#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/73/2237320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237320_Fobs loop_ _publ_author_name 'Lloyd, Barry A.' 'Arif, Atta M.' 'Coots, Robert J.' _publ_section_title ; endo,endo-Tetracyclo[6.2.1.1^3,6^.0^2,7^]dodeca-9-en-anti-11-yl 4-bromobenzoate ; _journal_coeditor_code HB7005 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o202 _journal_page_last o203 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.012 _cell_angle_gamma 90.000 _cell_length_a 13.2569 _cell_length_b 10.5045 _cell_length_c 12.2039 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file hb7005Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '8-OPBB @150K Clrless Plate Monoclinic P21/c 2/7/2011 SHELXL97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1806.59 1808.98 26.72 o 3 0 0 17661.81 18061.04 260.20 o 4 0 0 28169.12 28383.97 401.98 o 5 0 0 20509.44 20773.04 299.76 o 6 0 0 5651.55 5708.03 88.21 o 7 0 0 47.29 73.07 6.64 o 8 0 0 37.62 42.51 6.64 o 9 0 0 4362.55 4456.59 85.29 o 10 0 0 4295.37 4285.92 77.27 o 11 0 0 281.88 329.53 14.62 o 12 0 0 67.34 58.46 9.30 o 13 0 0 46.29 53.14 9.30 o 14 0 0 169.32 191.33 13.29 o 15 0 0 292.23 272.39 19.93 o 1 1 0 2907.58 2890.36 114.28 o 2 1 0 4019.68 4122.96 67.15 o 3 1 0 12861.09 12904.13 131.89 o 4 1 0 2004.59 2002.92 24.01 o 5 1 0 643.99 672.12 10.34 o 6 1 0 796.19 886.69 13.06 o 7 1 0 325.36 339.67 7.95 o 8 1 0 29.15 45.36 11.29 o 9 1 0 307.68 293.77 8.46 o 10 1 0 282.04 287.72 10.63 o 11 1 0 673.47 708.92 13.60 o 12 1 0 28.53 31.09 4.15 o 13 1 0 0.45 3.32 3.76 o 14 1 0 74.38 44.26 13.40 o 15 1 0 8.14 -20.96 34.54 o 0 2 0 1142.16 1184.15 20.81 o 1 2 0 19987.87 19833.83 202.26 o 2 2 0 112.18 110.44 3.99 o 3 2 0 71.06 73.75 3.19 o 4 2 0 8633.40 8458.12 93.96 o 5 2 0 6559.77 6353.96 73.75 o 6 2 0 1573.23 1466.90 27.94 o 7 2 0 498.64 489.11 9.97 o 8 2 0 761.66 754.96 12.76 o 9 2 0 2455.23 2443.05 31.76 o 10 2 0 1902.79 1903.09 25.19 o 11 2 0 781.14 735.41 10.78 o 12 2 0 11.33 8.77 8.84 o 13 2 0 314.17 347.18 45.84 o 14 2 0 416.82 458.36 25.91 o 15 2 0 227.67 227.14 27.00 o 1 3 0 119.49 114.11 6.64 o 2 3 0 580.96 534.62 7.52 o 3 3 0 24.66 28.15 2.82 o 4 3 0 8.68 7.09 2.38 o 5 3 0 430.89 432.83 7.85 o 6 3 0 6.36 9.30 4.65 o 7 3 0 929.36 990.43 14.01 o 8 3 0 101.58 100.26 5.98 o 9 3 0 10.71 8.82 3.32 o 10 3 0 93.73 90.80 15.28 o 11 3 0 13.49 12.95 9.96 o 12 3 0 57.49 72.78 10.57 o 13 3 0 3.16 10.02 11.27 o 14 3 0 18.57 23.75 14.68 o 15 3 0 26.86 35.97 37.20 o 0 4 0 2490.40 2490.03 41.30 o 1 4 0 7767.02 7638.16 86.78 o 2 4 0 479.72 493.03 18.61 o 3 4 0 182.61 159.26 4.15 o 4 4 0 1060.98 986.14 13.42 o 5 4 0 7069.14 6886.49 74.73 o 6 4 0 3411.56 3455.69 39.90 o 7 4 0 523.26 531.92 9.57 o 8 4 0 784.35 841.49 13.03 o 9 4 0 1166.60 1172.98 18.41 o 10 4 0 633.41 603.76 19.94 o 11 4 0 787.58 817.89 22.04 o 12 4 0 6.92 9.80 10.25 o 13 4 0 3.43 6.09 11.76 o 14 4 0 229.36 210.97 26.57 o 1 5 0 689.45 747.40 12.46 o 2 5 0 534.25 607.78 13.29 o 3 5 0 685.05 785.72 11.28 o 4 5 0 433.05 494.54 8.46 o 5 5 0 53.86 62.98 4.42 o 6 5 0 1.21 -1.81 4.61 o 7 5 0 159.27 167.66 7.31 o 8 5 0 68.30 79.16 6.64 o 9 5 0 54.11 44.26 5.08 o 10 5 0 60.80 55.71 8.52 o 11 5 0 207.49 194.30 23.92 o 12 5 0 18.04 31.98 11.45 o 13 5 0 2.72 17.76 16.61 o 14 5 0 6.02 20.64 49.16 o 0 6 0 4193.23 4002.47 68.48 o 1 6 0 1564.52 1419.32 29.27 o 2 6 0 4177.63 4338.79 53.72 o 3 6 0 1017.94 1046.85 16.27 o 4 6 0 6167.26 6141.28 71.45 o 5 6 0 3517.79 3338.32 43.09 o 6 6 0 2985.78 2982.56 42.81 o 7 6 0 69.04 60.16 5.81 o 8 6 0 1086.50 1072.87 19.50 o 9 6 0 1118.43 1164.06 20.54 o 10 6 0 1980.28 2059.25 43.89 o 11 6 0 777.38 686.61 29.24 o 12 6 0 190.66 194.81 19.80 o 13 6 0 360.60 380.14 28.27 o 1 7 0 519.82 584.06 11.27 o 2 7 0 47.76 44.20 5.41 o 3 7 0 1493.31 1431.97 22.68 o 4 7 0 129.06 126.33 7.31 o 5 7 0 9.61 16.55 5.10 o 6 7 0 55.27 65.61 6.05 o 7 7 0 200.11 195.64 13.95 o 8 7 0 0.05 6.95 4.86 o 9 7 0 17.42 27.76 13.29 o 10 7 0 51.02 36.93 20.59 o 11 7 0 158.76 165.90 19.49 o 12 7 0 14.57 13.06 34.54 o 13 7 0 85.61 74.42 22.33 o 0 8 0 3814.55 3808.29 70.05 o 1 8 0 2993.75 3023.32 53.25 o 2 8 0 39.57 29.65 6.63 o 3 8 0 173.91 178.81 8.03 o 4 8 0 724.02 739.02 14.55 o 5 8 0 1693.50 1682.26 26.60 o 6 8 0 2977.47 2952.00 48.26 o 7 8 0 207.94 207.81 9.23 o 8 8 0 40.91 30.79 6.13 o 9 8 0 667.20 682.61 51.17 o 10 8 0 909.54 891.51 85.07 o 11 8 0 1135.57 1225.52 45.30 o 12 8 0 26.90 6.89 19.59 o 1 9 0 184.04 205.67 9.30 o 2 9 0 439.68 480.23 12.47 o 3 9 0 180.83 165.62 8.84 o 4 9 0 149.20 158.86 8.84 o 5 9 0 16.52 21.66 7.97 o 6 9 0 12.02 4.09 7.31 o 7 9 0 306.92 318.29 31.23 o 8 9 0 58.85 48.97 14.61 o 9 9 0 128.14 145.21 14.93 o 10 9 0 93.26 116.86 22.59 o 11 9 0 225.32 197.37 47.17 o 0 10 0 1809.53 1893.43 45.94 o 1 10 0 910.34 994.47 32.57 o 2 10 0 41.14 32.88 8.64 o 3 10 0 27.29 38.50 13.29 o 4 10 0 804.15 892.57 20.90 o 5 10 0 1528.69 1596.64 31.22 o 6 10 0 199.85 184.06 14.62 o 7 10 0 330.03 308.74 25.91 o 8 10 0 3.63 8.93 12.47 o 9 10 0 519.68 540.08 69.10 o 10 10 0 1028.02 886.94 46.97 o 1 11 0 12.66 16.09 14.61 o 2 11 0 31.20 52.88 7.40 o 3 11 0 9.33 2.27 9.96 o 4 11 0 37.83 26.20 8.67 o 5 11 0 10.91 20.94 11.29 o 6 11 0 12.41 7.37 10.38 o 7 11 0 163.10 203.90 91.01 o 8 11 0 0.04 14.91 16.60 o 9 11 0 73.55 2.73 26.66 o 0 12 0 2058.70 2173.86 174.22 o 1 12 0 947.49 931.25 60.48 o 2 12 0 36.96 15.94 7.52 o 3 12 0 212.02 241.82 13.29 o 4 12 0 680.53 711.15 24.84 o 5 12 0 1061.57 1144.87 67.13 o 6 12 0 353.43 300.10 29.74 o 7 12 0 119.13 93.19 23.23 o 1 13 0 128.54 73.20 18.46 o 2 13 0 1.25 -16.91 16.91 o 3 13 0 14.09 5.50 51.15 o 4 13 0 36.57 57.11 31.10 o -15 1 1 479.19 475.54 42.52 o -14 1 1 90.83 69.56 10.21 o -13 1 1 1005.55 987.19 39.21 o -12 1 1 1607.51 1569.56 61.17 o -11 1 1 2006.00 2011.89 25.85 o -10 1 1 669.00 692.68 10.78 o -9 1 1 30.53 25.31 2.82 o -8 1 1 3888.27 3890.10 42.91 o -7 1 1 3353.55 3261.17 34.16 o -6 1 1 4121.88 3902.81 41.04 o -5 1 1 7414.08 7094.92 70.59 o -4 1 1 2247.39 2379.49 72.01 o -3 1 1 13499.28 13376.11 146.60 o -2 1 1 4360.03 4322.86 52.34 o -1 1 1 1850.32 1769.41 28.29 o 0 1 1 223.80 237.87 9.97 o 1 1 1 544.30 546.26 7.01 o 2 1 1 1343.96 1271.51 21.32 o 3 1 1 208.11 175.43 4.15 o 4 1 1 4688.50 4391.39 45.66 o 5 1 1 4864.35 4894.15 53.84 o 6 1 1 59.27 51.95 4.70 o 7 1 1 1851.29 1688.04 23.47 o 8 1 1 1871.89 1834.27 26.70 o 9 1 1 2843.60 2857.57 42.82 o 10 1 1 178.58 190.00 8.89 o 11 1 1 5.42 2.30 14.61 o 12 1 1 456.56 473.23 13.60 o 13 1 1 713.94 727.04 16.92 o 14 1 1 618.89 583.78 21.71 o -15 2 1 1.51 -14.09 14.09 o -14 2 1 0.97 16.87 10.06 o -13 2 1 3.72 -1.90 9.05 o -12 2 1 279.99 283.93 13.48 o -11 2 1 338.58 347.76 12.81 o -10 2 1 189.34 186.52 10.25 o -9 2 1 11.64 9.30 4.61 o -8 2 1 722.01 738.83 19.28 o -7 2 1 1322.02 1414.28 21.90 o -6 2 1 1131.48 1276.85 38.57 o -5 2 1 0.69 0.50 3.42 o -4 2 1 1817.64 1768.59 20.37 o -3 2 1 3523.14 3551.10 40.80 o -2 2 1 448.08 459.20 7.01 o -1 2 1 96.59 83.80 2.82 o 0 2 1 351.40 404.30 6.58 o 1 2 1 183.83 212.65 4.70 o 2 2 1 438.71 482.28 7.00 o 3 2 1 45.14 46.69 3.19 o 4 2 1 4609.10 4766.88 59.04 o 5 2 1 396.71 430.65 8.46 o 6 2 1 74.33 77.43 5.31 o 7 2 1 57.68 71.82 7.31 o 8 2 1 8.57 17.15 5.10 o 9 2 1 68.57 66.75 6.05 o 10 2 1 58.15 70.77 10.63 o 11 2 1 68.30 71.55 11.96 o 12 2 1 2.89 7.37 6.64 o 13 2 1 223.91 227.39 13.95 o 14 2 1 29.43 0.66 15.03 o -15 3 1 142.44 155.93 19.66 o -14 3 1 29.98 35.69 12.47 o -13 3 1 173.66 173.75 15.94 o -12 3 1 2567.40 2599.17 85.81 o -11 3 1 1101.15 1119.17 25.31 o -10 3 1 1625.76 1583.10 54.53 o -9 3 1 809.74 805.74 24.59 o -8 3 1 913.75 908.81 17.58 o -7 3 1 10563.07 10721.98 139.48 o -6 3 1 5909.02 5760.12 65.87 o -5 3 1 178.82 134.68 9.97 o -4 3 1 60.75 60.27 3.19 o -3 3 1 6032.75 6096.55 65.60 o -2 3 1 14166.20 14273.33 139.93 o -1 3 1 10392.81 10189.34 112.55 o 0 3 1 7413.48 7317.45 83.34 o 1 3 1 757.86 785.87 11.31 o 2 3 1 5161.07 5037.39 58.70 o 3 3 1 17231.08 16891.15 182.41 o 4 3 1 5477.34 5242.47 57.49 o 5 3 1 599.81 566.04 9.84 o 6 3 1 20.44 9.96 3.42 o 7 3 1 1330.65 1274.46 17.47 o 8 3 1 4353.22 4307.96 49.51 o 9 3 1 1129.99 1148.31 19.68 o 10 3 1 1173.86 1181.56 19.68 o 11 3 1 70.25 85.23 5.41 o 12 3 1 279.39 270.98 15.94 o 13 3 1 799.80 850.27 31.19 o 14 3 1 272.88 287.98 45.18 o -15 4 1 31.75 24.16 38.53 o -14 4 1 41.29 -2.42 55.14 o -13 4 1 96.12 96.62 15.28 o -12 4 1 3.70 30.73 21.26 o -11 4 1 69.16 43.87 10.63 o -10 4 1 1.00 -2.44 9.96 o -9 4 1 95.49 87.31 7.85 o -8 4 1 360.64 401.75 12.19 o -7 4 1 501.31 544.91 16.61 o -6 4 1 0.13 0.50 3.88 o -5 4 1 341.25 361.88 13.95 o -4 4 1 920.46 941.83 12.77 o -3 4 1 3234.98 3505.23 39.41 o -2 4 1 1500.02 1560.04 18.75 o -1 4 1 322.90 353.21 7.00 o 0 4 1 1017.24 1045.34 14.70 o 1 4 1 1602.58 1705.88 21.75 o 2 4 1 77.53 103.39 4.42 o 3 4 1 605.18 620.18 9.40 o 4 4 1 295.90 320.29 7.31 o 5 4 1 31.82 32.82 4.42 o 6 4 1 1176.35 1200.58 16.92 o 7 4 1 276.49 301.30 7.62 o 8 4 1 42.06 36.42 4.42 o 9 4 1 82.70 82.91 5.41 o 10 4 1 235.00 254.20 7.85 o 11 4 1 90.48 95.00 8.64 o 12 4 1 0.03 2.76 21.26 o 13 4 1 40.75 37.62 19.26 o 14 4 1 16.71 25.01 30.17 o -14 5 1 36.55 42.85 36.54 o -13 5 1 181.89 177.50 27.24 o -12 5 1 536.67 552.74 55.15 o -11 5 1 2353.39 2435.29 65.85 o -10 5 1 170.48 172.77 10.70 o -9 5 1 136.45 128.94 16.61 o -8 5 1 2503.81 2505.03 34.62 o -7 5 1 2392.04 2303.17 34.21 o -6 5 1 5539.50 5460.81 65.41 o -5 5 1 1285.34 1295.15 23.94 o -4 5 1 27.49 36.84 3.76 o -3 5 1 773.67 725.00 11.16 o -2 5 1 9211.74 9178.29 98.64 o -1 5 1 20619.98 21637.33 325.98 o 0 5 1 3266.79 3318.56 39.40 o 1 5 1 2.01 10.63 4.15 o 2 5 1 8066.31 8264.84 87.73 o 3 5 1 11973.45 12103.91 143.44 o 4 5 1 8697.45 8648.66 99.11 o 5 5 1 133.08 135.99 11.29 o 6 5 1 745.22 766.10 19.94 o 7 5 1 1521.20 1551.77 21.90 o 8 5 1 2718.24 2675.06 35.69 o 9 5 1 1740.83 1698.08 25.34 o 10 5 1 45.52 53.99 5.41 o 11 5 1 16.38 29.71 10.42 o 12 5 1 595.98 630.08 48.51 o 13 5 1 372.17 354.15 30.56 o -14 6 1 20.38 -0.20 18.89 o -13 6 1 4.56 4.80 14.57 o -12 6 1 112.99 89.81 43.84 o -11 6 1 124.32 129.62 12.10 o -10 6 1 26.45 35.42 9.23 o -9 6 1 8.89 21.85 13.29 o -8 6 1 198.91 186.66 37.87 o -7 6 1 65.35 63.77 6.34 o -6 6 1 3.46 -1.59 4.42 o -5 6 1 64.80 65.15 5.31 o -4 6 1 59.55 50.80 4.70 o -3 6 1 311.26 370.17 8.89 o -2 6 1 377.05 412.41 11.96 o -1 6 1 298.50 328.72 7.85 o 0 6 1 6.42 19.78 4.65 o 1 6 1 4.75 17.88 4.61 o 2 6 1 89.65 94.51 5.10 o 3 6 1 91.25 101.90 5.41 o 4 6 1 68.15 77.94 5.41 o 5 6 1 78.13 67.35 5.63 o 6 6 1 115.42 125.01 5.81 o 7 6 1 7.51 5.68 4.61 o 8 6 1 203.06 215.48 7.85 o 9 6 1 0.24 6.64 4.75 o 10 6 1 40.17 41.44 18.60 o 11 6 1 0.04 14.77 20.59 o 12 6 1 23.58 -1.22 16.61 o 13 6 1 0.72 -15.36 18.29 o -13 7 1 27.30 -6.05 23.25 o -12 7 1 139.26 151.82 19.93 o -11 7 1 706.36 744.42 29.90 o -10 7 1 433.09 459.90 33.89 o -9 7 1 4.49 10.57 9.30 o -8 7 1 200.15 198.58 15.28 o -7 7 1 4171.14 4122.13 61.17 o -6 7 1 2783.50 2827.11 37.09 o -5 7 1 582.87 584.08 11.72 o -4 7 1 210.39 210.61 7.52 o -3 7 1 1125.50 1149.69 18.80 o -2 7 1 6238.05 6087.81 75.61 o -1 7 1 2900.77 2814.42 36.79 o 0 7 1 992.51 1001.37 16.23 o 1 7 1 24.25 36.05 11.29 o 2 7 1 2050.72 2042.50 40.58 o 3 7 1 5490.57 5403.86 61.91 o 4 7 1 1104.83 1071.64 16.61 o 5 7 1 420.07 418.50 15.28 o 6 7 1 141.38 140.26 7.94 o 7 7 1 1444.73 1424.51 24.92 o 8 7 1 1238.49 1262.89 21.13 o 9 7 1 1180.23 1226.51 22.59 o 10 7 1 161.43 139.72 15.28 o 11 7 1 28.70 32.55 15.93 o 12 7 1 460.59 524.33 70.43 o -12 8 1 2.12 -25.69 43.84 o -11 8 1 38.40 20.50 33.88 o -10 8 1 95.25 83.58 17.27 o -9 8 1 84.83 87.22 23.25 o -8 8 1 155.95 169.68 10.08 o -7 8 1 68.24 66.83 14.61 o -6 8 1 87.93 79.45 7.00 o -5 8 1 576.67 597.36 18.61 o -4 8 1 1373.11 1387.65 25.54 o -3 8 1 2.34 -2.66 4.86 o -2 8 1 493.42 484.34 11.27 o -1 8 1 404.16 391.26 10.26 o 0 8 1 13.30 18.80 5.63 o 1 8 1 78.81 101.51 8.03 o 2 8 1 659.58 659.63 15.95 o 3 8 1 626.81 658.37 14.98 o 4 8 1 223.77 213.24 17.27 o 5 8 1 236.45 209.42 11.96 o 6 8 1 286.45 320.69 12.66 o 7 8 1 128.54 134.09 9.57 o 8 8 1 19.99 26.87 8.30 o 9 8 1 8.32 -8.60 8.60 o 10 8 1 87.59 69.06 12.10 o 11 8 1 53.17 52.59 18.83 o 12 8 1 22.94 -4.41 35.87 o -12 9 1 398.69 388.55 38.93 o -11 9 1 205.87 257.26 29.19 o -10 9 1 350.93 350.53 36.54 o -9 9 1 15.08 33.21 25.91 o -8 9 1 42.61 23.91 7.97 o -7 9 1 333.29 362.29 18.60 o -6 9 1 1396.60 1407.59 29.39 o -5 9 1 1828.69 1850.57 30.66 o -4 9 1 496.26 500.95 30.57 o -3 9 1 1752.33 1764.70 28.54 o -2 9 1 2218.06 2214.29 33.72 o -1 9 1 2834.52 2799.37 41.23 o 0 9 1 1030.22 1046.06 19.91 o 1 9 1 72.72 97.78 7.97 o 2 9 1 1167.98 1107.76 22.04 o 3 9 1 1959.67 1942.08 31.92 o 4 9 1 2411.51 2343.38 37.35 o 5 9 1 592.61 582.69 16.61 o 6 9 1 870.08 877.88 28.58 o 7 9 1 1106.16 1118.85 44.53 o 8 9 1 1386.79 1375.21 34.50 o 9 9 1 12.93 3.00 10.77 o 10 9 1 10.19 1.33 15.69 o 11 9 1 163.58 151.62 23.00 o -10 10 1 133.95 125.71 25.30 o -9 10 1 0.77 -16.33 41.18 o -8 10 1 6.51 -6.60 42.51 o -7 10 1 0.53 5.80 10.21 o -6 10 1 0.01 -2.79 11.96 o -5 10 1 145.68 114.17 11.72 o -4 10 1 47.12 49.07 7.31 o -3 10 1 241.99 247.93 9.38 o -2 10 1 39.31 33.21 6.20 o -1 10 1 120.26 110.09 7.24 o 0 10 1 0.01 -0.44 5.94 o 1 10 1 211.04 189.86 9.23 o 2 10 1 18.37 31.84 13.95 o 3 10 1 292.92 297.13 11.45 o 4 10 1 16.31 26.53 7.13 o 5 10 1 4.41 4.32 6.84 o 6 10 1 117.49 105.00 24.58 o 7 10 1 139.04 108.98 18.60 o 8 10 1 3.84 -1.70 11.49 o 9 10 1 10.24 -9.13 14.68 o -9 11 1 70.56 61.51 22.06 o -8 11 1 673.20 651.30 44.45 o -7 11 1 825.44 827.21 37.19 o -6 11 1 1127.51 1112.05 51.84 o -5 11 1 668.00 701.66 27.29 o -4 11 1 175.23 165.33 15.94 o -3 11 1 918.85 949.53 26.06 o -2 11 1 1520.96 1446.38 51.19 o -1 11 1 1315.67 1283.23 23.39 o 0 11 1 487.64 497.84 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