#------------------------------------------------------------------------------ #$Date: 2013-03-10 17:00:37 +0200 (Sun, 10 Mar 2013) $ #$Revision: 75609 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/73/2237388.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237388_Fobs loop_ _publ_author_name 'Mrad, Mohamed Lahbib' 'Zeller, Matthias' 'Rzaigui, Mohamed' 'Ben Nasr, Cherif' _publ_section_title ; 2-Chlorobenzene-1,4-diaminium bis(dihydrogenphosphate) ; _journal_coeditor_code RU2048 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o159 _journal_page_last o160 _journal_volume 69 _journal_year 2013 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.0084 _cell_length_b 7.9404 _cell_length_c 23.0644 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.6708 _[local]_cod_data_source_file ru2048Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 12mz312_0m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.35 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 265.66 314.83 6.66 o 6 0 0 328.51 323.59 14.70 o 8 0 0 119.06 121.44 10.23 o 10 0 0 520.38 510.12 24.53 o 1 1 0 1770.34 1905.16 40.14 o 3 1 0 836.89 871.66 12.55 o 4 1 0 227.37 254.56 5.63 o 5 1 0 267.63 277.92 6.20 o 6 1 0 1426.15 1458.95 28.09 o 7 1 0 576.32 511.50 14.88 o 8 1 0 1424.47 1401.07 29.82 o 9 1 0 40.77 47.46 5.80 o 10 1 0 143.61 156.14 9.29 o 1 2 0 850.22 831.04 8.87 o 3 2 0 0.16 8.28 1.11 o 4 2 0 6.97 15.53 1.96 o 5 2 0 250.52 234.66 6.05 o 6 2 0 0.37 6.98 3.93 o 7 2 0 62.98 71.28 5.19 o 8 2 0 1599.31 1559.94 32.38 o 9 2 0 68.89 76.36 6.29 o 10 2 0 45.20 51.44 8.89 o 2 3 0 3931.34 4446.23 46.63 o 3 3 0 343.03 371.58 7.77 o 4 3 0 2242.01 2206.11 25.05 o 5 3 0 0.19 9.60 1.70 o 6 3 0 1048.31 1042.51 22.39 o 7 3 0 126.83 108.24 6.48 o 8 3 0 260.25 256.08 10.72 o 9 3 0 200.14 190.97 9.81 o 10 3 0 1.33 5.90 3.44 o 0 4 0 3.23 2.54 0.84 o 1 4 0 6679.12 6781.30 99.14 o 2 4 0 1058.34 1004.92 13.22 o 3 4 0 93.58 113.06 4.54 o 4 4 0 73.28 79.52 2.86 o 5 4 0 810.46 795.87 14.55 o 6 4 0 179.58 177.18 7.84 o 7 4 0 30.25 30.74 4.29 o 8 4 0 2558.49 2566.84 48.10 o 9 4 0 96.91 77.25 9.80 o 1 5 0 9672.55 10393.44 154.44 o 2 5 0 2674.05 2817.28 32.19 o 3 5 0 2.85 13.48 1.67 o 4 5 0 177.01 172.01 10.09 o 5 5 0 80.62 76.47 4.11 o 6 5 0 1.42 7.30 1.94 o 7 5 0 40.43 45.94 5.24 o 8 5 0 89.94 89.89 10.41 o 0 6 0 4554.63 4247.86 54.65 o 1 6 0 1036.25 1097.37 13.72 o 2 6 0 6.90 11.60 3.38 o 3 6 0 2873.80 3028.36 35.37 o 4 6 0 147.01 146.62 5.62 o 5 6 0 467.67 453.83 11.06 o 6 6 0 4.49 7.40 4.17 o 7 6 0 268.22 266.90 16.70 o 8 6 0 237.19 239.56 16.53 o 1 7 0 3051.81 3029.56 35.88 o 2 7 0 46.94 48.36 3.04 o 3 7 0 244.09 255.43 9.96 o 4 7 0 26.80 30.51 3.28 o 5 7 0 58.80 57.80 6.09 o 6 7 0 93.16 102.26 10.74 o 7 7 0 1865.19 1941.50 57.88 o 0 8 0 244.27 231.14 12.32 o 1 8 0 131.21 118.67 4.64 o 2 8 0 0.07 1.80 1.34 o 3 8 0 2264.51 2282.36 29.53 o 4 8 0 0.41 2.82 2.12 o 5 8 0 1.30 6.21 4.59 o 6 8 0 20.33 20.31 4.55 o 7 8 0 552.90 614.17 28.30 o 1 9 0 1511.03 1475.65 21.87 o 2 9 0 496.00 515.69 15.54 o 3 9 0 65.16 62.39 7.43 o 4 9 0 7.13 10.60 4.23 o 5 9 0 21.53 30.20 5.35 o 6 9 0 22.04 33.37 5.54 o 0 10 0 1096.97 1094.91 38.58 o 1 10 0 108.60 122.92 10.34 o 2 10 0 579.77 561.62 14.45 o 3 10 0 223.10 215.97 11.76 o 4 10 0 32.54 26.57 7.51 o 5 10 0 79.47 97.74 8.19 o 1 11 0 866.38 884.59 24.90 o 2 11 0 313.81 296.56 13.43 o 1 0 1 335.98 379.70 4.31 o 3 0 1 196.19 211.77 3.32 o 4 0 1 2783.66 2998.06 31.73 o 5 0 1 424.40 421.63 11.09 o 6 0 1 2716.40 2605.83 44.55 o 7 0 1 1.80 4.54 2.10 o 8 0 1 19.79 27.08 4.16 o 9 0 1 1616.42 1620.75 34.47 o 10 0 1 350.05 372.51 14.52 o -10 1 1 48.51 45.35 6.02 o -9 1 1 400.66 409.48 14.52 o -8 1 1 55.66 71.48 5.72 o -7 1 1 62.00 67.56 4.95 o -6 1 1 2311.14 2347.67 40.27 o -5 1 1 1596.35 1511.13 27.99 o -3 1 1 675.88 728.47 8.80 o -2 1 1 3799.34 3660.43 54.41 o -1 1 1 668.20 664.07 7.55 o 0 1 1 45.09 44.09 1.19 o 1 1 1 638.31 624.71 8.50 o 2 1 1 3792.46 3747.90 77.70 o 3 1 1 665.44 695.91 10.66 o 5 1 1 1615.89 1572.98 21.93 o 6 1 1 2271.43 2225.65 39.83 o 7 1 1 62.47 58.26 4.79 o 8 1 1 52.77 58.17 5.20 o 9 1 1 399.97 409.94 14.51 o 10 1 1 49.94 45.99 5.92 o -10 2 1 329.40 341.95 19.69 o -9 2 1 42.39 52.96 6.06 o -8 2 1 367.10 370.03 12.86 o -7 2 1 60.30 66.87 5.04 o -6 2 1 766.34 728.73 17.26 o -5 2 1 1012.07 932.22 14.99 o -4 2 1 724.99 753.82 9.69 o -3 2 1 1123.20 1322.63 15.44 o -2 2 1 3117.18 3018.33 36.92 o -1 2 1 4232.98 4238.57 49.92 o 2 2 1 3207.46 3145.71 38.21 o 3 2 1 1163.10 1340.67 15.34 o 4 2 1 711.17 712.09 11.98 o 5 2 1 1015.46 936.00 15.11 o 6 2 1 776.19 735.57 17.24 o 7 2 1 64.29 61.84 4.88 o 8 2 1 367.41 339.81 14.69 o 9 2 1 43.07 44.89 5.58 o 10 2 1 321.63 340.19 19.22 o -10 3 1 19.20 17.21 4.98 o -9 3 1 59.68 58.24 6.38 o -8 3 1 207.18 193.79 9.32 o -7 3 1 533.81 515.25 15.09 o -6 3 1 564.73 550.23 14.77 o -5 3 1 1204.63 1204.91 18.52 o -4 3 1 3686.80 3792.83 40.75 o -3 3 1 831.84 870.45 14.94 o -2 3 1 2904.87 3129.56 30.08 o -1 3 1 2793.88 3087.39 52.28 o 0 3 1 169.01 173.34 2.74 o 1 3 1 2771.19 3093.45 95.62 o 2 3 1 2922.00 3141.46 39.10 o 3 3 1 832.55 839.02 10.06 o 4 3 1 3684.48 3769.21 40.63 o 5 3 1 1171.92 1119.64 18.22 o 6 3 1 556.51 572.33 17.08 o 7 3 1 541.38 547.02 15.34 o 8 3 1 209.38 204.76 9.92 o 9 3 1 60.84 67.92 6.32 o -9 4 1 123.72 122.34 8.06 o -8 4 1 28.16 40.27 5.13 o -7 4 1 15.67 19.96 3.62 o -6 4 1 101.83 95.62 5.84 o -5 4 1 3806.60 3765.36 48.94 o -4 4 1 395.10 395.88 7.94 o -3 4 1 2544.97 2458.50 27.84 o -2 4 1 2991.23 3060.42 30.13 o -1 4 1 3877.40 4097.90 39.31 o 0 4 1 698.15 555.11 6.68 o 1 4 1 3875.74 4081.39 39.44 o 2 4 1 2998.14 3098.20 39.55 o 3 4 1 2526.10 2394.52 27.61 o 4 4 1 395.90 412.40 8.91 o 5 4 1 3788.98 3671.08 48.63 o 6 4 1 104.25 100.73 5.80 o 7 4 1 12.93 15.56 3.16 o 8 4 1 29.12 41.65 5.21 o 9 4 1 126.69 144.12 12.71 o -8 5 1 256.95 260.07 11.33 o -7 5 1 235.72 275.38 10.94 o -6 5 1 411.05 421.47 13.19 o -5 5 1 31.98 36.45 3.35 o -4 5 1 1908.16 1935.52 34.27 o -3 5 1 2310.64 2285.87 27.02 o -2 5 1 630.32 592.71 7.73 o -1 5 1 435.90 440.74 13.47 o 0 5 1 3.89 6.41 0.87 o 1 5 1 432.00 434.74 10.32 o 2 5 1 647.56 608.20 12.26 o 3 5 1 2322.01 2276.18 27.05 o 4 5 1 1898.76 1889.77 24.09 o 5 5 1 29.54 29.07 2.96 o 6 5 1 420.76 419.95 10.48 o 7 5 1 237.62 228.41 9.90 o 8 5 1 255.72 274.71 17.22 o 9 5 1 359.61 369.42 21.27 o -8 6 1 76.34 73.13 10.80 o -7 6 1 19.04 24.53 6.86 o -6 6 1 11.23 22.01 4.20 o -5 6 1 2185.48 2183.49 32.34 o -4 6 1 36.79 45.56 4.62 o -3 6 1 5670.80 5732.22 61.90 o -2 6 1 1382.60 1332.84 16.17 o -1 6 1 369.59 386.04 5.59 o 0 6 1 62.86 64.15 2.29 o 1 6 1 345.97 362.87 6.48 o 2 6 1 1394.30 1351.51 21.08 o 3 6 1 5707.95 5690.32 61.99 o 4 6 1 34.66 43.10 3.51 o 5 6 1 2160.91 2111.71 31.98 o 6 6 1 9.19 12.58 3.24 o 7 6 1 17.74 25.44 6.56 o 8 6 1 75.98 79.62 10.19 o -7 7 1 122.70 154.83 13.62 o -6 7 1 595.32 621.38 26.38 o -5 7 1 59.94 64.52 5.20 o -4 7 1 50.08 46.65 4.53 o -3 7 1 413.20 394.07 8.46 o -2 7 1 410.87 416.96 7.61 o -1 7 1 1289.11 1288.31 14.82 o 0 7 1 13.73 15.93 1.91 o 1 7 1 1303.43 1293.20 18.12 o 2 7 1 407.40 414.66 8.62 o 3 7 1 420.08 404.86 8.56 o 4 7 1 54.31 53.50 3.88 o 5 7 1 63.14 64.10 5.61 o 6 7 1 583.92 594.83 14.47 o 7 7 1 121.40 143.75 13.06 o -7 8 1 158.34 170.11 14.67 o -6 8 1 39.60 52.56 9.22 o -5 8 1 414.37 428.04 21.21 o -3 8 1 2041.31 2035.35 30.70 o -2 8 1 250.44 247.40 7.98 o -1 8 1 92.78 94.50 4.69 o 0 8 1 19.88 28.46 3.36 o 1 8 1 92.84 94.94 4.71 o 2 8 1 257.26 264.86 7.07 o 3 8 1 2053.97 2032.42 31.72 o 4 8 1 29.95 31.36 4.57 o 5 8 1 408.30 408.03 11.93 o 6 8 1 39.99 41.47 5.67 o 7 8 1 158.16 143.25 13.08 o -6 9 1 95.03 103.28 8.09 o -5 9 1 371.76 398.71 21.26 o -3 9 1 48.75 48.45 5.29 o -2 9 1 300.65 300.97 11.33 o -1 9 1 304.55 313.99 9.58 o 0 9 1 157.17 155.14 6.38 o 1 9 1 307.31 323.84 8.79 o 2 9 1 297.05 298.77 8.51 o 3 9 1 49.56 55.02 5.04 o 4 9 1 228.19 233.47 9.15 o 5 9 1 363.23 364.82 14.27 o 6 9 1 94.98 99.69 7.97 o -5 10 1 411.94 411.21 16.21 o -4 10 1 138.43 149.58 14.08 o -3 10 1 745.76 741.66 21.50 o -2 10 1 439.79 449.69 15.98 o -1 10 1 8.75 14.14 3.76 o 0 10 1 237.96 239.67 11.60 o 1 10 1 10.01 13.15 2.81 o 2 10 1 440.15 428.20 12.46 o 3 10 1 760.03 766.44 21.84 o 4 10 1 141.77 140.74 8.89 o 5 10 1 414.68 429.77 16.33 o -2 11 1 232.52 237.06 11.96 o -1 11 1 165.61 177.36 27.63 o 0 11 1 9.79 12.77 4.06 o 1 11 1 166.58 176.18 10.75 o 2 11 1 230.10 239.41 11.93 o 1 0 2 234.76 246.97 3.54 o 3 0 2 2178.04 2637.75 27.70 o 4 0 2 104.85 113.54 3.26 o 5 0 2 5594.57 5722.92 87.04 o 6 0 2 1537.60 1431.15 27.55 o 7 0 2 46.13 68.22 7.47 o 8 0 2 773.82 747.69 19.49 o 9 0 2 38.69 46.07 5.89 o 10 0 2 121.40 132.09 8.51 o -10 1 2 41.80 46.11 6.05 o -9 1 2 295.88 295.80 12.17 o -8 1 2 648.31 628.26 25.19 o -7 1 2 14.58 23.56 3.55 o -6 1 2 1348.30 1309.41 26.19 o -5 1 2 1146.87 1147.76 22.02 o -4 1 2 1327.19 1496.28 20.21 o -3 1 2 3159.57 3237.58 34.09 o -2 1 2 829.50 831.25 9.17 o -1 1 2 312.75 326.32 4.24 o 0 1 2 489.47 498.08 6.57 o 1 1 2 300.78 318.07 5.88 o 2 1 2 811.01 816.86 10.70 o 3 1 2 3179.37 3282.34 40.09 o 4 1 2 1306.25 1509.47 17.51 o 5 1 2 1132.68 1113.45 14.05 o 6 1 2 1345.67 1354.78 26.20 o 7 1 2 14.87 14.40 4.38 o 8 1 2 657.76 651.81 17.76 o 9 1 2 297.54 296.26 16.94 o 10 1 2 38.73 44.13 8.54 o -10 2 2 645.26 632.67 28.04 o -9 2 2 442.11 448.27 15.48 o -8 2 2 139.28 140.16 7.89 o -7 2 2 423.02 431.22 13.26 o -6 2 2 720.34 695.56 16.77 o -5 2 2 514.95 541.52 13.83 o -4 2 2 236.04 268.09 4.60 o -3 2 2 462.88 432.49 7.12 o -2 2 2 2690.58 2872.34 47.58 o 0 2 2 4193.00 4126.94 84.56 o 2 2 2 2650.55 2797.56 30.18 o 3 2 2 447.61 439.43 6.73 o 4 2 2 233.58 241.33 5.83 o 5 2 2 521.27 539.57 10.27 o 6 2 2 708.07 689.24 16.51 o 7 2 2 421.90 428.43 13.08 o 8 2 2 142.23 146.56 7.91 o 9 2 2 447.27 454.00 15.34 o 10 2 2 637.38 712.75 29.30 o -10 3 2 33.98 37.50 7.18 o -9 3 2 261.01 288.00 12.23 o -8 3 2 369.00 369.95 13.29 o -7 3 2 400.80 390.00 12.69 o -6 3 2 136.84 120.82 6.44 o -5 3 2 755.74 747.79 13.31 o -4 3 2 698.47 644.21 9.50 o -3 3 2 92.93 98.73 3.14 o -2 3 2 1712.05 1795.74 18.10 o -1 3 2 3.41 5.80 0.77 o 0 3 2 1.21 5.19 1.50 o 1 3 2 6.75 9.57 1.17 o 2 3 2 1676.94 1744.24 23.46 o 3 3 2 93.95 102.17 2.53 o 4 3 2 718.52 701.35 11.89 o 5 3 2 749.10 740.32 13.27 o 6 3 2 142.06 139.36 6.60 o 7 3 2 399.14 378.02 12.39 o 8 3 2 362.20 379.57 13.22 o 9 3 2 258.40 266.58 11.68 o -9 4 2 81.57 98.12 7.29 o -8 4 2 93.33 96.06 6.77 o -7 4 2 507.67 523.52 15.44 o -6 4 2 63.50 58.54 4.64 o -5 4 2 269.98 236.42 6.91 o -4 4 2 2550.92 2541.71 33.49 o -3 4 2 2082.94 2041.75 27.27 o -2 4 2 2065.61 2189.35 22.75 o -1 4 2 216.46 236.34 7.30 o 0 4 2 777.44 683.59 27.45 o 1 4 2 207.89 225.10 8.40 o 2 4 2 2054.49 2163.72 29.05 o 3 4 2 2056.48 2013.62 23.68 o 4 4 2 2564.28 2579.96 30.23 o 5 4 2 261.10 218.93 6.57 o 6 4 2 66.70 67.02 4.14 o 7 4 2 512.98 489.03 14.72 o 8 4 2 94.29 90.40 6.44 o 9 4 2 77.01 87.65 10.61 o -8 5 2 14.04 15.98 3.50 o -7 5 2 654.38 653.45 18.31 o -6 5 2 943.93 973.20 22.40 o -5 5 2 39.85 47.62 4.44 o -4 5 2 1924.13 1818.47 26.07 o -3 5 2 1123.54 1148.41 15.56 o -2 5 2 180.96 160.40 4.56 o -1 5 2 535.67 546.95 15.36 o 0 5 2 217.93 220.30 4.24 o 1 5 2 537.74 547.90 14.77 o 2 5 2 182.75 167.34 9.32 o 3 5 2 1131.15 1142.97 15.55 o 4 5 2 1943.38 1871.29 25.49 o 5 5 2 43.67 45.26 3.30 o 6 5 2 946.23 957.84 15.23 o 7 5 2 655.41 649.04 26.40 o 8 5 2 14.23 14.72 5.62 o -8 6 2 45.89 60.46 10.07 o -7 6 2 568.38 592.69 29.12 o -6 6 2 153.41 157.30 8.06 o -5 6 2 308.93 317.52 12.35 o -4 6 2 1171.12 1188.00 24.27 o -3 6 2 71.26 88.63 10.47 o -2 6 2 3867.61 3950.05 36.28 o -1 6 2 53.80 68.84 3.40 o 0 6 2 36.12 20.57 2.20 o 1 6 2 55.85 67.45 2.88 o 2 6 2 3854.80 3956.58 51.62 o 3 6 2 69.90 83.28 6.41 o 4 6 2 1165.98 1142.10 17.01 o 5 6 2 299.88 311.63 8.82 o 6 6 2 150.04 157.93 6.64 o 7 6 2 580.19 588.44 25.61 o 8 6 2 48.10 52.59 9.27 o -7 7 2 106.07 118.97 12.20 o -6 7 2 629.79 730.75 64.13 o -5 7 2 294.65 281.04 10.83 o -4 7 2 238.37 223.60 12.38 o -3 7 2 130.04 125.23 5.12 o -2 7 2 159.97 164.69 4.49 o -1 7 2 1583.94 1582.68 21.44 o 0 7 2 40.85 41.05 2.52 o 1 7 2 1561.23 1556.16 21.13 o 2 7 2 162.51 173.55 6.45 o 3 7 2 133.16 131.74 4.67 o 4 7 2 235.47 242.15 8.21 o 5 7 2 300.58 301.14 9.45 o 6 7 2 630.90 637.94 18.53 o 7 7 2 106.22 106.29 11.11 o -7 8 2 201.82 210.70 16.24 o -6 8 2 32.75 45.02 8.50 o -5 8 2 74.20 78.90 9.48 o -4 8 2 294.43 296.27 15.02 o -3 8 2 214.81 217.54 11.96 o -2 8 2 380.93 362.78 9.53 o -1 8 2 61.70 67.99 5.16 o 0 8 2 97.31 95.31 7.03 o 1 8 2 65.27 65.96 3.61 o 2 8 2 367.42 338.42 8.63 o 3 8 2 216.49 225.70 7.67 o 4 8 2 290.18 291.91 8.30 o 5 8 2 76.50 87.95 5.57 o 6 8 2 31.22 33.45 4.35 o 7 8 2 200.69 211.95 15.78 o -6 9 2 313.65 295.54 18.76 o -5 9 2 91.02 86.16 10.46 o -3 9 2 144.85 145.77 7.71 o -2 9 2 173.96 176.88 6.79 o -1 9 2 690.82 692.59 18.64 o 0 9 2 27.59 26.56 3.34 o 1 9 2 693.30 680.81 13.56 o 2 9 2 167.26 167.53 6.34 o 3 9 2 143.12 142.54 6.98 o 4 9 2 9.67 7.55 2.27 o 5 9 2 92.94 98.82 6.27 o 6 9 2 316.07 333.95 13.95 o -5 10 2 101.80 109.35 8.74 o -2 10 2 203.73 242.05 15.39 o -1 10 2 1.53 0.43 3.39 o 0 10 2 143.05 161.80 11.93 o 1 10 2 1.62 3.80 2.13 o 2 10 2 205.50 213.85 8.70 o 3 10 2 5.22 14.25 3.81 o 4 10 2 53.77 59.86 6.90 o 5 10 2 102.58 110.41 8.39 o -2 11 2 66.99 73.39 10.49 o -1 11 2 161.91 168.91 10.42 o 0 11 2 1.81 4.20 3.19 o 1 11 2 162.84 162.42 12.04 o 2 11 2 65.43 68.07 7.67 o 3 11 2 146.16 164.23 13.07 o 1 0 3 1591.59 1707.13 20.60 o 2 0 3 1967.01 1941.60 23.99 o 3 0 3 531.50 680.28 8.32 o 4 0 3 570.78 664.97 10.56 o 5 0 3 1163.04 1160.92 17.16 o 6 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29 209.63 235.99 10.78 o 4 1 29 581.01 617.81 27.56 o 5 1 29 503.13 510.92 25.10 o -5 2 29 25.61 35.85 5.42 o -4 2 29 40.23 48.99 8.51 o -3 2 29 151.91 163.27 13.16 o -2 2 29 483.80 475.57 13.09 o -1 2 29 48.32 46.32 4.60 o 0 2 29 76.20 90.96 5.47 o 1 2 29 47.54 50.50 4.75 o 2 2 29 486.83 496.86 13.36 o 3 2 29 161.47 180.59 7.81 o 4 2 29 39.04 35.30 5.41 o -4 3 29 121.87 139.33 11.62 o -3 3 29 260.41 266.27 9.83 o -2 3 29 223.56 219.47 8.73 o -1 3 29 3.52 5.46 2.66 o 0 3 29 1.45 3.27 2.08 o 1 3 29 4.22 12.75 2.69 o 2 3 29 219.87 214.46 8.71 o 3 3 29 255.76 263.64 9.75 o 4 3 29 120.58 116.53 8.50 o -4 4 29 132.64 135.02 12.63 o -3 4 29 124.46 147.73 7.41 o -2 4 29 525.34 542.02 12.56 o -1 4 29 0.90 4.09 1.90 o 0 4 29 42.22 43.61 4.79 o 1 4 29 0.80 3.46 2.08 o 2 4 29 526.33 545.82 14.79 o 3 4 29 123.73 137.02 7.20 o -2 5 29 1.90 5.31 2.30 o -1 5 29 12.58 14.55 2.74 o 0 5 29 81.65 85.00 4.99 o 1 5 29 13.39 17.23 3.35 o 2 5 29 1.67 3.41 2.93 o 3 5 29 170.86 154.50 12.55 o -1 6 29 84.15 80.98 10.31 o 0 6 29 44.14 68.04 10.64 o 1 6 29 86.12 96.65 11.10 o 0 0 30 2559.69 2671.37 71.27 o 1 0 30 241.07 301.72 12.55 o 2 0 30 337.19 361.21 13.74 o 3 0 30 113.13 122.82 8.01 o 4 0 30 4.32 6.28 4.40 o -4 1 30 4.48 6.38 4.18 o -3 1 30 344.71 364.14 20.31 o -2 1 30 409.89 410.64 14.76 o -1 1 30 64.50 75.85 6.52 o 0 1 30 71.84 81.13 14.05 o 1 1 30 63.93 79.69 6.56 o 2 1 30 412.65 413.62 14.90 o 3 1 30 345.80 350.78 13.53 o 4 1 30 3.73 6.78 4.59 o -4 2 30 42.27 49.96 8.93 o -3 2 30 3.32 9.61 4.83 o -2 2 30 762.20 818.33 18.32 o -1 2 30 372.14 393.56 11.86 o 0 2 30 470.92 448.92 12.78 o 1 2 30 366.53 370.50 11.49 o 2 2 30 755.79 798.36 18.16 o 3 2 30 4.52 11.76 2.76 o -4 3 30 278.96 266.77 17.25 o -3 3 30 134.13 125.15 11.57 o -2 3 30 2.50 7.73 2.45 o -1 3 30 666.11 719.36 18.10 o 0 3 30 51.65 55.77 6.55 o 1 3 30 668.48 706.52 17.10 o 2 3 30 2.75 8.83 2.57 o 3 3 30 133.07 143.20 7.23 o 4 3 30 284.21 275.21 18.37 o -3 4 30 2.16 3.94 3.78 o -2 4 30 392.78 418.32 12.63 o -1 4 30 574.60 597.58 15.67 o 0 4 30 5.77 4.97 2.23 o 1 4 30 580.87 604.86 15.89 o 2 4 30 396.08 412.64 14.02 o 3 4 30 2.31 2.69 2.22 o -2 5 30 411.97 425.13 22.92 o -1 5 30 467.69 473.16 17.19 o 0 5 30 118.87 115.48 12.17 o 1 0 31 2340.18 2559.84 49.26 o 2 0 31 371.71 406.79 15.05 o 3 0 31 62.27 80.18 9.88 o -3 1 31 738.71 805.26 32.50 o -2 1 31 601.27 669.42 34.19 o -1 1 31 10.72 12.67 3.82 o 0 1 31 0.36 7.25 3.05 o 1 1 31 11.09 19.46 6.70 o 2 1 31 593.43 643.10 19.64 o 3 1 31 735.71 812.22 22.45 o -3 2 31 183.01 180.10 14.31 o -2 2 31 132.71 136.74 7.05 o -1 2 31 324.47 381.97 11.90 o 0 2 31 69.89 124.44 6.71 o 1 2 31 328.55 407.37 28.46 o 2 2 31 138.07 139.65 8.72 o 3 2 31 180.43 176.76 13.12 o -2 3 31 410.95 424.96 12.91 o -1 3 31 32.17 40.08 4.58 o 0 3 31 116.91 128.56 6.99 o 1 3 31 33.46 40.12 4.64 o 2 3 31 412.36 427.69 13.02 o 3 3 31 123.24 136.30 11.74 o -1 4 31 141.39 152.12 9.57 o 0 4 31 258.91 240.12 12.18 o 1 4 31 143.97 152.81 9.35 o 2 4 31 392.74 402.76 22.96 o 0 0 32 659.59 654.54 28.39 o 1 0 32 1348.20 1477.46 33.55 o 2 0 32 771.08 715.56 21.08 o -2 1 32 88.42 99.18 7.61 o -1 1 32 106.67 102.84 19.70 o 0 1 32 80.07 81.56 7.45 o 1 1 32 108.46 109.59 13.56 o 2 1 32 89.09 118.07 16.01 o 3 1 32 316.57 221.35 15.02 o -2 2 32 89.14 95.83 10.35 o -1 2 32 523.00 569.06 18.54 o 0 2 32 1397.56 1421.95 55.92 o 1 2 32 535.11 579.28 18.74 o 2 2 32 85.82 82.65 9.58 o 3 2 32 8.55 13.03 5.01 o -2 3 32 434.00 405.93 22.93 o -1 3 32 252.57 245.92 12.02 o 0 3 32 443.84 437.90 23.92 o 1 3 32 253.36 230.62 15.82 o 2 3 32 429.41 415.87 22.73 o 1 0 33 55.83 92.10 10.32 o 2 0 33 170.30 179.32 13.89 o -2 1 33 26.30 24.95 6.54 o -1 1 33 31.91 47.23 8.71 o 0 1 33 22.72 28.84 8.22 o 1 1 33 30.82 46.10 8.54 o 2 1 33 27.86 32.75 7.13 o -2 2 33 91.49 78.81 9.66 o -1 2 33 38.90 51.35 8.94 o -1 3 33 21.40 33.88 7.20 o 0 3 33 34.17 34.20 7.40 o 1 3 33 18.25 15.56 4.91 o