#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/72/2237277.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237277_Fobs loop_ _publ_author_name 'Schumer, Benjamin N.' 'Downs, Robert T.' 'Domanik, Kenneth J.' 'Andrade, Marcelo B.' 'Origlieri, Marcus J.' _publ_section_title ; Pirquitasite, Ag~2~ZnSnS~4~ ; _journal_coeditor_code BR2219 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i8 _journal_page_last i9 _journal_volume 69 _journal_year 2013 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.7757 _cell_length_b 5.7757 _cell_length_c 10.8696 _exptl_crystal_F_000 469.52 _reflns_d_resolution_high 0.6701 _[local]_cod_data_source_file br2219Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pir2 in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 296.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 1509.70 1385.08 39.45 o 0 2 0 31592.52 29533.92 208.36 o 2 2 0 88030.37 81493.65 977.57 o -1 3 0 1106.04 1078.98 20.81 o 1 3 0 836.17 797.22 15.89 o 3 3 0 564.77 555.18 19.63 o -2 4 0 11027.22 10665.01 118.07 o 0 4 0 49805.24 48212.82 344.72 o 2 4 0 11069.41 11281.72 101.21 o 4 4 0 20717.15 20896.25 214.76 o -3 5 0 613.09 568.01 29.73 o -1 5 0 316.30 332.17 21.08 o 1 5 0 669.85 726.72 38.72 o 3 5 0 411.82 411.33 21.49 o 5 5 0 224.79 256.39 26.15 o -4 6 0 2550.48 2556.81 130.21 o -2 6 0 14300.81 13889.54 159.47 o 0 6 0 4841.40 4732.29 72.62 o 2 6 0 14182.96 14231.64 150.31 o 4 6 0 2597.97 2615.38 109.87 o 6 6 0 3876.05 3830.43 81.31 o -5 7 0 298.55 277.68 30.87 o -3 7 0 127.08 146.57 23.31 o -1 7 0 509.11 518.39 44.27 o 1 7 0 176.78 177.87 20.30 o 3 7 0 314.92 309.02 26.25 o 5 7 0 211.32 202.79 26.01 o -2 8 0 1486.08 1585.84 74.23 o 0 8 0 5281.96 5046.95 84.74 o 2 8 0 1536.82 1572.62 53.92 o 1 0 1 702.06 602.02 9.83 o 3 0 1 649.59 810.65 18.35 o 5 0 1 708.30 684.40 23.45 o 7 0 1 256.81 242.88 23.46 o -8 1 1 533.57 441.03 35.78 o -6 1 1 103.48 169.53 15.81 o -4 1 1 1028.60 930.02 23.57 o 0 1 1 639.10 555.72 11.11 o 2 1 1 1138.36 1213.15 18.93 o 4 1 1 136.01 189.98 15.36 o 6 1 1 740.99 667.98 30.49 o 8 1 1 197.59 178.23 23.70 o -7 2 1 513.18 562.64 28.02 o -5 2 1 553.90 549.58 22.34 o -3 2 1 374.58 328.89 14.87 o -1 2 1 1225.72 1344.96 27.04 o 3 2 1 948.67 785.43 48.40 o 5 2 1 191.68 228.90 25.44 o 7 2 1 659.17 691.98 38.37 o -8 3 1 104.96 70.05 25.07 o -6 3 1 814.09 758.90 29.28 o -4 3 1 63.11 164.15 14.52 o -2 3 1 877.47 787.35 25.08 o 0 3 1 587.20 761.84 16.39 o 2 3 1 341.67 358.02 12.10 o 4 3 1 747.16 775.38 29.33 o 6 3 1 310.11 374.05 28.42 o 8 3 1 358.04 282.34 29.71 o -7 4 1 338.60 291.52 29.20 o -5 4 1 463.07 505.25 30.67 o -3 4 1 828.38 849.79 31.73 o -1 4 1 155.43 169.36 12.24 o 1 4 1 1113.52 1040.71 17.84 o 3 4 1 86.65 171.33 14.88 o 5 4 1 892.51 818.29 35.65 o 7 4 1 106.50 14.33 28.02 o -6 5 1 74.98 86.99 22.37 o -4 5 1 837.09 834.17 104.82 o -2 5 1 152.76 199.11 18.58 o 0 5 1 667.83 641.41 23.30 o 2 5 1 485.74 463.38 19.63 o 4 5 1 452.88 487.29 28.33 o 6 5 1 380.92 341.41 29.72 o -5 6 1 434.33 407.44 32.83 o -3 6 1 315.83 307.90 25.78 o -1 6 1 814.95 823.58 37.65 o 1 6 1 114.42 134.14 14.06 o 3 6 1 875.48 922.48 34.54 o 5 6 1 86.34 89.16 33.18 o -4 7 1 89.12 16.14 36.50 o -2 7 1 624.60 680.18 36.16 o 0 7 1 213.67 167.33 23.60 o 2 7 1 498.16 494.54 26.95 o 4 7 1 292.08 228.93 58.63 o -3 8 1 400.98 444.39 34.56 o -1 8 1 202.30 180.99 27.65 o 1 8 1 580.41 591.89 29.99 o 3 8 1 111.46 67.10 18.43 o 0 0 2 1306.37 1167.93 22.36 o 2 0 2 1468.58 1404.82 21.08 o 4 0 2 590.22 571.55 20.04 o 6 0 2 452.45 476.15 26.36 o 8 0 2 238.41 208.08 25.47 o -7 1 2 5649.40 5578.22 90.46 o -5 1 2 17158.25 17559.31 153.23 o -3 1 2 43720.97 43187.56 336.65 o -1 1 2 87997.52 92595.15 1131.10 o 1 1 2 85926.97 88568.55 557.47 o 3 1 2 44768.15 44172.37 356.00 o 5 1 2 16722.62 16104.11 139.02 o 7 1 2 5818.69 5665.91 91.64 o -8 2 2 234.11 278.75 29.50 o -6 2 2 328.03 300.97 20.70 o -4 2 2 684.84 670.83 21.72 o -2 2 2 787.53 787.78 22.62 o 0 2 2 1468.71 1407.18 15.61 o 2 2 2 787.70 773.18 13.69 o 4 2 2 698.98 730.12 46.47 o 6 2 2 350.68 349.34 34.30 o 8 2 2 247.34 207.49 26.46 o -7 3 2 4202.81 4174.49 80.33 o -5 3 2 11291.33 11498.91 137.53 o -3 3 2 26712.04 26477.47 249.96 o -1 3 2 43611.35 44193.55 311.86 o 1 3 2 44876.53 44519.32 309.70 o 3 3 2 25912.26 25013.82 163.64 o 5 3 2 11687.59 11828.20 153.97 o 7 3 2 4099.01 4036.91 79.93 o -6 4 2 302.21 279.13 27.99 o -4 4 2 384.15 376.54 34.30 o -2 4 2 700.54 718.76 22.93 o 0 4 2 589.18 632.96 15.00 o 2 4 2 685.13 722.79 15.88 o 4 4 2 385.68 400.35 23.92 o 6 4 2 315.24 318.78 27.93 o -5 5 2 5783.65 6118.41 124.85 o -3 5 2 11250.57 11553.90 139.01 o -1 5 2 17310.96 17536.78 177.02 o 1 5 2 16573.12 16927.28 120.19 o 3 5 2 11723.52 12358.95 135.72 o 5 5 2 5543.91 5361.86 85.86 o -6 6 2 198.45 185.59 28.17 o -4 6 2 319.07 310.29 28.91 o -2 6 2 346.45 315.63 24.10 o 0 6 2 455.92 463.73 26.56 o 2 6 2 326.09 338.42 35.43 o 4 6 2 301.96 301.33 40.56 o 6 6 2 200.62 199.27 36.13 o -3 7 2 4282.06 4417.69 92.68 o -1 7 2 5574.71 5777.72 87.75 o 1 7 2 5889.56 6247.57 83.96 o 3 7 2 4026.96 3914.03 68.93 o -2 8 2 252.74 299.46 28.09 o 0 8 2 233.52 200.10 23.23 o 1 0 3 634.42 785.54 18.03 o 3 0 3 616.27 565.91 20.89 o 5 0 3 266.02 295.88 18.11 o 7 0 3 629.75 685.48 62.35 o -8 1 3 143.28 113.29 21.93 o -6 1 3 826.17 777.04 28.61 o -4 1 3 100.66 127.44 12.81 o -2 1 3 922.74 857.58 56.94 o 0 1 3 694.39 792.00 13.14 o 2 1 3 240.30 222.30 15.08 o 4 1 3 846.80 850.61 23.58 o 6 1 3 211.42 203.26 21.73 o 8 1 3 452.52 395.91 31.54 o -7 2 3 231.83 147.91 19.18 o -5 2 3 602.98 642.60 46.40 o -3 2 3 587.63 617.12 24.17 o -1 2 3 201.10 196.86 19.67 o 1 2 3 843.70 787.99 22.80 o 3 2 3 185.14 311.31 12.23 o 5 2 3 884.12 911.85 32.60 o 7 2 3 105.33 122.24 45.72 o -6 3 3 79.69 70.69 49.03 o -4 3 3 1044.72 1062.02 35.43 o -2 3 3 224.06 353.43 28.03 o 0 3 3 672.05 630.27 12.29 o 2 3 3 658.26 701.86 16.73 o 4 3 3 384.92 375.33 22.51 o 6 3 3 516.86 439.18 29.68 o -7 4 3 435.54 478.44 147.16 o -5 4 3 382.84 377.48 30.24 o -3 4 3 363.59 386.14 20.14 o -1 4 3 768.12 744.68 22.71 o 1 4 3 75.93 163.83 17.98 o 3 4 3 975.93 986.24 27.83 o 5 4 3 60.42 103.58 29.12 o 7 4 3 616.22 593.25 37.03 o -6 5 3 713.38 733.77 110.32 o -4 5 3 83.67 94.52 22.86 o -2 5 3 935.93 1016.61 60.92 o 0 5 3 317.84 367.34 14.01 o 2 5 3 630.57 662.13 50.19 o 4 5 3 442.98 402.37 23.23 o 6 5 3 388.87 380.66 29.56 o -5 6 3 380.72 378.60 33.85 o -3 6 3 457.41 392.51 28.78 o -1 6 3 197.25 203.32 18.53 o 1 6 3 761.44 744.95 81.56 o 3 6 3 64.78 88.48 31.70 o 5 6 3 671.61 736.38 32.25 o -4 7 3 649.43 689.18 43.16 o -2 7 3 134.67 72.96 18.23 o 0 7 3 656.41 739.84 64.20 o -1 8 3 410.33 376.98 25.43 o 0 0 4 29434.19 28431.49 346.23 o 2 0 4 84942.57 85724.52 1675.75 o 4 0 4 10372.11 10081.88 94.68 o 6 0 4 14028.27 13747.92 132.52 o 8 0 4 1436.92 1388.84 49.28 o -7 1 4 410.29 416.98 28.91 o -5 1 4 346.46 348.10 25.19 o -3 1 4 831.76 813.22 34.72 o -1 1 4 1170.33 1063.07 23.56 o 1 1 4 1170.68 1094.75 17.74 o 3 1 4 631.11 620.81 24.85 o 5 1 4 675.43 682.92 25.62 o 7 1 4 137.08 103.25 25.81 o -8 2 4 3823.36 3618.37 104.44 o -6 2 4 3303.96 3309.64 67.37 o -4 2 4 30594.14 30577.83 289.84 o -2 2 4 17069.52 17256.75 136.78 o 0 2 4 84939.37 89841.91 535.17 o 2 2 4 17073.73 17564.20 134.45 o 4 2 4 30653.38 29925.65 281.49 o 6 2 4 3254.52 3347.43 65.97 o 8 2 4 3897.19 3798.01 81.44 o -7 3 4 196.90 176.74 25.63 o -5 3 4 382.77 379.11 28.04 o -3 3 4 669.72 689.15 57.95 o -1 3 4 632.04 661.53 16.04 o 1 3 4 830.83 842.97 22.15 o 3 3 4 671.08 708.20 16.66 o 5 3 4 238.71 228.50 20.89 o 7 3 4 400.97 414.67 31.61 o -6 4 4 7061.44 7535.11 133.21 o -4 4 4 4591.54 4926.74 82.95 o -2 4 4 30654.16 31395.57 259.40 o 0 4 4 10379.37 10745.31 69.14 o 2 4 4 30584.03 30436.24 292.18 o 4 4 4 4598.97 4475.74 66.47 o 6 4 4 7129.35 7022.29 184.95 o -5 5 4 352.77 352.91 32.22 o -3 5 4 240.23 240.17 23.62 o -1 5 4 673.86 689.82 39.86 o 1 5 4 348.03 407.20 39.83 o 3 5 4 381.25 357.77 40.57 o 5 5 4 353.91 389.42 25.33 o -4 6 4 7132.97 7020.94 141.04 o -2 6 4 3256.11 3242.38 61.20 o 0 6 4 14020.57 13981.06 143.07 o 4 6 4 7053.13 6878.59 166.70 o -3 7 4 399.97 382.40 30.83 o -1 7 4 138.36 129.30 17.60 o -2 8 4 3895.61 3801.17 72.21 o 0 8 4 1441.82 1422.49 85.67 o 1 0 5 454.82 487.03 13.20 o 3 0 5 488.00 415.43 43.91 o 5 0 5 343.48 303.52 31.74 o 7 0 5 474.61 462.56 32.97 o -8 1 5 147.95 143.79 33.92 o -6 1 5 724.18 676.65 35.61 o -4 1 5 92.98 168.72 17.64 o -2 1 5 696.07 597.65 17.45 o 0 1 5 397.08 457.15 13.09 o 2 1 5 150.74 179.24 19.91 o 4 1 5 811.69 794.48 26.29 o 6 1 5 208.11 262.73 23.99 o 8 1 5 433.00 468.05 35.73 o -7 2 5 330.93 321.36 30.83 o -5 2 5 464.23 470.13 29.09 o -3 2 5 686.06 790.68 36.18 o -1 2 5 179.90 173.91 15.86 o 1 2 5 771.88 699.63 11.49 o 3 2 5 175.70 202.99 14.39 o 5 2 5 682.71 670.08 30.37 o 7 2 5 175.03 98.76 21.11 o -6 3 5 103.92 131.50 37.60 o -4 3 5 796.33 769.24 78.62 o -2 3 5 139.35 178.59 14.01 o 0 3 5 441.37 416.10 10.32 o 2 3 5 610.18 647.55 13.65 o 4 3 5 317.85 411.88 22.78 o 6 3 5 537.55 540.92 32.26 o -7 4 5 351.89 303.10 32.75 o -5 4 5 532.37 537.07 42.79 o -3 4 5 326.13 393.34 21.66 o -1 4 5 896.41 941.01 23.74 o 1 4 5 108.48 190.95 19.65 o 3 4 5 865.78 876.38 50.94 o 5 4 5 117.04 100.35 16.86 o 7 4 5 496.00 509.25 34.18 o -6 5 5 539.93 523.00 39.70 o -4 5 5 98.39 117.59 22.35 o -2 5 5 634.22 623.58 29.73 o 0 5 5 290.24 299.46 36.14 o 2 5 5 446.38 546.68 45.74 o 4 5 5 466.89 526.00 52.38 o 6 5 5 323.09 348.12 50.15 o -5 6 5 322.86 376.76 35.46 o -3 6 5 603.47 680.92 37.04 o -1 6 5 210.81 258.87 18.76 o 1 6 5 793.45 853.98 62.74 o 5 6 5 582.48 545.22 59.76 o -4 7 5 463.08 404.85 34.45 o -2 7 5 148.19 102.04 18.82 o 0 7 5 451.91 464.74 53.85 o -1 8 5 479.28 516.37 60.49 o 0 0 6 1510.91 1401.62 39.24 o 2 0 6 395.50 384.19 15.90 o 4 0 6 765.86 823.13 32.84 o 6 0 6 244.48 240.31 34.66 o 8 0 6 245.17 312.68 42.04 o -7 1 6 3975.32 3896.90 138.21 o -5 1 6 10833.53 10502.25 137.99 o -3 1 6 25001.81 23836.35 229.74 o -1 1 6 40445.09 40905.54 291.85 o 1 1 6 41594.45 41981.19 297.22 o 3 1 6 24407.18 23470.24 266.92 o 5 1 6 11014.13 11429.62 162.03 o 7 1 6 3988.79 3725.47 107.46 o -6 2 6 385.01 440.65 32.42 o -4 2 6 286.22 279.16 22.88 o -2 2 6 1024.21 1012.71 25.44 o 0 2 6 395.40 436.52 12.13 o 2 2 6 1024.01 1023.74 19.52 o 4 2 6 297.77 294.25 44.26 o 6 2 6 400.88 405.71 44.26 o -7 3 6 3028.94 3142.26 76.92 o -5 3 6 7593.91 7937.53 116.85 o -3 3 6 15875.34 16247.93 161.42 o -1 3 6 25214.02 25885.24 169.45 o 1 3 6 24195.86 24881.03 195.11 o 3 3 6 16468.25 16894.55 179.94 o 5 3 6 7405.54 6863.84 149.05 o 7 3 6 3072.52 3132.04 108.79 o -6 4 6 194.44 182.43 43.14 o -4 4 6 469.57 506.04 26.83 o -2 4 6 296.13 286.75 17.98 o 0 4 6 766.98 828.94 13.62 o 2 4 6 285.99 262.59 33.19 o 4 4 6 468.03 485.44 45.74 o 6 4 6 208.22 196.90 40.56 o -5 5 6 4013.02 4317.79 88.30 o -3 5 6 7735.86 7867.99 111.54 o -1 5 6 10571.33 11352.19 126.06 o 1 5 6 11273.82 10706.65 195.12 o 3 5 6 7267.40 6773.80 151.26 o 5 5 6 4195.01 4332.10 131.21 o -4 6 6 204.75 225.63 28.70 o -2 6 6 404.74 454.21 28.04 o 0 6 6 241.34 239.69 39.09 o -3 7 6 2933.12 3019.02 67.64 o -1 7 6 4173.88 3982.85 126.76 o 1 0 7 379.80 335.04 14.87 o 3 0 7 186.87 183.42 15.02 o 5 0 7 715.56 723.62 36.00 o 7 0 7 118.99 47.93 27.28 o -6 1 7 130.35 101.89 31.34 o -4 1 7 748.95 761.07 31.27 o -2 1 7 156.23 151.03 12.76 o 0 1 7 433.06 372.59 25.37 o 2 1 7 464.16 440.29 17.45 o 4 1 7 240.09 208.92 23.23 o 6 1 7 492.58 469.36 59.76 o -7 2 7 494.72 501.18 70.45 o -5 2 7 213.12 161.20 21.88 o -3 2 7 477.37 442.97 29.10 o -1 2 7 402.53 404.75 30.69 o 1 2 7 121.41 137.43 8.07 o 3 2 7 786.31 838.70 25.23 o 5 2 7 81.65 48.66 25.07 o 7 2 7 598.61 595.40 56.07 o -6 3 7 685.74 785.92 36.62 o -4 3 7 79.25 103.00 15.95 o -2 3 7 846.01 895.52 27.03 o 0 3 7 232.47 293.36 14.21 o 2 3 7 514.24 490.85 12.98 o 4 3 7 398.24 286.23 36.15 o 6 3 7 328.17 273.63 39.83 o -5 4 7 463.11 483.43 33.09 o -3 4 7 342.31 286.04 20.81 o -1 4 7 214.15 231.88 16.00 o 1 4 7 684.58 755.82 48.71 o 3 4 7 56.67 98.06 27.28 o 5 4 7 742.19 690.75 59.78 o -4 5 7 785.79 840.27 49.82 o -2 5 7 112.26 92.42 18.14 o 0 5 7 754.69 882.03 59.05 o 4 5 7 481.85 475.09 50.90 o -3 6 7 312.28 301.50 47.94 o -1 6 7 442.25 443.21 20.70 o -2 7 7 627.10 773.50 60.50 o 0 0 8 45072.73 44102.30 538.78 o 2 0 8 8629.55 8431.61 82.81 o 4 0 8 19337.12 18831.25 164.01 o 6 0 8 2087.51 2127.03 93.16 o -7 1 8 144.46 124.58 25.62 o -5 1 8 428.68 395.31 24.89 o -3 1 8 487.10 515.61 23.29 o -1 1 8 663.86 676.29 20.97 o 1 1 8 662.70 647.07 19.92 o 3 1 8 612.74 633.40 23.70 o 5 1 8 227.47 206.98 23.47 o 7 1 8 350.22 277.32 42.78 o -6 2 8 6811.30 6813.37 92.34 o -4 2 8 3887.53 3941.20 67.21 o -2 2 8 28830.60 28925.27 225.94 o 0 2 8 8633.27 8743.20 82.52 o 2 2 8 28825.57 29229.84 222.30 o 4 2 8 3874.62 3926.27 56.28 o 6 2 8 6867.91 6561.61 154.00 o -5 3 8 295.21 357.70 26.08 o -3 3 8 359.23 419.78 23.35 o -1 3 8 610.44 577.08 22.69 o 1 3 8 489.40 560.10 31.12 o 3 3 8 356.47 340.94 17.01 o 5 3 8 415.80 416.13 27.15 o -6 4 8 1274.56 1238.73 51.93 o -4 4 8 9467.48 9410.30 163.10 o -2 4 8 3873.84 3879.11 56.56 o 0 4 8 19327.64 19919.45 161.61 o 4 4 8 9457.94 9203.15 104.97 o 6 4 8 1254.81 1148.58 38.69 o -5 5 8 165.88 154.72 27.80 o -3 5 8 413.20 414.41 31.54 o -1 5 8 230.32 242.96 18.84 o -4 6 8 1250.25 1394.92 80.85 o -2 6 8 6865.62 7388.61 103.65 o 1 0 9 351.99 300.08 16.17 o 3 0 9 321.12 258.71 17.89 o 5 0 9 412.14 430.24 43.68 o 7 0 9 237.55 124.67 25.03 o -6 1 9 172.45 220.12 22.83 o -4 1 9 575.33 590.74 27.77 o -2 1 9 176.43 144.51 24.15 o 0 1 9 307.82 281.78 19.22 o 2 1 9 458.39 485.29 20.57 o 4 1 9 239.04 306.57 20.11 o 6 1 9 487.80 534.49 30.09 o -5 2 9 394.53 354.92 25.35 o -3 2 9 345.24 362.81 21.42 o -1 2 9 526.59 538.86 22.45 o 1 2 9 203.75 206.61 17.33 o 3 2 9 528.86 526.23 23.27 o 5 2 9 201.35 121.13 20.68 o -6 3 9 463.31 486.14 32.46 o -4 3 9 144.11 150.61 22.38 o -2 3 9 476.27 471.47 30.78 o 0 3 9 270.31 224.80 20.65 o 2 3 9 328.24 326.97 18.87 o 4 3 9 482.39 481.91 42.79 o 6 3 9 262.36 278.37 27.01 o -5 4 9 322.67 381.78 28.87 o -3 4 9 550.33 673.01 31.09 o -1 4 9 245.45 243.63 17.67 o 1 4 9 644.06 695.90 51.66 o 5 4 9 478.41 426.05 74.14 o -4 5 9 437.07 392.58 34.66 o -2 5 9 172.54 107.72 19.84 o -3 6 9 260.69 320.05 42.41 o 0 0 10 139.22 141.58 24.33 o 2 0 10 828.34 742.77 25.78 o 4 0 10 144.82 160.41 17.97 o 6 0 10 341.45 359.70 27.10 o -5 1 10 5003.98 5135.77 76.85 o -3 1 10 9784.56 9722.54 103.13 o -1 1 10 14746.21 14343.76 156.55 o 1 1 10 14141.21 13824.58 150.63 o 3 1 10 10086.72 9846.85 101.26 o 5 1 10 4979.54 4665.75 71.26 o -6 2 10 136.70 114.12 21.13 o -4 2 10 502.04 533.66 44.93 o -2 2 10 141.05 164.94 16.84 o 0 2 10 828.52 803.79 33.96 o 2 2 10 141.34 119.02 16.27 o 4 2 10 507.94 507.63 25.06 o 6 2 10 147.57 109.03 22.66 o -5 3 10 3743.19 4018.02 72.10 o -3 3 10 7042.55 6831.66 86.40 o -1 3 10 9635.07 9837.22 220.00 o 1 3 10 10235.66 10863.77 123.60 o 3 3 10 6705.50 6578.70 88.17 o 5 3 10 3834.31 4013.18 145.22 o -4 4 10 142.81 103.57 19.91 o -2 4 10 509.48 515.49 27.02 o 0 4 10 143.76 172.01 16.75 o -3 5 10 3644.72 3971.68 80.92 o -1 5 10 5232.51 5431.26 94.30 o -2 6 10 144.56 116.50 22.86 o 1 0 11 209.97 234.02 21.36 o 3 0 11 543.50 541.93 26.25 o 5 0 11 95.93 60.04 16.65 o -6 1 11 442.65 440.91 34.65 o -4 1 11 144.07 105.32 18.06 o -2 1 11 526.35 497.18 30.25 o 0 1 11 249.67 256.62 21.83 o 2 1 11 318.81 292.63 23.72 o 4 1 11 384.87 366.07 43.86 o 6 1 11 210.24 130.36 26.90 o -5 2 11 471.86 481.59 31.23 o -3 2 11 183.20 194.45 20.01 o -1 2 11 284.73 287.45 23.52 o 1 2 11 476.45 485.90 28.04 o 3 2 11 81.83 64.73 15.54 o 5 2 11 596.99 699.44 48.70 o -4 3 11 628.72 638.51 33.91 o -2 3 11 108.14 101.76 19.79 o 0 3 11 585.53 672.21 53.13 o 2 3 11 222.70 206.18 29.87 o 4 3 11 362.85 376.91 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