#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/72/2237298.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237298_Fobs loop_ _publ_author_name 'Ghafoor, Ahmad Z.' 'Chang, Brian' 'King, Christopher L.' 'Butcher, Ray J.' 'Kulkarni, Amol A.' _publ_section_title ; Methyl 2-bromo-3-(4-chlorobenzenesulfonamido)benzoate ; _journal_coeditor_code DS2221 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o311 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.505 _cell_angle_gamma 90.000 _cell_length_a 7.9206 _cell_length_b 9.4600 _cell_length_c 20.0915 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.7950 _[local]_cod_data_source_file ds2221Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' amol12-1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12493.87 13971.70 108.34 o 2 0 0 4094.79 4648.79 79.96 o 3 0 0 1645.41 2134.75 68.53 o 4 0 0 3966.78 4046.80 70.01 o 5 0 0 6290.30 6106.46 139.62 o 6 0 0 3529.11 3268.18 86.17 o 7 0 0 1430.31 1325.71 48.50 o 8 0 0 465.73 449.44 25.92 o 9 0 0 2346.23 2478.18 49.33 o 1 1 0 1100.82 1114.58 21.90 o 2 1 0 1993.34 2105.00 24.71 o 3 1 0 4150.85 3648.39 62.06 o 4 1 0 6038.85 5895.85 90.13 o 5 1 0 5230.60 5280.26 87.40 o 6 1 0 4193.64 3910.50 44.53 o 7 1 0 2073.53 1956.67 41.28 o 8 1 0 36.13 57.00 6.94 o 9 1 0 6.30 14.13 5.40 o 0 2 0 4283.81 4410.82 47.02 o 2 2 0 5179.25 5351.85 163.12 o 3 2 0 3654.38 3501.56 93.30 o 4 2 0 4240.47 4174.03 112.64 o 5 2 0 269.44 292.58 21.79 o 6 2 0 1084.33 952.92 22.85 o 7 2 0 584.57 583.18 23.64 o 8 2 0 1219.22 1289.15 29.32 o 9 2 0 162.15 180.42 13.09 o 1 3 0 31.82 57.66 32.99 o 2 3 0 908.83 1081.47 53.70 o 3 3 0 186.69 208.23 24.98 o 4 3 0 3871.37 3703.33 111.50 o 5 3 0 2101.41 1987.16 96.72 o 6 3 0 223.83 222.56 11.22 o 7 3 0 79.32 69.20 7.74 o 8 3 0 681.69 772.07 21.18 o 9 3 0 40.52 33.40 6.75 o 0 4 0 77.00 79.29 8.17 o 1 4 0 138.22 138.35 8.25 o 2 4 0 1017.25 944.47 53.37 o 3 4 0 1060.17 979.17 57.86 o 4 4 0 2.36 2.37 6.16 o 5 4 0 7.39 10.45 3.80 o 6 4 0 226.82 219.66 19.96 o 7 4 0 597.61 642.45 33.63 o 8 4 0 231.04 259.29 19.65 o 9 4 0 42.86 38.52 14.16 o 1 5 0 121.26 139.10 20.73 o 2 5 0 1.75 7.20 6.80 o 3 5 0 404.87 396.26 40.36 o 4 5 0 1093.11 1156.63 68.38 o 5 5 0 18.51 19.72 4.95 o 6 5 0 134.36 132.92 15.75 o 7 5 0 105.90 112.65 14.81 o 8 5 0 58.34 54.62 6.13 o 0 6 0 171.02 188.13 22.28 o 1 6 0 23.56 28.17 9.70 o 2 6 0 1532.86 1759.63 84.66 o 3 6 0 557.62 638.89 53.21 o 4 6 0 762.94 738.26 27.13 o 5 6 0 1469.58 1440.04 55.76 o 6 6 0 25.31 29.51 6.55 o 7 6 0 245.84 225.74 17.03 o 8 6 0 252.84 251.50 14.21 o 1 7 0 1674.04 1647.28 34.28 o 2 7 0 753.10 766.73 24.80 o 3 7 0 3.04 6.15 4.17 o 4 7 0 426.84 417.66 27.35 o 5 7 0 1526.55 1402.83 49.41 o 6 7 0 0.19 6.51 4.91 o 7 7 0 1.22 2.94 3.55 o 8 7 0 1.61 3.21 1.78 o 0 8 0 2491.39 2258.22 117.47 o 1 8 0 1550.91 1398.85 48.92 o 2 8 0 470.18 499.44 26.64 o 3 8 0 609.39 585.98 29.58 o 4 8 0 26.43 43.63 9.24 o 5 8 0 1360.78 1343.03 42.08 o 6 8 0 235.61 238.64 15.29 o 7 8 0 137.79 126.59 8.01 o 1 9 0 337.01 297.00 12.47 o 2 9 0 202.63 224.25 16.69 o 3 9 0 2977.25 2803.32 57.22 o 4 9 0 752.83 713.11 27.39 o 5 9 0 122.09 117.31 10.00 o 6 9 0 660.60 673.80 13.85 o 0 10 0 2583.28 2523.45 44.86 o 1 10 0 1846.80 1867.51 26.60 o 2 10 0 621.08 583.17 21.94 o 3 10 0 343.59 385.12 17.41 o 4 10 0 237.21 234.54 11.99 o 5 10 0 366.24 361.07 11.74 o 1 11 0 329.69 313.35 12.23 o 2 11 0 258.88 224.36 10.07 o 3 11 0 408.76 394.41 12.02 o -9 1 1 0.62 4.98 2.98 o -8 1 1 21.45 32.39 5.70 o -7 1 1 760.93 678.74 20.31 o -6 1 1 4.67 8.74 3.06 o -5 1 1 2816.57 2790.40 176.66 o -4 1 1 79.92 99.83 11.44 o -3 1 1 406.11 477.24 15.26 o -2 1 1 10972.35 10412.94 68.23 o -1 1 1 1572.47 1605.40 22.21 o 0 1 1 9.06 19.74 3.26 o 1 1 1 9975.06 9781.34 342.49 o 2 1 1 809.33 722.11 34.32 o 3 1 1 23.60 49.17 8.23 o 4 1 1 311.93 332.92 21.18 o 5 1 1 12.19 22.92 5.79 o 6 1 1 2.62 13.31 5.77 o 7 1 1 156.54 160.36 11.87 o 8 1 1 87.00 85.19 8.12 o 9 1 1 33.50 43.02 4.84 o -9 2 1 228.20 264.10 10.67 o -8 2 1 18.29 13.39 4.36 o -7 2 1 420.34 369.10 14.39 o -6 2 1 16.96 13.04 4.10 o -5 2 1 2660.95 2487.60 62.99 o -4 2 1 2840.34 2411.37 84.95 o -3 2 1 236.35 223.74 23.62 o -2 2 1 235.31 313.90 24.75 o -1 2 1 11280.02 10516.95 124.98 o 0 2 1 12.83 53.79 7.56 o 1 2 1 3798.42 3551.30 91.30 o 2 2 1 889.85 900.73 38.40 o 3 2 1 122.65 129.58 18.60 o 4 2 1 1801.23 1697.01 71.50 o 5 2 1 2848.12 2650.82 95.67 o 6 2 1 118.79 130.74 8.53 o 7 2 1 35.70 35.42 5.89 o 8 2 1 871.60 942.07 35.00 o 9 2 1 505.44 522.16 18.92 o -9 3 1 3.43 4.68 3.89 o -8 3 1 1350.64 1501.93 30.06 o -7 3 1 1379.45 1381.05 48.66 o -6 3 1 874.37 890.67 28.73 o -5 3 1 69.98 54.73 10.28 o -4 3 1 4041.55 3709.43 112.37 o -3 3 1 1482.17 1405.81 62.77 o -2 3 1 3863.14 3958.49 177.33 o -1 3 1 15595.34 15395.90 181.35 o 0 3 1 3941.27 1774.41 1193.40 o 1 3 1 6620.80 6765.90 51.15 o 2 3 1 2820.06 2614.98 187.80 o 3 3 1 3503.46 3260.30 100.25 o 4 3 1 4527.50 4225.33 116.85 o 5 3 1 784.19 675.62 49.90 o 6 3 1 415.21 381.91 18.43 o 7 3 1 781.16 793.48 38.49 o 8 3 1 782.28 891.22 37.84 o 9 3 1 211.93 207.64 14.40 o -9 4 1 549.12 480.13 130.85 o -8 4 1 1251.95 1485.70 45.28 o -7 4 1 19.99 25.38 8.29 o -6 4 1 805.34 852.51 26.23 o -5 4 1 994.11 926.72 44.55 o -4 4 1 4.51 2.75 4.26 o -3 4 1 10021.60 8827.72 173.47 o -2 4 1 8580.84 7886.88 153.10 o -1 4 1 6893.33 6584.18 367.20 o 0 4 1 4831.57 3925.15 74.00 o 1 4 1 3351.71 3189.53 180.83 o 2 4 1 154.70 161.25 14.90 o 3 4 1 508.65 564.89 46.38 o 4 4 1 365.95 307.43 35.14 o 5 4 1 861.90 828.85 30.19 o 6 4 1 3835.93 3781.19 82.60 o 7 4 1 735.43 809.94 38.48 o 8 4 1 841.57 966.05 37.00 o 9 4 1 16.77 15.79 4.04 o -9 5 1 725.97 793.82 19.09 o -8 5 1 0.66 -0.67 3.16 o -7 5 1 765.80 822.43 36.42 o -6 5 1 2668.32 2654.34 67.95 o -5 5 1 9693.70 9760.76 496.04 o -4 5 1 350.84 355.04 25.64 o -3 5 1 2861.64 2605.51 97.66 o -2 5 1 221.47 186.34 26.35 o -1 5 1 1225.21 1571.89 68.45 o 0 5 1 2488.76 2255.02 225.38 o 1 5 1 3553.92 3417.58 102.19 o 2 5 1 8174.90 9140.40 188.96 o 3 5 1 12868.37 13786.94 251.16 o 4 5 1 8058.14 8254.17 189.98 o 5 5 1 1251.79 1126.82 51.47 o 6 5 1 0.40 7.48 5.60 o 7 5 1 6.38 12.52 6.65 o 8 5 1 110.69 100.09 8.14 o -8 6 1 220.83 221.49 13.70 o -7 6 1 113.67 96.40 9.72 o -6 6 1 2.18 1.04 5.26 o -5 6 1 129.72 129.90 18.02 o -4 6 1 6181.74 5906.15 88.55 o -3 6 1 3865.59 3865.87 98.94 o -2 6 1 6773.59 6977.09 626.53 o -1 6 1 745.75 821.83 48.34 o 0 6 1 7200.61 6308.87 117.87 o 1 6 1 1383.78 1359.62 67.47 o 2 6 1 226.05 239.68 32.54 o 3 6 1 2477.35 2591.12 111.35 o 4 6 1 6.14 17.68 4.39 o 5 6 1 159.88 161.83 13.96 o 6 6 1 151.25 136.44 11.77 o 7 6 1 2143.75 1958.88 51.81 o 8 6 1 78.33 82.77 6.17 o -8 7 1 919.65 913.83 19.00 o -7 7 1 611.43 585.27 24.03 o -6 7 1 2191.88 2067.57 55.20 o -5 7 1 324.41 297.29 23.38 o -4 7 1 2777.51 2535.43 68.74 o -3 7 1 3.57 5.78 12.17 o -2 7 1 99.63 108.25 7.45 o -1 7 1 343.83 347.74 15.73 o 0 7 1 607.69 573.95 28.38 o 1 7 1 1569.82 1488.13 32.47 o 2 7 1 4074.79 4423.10 87.40 o 3 7 1 1987.08 1916.12 170.13 o 4 7 1 1604.49 1499.20 50.99 o 5 7 1 367.00 359.71 24.74 o 6 7 1 3.30 9.97 5.52 o 7 7 1 112.75 118.66 10.59 o -7 8 1 6.49 4.82 2.26 o -6 8 1 116.64 121.73 11.34 o -5 8 1 1019.58 999.66 36.76 o -4 8 1 15.26 21.65 6.90 o -3 8 1 1.54 10.68 4.98 o -2 8 1 571.53 541.19 18.84 o -1 8 1 6324.92 5739.04 170.67 o 0 8 1 21.84 39.02 6.19 o 1 8 1 17.68 20.32 3.94 o 2 8 1 529.40 485.56 25.77 o 3 8 1 1581.26 1473.54 45.67 o 4 8 1 1170.31 1166.12 41.04 o 5 8 1 18.00 23.68 6.60 o 6 8 1 24.86 24.61 5.29 o 7 8 1 50.78 52.80 3.35 o -6 9 1 4.08 8.15 2.72 o -5 9 1 1.03 4.13 3.22 o -4 9 1 29.41 30.50 6.43 o -3 9 1 7.40 9.63 4.59 o -2 9 1 414.99 410.00 14.68 o -1 9 1 11.19 18.38 3.44 o 0 9 1 40.22 52.74 16.41 o 1 9 1 60.92 65.44 5.96 o 2 9 1 704.09 634.11 27.37 o 3 9 1 869.51 825.15 30.29 o 4 9 1 76.42 75.01 9.19 o 5 9 1 628.40 627.55 21.88 o 6 9 1 11.87 12.70 2.00 o -5 10 1 0.29 2.29 1.68 o -4 10 1 34.00 43.45 5.49 o -3 10 1 13.97 10.18 3.39 o -2 10 1 41.50 39.72 6.16 o -1 10 1 595.87 572.14 14.87 o 0 10 1 105.92 119.87 7.00 o 1 10 1 11.57 9.74 3.50 o 2 10 1 25.31 15.39 4.24 o 3 10 1 402.29 367.67 16.92 o 4 10 1 174.20 184.15 10.58 o 5 10 1 34.86 35.93 3.81 o -3 11 1 3.12 2.25 1.52 o -2 11 1 100.85 104.95 6.79 o -1 11 1 2.26 4.33 1.97 o 0 11 1 109.32 115.62 7.33 o 1 11 1 230.00 223.82 10.39 o 2 11 1 634.41 606.59 16.61 o 3 11 1 75.79 75.89 5.29 o -9 0 2 1.36 4.84 3.97 o -8 0 2 106.17 97.73 13.04 o -7 0 2 57.90 68.43 8.70 o -6 0 2 3722.11 3461.36 78.22 o -5 0 2 3116.07 2638.58 96.90 o -4 0 2 4642.46 4586.61 96.91 o -3 0 2 8050.16 8223.90 402.08 o -1 0 2 2867.39 3187.34 121.70 o 0 0 2 3697.68 4127.31 57.23 o 1 0 2 61.48 265.39 30.94 o 2 0 2 15154.22 16105.42 999.55 o 3 0 2 18220.86 18808.21 199.44 o 4 0 2 1027.73 954.67 48.59 o 5 0 2 4911.38 4477.92 114.20 o 6 0 2 202.45 206.58 27.05 o 7 0 2 6758.39 6617.19 104.78 o 8 0 2 528.52 532.03 27.50 o 9 0 2 181.08 193.12 13.42 o -9 1 2 1712.49 1817.46 45.23 o -8 1 2 2128.76 2033.48 38.95 o -7 1 2 494.47 434.77 26.57 o -6 1 2 9.83 16.02 6.17 o -5 1 2 3406.78 3095.86 176.94 o -4 1 2 86.77 101.59 8.40 o -3 1 2 138.08 191.41 9.60 o -2 1 2 7607.97 7503.71 61.99 o -1 1 2 312.13 324.00 9.11 o 0 1 2 7143.17 7626.82 73.60 o 1 1 2 11015.51 11096.44 83.25 o 2 1 2 11764.49 11799.79 488.91 o 3 1 2 5563.75 6098.66 193.46 o 4 1 2 1952.45 1894.70 62.01 o 5 1 2 6.07 3.02 4.11 o 6 1 2 798.52 763.72 21.73 o 7 1 2 2208.71 2195.46 42.00 o 8 1 2 128.97 146.76 10.33 o 9 1 2 365.65 427.27 17.61 o -9 2 2 646.44 692.49 17.25 o -8 2 2 114.79 118.27 9.48 o -7 2 2 60.37 54.69 7.49 o -6 2 2 1444.39 1236.00 22.99 o -5 2 2 3935.67 3739.51 78.57 o -4 2 2 8725.20 8281.56 292.01 o -3 2 2 11765.91 11175.67 167.98 o -2 2 2 14.51 12.12 6.17 o 0 2 2 84.66 96.92 7.07 o 1 2 2 856.27 808.78 29.18 o 3 2 2 1402.50 1436.31 43.09 o 4 2 2 7025.65 6839.37 143.09 o 5 2 2 1661.82 1735.44 76.04 o 6 2 2 2266.15 2241.29 51.31 o 7 2 2 20.80 20.93 4.71 o 8 2 2 303.39 362.75 15.31 o 9 2 2 3.50 7.69 4.77 o -9 3 2 28.04 27.23 5.89 o -8 3 2 19.33 24.12 4.69 o -7 3 2 379.75 387.03 18.00 o -6 3 2 2407.59 2390.08 63.80 o -5 3 2 3362.62 3239.01 87.27 o -4 3 2 75.98 86.32 11.93 o -3 3 2 656.90 577.29 39.70 o -2 3 2 22.97 35.92 6.99 o 0 3 2 109.00 95.81 6.68 o 1 3 2 1582.47 1754.51 28.30 o 2 3 2 1111.23 1059.01 68.05 o 3 3 2 5428.27 5216.59 89.09 o 4 3 2 381.19 389.31 36.78 o 5 3 2 783.09 708.45 50.85 o 6 3 2 132.69 135.13 11.14 o 7 3 2 88.44 98.14 14.36 o 8 3 2 812.36 988.20 39.66 o 9 3 2 462.92 418.09 20.46 o -9 4 2 138.27 117.74 36.37 o -8 4 2 86.77 90.56 12.36 o -7 4 2 1169.95 1260.73 45.72 o -6 4 2 1.38 2.88 4.95 o -5 4 2 657.56 675.51 54.86 o -4 4 2 3874.33 3570.19 77.95 o -3 4 2 1065.83 1022.07 55.43 o -2 4 2 629.72 558.06 50.78 o -1 4 2 1251.55 1414.86 58.49 o 0 4 2 5271.51 5423.45 210.73 o 1 4 2 6222.89 6143.01 441.99 o 2 4 2 3342.09 3321.89 222.11 o 3 4 2 1356.71 1358.36 73.57 o 4 4 2 26.37 22.64 12.19 o 5 4 2 1165.02 1109.23 35.92 o 6 4 2 967.47 940.35 42.40 o 7 4 2 46.12 52.26 11.67 o 8 4 2 24.55 25.92 7.97 o 9 4 2 389.16 420.16 24.60 o -9 5 2 224.12 235.47 10.53 o -8 5 2 112.34 101.55 11.59 o -7 5 2 0.24 5.17 5.94 o -6 5 2 771.11 786.33 27.87 o -5 5 2 613.02 675.84 32.48 o -4 5 2 5.77 7.02 4.93 o -3 5 2 416.41 396.82 25.35 o -2 5 2 1076.86 1095.55 53.40 o -1 5 2 907.45 956.21 33.06 o 0 5 2 524.21 516.54 57.94 o 1 5 2 902.99 1017.79 36.85 o 2 5 2 151.70 169.33 17.22 o 3 5 2 448.00 460.46 46.54 o 4 5 2 1408.66 1488.50 80.81 o 5 5 2 464.89 440.92 39.17 o 6 5 2 1.03 8.18 7.15 o 7 5 2 335.87 347.37 24.96 o 8 5 2 113.99 106.44 8.52 o -8 6 2 107.97 117.28 10.21 o -7 6 2 217.24 218.33 18.33 o -6 6 2 479.74 458.48 30.66 o -5 6 2 376.52 416.49 31.42 o -4 6 2 4363.03 4307.72 101.65 o -3 6 2 2698.14 2842.94 96.96 o -2 6 2 256.02 311.42 22.00 o -1 6 2 18.04 34.39 5.79 o 0 6 2 843.21 784.14 32.64 o 1 6 2 754.79 780.69 51.03 o 2 6 2 2228.82 2397.90 98.81 o 3 6 2 171.85 181.08 15.28 o 4 6 2 9.02 21.11 8.18 o 5 6 2 2084.78 1821.70 101.30 o 6 6 2 268.24 247.20 15.23 o 7 6 2 209.14 186.63 15.80 o 8 6 2 189.72 184.15 8.55 o -8 7 2 200.20 194.40 8.86 o -7 7 2 734.18 725.19 26.77 o -6 7 2 25.39 27.73 7.45 o -5 7 2 6.94 9.35 5.01 o -4 7 2 237.05 251.13 21.72 o -3 7 2 6.18 8.05 3.43 o -2 7 2 2221.96 2159.43 71.28 o -1 7 2 1998.28 1841.12 41.18 o 0 7 2 1431.42 1415.57 31.12 o 1 7 2 47.71 64.19 6.93 o 2 7 2 564.73 554.45 47.89 o 3 7 2 717.72 718.76 50.24 o 4 7 2 7.71 1.53 3.85 o 5 7 2 40.60 42.69 9.10 o 6 7 2 14.90 22.01 6.32 o 7 7 2 185.93 185.61 8.03 o -7 8 2 9.58 14.92 3.17 o -6 8 2 930.03 976.96 30.84 o -5 8 2 2018.15 2093.60 52.93 o -4 8 2 590.03 638.52 31.12 o -3 8 2 627.77 662.02 31.84 o -2 8 2 1894.95 1848.61 35.35 o -1 8 2 506.41 495.63 18.21 o 0 8 2 32.13 27.91 4.39 o 1 8 2 209.45 213.13 16.84 o 2 8 2 727.29 633.24 29.31 o 3 8 2 1558.79 1438.85 44.75 o 4 8 2 554.85 525.52 27.05 o 5 8 2 1094.84 1077.96 35.77 o 6 8 2 556.43 563.74 21.76 o 7 8 2 347.77 345.08 11.82 o -6 9 2 733.12 775.30 19.41 o -5 9 2 531.49 543.58 21.06 o -4 9 2 4.48 11.21 4.41 o -3 9 2 1094.64 1126.29 36.27 o -2 9 2 113.51 104.68 7.66 o -1 9 2 474.50 429.53 15.20 o 0 9 2 2600.87 2373.26 69.85 o 1 9 2 4264.15 3793.74 67.67 o 2 9 2 1119.87 1008.67 24.23 o 3 9 2 131.25 123.28 11.94 o 4 9 2 357.89 371.06 18.94 o 5 9 2 151.04 158.10 10.79 o 6 9 2 540.44 529.57 10.34 o -5 10 2 1077.19 1052.62 20.60 o -4 10 2 279.02 272.79 12.95 o -3 10 2 752.60 745.39 23.48 o -2 10 2 1991.69 2040.65 73.71 o -1 10 2 567.78 556.63 24.07 o 0 10 2 29.70 23.05 3.25 o 1 10 2 100.75 87.85 8.82 o 2 10 2 100.94 94.78 9.01 o 3 10 2 1140.23 1084.23 28.52 o 4 10 2 2475.04 2368.89 36.89 o 5 10 2 6.78 10.08 2.16 o -3 11 2 11.24 12.93 2.31 o -2 11 2 417.75 422.44 12.75 o -1 11 2 411.96 460.92 12.25 o 0 11 2 580.48 601.54 16.56 o 1 11 2 296.77 307.81 12.21 o 2 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