#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/73/2237310.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237310_Fobs loop_ _publ_author_name 'Maloney, Sarah' 'Slawin, Alexandra M. Z.' 'Woollins, J. Derek' _publ_section_title ; 2,2-Dimethyl-2,3-dihydro-1H-perimidine ; _journal_coeditor_code GG2107 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o246 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.131 _cell_angle_gamma 90.000 _cell_length_a 16.2608 _cell_length_b 7.7105 _cell_length_c 17.4825 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.8378 _[local]_cod_data_source_file gg2107Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SARAH8' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 548.68 421.72 22.28 o 3 0 0 6029.81 5321.57 175.28 o 4 0 0 1289.03 1093.37 40.73 o 5 0 0 61.22 34.34 8.98 o 6 0 0 623.19 663.62 37.91 o 7 0 0 1220.62 1231.77 62.79 o 8 0 0 84.24 70.18 12.05 o 9 0 0 32.09 46.31 10.14 o 10 0 0 770.56 857.06 43.06 o 11 0 0 125.59 151.22 26.14 o 12 0 0 1.21 1.73 6.74 o 13 0 0 28.83 28.72 7.75 o 14 0 0 104.68 82.78 21.61 o 15 0 0 263.92 278.40 65.79 o 16 0 0 127.70 60.13 33.51 o 17 0 0 11.67 -39.85 45.28 o 18 0 0 78.09 68.94 19.88 o 1 1 0 762.25 617.39 11.79 o 2 1 0 7993.66 7365.21 70.23 o 3 1 0 25060.60 22814.55 129.82 o 4 1 0 3041.14 2891.03 45.03 o 5 1 0 844.13 751.91 22.49 o 6 1 0 71.74 81.49 13.36 o 7 1 0 2.53 4.84 9.19 o 8 1 0 2115.74 2261.40 60.52 o 9 1 0 661.89 605.92 105.17 o 10 1 0 114.16 142.52 17.69 o 11 1 0 0.86 7.16 8.02 o 12 1 0 289.37 263.93 40.03 o 13 1 0 1039.67 1066.35 138.21 o 14 1 0 971.90 813.61 67.77 o 15 1 0 187.48 148.98 28.96 o 16 1 0 10.92 7.50 24.83 o 17 1 0 9.33 49.64 18.06 o 18 1 0 54.55 93.92 30.28 o 0 2 0 12458.87 11347.93 82.61 o 1 2 0 268.01 268.10 11.86 o 2 2 0 2184.16 2063.75 34.57 o 3 2 0 2138.52 2097.87 29.73 o 4 2 0 3342.40 3150.14 39.09 o 5 2 0 86.46 86.94 9.24 o 6 2 0 2655.80 2879.93 61.73 o 7 2 0 648.50 811.01 32.31 o 8 2 0 1212.18 1230.76 39.03 o 9 2 0 74.24 78.38 10.11 o 10 2 0 17.42 17.11 9.04 o 11 2 0 3.99 -5.74 16.81 o 12 2 0 307.55 322.90 47.07 o 13 2 0 362.83 296.20 83.13 o 14 2 0 296.89 295.97 43.70 o 15 2 0 93.08 132.14 24.14 o 16 2 0 32.22 53.48 21.63 o 17 2 0 0.92 2.15 22.35 o 18 2 0 0.53 19.82 35.33 o 1 3 0 588.41 568.05 23.87 o 2 3 0 90.13 103.60 11.65 o 3 3 0 454.78 473.43 21.49 o 4 3 0 650.64 673.03 23.18 o 5 3 0 476.38 531.97 31.03 o 6 3 0 2685.80 2951.09 59.20 o 7 3 0 357.87 331.95 32.16 o 8 3 0 3.82 -1.17 6.90 o 9 3 0 16.92 37.94 8.90 o 10 3 0 39.31 46.46 9.61 o 11 3 0 11.55 9.56 9.45 o 12 3 0 109.92 135.11 23.75 o 13 3 0 117.13 154.95 40.29 o 14 3 0 1.61 14.41 16.58 o 15 3 0 64.24 72.91 29.62 o 16 3 0 63.52 65.26 24.20 o 17 3 0 0.01 -26.13 30.14 o 0 4 0 24.40 23.52 5.33 o 1 4 0 629.66 677.68 22.86 o 2 4 0 8.84 28.30 6.22 o 3 4 0 178.00 210.48 25.17 o 4 4 0 124.02 153.73 16.26 o 5 4 0 155.87 158.23 16.41 o 6 4 0 55.26 52.97 8.07 o 7 4 0 5.12 16.00 6.80 o 8 4 0 53.68 38.54 8.78 o 9 4 0 7.87 12.84 6.19 o 10 4 0 169.05 137.68 17.40 o 11 4 0 0.38 19.71 12.60 o 12 4 0 51.27 69.17 17.80 o 13 4 0 736.52 712.30 109.56 o 14 4 0 16.02 18.55 30.01 o 15 4 0 9.36 12.25 12.10 o 16 4 0 0.35 -3.14 21.21 o 1 5 0 893.71 912.33 38.33 o 2 5 0 23.94 19.41 4.11 o 3 5 0 22.14 29.77 4.87 o 4 5 0 0.24 0.71 4.55 o 5 5 0 0.03 0.63 5.31 o 6 5 0 5.62 2.31 7.68 o 7 5 0 14.09 14.05 7.54 o 8 5 0 93.77 109.48 15.64 o 9 5 0 33.69 35.45 13.65 o 10 5 0 278.15 233.84 36.34 o 11 5 0 47.43 60.85 23.82 o 12 5 0 535.99 451.90 62.90 o 13 5 0 205.30 182.75 50.52 o 14 5 0 54.49 48.88 23.41 o 15 5 0 0.04 16.69 17.90 o 0 6 0 1060.66 1194.59 53.59 o 1 6 0 622.40 581.35 32.85 o 2 6 0 167.49 150.49 15.53 o 3 6 0 253.22 268.57 32.98 o 4 6 0 0.74 1.60 8.27 o 5 6 0 0.66 1.34 5.71 o 6 6 0 144.92 127.22 17.26 o 7 6 0 233.69 216.99 29.69 o 8 6 0 41.48 47.33 14.48 o 9 6 0 339.26 369.04 52.18 o 10 6 0 26.57 6.52 20.46 o 11 6 0 46.68 32.72 16.83 o 12 6 0 86.70 137.24 23.73 o 13 6 0 4.53 42.55 30.32 o 14 6 0 11.70 71.59 47.32 o 1 7 0 11.87 10.55 5.45 o 2 7 0 14.39 19.66 6.66 o 3 7 0 21.24 15.29 7.18 o 4 7 0 14.86 20.37 6.11 o 5 7 0 774.98 908.36 85.18 o 6 7 0 259.00 315.35 78.51 o 7 7 0 25.72 32.04 12.34 o 8 7 0 333.51 313.89 51.06 o 9 7 0 146.98 116.59 27.53 o 10 7 0 72.47 49.19 19.18 o 11 7 0 25.09 24.73 17.81 o 12 7 0 44.97 49.24 26.94 o 0 8 0 292.27 247.36 66.70 o 1 8 0 180.82 164.69 29.29 o 2 8 0 42.99 45.69 16.72 o 3 8 0 67.06 95.31 14.20 o 4 8 0 10.28 11.31 20.18 o 5 8 0 272.04 253.07 63.81 o 6 8 0 111.28 99.48 46.29 o 7 8 0 198.97 153.97 29.74 o 8 8 0 12.49 0.63 25.76 o 9 8 0 20.66 39.12 56.09 o 1 9 0 141.90 167.71 75.22 o 2 9 0 18.07 39.48 15.44 o 3 9 0 52.40 72.87 41.28 o -18 1 1 0.05 14.35 21.32 o -17 1 1 11.70 -0.70 23.97 o -16 1 1 5.57 3.99 13.77 o -15 1 1 103.21 101.76 20.62 o -14 1 1 366.55 375.21 53.92 o -13 1 1 1039.67 1048.07 131.80 o -12 1 1 36.55 44.03 13.89 o -11 1 1 57.57 59.36 14.07 o -10 1 1 82.66 103.27 14.92 o -9 1 1 3.68 10.18 8.74 o -8 1 1 542.12 478.10 90.64 o -7 1 1 54.56 57.89 9.26 o -6 1 1 54.18 32.06 9.85 o -5 1 1 6.04 7.16 5.15 o -4 1 1 1877.33 1718.45 27.02 o -3 1 1 339.99 327.38 11.29 o -2 1 1 313.95 286.38 8.29 o -1 1 1 258.60 236.55 7.73 o 0 1 1 250.85 240.11 6.90 o 1 1 1 24189.56 21335.85 91.61 o 2 1 1 529.57 471.28 17.24 o 3 1 1 9976.17 9039.73 75.30 o 4 1 1 4848.85 4881.43 49.50 o 5 1 1 706.78 770.01 23.55 o 6 1 1 6.17 11.89 6.62 o 7 1 1 2579.96 2686.27 61.07 o 8 1 1 547.85 492.17 31.60 o 9 1 1 1143.51 1193.20 40.72 o 10 1 1 183.37 179.47 22.78 o 11 1 1 1744.28 1843.50 51.31 o 12 1 1 0.90 0.51 9.28 o 13 1 1 650.92 639.63 51.67 o 14 1 1 99.15 94.03 28.29 o 15 1 1 79.03 104.21 23.53 o 16 1 1 9.81 -7.23 29.81 o 17 1 1 114.23 153.20 20.57 o 18 1 1 17.41 12.08 22.13 o -18 2 1 0.61 26.00 22.13 o -17 2 1 37.71 6.00 23.42 o -16 2 1 0.39 18.45 13.21 o -15 2 1 22.50 23.35 10.85 o -14 2 1 24.44 24.42 14.26 o -13 2 1 14.65 26.32 12.72 o -12 2 1 158.77 163.69 29.96 o -11 2 1 258.88 261.57 39.00 o -10 2 1 198.11 179.55 21.82 o -9 2 1 235.98 217.40 26.39 o -8 2 1 85.62 93.42 13.58 o -7 2 1 2951.42 3201.14 50.00 o -6 2 1 611.53 617.72 25.85 o -5 2 1 3237.26 3315.40 42.61 o -4 2 1 2030.13 2006.22 31.55 o -3 2 1 600.77 585.16 14.85 o -2 2 1 1256.38 1106.93 19.26 o -1 2 1 765.98 660.03 11.98 o 0 2 1 189.05 173.83 13.02 o 1 2 1 299.70 291.15 12.43 o 2 2 1 8250.08 7894.59 101.42 o 3 2 1 9911.44 9312.11 96.62 o 4 2 1 853.17 867.14 23.84 o 5 2 1 2118.32 2147.26 41.80 o 6 2 1 2323.10 2417.84 51.65 o 7 2 1 3102.11 3528.52 62.23 o 8 2 1 141.23 141.73 18.72 o 9 2 1 122.72 123.47 17.12 o 10 2 1 408.68 414.93 67.24 o 11 2 1 128.51 127.81 23.83 o 12 2 1 16.20 15.57 16.45 o 13 2 1 251.52 224.56 37.85 o 14 2 1 8.71 19.97 16.16 o 15 2 1 25.58 54.56 21.51 o 16 2 1 14.56 48.01 26.20 o 17 2 1 26.88 33.59 24.11 o -17 3 1 10.76 22.15 19.01 o -16 3 1 39.54 38.43 32.26 o -15 3 1 33.11 55.78 22.17 o -14 3 1 75.46 62.06 19.71 o -13 3 1 7.11 14.37 18.62 o -12 3 1 2.23 12.27 5.12 o -11 3 1 29.38 31.61 10.62 o -10 3 1 11.87 16.33 5.90 o -9 3 1 367.49 396.15 53.92 o -8 3 1 15.06 12.69 6.03 o -7 3 1 730.51 809.77 34.02 o -6 3 1 348.36 381.81 33.46 o -5 3 1 384.59 413.22 30.25 o -4 3 1 1178.86 1256.57 31.70 o -3 3 1 48.10 54.66 5.11 o -2 3 1 377.71 343.41 28.32 o -1 3 1 1.49 4.77 2.62 o 0 3 1 148.46 161.17 13.54 o 1 3 1 915.67 910.70 22.49 o 2 3 1 140.98 131.26 11.53 o 3 3 1 94.04 108.15 14.56 o 4 3 1 681.15 742.66 25.26 o 5 3 1 7579.23 8009.76 80.92 o 6 3 1 417.46 394.01 64.88 o 7 3 1 155.71 194.37 20.63 o 8 3 1 0.07 1.48 5.26 o 9 3 1 52.11 34.70 8.43 o 10 3 1 33.76 23.88 9.22 o 11 3 1 18.03 34.26 12.80 o 12 3 1 96.53 113.92 29.59 o 13 3 1 0.30 32.46 19.07 o 14 3 1 251.56 271.31 37.02 o 15 3 1 18.07 29.84 15.00 o 16 3 1 123.91 116.41 23.12 o 17 3 1 17.02 48.64 40.15 o -17 4 1 48.42 67.59 24.98 o -16 4 1 51.04 56.29 34.90 o -15 4 1 97.28 118.94 29.51 o -14 4 1 0.15 21.22 15.20 o -13 4 1 2.18 16.67 13.43 o -12 4 1 281.31 236.27 33.68 o -11 4 1 26.28 20.88 8.84 o -10 4 1 19.46 24.61 10.47 o -9 4 1 112.28 123.28 13.37 o -8 4 1 12.04 6.49 6.29 o -7 4 1 51.56 56.87 8.95 o -6 4 1 862.90 929.19 32.55 o -5 4 1 341.69 337.85 25.86 o -4 4 1 147.73 155.68 15.75 o -3 4 1 1642.73 1766.44 50.46 o -2 4 1 79.74 101.69 11.41 o -1 4 1 1817.20 2021.14 29.60 o 0 4 1 927.65 910.03 29.61 o 1 4 1 90.91 90.82 9.47 o 2 4 1 446.69 456.61 20.92 o 3 4 1 115.36 138.79 12.25 o 4 4 1 989.80 1095.93 34.31 o 5 4 1 434.46 455.01 57.39 o 6 4 1 6.28 8.75 4.07 o 7 4 1 785.20 782.14 57.15 o 8 4 1 64.93 77.41 10.82 o 9 4 1 0.50 4.98 6.10 o 10 4 1 14.83 29.56 13.23 o 11 4 1 124.84 104.56 14.57 o 12 4 1 0.15 3.22 13.37 o 13 4 1 2.23 6.91 19.70 o 14 4 1 141.71 90.06 26.26 o 15 4 1 3.32 7.83 22.23 o 16 4 1 6.43 26.45 23.52 o -15 5 1 103.22 81.01 22.77 o -14 5 1 55.86 34.64 21.32 o -13 5 1 58.82 70.47 16.31 o -12 5 1 48.35 39.58 14.77 o -11 5 1 0.14 13.17 24.46 o -10 5 1 203.85 174.72 27.33 o -9 5 1 300.68 268.87 50.24 o -8 5 1 12.69 14.12 9.21 o -7 5 1 166.36 175.45 21.58 o -6 5 1 87.67 81.27 10.93 o -5 5 1 0.78 4.14 5.04 o -4 5 1 151.06 117.07 16.39 o -3 5 1 331.14 380.34 27.27 o -2 5 1 68.57 76.17 7.05 o -1 5 1 11.08 12.21 4.06 o 0 5 1 17.57 25.58 5.10 o 1 5 1 507.24 588.47 27.27 o 2 5 1 538.48 594.91 67.74 o 3 5 1 87.11 102.95 11.81 o 4 5 1 136.51 140.21 14.26 o 5 5 1 27.63 21.88 5.77 o 6 5 1 71.56 69.02 9.20 o 7 5 1 207.05 199.79 21.13 o 8 5 1 0.66 4.17 6.98 o 9 5 1 141.28 128.55 17.59 o 10 5 1 100.20 88.80 13.71 o 11 5 1 86.39 61.53 21.13 o 12 5 1 268.62 259.62 53.99 o 13 5 1 18.94 31.82 18.45 o 14 5 1 5.92 31.29 12.23 o 15 5 1 1.12 7.64 20.55 o -14 6 1 4.86 89.52 45.21 o -13 6 1 32.43 45.06 37.40 o -12 6 1 2.64 -10.34 24.67 o -11 6 1 290.32 239.39 54.85 o -10 6 1 135.21 102.38 25.26 o -9 6 1 3.95 5.50 10.67 o -8 6 1 364.64 394.97 37.65 o -7 6 1 2.59 6.94 10.74 o -6 6 1 27.97 37.65 8.30 o -5 6 1 249.32 254.68 35.91 o -4 6 1 46.38 38.55 8.42 o -3 6 1 16.43 11.52 6.34 o -2 6 1 308.57 272.56 33.69 o -1 6 1 28.39 30.34 5.77 o 0 6 1 1.31 1.76 4.87 o 1 6 1 137.84 157.18 16.08 o 2 6 1 2.20 8.41 6.16 o 3 6 1 15.37 19.22 10.08 o 4 6 1 0.93 16.49 8.43 o 5 6 1 1.70 7.86 6.60 o 6 6 1 110.53 113.62 13.69 o 7 6 1 157.94 184.49 26.17 o 8 6 1 993.15 941.69 121.13 o 9 6 1 16.53 16.25 12.50 o 10 6 1 15.46 18.41 20.45 o 11 6 1 109.74 97.46 27.42 o 12 6 1 240.97 230.41 51.40 o 13 6 1 73.42 80.53 21.37 o -12 7 1 61.77 79.96 29.60 o -11 7 1 109.01 113.96 29.20 o -10 7 1 18.25 9.19 22.12 o -9 7 1 196.26 255.00 48.05 o -8 7 1 711.71 886.73 166.77 o -7 7 1 15.61 17.95 13.29 o -6 7 1 20.09 33.30 8.73 o -5 7 1 502.60 595.17 119.18 o -4 7 1 457.54 467.24 60.01 o -3 7 1 18.21 3.22 6.23 o -2 7 1 33.80 40.99 7.54 o -1 7 1 112.97 114.14 13.43 o 0 7 1 0.13 1.70 6.01 o 1 7 1 33.18 31.26 6.37 o 2 7 1 13.36 15.86 6.88 o 3 7 1 132.50 147.88 17.33 o 4 7 1 20.32 26.44 10.98 o 5 7 1 74.82 83.74 14.52 o 6 7 1 201.72 213.05 23.74 o 7 7 1 2.78 4.19 12.05 o 8 7 1 67.05 98.59 21.25 o 9 7 1 201.31 210.31 49.10 o 10 7 1 4.16 -4.63 29.95 o 11 7 1 46.00 69.58 17.46 o -9 8 1 56.58 99.03 41.39 o -8 8 1 323.84 313.75 57.25 o -7 8 1 139.55 213.15 49.57 o -6 8 1 119.48 70.90 23.46 o -5 8 1 5.07 9.80 19.36 o -4 8 1 132.33 131.72 41.47 o -3 8 1 124.24 150.02 42.38 o -2 8 1 0.40 6.06 8.42 o -1 8 1 1.95 4.96 8.61 o 0 8 1 162.28 152.25 33.86 o 1 8 1 0.14 -7.46 14.34 o 2 8 1 39.58 29.79 11.87 o 3 8 1 186.63 194.27 42.94 o 4 8 1 43.09 35.89 15.40 o 5 8 1 268.93 279.01 66.08 o 6 8 1 501.14 431.98 180.53 o 7 8 1 54.21 65.44 26.30 o 8 8 1 8.13 31.09 15.39 o -4 9 1 116.41 48.26 44.14 o -3 9 1 39.53 26.94 20.41 o -2 9 1 187.76 150.79 76.51 o 0 9 1 4.50 29.88 21.24 o 1 9 1 17.95 -12.60 34.89 o 2 9 1 18.74 29.21 22.32 o 3 9 1 101.60 131.62 62.93 o -19 0 2 47.26 67.51 39.25 o -18 0 2 67.44 46.10 27.70 o -17 0 2 460.69 335.87 85.13 o -16 0 2 0.39 3.65 20.38 o -15 0 2 311.40 258.83 39.27 o -14 0 2 910.39 804.83 152.66 o -13 0 2 9882.81 10241.51 498.63 o -12 0 2 2924.17 3228.66 188.65 o -11 0 2 44.58 54.12 17.81 o -10 0 2 26.53 60.06 23.21 o -9 0 2 100.96 150.13 29.86 o -8 0 2 229.91 221.28 38.30 o -7 0 2 858.04 801.27 43.61 o -6 0 2 43.41 43.01 12.40 o -5 0 2 263.66 210.12 65.37 o -4 0 2 328.73 291.88 26.33 o -3 0 2 2753.30 2329.24 116.12 o -2 0 2 27722.42 24870.29 167.40 o -1 0 2 328.82 244.57 12.95 o 0 0 2 961.33 780.36 30.64 o 1 0 2 2159.04 1642.36 103.09 o 2 0 2 2618.80 2520.86 52.77 o 3 0 2 2612.17 2432.18 61.77 o 4 0 2 602.19 555.82 41.76 o 5 0 2 139.12 125.70 22.29 o 6 0 2 210.51 265.70 59.59 o 7 0 2 1800.90 2011.22 76.21 o 8 0 2 6.58 -12.92 17.76 o 9 0 2 8552.23 8749.01 175.89 o 10 0 2 80.39 89.56 18.10 o 11 0 2 251.69 261.57 102.60 o 12 0 2 1793.40 1820.51 136.84 o 13 0 2 104.01 99.35 25.56 o 14 0 2 14.47 -28.05 40.00 o 15 0 2 0.30 -22.47 45.11 o 16 0 2 584.02 708.19 232.61 o 17 0 2 15.38 18.29 35.62 o 18 0 2 219.73 237.48 76.75 o -18 1 2 17.18 35.78 19.65 o -17 1 2 3.11 30.40 21.48 o -16 1 2 6.48 9.72 10.51 o -15 1 2 6.92 7.87 11.00 o -14 1 2 824.12 874.67 146.07 o -13 1 2 339.93 331.10 77.39 o -12 1 2 95.97 85.91 16.69 o -11 1 2 1.79 9.10 11.15 o -10 1 2 670.63 646.65 89.52 o -9 1 2 27.39 31.43 8.60 o -8 1 2 146.47 135.83 17.66 o -7 1 2 18.58 12.46 6.13 o -6 1 2 36.82 36.37 5.63 o -5 1 2 272.11 272.33 25.75 o -4 1 2 2601.46 2377.96 49.27 o -3 1 2 585.88 509.86 15.13 o -2 1 2 655.51 480.95 10.27 o -1 1 2 60.57 49.91 4.72 o 0 1 2 15032.73 13689.30 61.32 o 1 1 2 152.49 139.69 18.38 o 2 1 2 13469.85 12188.39 162.12 o 3 1 2 13.66 12.45 4.68 o 4 1 2 372.59 327.18 13.63 o 5 1 2 773.67 799.88 18.88 o 6 1 2 2137.93 2303.89 42.13 o 7 1 2 1256.01 1336.17 50.46 o 8 1 2 266.14 284.32 41.86 o 9 1 2 546.79 550.69 89.63 o 10 1 2 82.30 85.84 15.18 o 11 1 2 0.16 3.74 19.71 o 12 1 2 4204.29 4565.52 256.24 o 13 1 2 35.95 22.51 14.98 o 14 1 2 194.52 206.49 44.49 o 15 1 2 60.69 80.14 20.66 o 16 1 2 60.43 67.83 29.31 o 17 1 2 1.75 3.97 32.35 o 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