#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/73/2237305.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237305_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Schw\"orer, Ralf' _publ_section_title ; 2-(Acetoxymethyl)benzoic acid ; _journal_coeditor_code FY2082 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o259 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 77.540 _cell_angle_beta 83.364 _cell_angle_gamma 73.081 _cell_length_a 6.2134 _cell_length_b 8.2415 _cell_length_c 9.6280 _exptl_crystal_F_000 204.00 _reflns_d_resolution_high 0.8036 _[local]_cod_data_source_file fy2082Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ratt in P-1 # 2 (Rattd via P1 soln)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 58.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 605.79 621.45 4.23 o 3 0 0 81.66 86.01 1.55 o 4 0 0 9.52 11.07 0.43 o 5 0 0 78.48 79.63 0.94 o 6 0 0 36.07 35.75 1.19 o 7 0 0 19.48 20.05 0.66 o -7 1 0 2.71 2.41 0.19 o -6 1 0 31.69 29.60 0.70 o -5 1 0 10.36 9.74 0.44 o -4 1 0 38.97 46.68 1.18 o -3 1 0 107.17 103.73 1.25 o -2 1 0 291.58 293.70 1.86 o -1 1 0 167.48 157.67 1.06 o 1 1 0 153.16 166.58 1.22 o 2 1 0 55.20 65.93 0.76 o 3 1 0 235.13 227.46 1.56 o 4 1 0 4.62 5.19 0.29 o 5 1 0 97.32 96.68 0.91 o 6 1 0 377.02 407.96 5.12 o 7 1 0 8.84 9.38 0.49 o -6 2 0 0.99 0.71 0.11 o -5 2 0 36.33 40.63 0.96 o -4 2 0 1.80 1.88 0.25 o -3 2 0 0.05 0.42 0.15 o -2 2 0 0.32 0.27 0.04 o -1 2 0 46.36 41.55 0.41 o 0 2 0 571.64 491.46 4.69 o 2 2 0 158.02 163.05 1.86 o 3 2 0 0.54 0.75 0.07 o 4 2 0 0.98 0.53 0.10 o 5 2 0 65.31 64.76 1.47 o 6 2 0 2.73 2.65 0.24 o 7 2 0 1.42 1.12 0.20 o -6 3 0 1.09 0.76 0.14 o -5 3 0 147.41 135.65 5.32 o -4 3 0 34.83 28.05 0.52 o -3 3 0 46.26 42.16 1.23 o -2 3 0 388.93 415.64 4.76 o -1 3 0 28.56 32.04 0.76 o 0 3 0 4.98 2.53 0.21 o 1 3 0 19.12 22.11 0.63 o 2 3 0 350.00 351.37 2.55 o 3 3 0 0.01 0.34 0.08 o 4 3 0 87.18 95.71 4.20 o 5 3 0 58.75 58.34 1.08 o 6 3 0 0.04 0.06 0.08 o 7 3 0 53.77 52.95 1.19 o -5 4 0 1.01 0.37 0.09 o -4 4 0 4.07 3.05 0.21 o -3 4 0 144.02 135.76 2.21 o -2 4 0 9.21 10.04 0.59 o -1 4 0 21.09 22.17 0.73 o 0 4 0 124.27 124.37 1.98 o 1 4 0 1251.87 1295.60 12.22 o 2 4 0 403.54 393.96 4.52 o 3 4 0 2.49 2.64 0.27 o 4 4 0 413.22 413.32 3.54 o 5 4 0 0.47 0.40 0.10 o 6 4 0 26.65 27.36 0.57 o 7 4 0 39.58 37.39 0.65 o -4 5 0 9.15 9.53 0.33 o -3 5 0 200.27 199.42 1.90 o -2 5 0 90.10 87.80 1.28 o -1 5 0 19.41 17.94 0.74 o 0 5 0 52.49 58.87 1.43 o 1 5 0 25.68 26.15 0.93 o 2 5 0 62.65 54.28 1.40 o 3 5 0 13.77 12.24 0.65 o 4 5 0 186.47 170.34 2.03 o 5 5 0 0.46 0.44 0.13 o 6 5 0 8.67 11.37 0.69 o 7 5 0 10.91 10.25 0.48 o -4 6 0 15.56 16.63 0.61 o -3 6 0 24.32 25.64 1.85 o -2 6 0 18.66 17.80 0.49 o -1 6 0 45.08 43.07 1.36 o 0 6 0 99.36 102.03 2.60 o 1 6 0 48.64 49.22 2.42 o 2 6 0 29.50 30.09 0.76 o 3 6 0 6.45 5.83 0.34 o 4 6 0 15.57 14.60 0.79 o 5 6 0 39.57 43.39 1.41 o 6 6 0 4.46 4.57 0.42 o 7 6 0 11.44 11.20 0.44 o -3 7 0 2.24 3.17 0.30 o -2 7 0 35.52 37.37 0.87 o -1 7 0 390.36 401.42 5.49 o 0 7 0 240.33 237.39 2.57 o 1 7 0 7.63 4.88 0.47 o 2 7 0 11.16 9.70 0.43 o 3 7 0 10.12 9.86 0.43 o 4 7 0 15.95 15.85 0.53 o 5 7 0 172.78 182.87 3.00 o 6 7 0 15.34 16.25 0.67 o -2 8 0 0.00 -0.01 0.07 o -1 8 0 25.45 26.09 0.52 o 0 8 0 4.58 4.64 0.28 o 1 8 0 1.12 1.30 0.17 o 2 8 0 8.72 9.11 0.61 o 3 8 0 1.60 2.26 0.28 o 4 8 0 12.16 12.49 1.17 o 5 8 0 211.61 226.53 3.06 o 6 8 0 55.37 51.49 0.95 o 0 9 0 4.33 3.23 0.26 o 1 9 0 10.58 10.24 0.56 o 2 9 0 22.56 21.54 0.73 o 3 9 0 0.00 0.11 0.07 o 4 9 0 28.99 27.70 0.56 o 5 9 0 9.92 9.90 0.36 o 2 10 0 0.01 0.07 0.06 o -4 -9 1 4.77 4.19 0.36 o -3 -9 1 1.50 1.38 0.14 o -2 -9 1 0.55 0.61 0.10 o -1 -9 1 38.99 38.35 1.00 o 0 -9 1 0.12 0.16 0.08 o -5 -8 1 11.69 11.71 0.35 o -4 -8 1 14.04 13.46 0.50 o -3 -8 1 31.68 33.78 1.12 o -2 -8 1 7.83 7.71 0.54 o -1 -8 1 52.61 53.25 1.64 o 0 -8 1 5.01 4.53 0.27 o 1 -8 1 2.57 2.95 0.21 o 2 -8 1 0.46 1.02 0.10 o -6 -7 1 13.67 14.60 0.57 o -5 -7 1 27.41 29.13 1.00 o -4 -7 1 5.39 5.03 0.30 o -3 -7 1 0.20 0.14 0.10 o -2 -7 1 0.27 0.23 0.14 o -1 -7 1 3.09 3.16 0.26 o 0 -7 1 66.04 61.24 2.57 o 1 -7 1 8.12 7.40 0.64 o 2 -7 1 27.67 30.64 2.62 o 3 -7 1 35.30 38.43 2.15 o -7 -6 1 0.13 0.30 0.08 o -6 -6 1 35.07 37.57 1.13 o -5 -6 1 7.56 7.81 0.58 o -4 -6 1 15.60 15.10 0.53 o -3 -6 1 21.70 20.66 0.64 o -2 -6 1 64.07 71.39 1.25 o -1 -6 1 47.96 46.40 1.00 o 0 -6 1 87.13 82.97 1.14 o 1 -6 1 412.04 404.24 10.81 o 2 -6 1 26.65 27.58 0.62 o 3 -6 1 5.53 5.10 0.31 o 4 -6 1 30.47 28.22 0.86 o -7 -5 1 1.74 1.90 0.20 o -6 -5 1 7.72 7.99 0.57 o -5 -5 1 0.19 0.99 0.25 o -4 -5 1 0.07 -0.02 0.16 o -3 -5 1 27.36 29.23 1.06 o -2 -5 1 209.57 214.68 3.27 o -1 -5 1 169.31 175.36 2.85 o 0 -5 1 50.42 51.60 1.36 o 1 -5 1 2.90 2.69 0.30 o 2 -5 1 10.79 10.91 0.34 o 3 -5 1 1.50 2.06 0.18 o 4 -5 1 22.70 18.25 0.55 o 5 -5 1 16.13 17.76 0.48 o -7 -4 1 3.87 3.67 0.30 o -6 -4 1 0.03 0.09 0.09 o -5 -4 1 12.19 12.64 0.51 o -4 -4 1 3.11 2.72 0.18 o -3 -4 1 72.10 69.18 1.55 o -2 -4 1 93.48 97.90 1.83 o -1 -4 1 1.90 1.89 0.23 o 0 -4 1 92.05 86.56 1.63 o 1 -4 1 85.21 82.75 1.53 o 2 -4 1 250.76 243.90 3.55 o 3 -4 1 261.14 239.56 2.00 o 4 -4 1 9.78 9.05 0.35 o 5 -4 1 3.16 3.99 0.30 o -7 -3 1 58.95 56.41 1.14 o -6 -3 1 7.42 7.52 0.38 o -5 -3 1 18.38 18.99 0.49 o -4 -3 1 322.85 308.99 3.92 o -3 -3 1 79.54 77.31 1.01 o -2 -3 1 6.46 7.24 0.43 o -1 -3 1 92.51 91.07 0.86 o 0 -3 1 135.57 128.62 1.84 o 1 -3 1 702.05 704.82 6.81 o 2 -3 1 95.63 106.73 1.91 o 3 -3 1 0.51 0.95 0.11 o 4 -3 1 21.72 21.75 0.53 o 5 -3 1 29.50 33.47 1.22 o 6 -3 1 9.16 8.39 0.27 o -7 -2 1 134.00 126.53 1.97 o -6 -2 1 126.13 135.13 1.79 o -5 -2 1 0.10 0.07 0.06 o -4 -2 1 68.18 58.70 1.45 o -3 -2 1 1.90 3.46 0.19 o -2 -2 1 278.73 267.77 2.91 o -1 -2 1 1065.02 1111.24 10.09 o 0 -2 1 772.38 726.85 4.78 o 1 -2 1 11.73 10.23 0.41 o 2 -2 1 1371.51 1436.50 9.24 o 3 -2 1 0.03 0.10 0.05 o 4 -2 1 21.94 21.46 0.52 o 5 -2 1 9.19 11.94 0.49 o 6 -2 1 24.92 22.09 0.43 o -7 -1 1 0.53 0.59 0.09 o -6 -1 1 0.50 0.64 0.20 o -5 -1 1 71.30 74.11 1.07 o -4 -1 1 310.70 309.24 2.88 o -3 -1 1 92.87 92.40 1.15 o -2 -1 1 1072.72 1137.81 14.77 o -1 -1 1 338.14 335.30 3.18 o 0 -1 1 699.64 687.19 6.15 o 1 -1 1 107.78 98.71 0.67 o 2 -1 1 27.99 37.00 0.43 o 3 -1 1 50.90 42.81 1.04 o 4 -1 1 16.38 16.29 0.51 o 5 -1 1 3.42 3.28 0.26 o 6 -1 1 8.96 10.05 0.32 o -7 0 1 10.96 10.38 1.11 o -6 0 1 0.00 -0.18 0.18 o -5 0 1 2.27 2.49 0.22 o -4 0 1 7.80 6.06 0.32 o -3 0 1 1.44 1.91 0.15 o -2 0 1 19.30 20.41 0.63 o 2 0 1 21.03 22.00 0.29 o 3 0 1 925.00 908.96 6.29 o 4 0 1 71.86 73.33 1.59 o 5 0 1 13.27 12.66 0.40 o 6 0 1 10.87 11.17 0.43 o 7 0 1 8.93 8.33 0.41 o -7 1 1 8.67 7.04 0.32 o -6 1 1 10.33 10.97 0.64 o -5 1 1 26.41 28.01 0.63 o -4 1 1 0.48 0.49 0.10 o -3 1 1 780.83 830.47 10.53 o -2 1 1 17.81 16.06 0.35 o -1 1 1 702.58 631.74 2.88 o 2 1 1 75.90 68.56 0.56 o 3 1 1 159.34 150.26 1.55 o 4 1 1 40.22 38.49 1.12 o 5 1 1 227.45 229.34 2.42 o 6 1 1 241.37 237.33 3.62 o 7 1 1 23.33 24.25 0.80 o -6 2 1 13.78 13.96 0.66 o -5 2 1 20.32 20.06 0.52 o -4 2 1 10.12 8.72 0.29 o -3 2 1 188.50 205.80 3.05 o -2 2 1 1008.04 1024.34 4.73 o -1 2 1 293.38 252.25 1.30 o 0 2 1 149.44 138.03 2.31 o 2 2 1 175.39 173.39 1.17 o 3 2 1 852.24 869.96 4.75 o 4 2 1 41.08 44.85 1.22 o 5 2 1 22.58 23.21 0.53 o 6 2 1 166.73 170.61 1.60 o 7 2 1 11.86 12.53 0.59 o -6 3 1 8.74 8.52 0.28 o -5 3 1 1.40 1.07 0.26 o -4 3 1 274.26 255.72 2.26 o -3 3 1 169.72 169.90 2.72 o -2 3 1 141.75 130.11 1.18 o -1 3 1 63.74 53.93 1.01 o 0 3 1 52.93 52.37 1.01 o 1 3 1 137.62 134.13 1.84 o 2 3 1 126.57 122.58 1.20 o 3 3 1 3.47 2.26 0.15 o 4 3 1 68.43 72.46 1.59 o 5 3 1 0.52 0.38 0.08 o 6 3 1 4.34 4.32 0.24 o 7 3 1 6.65 6.73 0.43 o -5 4 1 30.52 28.32 0.97 o -4 4 1 3.30 1.89 0.17 o -3 4 1 0.18 0.14 0.12 o -2 4 1 11.63 11.88 0.62 o -1 4 1 163.46 156.81 2.33 o 0 4 1 279.38 297.59 3.61 o 1 4 1 426.02 448.67 4.92 o 2 4 1 130.66 139.29 2.14 o 3 4 1 0.27 0.24 0.07 o 4 4 1 0.10 0.15 0.10 o 5 4 1 39.09 39.16 0.71 o 6 4 1 9.37 10.04 0.35 o 7 4 1 94.97 89.40 1.12 o -5 5 1 29.65 30.69 0.81 o -4 5 1 19.56 17.97 0.74 o -3 5 1 51.72 53.22 1.49 o -2 5 1 416.99 387.94 2.82 o -1 5 1 103.78 99.77 3.99 o 0 5 1 46.26 46.42 1.24 o 1 5 1 112.33 134.89 2.31 o 2 5 1 77.72 76.28 1.65 o 3 5 1 44.53 42.88 1.20 o 4 5 1 9.96 9.71 0.33 o 5 5 1 133.98 131.37 1.40 o 6 5 1 0.01 -0.07 0.10 o 7 5 1 120.85 111.03 1.80 o -4 6 1 34.32 35.67 0.93 o -3 6 1 9.60 10.46 0.44 o -2 6 1 28.21 27.43 0.77 o -1 6 1 165.00 145.86 1.91 o 0 6 1 12.62 12.61 0.57 o 1 6 1 1.73 1.72 0.23 o 2 6 1 6.93 5.41 0.26 o 3 6 1 0.31 0.14 0.08 o 4 6 1 73.09 68.47 1.21 o 5 6 1 27.28 26.39 0.74 o 6 6 1 0.94 0.93 0.22 o 7 6 1 23.33 21.62 0.64 o -3 7 1 0.01 0.08 0.11 o -2 7 1 1.91 2.17 0.22 o -1 7 1 0.99 1.08 0.17 o 0 7 1 170.01 150.33 2.86 o 1 7 1 6.39 4.38 0.45 o 2 7 1 100.87 96.65 2.07 o 3 7 1 26.16 25.35 1.03 o 4 7 1 14.24 13.36 0.77 o 5 7 1 4.43 4.74 0.45 o 6 7 1 1.57 1.72 0.24 o -2 8 1 0.15 0.12 0.11 o -1 8 1 0.20 0.06 0.17 o 0 8 1 77.85 74.06 2.92 o 1 8 1 3.62 3.83 0.42 o 2 8 1 0.16 0.08 0.09 o 3 8 1 0.19 0.21 0.12 o 4 8 1 11.70 12.02 0.59 o 5 8 1 27.55 28.81 0.95 o 6 8 1 27.22 28.43 0.75 o -1 9 1 5.54 4.73 0.25 o 0 9 1 0.63 0.56 0.15 o 1 9 1 14.71 14.21 0.68 o 2 9 1 103.17 99.72 1.44 o 3 9 1 65.06 61.01 1.29 o 4 9 1 41.72 42.60 1.49 o 5 9 1 13.84 15.25 0.50 o 2 10 1 6.98 7.32 0.35 o 3 10 1 3.25 2.60 0.19 o -4 -9 2 0.63 0.73 0.11 o -3 -9 2 2.31 2.24 0.15 o -2 -9 2 0.15 0.03 0.05 o -1 -9 2 1.90 1.87 0.19 o 0 -9 2 22.04 20.26 0.60 o -5 -8 2 7.02 6.23 0.30 o -4 -8 2 4.93 3.97 0.44 o -3 -8 2 2.26 1.96 0.19 o -2 -8 2 0.43 0.33 0.11 o -1 -8 2 93.72 100.49 2.62 o 0 -8 2 212.83 232.68 3.14 o 1 -8 2 17.81 18.24 0.47 o 2 -8 2 1.95 2.20 0.13 o -6 -7 2 7.97 7.80 0.33 o -5 -7 2 5.10 4.69 0.24 o -4 -7 2 1.51 1.30 0.16 o -3 -7 2 8.68 8.62 0.60 o -2 -7 2 12.45 14.85 0.78 o -1 -7 2 72.88 80.89 1.37 o 0 -7 2 68.30 71.27 0.96 o 1 -7 2 5.68 5.87 0.46 o 2 -7 2 23.87 25.50 0.80 o 3 -7 2 13.82 16.71 0.91 o -6 -6 2 1.21 1.28 0.20 o -5 -6 2 71.45 73.24 2.37 o -4 -6 2 0.83 0.74 0.13 o -3 -6 2 13.28 12.14 0.47 o -2 -6 2 0.54 0.86 0.15 o -1 -6 2 30.90 32.25 0.84 o 0 -6 2 4.15 3.72 0.23 o 1 -6 2 96.03 93.97 2.65 o 2 -6 2 156.84 160.18 2.07 o 3 -6 2 5.40 5.77 0.32 o 4 -6 2 7.14 8.24 0.39 o -6 -5 2 1.30 1.49 0.25 o -5 -5 2 94.01 99.37 1.49 o -4 -5 2 0.48 0.63 0.12 o -3 -5 2 87.61 86.76 1.08 o -2 -5 2 481.98 494.39 6.03 o -1 -5 2 10.49 8.92 0.59 o 0 -5 2 17.64 20.20 0.84 o 1 -5 2 19.90 21.05 0.51 o 2 -5 2 67.58 68.15 1.46 o 3 -5 2 5.69 4.53 0.32 o 4 -5 2 0.28 0.22 0.10 o 5 -5 2 0.69 0.88 0.12 o -6 -4 2 19.89 19.68 1.62 o -5 -4 2 55.19 60.92 1.18 o -4 -4 2 3.35 4.56 0.52 o -3 -4 2 100.06 97.61 2.01 o -2 -4 2 14.82 14.27 0.69 o -1 -4 2 8.14 6.87 0.46 o 0 -4 2 0.42 0.08 0.09 o 1 -4 2 288.51 299.18 3.66 o 2 -4 2 37.60 37.10 0.67 o 3 -4 2 24.48 19.29 0.52 o 4 -4 2 186.36 175.02 1.70 o 5 -4 2 3.85 3.49 0.31 o -7 -3 2 3.29 3.34 0.22 o -6 -3 2 11.39 10.00 0.46 o -5 -3 2 0.48 0.53 0.13 o -4 -3 2 1.24 1.28 0.15 o -3 -3 2 100.71 98.66 1.25 o -2 -3 2 504.99 514.94 4.34 o -1 -3 2 48.96 54.12 1.19 o 0 -3 2 88.08 87.37 1.51 o 1 -3 2 25.48 26.79 0.72 o 2 -3 2 9.95 10.93 0.56 o 3 -3 2 4.94 4.89 0.21 o 4 -3 2 31.74 38.49 0.73 o 5 -3 2 0.34 -0.01 0.07 o 6 -3 2 0.86 1.23 0.15 o -7 -2 2 140.32 124.37 4.41 o -6 -2 2 74.80 79.23 1.33 o -5 -2 2 6.61 7.69 0.42 o -4 -2 2 56.17 48.31 1.36 o -3 -2 2 34.39 35.72 0.98 o -2 -2 2 72.65 84.76 1.35 o -1 -2 2 176.40 165.98 2.09 o 0 -2 2 26.99 28.80 0.50 o 1 -2 2 379.67 366.50 2.98 o 2 -2 2 112.37 119.08 3.28 o 3 -2 2 50.02 60.21 0.98 o 4 -2 2 12.34 11.38 0.47 o 5 -2 2 50.93 48.66 1.00 o 6 -2 2 5.01 4.89 0.24 o -7 -1 2 29.19 24.96 1.25 o -6 -1 2 60.79 61.70 1.66 o -5 -1 2 11.61 13.17 0.45 o -4 -1 2 61.85 68.36 1.71 o -3 -1 2 170.87 160.30 2.46 o -2 -1 2 30.38 31.77 0.78 o 0 -1 2 1156.66 1093.25 9.78 o 1 -1 2 477.39 463.93 2.55 o 2 -1 2 27.96 28.14 0.61 o 3 -1 2 3.54 3.54 0.31 o 4 -1 2 91.97 92.86 1.56 o 5 -1 2 18.48 17.87 0.59 o 6 -1 2 37.76 36.39 0.77 o -7 0 2 11.20 9.54 1.07 o -6 0 2 5.53 4.97 0.46 o -5 0 2 16.89 18.68 0.68 o -4 0 2 31.54 27.22 1.08 o -3 0 2 64.24 56.87 1.36 o -2 0 2 76.92 81.03 1.40 o -1 0 2 511.46 470.84 4.29 o 0 0 2 152.12 147.78 1.63 o 1 0 2 6.28 9.46 0.20 o 2 0 2 349.61 364.53 3.65 o 3 0 2 0.88 0.54 0.13 o 4 0 2 86.25 72.20 1.65 o 5 0 2 705.89 715.45 7.87 o 6 0 2 18.71 20.03 0.89 o 7 0 2 2.68 2.61 0.21 o -6 1 2 19.72 20.09 0.88 o -5 1 2 0.04 0.19 0.28 o -4 1 2 3.99 4.05 0.24 o -3 1 2 32.60 32.44 1.04 o -2 1 2 19.75 21.71 0.69 o -1 1 2 545.08 487.47 2.61 o 1 1 2 90.90 96.59 1.12 o 2 1 2 1.17 1.45 0.07 o 3 1 2 17.15 17.88 0.54 o 4 1 2 140.37 130.54 2.34 o 5 1 2 1.37 1.59 0.14 o 6 1 2 0.37 0.48 0.13 o 7 1 2 11.74 11.88 0.53 o -6 2 2 71.31 65.99 1.50 o -5 2 2 33.87 34.79 0.93 o -4 2 2 25.02 23.64 0.60 o -3 2 2 236.36 250.27 3.57 o -2 2 2 49.67 55.26 2.12 o -1 2 2 35.16 44.37 0.48 o 0 2 2 229.29 235.33 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