47 o 7 -17 0 347.63 299.00 8.25 o 8 -17 0 396.24 300.37 8.03 o 9 -17 0 16.39 10.96 1.10 o 0 -16 0 2823.02 2470.31 83.20 o 1 -16 0 19219.30 17464.97 262.67 o 2 -16 0 350.93 323.66 9.59 o 3 -16 0 1623.08 1488.41 20.80 o 4 -16 0 24.98 22.75 3.87 o 5 -16 0 439.06 356.35 11.33 o 6 -16 0 13.06 9.76 2.00 o 7 -16 0 170.62 143.17 6.23 o 8 -16 0 404.35 347.95 8.73 o 9 -16 0 397.69 332.03 6.11 o 10 -16 0 24.95 19.24 1.30 o 1 -15 0 243.71 217.42 7.64 o 2 -15 0 547.17 496.03 11.77 o 3 -15 0 165.21 146.11 6.37 o 4 -15 0 256.18 219.65 8.57 o 5 -15 0 941.97 846.17 19.59 o 6 -15 0 263.13 206.90 6.91 o 7 -15 0 728.65 627.66 10.07 o 8 -15 0 6.09 4.45 1.78 o 9 -15 0 310.66 270.69 6.55 o 10 -15 0 56.76 45.29 2.17 o 0 -14 0 228.25 191.12 15.84 o 1 -14 0 180.58 186.40 6.62 o 2 -14 0 81.68 77.79 4.36 o 3 -14 0 46.43 39.63 3.33 o 4 -14 0 52.56 39.40 3.75 o 5 -14 0 609.67 506.86 15.02 o 6 -14 0 228.94 192.21 7.76 o 7 -14 0 377.44 319.95 7.50 o 8 -14 0 214.17 189.87 7.22 o 9 -14 0 14.17 9.38 2.42 o 10 -14 0 71.76 54.70 2.71 o 1 -13 0 7049.84 6431.19 67.07 o 2 -13 0 18.09 15.88 2.10 o 3 -13 0 274.70 259.96 6.41 o 4 -13 0 30.37 30.97 2.24 o 5 -13 0 223.16 220.42 8.44 o 6 -13 0 162.54 139.31 6.64 o 7 -13 0 366.36 304.07 8.53 o 8 -13 0 256.63 211.07 5.37 o 9 -13 0 24.30 15.32 2.26 o 10 -13 0 4.68 2.00 1.59 o 11 -13 0 6.15 5.31 0.97 o 0 -12 0 4194.61 3673.33 75.48 o 1 -12 0 334.77 278.18 7.64 o 2 -12 0 353.55 362.69 8.97 o 3 -12 0 132.56 125.67 4.25 o 4 -12 0 695.22 707.65 17.17 o 5 -12 0 800.53 754.27 14.52 o 6 -12 0 805.10 743.75 13.77 o 7 -12 0 9.24 6.93 1.83 o 8 -12 0 386.56 344.81 9.45 o 9 -12 0 30.68 20.89 2.42 o 10 -12 0 162.28 146.38 5.15 o 11 -12 0 81.80 66.47 2.01 o 1 -11 0 1030.92 980.34 19.82 o 2 -11 0 1750.54 1664.55 34.71 o 3 -11 0 1509.73 1399.77 28.14 o 4 -11 0 111.08 105.07 3.15 o 5 -11 0 898.93 942.99 12.33 o 6 -11 0 1107.83 1041.23 14.83 o 7 -11 0 159.64 137.37 3.92 o 8 -11 0 125.40 104.73 4.00 o 9 -11 0 281.76 238.80 6.50 o 10 -11 0 21.03 21.14 2.26 o 11 -11 0 40.72 38.27 1.77 o 0 -10 0 743.87 610.31 13.20 o 1 -10 0 3264.60 3103.22 36.65 o 2 -10 0 15.59 17.83 1.23 o 3 -10 0 1733.93 1634.06 17.85 o 4 -10 0 2903.98 2923.28 54.28 o 5 -10 0 2514.40 2516.36 23.06 o 6 -10 0 89.19 88.19 3.10 o 7 -10 0 280.73 259.97 5.46 o 8 -10 0 96.31 86.94 3.32 o 9 -10 0 377.27 318.52 6.50 o 10 -10 0 15.50 14.85 2.25 o 11 -10 0 872.26 742.09 10.74 o 12 -10 0 557.31 468.56 10.13 o 1 -9 0 9743.32 9012.86 73.15 o 2 -9 0 1882.41 1730.63 19.94 o 3 -9 0 7054.55 7066.70 145.43 o 4 -9 0 2529.48 2507.29 24.44 o 5 -9 0 1883.06 1918.84 17.59 o 6 -9 0 186.95 174.66 4.67 o 7 -9 0 123.64 110.42 3.19 o 8 -9 0 77.44 61.90 2.59 o 9 -9 0 606.33 539.57 7.40 o 10 -9 0 436.04 387.66 8.58 o 11 -9 0 390.81 352.53 5.82 o 12 -9 0 375.01 317.68 6.08 o 0 -8 0 893.77 816.67 22.24 o 1 -8 0 9447.15 8361.33 78.66 o 2 -8 0 1601.06 1489.72 14.20 o 3 -8 0 1225.29 1217.49 22.17 o 4 -8 0 1823.19 1887.25 18.41 o 5 -8 0 572.06 609.86 7.70 o 6 -8 0 1140.67 1125.15 12.86 o 7 -8 0 161.32 145.68 3.50 o 8 -8 0 196.70 174.57 4.12 o 9 -8 0 453.98 386.77 6.68 o 10 -8 0 71.12 58.78 3.15 o 11 -8 0 79.13 80.81 2.55 o 12 -8 0 657.53 602.04 11.72 o 1 -7 0 1137.40 1028.96 13.62 o 2 -7 0 3531.24 3251.03 24.07 o 3 -7 0 2838.35 2738.82 22.80 o 4 -7 0 1914.67 1864.77 23.80 o 5 -7 0 1690.91 1675.19 14.11 o 6 -7 0 686.10 666.70 8.60 o 7 -7 0 835.67 759.18 8.11 o 8 -7 0 254.97 240.77 5.22 o 9 -7 0 264.77 239.31 5.24 o 10 -7 0 362.30 349.65 7.03 o 11 -7 0 758.02 723.79 9.35 o 12 -7 0 160.45 139.52 4.15 o 0 -6 0 22270.74 20164.64 308.27 o 1 -6 0 2751.10 2250.43 30.85 o 2 -6 0 5512.03 4997.17 52.75 o 3 -6 0 800.78 748.83 8.52 o 4 -6 0 2597.24 2467.67 20.22 o 5 -6 0 110.82 104.18 2.69 o 6 -6 0 465.27 426.98 6.17 o 7 -6 0 341.19 334.47 5.36 o 8 -6 0 44.65 40.38 1.82 o 9 -6 0 433.84 412.75 8.15 o 10 -6 0 265.01 260.05 5.60 o 11 -6 0 361.62 327.75 6.16 o 12 -6 0 852.51 767.06 15.54 o 1 -5 0 886.92 723.06 11.44 o 2 -5 0 1011.31 878.86 8.24 o 3 -5 0 1534.55 1393.33 15.82 o 4 -5 0 963.75 825.04 8.98 o 5 -5 0 61.54 62.28 2.05 o 6 -5 0 208.25 214.27 4.42 o 7 -5 0 682.34 646.71 8.72 o 8 -5 0 219.56 202.70 3.57 o 9 -5 0 974.29 924.50 10.24 o 10 -5 0 869.44 847.78 10.70 o 11 -5 0 209.81 196.23 4.27 o 12 -5 0 13.37 15.56 1.42 o 1 -4 0 2539.19 2273.79 27.60 o 2 -4 0 1324.01 1187.90 11.36 o 3 -4 0 1206.74 1078.99 11.94 o 4 -4 0 3372.58 3035.48 38.11 o 5 -4 0 43.19 37.48 1.60 o 6 -4 0 1097.17 1002.16 10.67 o 7 -4 0 105.39 105.92 3.59 o 8 -4 0 12.43 15.37 2.03 o 9 -4 0 511.16 483.85 6.88 o 10 -4 0 366.32 369.42 6.29 o 11 -4 0 206.97 187.87 4.52 o 12 -4 0 433.15 432.80 8.70 o 1 -3 0 10918.35 9664.73 84.91 o 2 -3 0 21.05 16.93 1.22 o 3 -3 0 2804.34 2574.84 24.97 o 4 -3 0 1148.35 960.37 12.68 o 5 -3 0 3526.85 3333.54 40.52 o 6 -3 0 129.67 107.88 4.17 o 7 -3 0 207.73 217.59 5.96 o 8 -3 0 65.34 61.05 1.97 o 9 -3 0 625.53 597.59 7.76 o 10 -3 0 531.46 523.23 7.63 o 11 -3 0 144.36 155.11 4.12 o 12 -3 0 217.31 225.54 6.65 o 13 -3 0 221.10 206.33 7.48 o 1 -2 0 684.72 620.92 9.21 o 2 -2 0 4885.70 4586.93 43.02 o 3 -2 0 2589.55 2360.71 17.28 o 4 -2 0 10575.99 9901.91 107.32 o 5 -2 0 191.43 174.85 3.11 o 6 -2 0 706.84 660.54 8.64 o 7 -2 0 277.26 282.33 6.67 o 8 -2 0 588.98 604.63 6.63 o 9 -2 0 790.39 792.58 9.11 o 10 -2 0 116.02 114.81 3.21 o 11 -2 0 34.04 33.36 2.66 o 12 -2 0 623.66 639.06 9.70 o 13 -2 0 185.33 170.81 4.72 o 1 -1 0 3974.21 3743.76 33.64 o 2 -1 0 23603.31 22669.45 242.89 o 3 -1 0 7218.11 6824.70 40.12 o 4 -1 0 755.07 697.00 8.68 o 5 -1 0 1000.77 912.77 8.16 o 6 -1 0 521.56 538.80 7.57 o 7 -1 0 100.69 109.83 4.75 o 8 -1 0 60.99 60.98 2.03 o 9 -1 0 2642.50 2575.34 19.78 o 10 -1 0 193.32 196.50 4.19 o 11 -1 0 120.62 117.90 4.62 o 12 -1 0 55.02 53.00 2.38 o 13 -1 0 55.38 55.27 3.18 o 1 0 0 794.05 705.13 50.27 o 2 0 0 8829.23 8725.31 60.92 o 3 0 0 4434.86 4334.67 30.11 o 4 0 0 2953.25 2870.89 23.34 o 5 0 0 189.04 198.26 3.90 o 6 0 0 214.64 220.37 5.24 o 7 0 0 981.87 993.11 16.01 o 8 0 0 185.74 193.36 3.54 o 9 0 0 26.97 33.48 1.85 o 10 0 0 114.19 121.11 3.48 o 11 0 0 33.32 32.26 2.25 o 12 0 0 87.42 85.15 3.37 o 13 0 0 44.14 42.45 3.47 o 1 1 0 3984.44 3862.54 29.08 o 2 1 0 23594.21 23034.61 176.90 o 3 1 0 7223.54 7095.21 51.42 o 4 1 0 758.12 695.74 12.01 o 5 1 0 1003.43 941.47 12.63 o 6 1 0 531.68 563.84 8.16 o 7 1 0 102.73 115.65 4.23 o 8 1 0 60.82 61.38 1.89 o 9 1 0 2634.24 2659.92 18.91 o 10 1 0 191.22 198.17 4.79 o 11 1 0 121.02 122.11 4.30 o 12 1 0 53.86 51.12 2.64 o 13 1 0 55.43 53.52 2.85 o 0 2 0 7785.68 7317.61 124.42 o 1 2 0 719.89 682.39 5.66 o 2 2 0 4892.85 4693.03 54.47 o 3 2 0 2583.01 2525.11 19.11 o 4 2 0 10542.42 10417.95 88.68 o 5 2 0 194.00 187.42 4.04 o 6 2 0 709.92 701.87 12.58 o 7 2 0 280.82 297.80 6.32 o 8 2 0 594.45 635.60 6.39 o 9 2 0 790.97 831.26 9.11 o 10 2 0 118.56 124.86 3.47 o 11 2 0 33.26 33.12 2.07 o 12 2 0 620.13 657.59 13.89 o 13 2 0 186.53 193.31 5.43 o 1 3 0 10894.83 10392.11 222.42 o 2 3 0 21.29 17.15 0.92 o 3 3 0 2808.82 2789.84 18.09 o 4 3 0 1155.27 1040.96 9.77 o 5 3 0 3547.02 3566.63 44.95 o 6 3 0 127.58 104.73 3.40 o 7 3 0 211.93 234.64 5.63 o 8 3 0 66.19 69.19 2.26 o 9 3 0 618.10 641.82 8.33 o 10 3 0 531.32 567.98 7.68 o 11 3 0 146.95 165.81 4.21 o 12 3 0 219.54 233.76 5.28 o 13 3 0 224.02 246.99 6.14 o 0 4 0 53005.70 45974.48 2193.60 o 1 4 0 2541.85 2503.12 31.20 o 2 4 0 1334.02 1316.58 16.63 o 3 4 0 1204.39 1209.27 18.90 o 4 4 0 3395.85 3408.16 66.92 o 5 4 0 41.64 41.61 1.98 o 6 4 0 1097.43 1081.51 12.37 o 7 4 0 106.40 104.67 4.93 o 8 4 0 12.26 11.08 1.02 o 9 4 0 511.71 534.80 7.49 o 10 4 0 367.95 412.36 6.88 o 11 4 0 204.88 209.65 4.72 o 12 4 0 435.00 462.69 7.74 o 1 5 0 888.81 803.56 8.62 o 2 5 0 1001.93 990.24 9.08 o 3 5 0 1531.90 1559.06 17.11 o 4 5 0 954.94 916.66 8.78 o 5 5 0 62.35 69.81 2.30 o 6 5 0 206.46 231.53 5.18 o 7 5 0 690.95 715.32 11.44 o 8 5 0 219.80 230.59 4.29 o 9 5 0 978.25 1030.13 10.34 o 10 5 0 869.62 944.55 11.01 o 11 5 0 209.95 224.44 5.37 o 12 5 0 14.80 17.48 1.90 o 0 6 0 22281.75 21423.27 301.06 o 1 6 0 2748.88 2541.07 21.91 o 2 6 0 5496.10 5677.71 51.30 o 3 6 0 811.15 865.65 8.02 o 4 6 0 2595.13 2822.19 31.17 o 5 6 0 107.14 112.90 3.22 o 6 6 0 467.78 463.12 9.04 o 7 6 0 345.71 389.00 6.45 o 8 6 0 46.25 52.77 2.36 o 9 6 0 432.99 462.30 8.01 o 10 6 0 261.94 307.40 6.33 o 11 6 0 365.93 388.01 7.04 o 12 6 0 843.63 870.66 13.10 o 1 7 0 1139.20 1226.03 19.26 o 2 7 0 3530.01 3825.61 47.72 o 3 7 0 2805.54 3188.45 35.99 o 4 7 0 1935.62 2133.46 19.51 o 5 7 0 1688.05 1888.64 22.01 o 6 7 0 684.98 719.11 11.05 o 7 7 0 837.97 884.96 9.61 o 8 7 0 255.98 281.70 4.57 o 9 7 0 262.41 273.54 6.04 o 10 7 0 358.64 402.24 7.85 o 11 7 0 771.07 864.71 11.53 o 12 7 0 161.84 173.36 4.98 o 0 8 0 902.06 916.89 10.90 o 1 8 0 9464.22 9942.04 88.77 o 2 8 0 1586.69 1768.20 25.20 o 3 8 0 1247.29 1429.23 21.23 o 4 8 0 1807.79 2155.61 22.89 o 5 8 0 578.55 692.34 9.66 o 6 8 0 1141.35 1247.75 16.23 o 7 8 0 162.83 173.42 3.65 o 8 8 0 196.69 209.52 4.74 o 9 8 0 453.96 485.70 10.19 o 10 8 0 71.17 77.04 3.74 o 11 8 0 77.11 101.52 4.89 o 12 8 0 665.58 714.30 26.35 o 1 9 0 9732.34 11009.84 85.46 o 2 9 0 1907.24 2110.70 24.66 o 3 9 0 7043.30 8209.78 58.68 o 4 9 0 2534.29 2953.14 30.66 o 5 9 0 1881.03 2197.04 21.75 o 6 9 0 181.11 200.38 4.52 o 7 9 0 124.96 134.58 3.36 o 8 9 0 76.27 73.41 2.86 o 9 9 0 607.37 680.32 9.99 o 10 9 0 436.51 484.37 8.74 o 11 9 0 391.44 451.89 6.78 o 12 9 0 370.74 390.33 12.40 o 0 10 0 742.28 717.30 10.40 o 1 10 0 3265.95 3823.48 32.07 o 2 10 0 16.63 27.05 1.86 o 3 10 0 1729.43 1951.04 26.68 o 4 10 0 2915.01 3370.05 41.94 o 5 10 0 2517.33 2895.91 30.64 o 6 10 0 87.70 105.50 2.71 o 7 10 0 282.04 319.71 5.07 o 8 10 0 96.35 98.76 3.65 o 9 10 0 378.59 400.45 7.36 o 10 10 0 15.80 21.39 2.04 o 11 10 0 881.82 975.97 11.54 o 12 10 0 547.18 624.17 11.37 o 1 11 0 1039.12 1137.78 11.95 o 2 11 0 1761.61 2058.50 23.33 o 3 11 0 1519.13 1679.33 24.52 o 4 11 0 110.68 121.49 4.13 o 5 11 0 890.43 1133.22 17.23 o 6 11 0 1101.27 1247.96 10.44 o 7 11 0 155.51 174.11 3.81 o 8 11 0 127.08 134.85 4.25 o 9 11 0 281.25 304.41 6.24 o 10 11 0 19.96 25.73 1.71 o 11 11 0 39.43 49.80 2.51 o 0 12 0 4195.67 4456.49 44.57 o 1 12 0 341.77 334.96 6.55 o 2 12 0 354.06 440.84 8.75 o 3 12 0 129.35 135.91 5.46 o 4 12 0 685.77 849.17 16.20 o 5 12 0 790.25 917.21 10.08 o 6 12 0 804.16 951.20 9.64 o 7 12 0 9.57 10.55 1.45 o 8 12 0 386.09 440.02 7.30 o 9 12 0 29.49 31.21 2.24 o 10 12 0 164.15 192.48 4.96 o 11 12 0 79.94 90.19 3.06 o 1 13 0 7055.99 7384.54 74.52 o 2 13 0 18.39 17.98 2.67 o 3 13 0 273.66 284.27 9.49 o 4 13 0 30.64 37.62 1.43 o 5 13 0 222.69 266.07 4.25 o 6 13 0 160.63 172.79 4.08 o 7 13 0 366.12 412.26 6.69 o 8 13 0 258.82 291.70 5.88 o 9 13 0 25.51 30.22 2.40 o 10 13 0 4.61 4.50 1.27 o 11 13 0 5.75 8.13 1.22 o 0 14 0 224.24 190.74 11.27 o 1 14 0 180.92 222.01 10.01 o 2 14 0 80.22 95.88 3.34 o 3 14 0 44.53 50.05 1.81 o 4 14 0 54.05 60.66 2.96 o 5 14 0 602.65 665.46 7.42 o 6 14 0 233.55 261.06 5.30 o 7 14 0 376.13 444.23 6.99 o 8 14 0 215.84 261.22 6.81 o 9 14 0 13.77 13.13 1.90 o 10 14 0 69.54 77.18 3.04 o 1 15 0 248.73 248.90 6.05 o 2 15 0 557.76 639.42 9.15 o 3 15 0 164.43 186.36 3.81 o 4 15 0 256.59 284.90 6.76 o 5 15 0 936.73 1111.68 16.85 o 6 15 0 265.20 301.62 7.97 o 7 15 0 729.64 844.43 13.11 o 8 15 0 6.85 8.55 1.33 o 9 15 0 310.31 379.54 7.69 o 10 15 0 54.67 59.30 3.00 o 0 16 0 2828.60 3024.18 64.16 o 1 16 0 19223.44 21407.21 241.24 o 2 16 0 356.43 410.75 6.51 o 3 16 0 1615.05 1856.24 27.87 o 4 16 0 26.50 29.34 2.10 o 5 16 0 437.13 451.28 8.41 o 6 16 0 12.65 10.72 1.79 o 7 16 0 170.70 205.77 5.66 o 8 16 0 402.33 476.38 8.13 o 9 16 0 398.67 459.45 12.66 o 10 16 0 24.54 28.24 1.84 o 1 17 0 1223.01 1399.99 14.47 o 2 17 0 2145.66 2399.79 24.04 o 3 17 0 154.85 153.01 4.50 o 4 17 0 319.26 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5.66 o -5 3 14 14.17 14.53 1.28 o -4 3 14 1134.96 1158.22 10.72 o -3 3 14 293.94 290.36 5.85 o -2 3 14 57.63 57.75 2.10 o -1 3 14 90.95 95.42 2.94 o 0 3 14 21.36 21.55 1.60 o -6 4 14 56.79 63.63 1.97 o -5 4 14 47.34 54.29 2.44 o -4 4 14 185.67 197.56 4.32 o -3 4 14 74.15 72.41 2.25 o -2 4 14 382.89 391.47 7.48 o -1 4 14 325.39 324.31 8.01 o 0 4 14 75.78 82.20 2.47 o -6 5 14 165.89 183.52 5.25 o -5 5 14 266.18 290.50 4.59 o -4 5 14 709.30 785.95 12.38 o -3 5 14 286.29 275.97 5.92 o -2 5 14 212.48 203.25 6.22 o -1 5 14 51.98 49.22 1.92 o 0 5 14 244.23 195.44 7.79 o -6 6 14 144.31 167.55 6.68 o -5 6 14 264.88 284.71 7.45 o -4 6 14 84.16 90.61 2.64 o -3 6 14 393.58 409.70 8.76 o -2 6 14 11.08 10.78 1.31 o -1 6 14 46.51 44.76 2.77 o -5 7 14 28.93 31.65 2.06 o -4 7 14 245.24 273.53 8.31 o -3 7 14 51.84 55.32 2.78 o -2 7 14 44.60 52.02 2.59 o -4 8 14 35.96 38.52 3.20 o -3 8 14 64.33 63.54 4.12 o