#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/74/2237472.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237472_Fobs loop_ _publ_author_name 'Beginn, Uwe' 'Frosinn, Martin' 'Reichelt, Martin' 'Reuter, Hans' _publ_section_title ; 3-Methylideneoxolane-2,5-dione ; _journal_coeditor_code GG2110 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o321 _journal_volume 69 _journal_year 2013 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.4854 _cell_length_b 7.3498 _cell_length_c 12.1871 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file gg2110Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MF001_0m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4324.98 4523.49 22.30 o 4 0 0 0.23 0.43 0.62 o 6 0 0 252.19 243.56 5.55 o 1 1 0 1369.18 1345.10 5.06 o 2 1 0 668.96 623.19 2.54 o 3 1 0 93.43 91.28 0.84 o 4 1 0 122.96 124.69 1.52 o 5 1 0 59.73 59.89 1.23 o 6 1 0 0.35 0.02 1.18 o 7 1 0 10.34 9.48 2.56 o 0 2 0 7.61 9.71 0.43 o 1 2 0 730.28 660.97 2.87 o 2 2 0 54.91 61.34 0.74 o 3 2 0 731.28 720.48 3.32 o 4 2 0 0.33 0.10 0.47 o 5 2 0 119.23 113.58 1.87 o 6 2 0 9.24 10.47 1.49 o 7 2 0 18.42 22.82 3.17 o 1 3 0 160.68 162.44 1.32 o 2 3 0 59.08 67.08 0.87 o 3 3 0 78.17 79.28 1.01 o 4 3 0 176.88 178.35 1.75 o 5 3 0 10.45 8.14 1.03 o 6 3 0 37.94 41.71 2.17 o 0 4 0 10.59 11.65 0.72 o 1 4 0 326.04 310.11 2.02 o 2 4 0 19.05 18.88 0.67 o 3 4 0 178.19 180.13 1.66 o 4 4 0 25.87 26.35 1.14 o 5 4 0 11.60 9.22 1.42 o 6 4 0 63.38 77.09 4.01 o 1 5 0 15.76 16.21 0.71 o 2 5 0 0.05 0.43 0.55 o 3 5 0 135.61 131.34 2.00 o 4 5 0 0.20 0.95 1.00 o 5 5 0 35.80 29.10 2.16 o 6 5 0 5.36 5.80 6.39 o 0 6 0 127.72 128.55 2.49 o 1 6 0 210.18 206.43 2.34 o 2 6 0 52.51 50.90 1.48 o 3 6 0 47.84 53.27 1.87 o 4 6 0 1.62 0.24 1.41 o 5 6 0 12.51 14.77 3.61 o 1 7 0 15.22 20.35 2.30 o 2 7 0 7.27 10.09 1.51 o 3 7 0 45.78 53.07 2.69 o 4 7 0 6.17 9.10 2.95 o 5 7 0 0.97 1.73 4.60 o 0 8 0 5.78 3.95 2.18 o 1 8 0 251.41 253.41 4.49 o 2 8 0 93.83 97.30 3.30 o 3 8 0 0.44 1.85 2.40 o 4 8 0 84.02 82.35 6.49 o 2 9 0 23.71 22.95 5.38 o 1 0 1 564.20 547.04 2.21 o 2 0 1 9.49 15.85 0.37 o 3 0 1 94.17 100.06 0.89 o 4 0 1 17.47 21.69 0.64 o 5 0 1 27.53 30.31 1.03 o 6 0 1 26.94 26.20 1.64 o 7 0 1 7.06 5.99 2.82 o 0 1 1 1276.00 1256.81 4.52 o 1 1 1 1521.56 1503.65 4.02 o 2 1 1 713.80 724.77 2.06 o 3 1 1 619.92 622.08 1.96 o 4 1 1 9.25 8.88 0.39 o 5 1 1 43.76 41.17 0.81 o 6 1 1 22.98 22.15 1.19 o 7 1 1 6.95 7.67 1.64 o 0 2 1 49.47 42.48 0.52 o 1 2 1 2147.96 2184.25 5.92 o 2 2 1 106.37 114.16 0.66 o 3 2 1 54.58 55.15 0.54 o 4 2 1 83.10 76.29 0.75 o 5 2 1 50.75 48.34 0.91 o 6 2 1 34.01 29.96 1.28 o 7 2 1 63.84 70.57 3.41 o 0 3 1 68.39 73.85 0.85 o 1 3 1 45.16 48.05 0.51 o 2 3 1 73.89 75.49 0.63 o 3 3 1 35.60 34.98 0.56 o 4 3 1 155.00 153.45 1.10 o 5 3 1 6.78 6.57 0.73 o 6 3 1 9.73 9.55 1.16 o 0 4 1 1.07 1.41 0.42 o 1 4 1 88.62 94.65 0.74 o 2 4 1 67.83 69.69 0.70 o 3 4 1 12.16 12.74 0.47 o 4 4 1 119.15 122.57 1.36 o 5 4 1 13.31 13.37 1.03 o 6 4 1 39.90 37.83 2.00 o 0 5 1 455.09 459.94 2.95 o 1 5 1 69.22 70.18 0.76 o 2 5 1 73.63 72.24 0.83 o 3 5 1 179.64 177.10 1.60 o 4 5 1 18.25 18.31 1.02 o 5 5 1 77.78 83.13 1.96 o 6 5 1 37.54 42.25 3.81 o 0 6 1 36.16 41.56 1.31 o 1 6 1 27.55 29.76 0.73 o 2 6 1 67.99 68.32 1.20 o 3 6 1 24.27 23.68 1.07 o 4 6 1 3.88 1.69 1.09 o 5 6 1 1.56 0.40 1.77 o 0 7 1 30.11 32.37 1.60 o 1 7 1 130.63 126.23 1.85 o 2 7 1 82.79 81.20 1.75 o 3 7 1 1.30 2.70 1.14 o 4 7 1 61.50 71.10 3.45 o 5 7 1 24.59 25.58 3.13 o 0 8 1 109.84 114.43 2.96 o 1 8 1 9.19 8.91 1.18 o 2 8 1 21.24 22.98 1.60 o 3 8 1 4.74 2.80 1.88 o 4 8 1 13.15 14.49 2.61 o 1 9 1 14.37 12.36 9.71 o 2 9 1 4.14 0.10 3.13 o 0 0 2 152.13 137.69 1.01 o 1 0 2 834.33 780.68 4.28 o 2 0 2 696.70 682.27 3.15 o 3 0 2 7.91 8.41 0.39 o 4 0 2 495.07 474.09 2.66 o 5 0 2 139.61 136.16 1.88 o 6 0 2 43.19 43.23 1.85 o 7 0 2 0.41 0.84 1.87 o 0 1 2 1732.48 1683.62 5.85 o 1 1 2 542.17 505.21 1.59 o 2 1 2 130.84 132.44 0.74 o 3 1 2 303.60 306.52 1.25 o 4 1 2 103.35 102.41 0.82 o 5 1 2 77.00 76.88 1.04 o 6 1 2 11.91 9.94 0.97 o 7 1 2 21.97 22.07 1.70 o 0 2 2 2713.87 2846.88 10.23 o 1 2 2 3664.11 3863.44 10.10 o 2 2 2 265.84 263.72 1.09 o 3 2 2 94.28 87.11 0.71 o 4 2 2 33.28 33.79 0.55 o 5 2 2 4.55 4.96 0.59 o 6 2 2 15.36 15.07 1.13 o 7 2 2 17.55 20.08 1.98 o 0 3 2 557.57 572.66 3.28 o 1 3 2 438.60 435.62 1.56 o 2 3 2 932.98 959.84 3.13 o 3 3 2 71.39 67.78 0.67 o 4 3 2 67.32 67.66 0.91 o 5 3 2 108.87 100.80 1.55 o 6 3 2 12.28 14.42 1.22 o 0 4 2 0.00 -0.50 0.38 o 1 4 2 188.93 195.13 1.07 o 2 4 2 39.50 39.54 0.65 o 3 4 2 24.40 23.25 0.63 o 4 4 2 15.70 15.01 0.68 o 5 4 2 24.52 25.07 1.17 o 6 4 2 1.81 0.64 1.21 o 0 5 2 109.69 111.70 1.28 o 1 5 2 7.36 5.96 0.41 o 2 5 2 42.35 42.36 0.73 o 3 5 2 6.16 4.74 0.64 o 4 5 2 105.52 103.19 1.69 o 5 5 2 21.40 23.41 1.64 o 6 5 2 40.68 42.99 3.66 o 0 6 2 177.35 177.46 2.28 o 1 6 2 13.61 14.72 0.64 o 2 6 2 191.30 180.37 1.84 o 3 6 2 175.08 174.74 2.17 o 4 6 2 26.40 29.98 1.43 o 5 6 2 22.71 26.91 2.44 o 0 7 2 27.45 28.13 1.56 o 1 7 2 42.63 44.65 1.26 o 2 7 2 107.53 105.97 1.95 o 3 7 2 0.96 2.51 1.10 o 4 7 2 19.96 20.17 2.10 o 0 8 2 48.20 48.36 2.43 o 1 8 2 27.67 28.22 1.53 o 2 8 2 25.02 23.15 1.78 o 3 8 2 4.96 0.77 1.91 o 4 8 2 2.58 -0.98 2.09 o 0 9 2 95.51 81.58 10.72 o 1 9 2 53.38 46.28 4.86 o 2 9 2 53.66 59.94 5.97 o 1 0 3 580.06 592.49 3.63 o 2 0 3 267.75 288.54 2.93 o 3 0 3 15.59 19.61 0.46 o 4 0 3 15.07 14.08 0.57 o 5 0 3 10.86 10.04 0.84 o 6 0 3 13.97 15.51 1.24 o 7 0 3 0.65 1.64 1.48 o 0 1 3 574.28 529.34 2.16 o 1 1 3 318.13 308.58 1.12 o 2 1 3 78.80 67.61 0.49 o 3 1 3 169.65 166.45 0.93 o 4 1 3 48.22 45.92 0.59 o 5 1 3 4.43 5.18 0.56 o 6 1 3 102.40 104.47 1.62 o 7 1 3 7.82 7.08 1.36 o 0 2 3 52.44 51.37 0.76 o 1 2 3 479.80 510.67 1.69 o 2 2 3 81.63 82.77 0.61 o 3 2 3 316.00 317.14 1.63 o 4 2 3 50.44 51.39 0.74 o 5 2 3 262.68 256.05 1.98 o 6 2 3 65.34 70.24 1.57 o 0 3 3 232.60 230.90 1.40 o 1 3 3 398.78 403.13 1.48 o 2 3 3 394.05 401.40 1.60 o 3 3 3 77.92 75.95 0.76 o 4 3 3 1.88 2.31 0.46 o 5 3 3 26.72 27.76 0.93 o 6 3 3 0.24 -0.31 1.08 o 0 4 3 556.43 533.02 2.79 o 1 4 3 22.86 27.55 0.48 o 2 4 3 803.96 813.06 3.03 o 3 4 3 296.16 284.72 1.61 o 4 4 3 220.38 209.27 1.78 o 5 4 3 8.79 10.60 0.96 o 6 4 3 65.33 74.83 2.43 o 0 5 3 0.32 -0.02 0.47 o 1 5 3 176.21 181.77 1.19 o 2 5 3 125.84 126.92 1.15 o 3 5 3 39.46 39.14 0.91 o 4 5 3 39.28 41.26 1.27 o 5 5 3 17.86 21.36 1.32 o 6 5 3 31.28 29.94 2.45 o 0 6 3 40.99 43.57 1.40 o 1 6 3 11.38 12.53 0.70 o 2 6 3 0.52 1.45 0.66 o 3 6 3 61.63 62.99 1.43 o 4 6 3 4.33 5.21 1.09 o 5 6 3 38.64 37.23 2.60 o 0 7 3 96.82 101.81 2.46 o 1 7 3 17.94 19.94 1.15 o 2 7 3 13.50 15.66 1.16 o 3 7 3 10.43 9.27 1.25 o 4 7 3 6.24 5.09 1.67 o 0 8 3 26.15 27.70 2.20 o 1 8 3 3.00 2.72 1.16 o 2 8 3 16.48 18.29 1.80 o 3 8 3 13.33 10.14 2.22 o 0 9 3 0.34 -2.72 6.16 o 1 9 3 7.59 7.42 2.56 o 2 9 3 10.04 8.22 2.96 o 0 0 4 911.91 848.69 4.80 o 1 0 4 4.12 4.76 0.40 o 2 0 4 71.12 73.08 1.08 o 3 0 4 37.97 37.11 0.97 o 4 0 4 97.00 91.18 1.20 o 5 0 4 49.58 54.50 1.55 o 6 0 4 46.56 46.70 2.18 o 7 0 4 0.57 -2.90 3.99 o 0 1 4 28.02 30.33 0.60 o 1 1 4 329.54 333.51 1.33 o 2 1 4 439.51 434.95 1.81 o 3 1 4 28.46 27.82 0.45 o 4 1 4 68.63 68.51 0.76 o 5 1 4 12.88 15.06 0.79 o 6 1 4 1.38 2.68 1.03 o 0 2 4 126.81 126.19 0.91 o 1 2 4 219.56 235.21 1.01 o 2 2 4 433.17 445.11 1.67 o 3 2 4 2.71 1.98 0.30 o 4 2 4 201.32 206.85 1.28 o 5 2 4 65.67 63.73 1.03 o 6 2 4 25.34 28.36 1.42 o 0 3 4 202.80 226.68 1.40 o 1 3 4 43.50 42.87 0.46 o 2 3 4 76.99 81.64 0.70 o 3 3 4 279.02 287.38 1.52 o 4 3 4 163.85 153.27 1.32 o 5 3 4 121.15 128.18 1.58 o 6 3 4 2.52 1.88 0.88 o 0 4 4 391.50 397.48 2.26 o 1 4 4 792.67 794.15 2.73 o 2 4 4 230.91 226.84 1.25 o 3 4 4 187.11 186.34 1.40 o 4 4 4 37.49 33.85 0.87 o 5 4 4 55.52 55.57 1.29 o 6 4 4 13.49 18.23 1.95 o 0 5 4 7.24 9.10 0.59 o 1 5 4 247.78 246.35 1.44 o 2 5 4 37.69 37.48 0.70 o 3 5 4 33.20 31.14 0.86 o 4 5 4 20.57 21.24 1.05 o 5 5 4 4.19 2.05 1.04 o 0 6 4 42.79 43.65 1.25 o 1 6 4 46.47 45.44 0.95 o 2 6 4 121.36 121.75 1.59 o 3 6 4 90.93 86.10 1.61 o 4 6 4 4.15 2.10 1.01 o 5 6 4 40.96 44.56 2.11 o 0 7 4 0.19 -0.24 1.21 o 1 7 4 81.61 82.50 1.76 o 2 7 4 11.11 8.94 1.04 o 3 7 4 23.62 22.07 1.47 o 4 7 4 0.42 -0.66 1.61 o 0 8 4 0.60 2.30 1.62 o 1 8 4 11.84 8.99 1.28 o 2 8 4 64.68 62.29 2.98 o 3 8 4 11.77 10.02 2.77 o 0 9 4 7.44 9.81 3.01 o 1 9 4 65.50 63.84 4.08 o 2 9 4 37.16 38.81 3.87 o 1 0 5 358.34 361.59 2.20 o 2 0 5 0.00 -0.26 0.55 o 3 0 5 506.22 510.56 3.26 o 4 0 5 88.61 91.62 1.36 o 5 0 5 424.67 422.98 4.54 o 6 0 5 1.66 2.38 1.52 o 0 1 5 90.64 101.95 1.04 o 1 1 5 126.12 128.19 0.71 o 2 1 5 432.69 446.37 2.00 o 3 1 5 149.92 146.03 1.20 o 4 1 5 232.57 234.84 1.70 o 5 1 5 3.36 6.02 0.75 o 6 1 5 26.67 25.24 1.50 o 0 2 5 535.87 536.89 2.53 o 1 2 5 376.69 385.36 1.42 o 2 2 5 404.19 408.37 1.65 o 3 2 5 132.00 132.10 0.97 o 4 2 5 162.30 153.49 1.36 o 5 2 5 33.58 34.12 1.17 o 6 2 5 41.22 44.50 1.81 o 0 3 5 45.79 49.35 0.69 o 1 3 5 74.75 80.47 0.64 o 2 3 5 83.73 84.45 0.77 o 3 3 5 9.48 7.16 0.43 o 4 3 5 33.66 30.13 0.70 o 5 3 5 85.53 84.22 1.60 o 6 3 5 0.04 -0.53 1.28 o 0 4 5 0.44 1.47 0.46 o 1 4 5 110.30 113.62 0.88 o 2 4 5 400.66 390.93 1.96 o 3 4 5 29.03 27.25 0.71 o 4 4 5 134.32 126.92 1.45 o 5 4 5 11.64 13.14 0.87 o 6 4 5 61.17 63.96 2.64 o 0 5 5 6.29 6.00 0.62 o 1 5 5 11.59 11.96 0.52 o 2 5 5 52.59 53.88 0.86 o 3 5 5 194.78 185.31 1.77 o 4 5 5 13.51 14.99 0.95 o 5 5 5 28.24 28.10 1.60 o 0 6 5 33.45 33.42 1.37 o 1 6 5 53.12 54.07 1.11 o 2 6 5 66.80 68.34 1.28 o 3 6 5 108.38 103.94 1.84 o 4 6 5 45.99 44.63 1.61 o 5 6 5 51.62 53.47 2.73 o 0 7 5 202.58 198.26 3.91 o 1 7 5 21.03 21.57 1.26 o 2 7 5 30.34 30.03 1.39 o 3 7 5 26.02 27.15 1.63 o 4 7 5 66.56 66.36 3.87 o 0 8 5 1.03 1.85 1.68 o 1 8 5 53.60 55.04 2.20 o 2 8 5 1.75 2.61 2.15 o 3 8 5 19.04 21.30 3.14 o 0 9 5 0.15 -1.86 2.43 o 1 9 5 23.05 21.87 3.11 o 0 0 6 593.65 638.12 4.46 o 1 0 6 163.27 175.68 1.41 o 2 0 6 28.44 27.93 0.89 o 3 0 6 31.31 27.87 1.04 o 4 0 6 0.56 0.45 0.76 o 5 0 6 64.91 61.51 1.90 o 6 0 6 15.22 15.47 1.74 o 0 1 6 122.64 120.72 0.92 o 1 1 6 407.00 421.28 1.66 o 2 1 6 39.30 42.19 0.57 o 3 1 6 244.38 251.70 1.60 o 4 1 6 208.87 200.08 1.75 o 5 1 6 49.83 49.82 1.18 o 6 1 6 30.68 32.09 1.56 o 0 2 6 4.02 4.64 0.39 o 1 2 6 11.69 12.61 0.32 o 2 2 6 183.72 191.26 1.13 o 3 2 6 13.74 13.83 0.57 o 4 2 6 112.50 108.10 1.50 o 5 2 6 25.48 26.09 1.05 o 6 2 6 14.11 13.24 1.35 o 0 3 6 367.89 365.13 2.11 o 1 3 6 149.84 157.26 1.00 o 2 3 6 6.78 4.08 0.37 o 3 3 6 141.28 136.24 1.10 o 4 3 6 52.02 51.48 1.26 o 5 3 6 8.34 6.68 1.02 o 6 3 6 3.74 0.44 1.49 o 0 4 6 67.86 70.68 0.99 o 1 4 6 4.41 4.52 0.37 o 2 4 6 16.69 14.76 0.55 o 3 4 6 3.66 2.59 0.55 o 4 4 6 0.69 1.69 0.56 o 5 4 6 15.36 15.74 1.32 o 6 4 6 29.51 32.30 3.85 o 0 5 6 242.62 241.43 2.29 o 1 5 6 32.41 32.45 0.75 o 2 5 6 108.22 107.10 1.32 o 3 5 6 156.79 154.60 1.69 o 4 5 6 3.89 4.63 0.76 o 5 5 6 85.28 89.29 2.03 o 0 6 6 80.21 84.64 2.08 o 1 6 6 116.75 114.21 1.61 o 2 6 6 37.94 39.08 1.17 o 3 6 6 181.67 165.91 2.46 o 4 6 6 17.21 17.29 1.50 o 5 6 6 3.49 5.21 1.81 o 0 7 6 2.90 3.34 1.51 o 1 7 6 123.53 125.28 2.37 o 2 7 6 39.65 40.43 1.80 o 3 7 6 47.20 48.68 2.37 o 4 7 6 71.53 66.06 3.47 o 0 8 6 0.15 -0.90 1.96 o 1 8 6 26.27 28.39 2.04 o 2 8 6 10.25 11.26 2.71 o 3 8 6 13.30 11.04 2.76 o 0 9 6 39.05 39.24 4.48 o 1 0 7 922.74 946.71 4.90 o 2 0 7 80.44 72.13 1.38 o 3 0 7 875.64 859.15 7.64 o 4 0 7 0.23 0.63 1.30 o 5 0 7 233.26 229.07 3.30 o 6 0 7 0.05 -0.87 1.53 o 0 1 7 1.60 1.28 0.36 o 1 1 7 39.60 40.10 0.57 o 2 1 7 137.96 144.03 1.06 o 3 1 7 94.76 88.85 1.31 o 4 1 7 40.05 40.80 1.18 o 5 1 7 23.21 23.58 0.98 o 6 1 7 29.50 28.04 1.71 o 0 2 7 16.09 17.51 0.87 o 1 2 7 205.28 205.36 1.04 o 2 2 7 215.59 218.06 1.25 o 3 2 7 124.18 119.08 1.20 o 4 2 7 403.27 402.39 3.09 o 5 2 7 7.55 5.40 0.82 o 6 2 7 100.38 110.26 2.96 o 0 3 7 60.82 55.13 0.91 o 1 3 7 29.43 30.94 0.51 o 2 3 7 27.78 26.52 0.51 o 3 3 7 48.60 44.51 0.96 o 4 3 7 47.84 50.26 1.14 o 5 3 7 20.93 21.81 1.27 o 6 3 7 8.29 5.91 2.15 o 0 4 7 31.20 34.65 0.83 o 1 4 7 5.95 6.61 0.45 o 2 4 7 66.34 65.29 0.93 o 3 4 7 73.78 79.91 1.13 o 4 4 7 25.41 23.86 1.06 o 5 4 7 5.87 6.65 1.29 o 0 5 7 170.56 159.78 2.13 o 1 5 7 5.12 5.00 0.59 o 2 5 7 18.47 16.73 0.78 o 3 5 7 12.83 14.66 0.82 o 4 5 7 16.66 15.11 0.86 o 5 5 7 13.98 18.87 2.84 o 0 6 7 228.57 221.37 3.35 o 1 6 7 12.15 10.06 0.94 o 2 6 7 111.70 109.24 1.98 o 3 6 7 22.56 25.28 1.28 o 4 6 7 9.62 7.87 1.42 o 0 7 7 33.90 34.96 2.22 o 1 7 7 47.28 47.19 1.99 o 2 7 7 2.62 4.13 1.22 o 3 7 7 29.43 27.09 2.27 o 0 8 7 2.40 2.19 2.28 o 1 8 7 19.76 19.25 2.04 o 2 8 7 45.83 44.88 3.34 o 0 0 8 210.38 219.97 2.44 o 1 0 8 12.80 15.74 0.58 o 2 0 8 11.31 14.43 0.87 o 3 0 8 105.19 106.90 2.44 o 4 0 8 87.08 82.17 2.89 o 5 0 8 162.19 170.81 4.17 o 6 0 8 6.44 0.67 3.24 o 0 1 8 269.57 255.05 1.86 o 1 1 8 80.34 85.82 0.72 o 2 1 8 2.93 3.08 0.39 o 3 1 8 44.83 41.69 1.30 o 4 1 8 0.88 0.91 0.97 o 5 1 8 41.96 43.23 1.49 o 6 1 8 41.90 46.98 5.00 o 0 2 8 209.90 215.12 1.75 o 1 2 8 12.81 13.70 0.39 o 2 2 8 164.17 163.75 1.24 o 3 2 8 10.75 11.06 0.67 o 4 2 8 75.98 75.33 1.33 o 5 2 8 1.27 1.20 0.80 o 6 2 8 23.15 18.85 3.19 o 0 3 8 46.02 48.62 0.88 o 1 3 8 176.00 171.23 1.14 o 2 3 8 61.22 61.31 0.81 o 3 3 8 68.32 64.93 1.23 o 4 3 8 16.77 17.41 0.96 o 5 3 8 7.50 7.06 1.15 o 0 4 8 24.97 25.24 0.89 o 1 4 8 181.75 181.17 1.44 o 2 4 8 201.40 191.21 1.69 o 3 4 8 164.54 155.63 1.75 o 4 4 8 9.53 9.76 1.03 o 5 4 8 33.87 34.08 2.07 o 0 5 8 310.10 317.01 3.61 o 1 5 8 72.50 73.07 1.28 o 2 5 8 86.46 85.98 1.42 o 3 5 8 19.87 19.49 1.04 o 4 5 8 1.39 0.98 1.13 o 5 5 8 1.88 1.61 2.62 o 0 6 8 62.38 58.43 2.24 o 1 6 8 0.30 -0.06 0.88 o 2 6 8 10.53 8.44 1.08 o 3 6 8 23.39 22.78 1.49 o 4 6 8 11.24 10.43 1.30 o 0 7 8 5.17 5.83 1.78 o 1 7 8 6.57 9.41 1.47 o 2 7 8 3.89 5.34 1.34 o 3 7 8 37.23 31.35 2.18 o 0 8 8 7.76 10.29 3.13 o 1 8 8 26.72 29.83 2.58 o 1 0 9 0.02 -0.76 0.51 o 2 0 9 116.08 118.08 1.75 o 3 0 9 191.63 180.18 3.95 o 4 0 9 37.14 40.62 2.53 o 5 0 9 35.19 42.23 4.38 o 0 1 9 14.70 14.86 0.60 o 1 1 9 51.73 53.86 0.74 o 2 1 9 116.32 116.63 1.20 o 3 1 9 5.35 4.64 0.95 o 4 1 9 50.36 50.99 1.96 o 5 1 9 22.71 19.69 1.94 o 0 2 9 161.10 159.07 1.58 o 1 2 9 11.68 9.69 0.40 o 2 2 9 26.47 25.97 0.67 o 3 2 9 234.49 235.60 2.52 o 4 2 9 17.33 22.07 1.29 o 5 2 9 18.99 18.66 2.99 o 0 3 9 224.19 220.90 1.93 o 1 3 9 276.90 265.60 1.58 o 2 3 9 91.47 84.76 1.20 o 3 3 9 44.76 40.71 1.09 o 4 3 9 11.46 12.34 0.90 o 5 3 9 8.17 8.32 1.36 o 0 4 9 47.17 41.02 1.11 o 1 4 9 25.52 25.38 0.76 o 2 4 9 72.72 73.14 1.10 o 3 4 9 65.67 69.99 1.47 o 4 4 9 37.96 38.80 1.86 o 5 4 9 44.99 46.69 2.99 o 0 5 9 16.62 13.89 1.33 o 1 5 9 118.63 117.33 1.81 o 2 5 9 27.63 27.79 0.99 o 3 5 9 6.04 5.93 0.84 o 4 5 9 18.26 16.92 1.61 o 0 6 9 5.19 3.79 1.59 o 1 6 9 16.12 13.70 1.22 o 2 6 9 9.86 9.08 1.13 o 3 6 9 5.62 4.64 1.23 o 4 6 9 2.22 0.58 1.71 o 0 7 9 23.71 27.34 3.54 o 1 7 9 1.04 1.63 1.49 o 2 7 9 16.34 19.04 1.71 o 0 8 9 0.00 2.17 2.72 o 0 0 10 29.17 26.38 1.08 o 1 0 10 13.59 14.73 0.75 o 2 0 10 98.18 101.62 1.62 o 3 0 10 2.33 1.39 1.62 o 4 0 10 96.20 87.86 4.75 o 0 1 10 23.84 22.85 0.73 o 1 1 10 33.90 30.93 0.65 o 2 1 10 47.48 49.76 0.96 o 3 1 10 16.85 13.45 1.39 o 4 1 10 3.64 3.47 1.49 o 0 2 10 246.23 252.29 2.24 o 1 2 10 167.85 164.37 1.31 o 2 2 10 253.41 245.23 2.06 o 3 2 10 16.93 17.47 1.10 o 4 2 10 44.78 45.30 2.06 o 5 2 10 32.74 30.84 2.88 o 0 3 10 245.96 242.72 2.39 o 1 3 10 0.21 -0.11 0.47 o 2 3 10 264.61 246.54 2.23 o 3 3 10 5.65 5.18 0.80 o 4 3 10 0.13 0.55 0.80 o 5 3 10 6.86 3.61 2.75 o 0 4 10 70.88 72.41 1.75 o 1 4 10 265.00 253.84 2.20 o 2 4 10 6.87 4.95 0.73 o 3 4 10 11.64 9.85 1.03 o 4 4 10 1.20 0.55 1.06 o 0 5 10 0.01 0.86 1.16 o 1 5 10 57.33 59.46 1.44 o 2 5 10 11.21 12.44 0.83 o 3 5 10 9.24 7.04 1.21 o 4 5 10 9.85 8.65 1.87 o 0 6 10 25.98 28.24 2.28 o 1 6 10 46.15 44.20 1.66 o 2 6 10 24.02 24.96 1.40 o 3 6 10 48.40 48.87 1.80 o 0 7 10 37.95 37.04 3.94 o 1 7 10 26.61 27.06 2.35 o 2 7 10 10.00 7.19 1.72 o 1 0 11 77.76 78.04 1.58 o 2 0 11 35.59 38.67 1.41 o 3 0 11 2.50 2.41 1.85 o 4 0 11 42.72 46.42 3.91 o 0 1 11 19.08 17.74 0.82 o 1 1 11 241.49 229.09 1.89 o 2 1 11 3.48 4.22 0.65 o 3 1 11 38.68 36.27 2.05 o 4 1 11 0.70 1.59 1.70 o 0 2 11 59.04 57.72 1.31 o 1 2 11 112.35 109.59 1.37 o 2 2 11 66.01 63.41 1.19 o 3 2 11 39.60 41.75 1.70 o 4 2 11 15.68 13.07 1.97 o 5 2 11 12.54 12.35 3.32 o 0 3 11 4.34 5.67 0.88 o 1 3 11 0.10 -0.79 0.53 o 2 3 11 30.27 32.97 1.49 o 3 3 11 0.48 -0.01 0.76 o 4 3 11 1.59 1.30 1.11 o 0 4 11 25.70 29.53 1.55 o 1 4 11 90.74 93.86 1.47 o 2 4 11 32.55 29.79 1.22 o 3 4 11 6.35 4.94 1.10 o 4 4 11 33.60 32.74 2.28 o 0 5 11 55.89 54.99 2.71 o 1 5 11 3.51 3.66 0.98 o 2 5 11 65.66 66.15 1.68 o 3 5 11 4.16 2.29 1.15 o 0 6 11 10.41 7.87 1.92 o 1 6 11 6.23 6.24 1.26 o 2 6 11 36.29 34.42 1.97 o 0 7 11 9.03 3.65 2.55 o 0 0 12 694.59 699.76 7.42 o 1 0 12 65.11 65.51 2.17 o 2 0 12 273.84 267.27 5.86 o 3 0 12 54.29 47.56 3.27 o 4 0 12 4.57 7.43 3.29 o 0 1 12 43.22 42.96 1.24 o 1 1 12 82.83 83.98 1.41 o 2 1 12 55.53 56.06 1.37 o 3 1 12 68.31 66.86 2.57 o 4 1 12 3.60 2.29 2.13 o 0 2 12 31.65 31.66 1.16 o 1 2 12 97.62 93.93 1.60 o 2 2 12 49.28 53.47 1.28 o 3 2 12 45.90 50.31 1.84 o 4 2 12 23.14 26.82 3.25 o 0 3 12 4.49 2.03 1.04 o 1 3 12 29.47 31.35 1.02 o 2 3 12 0.08 0.85 1.02 o 3 3 12 7.15 7.26 1.02 o 4 3 12 20.27 18.35 2.06 o 0 4 12 29.73 32.30 1.74 o 1 4 12 65.16 65.98 1.46 o 2 4 12 2.36 2.46 1.42 o 3 4 12 16.11 19.43 2.10 o 0 5 12 0.21 0.71 1.32 o 1 5 12 38.77 42.64 1.69 o 2 5 12 39.08 38.46 2.11 o 3 5 12 35.66 35.36 3.12 o 0 6 12 166.29 159.76 6.84 o 1 6 12 52.19 51.79 2.39 o 1 0 13 6.97 3.86 1.21 o 2 0 13 40.14 41.46 1.96 o 3 0 13 55.90 58.01 5.57 o 4 0 13 1.78 0.04 3.87 o 0 1 13 236.11 239.30 3.56 o 1 1 13 37.29 40.59 1.39 o 2 1 13 44.71 44.01 1.19 o 3 1 13 18.71 19.79 2.99 o 4 1 13 11.96 11.12 3.69 o 0 2 13 2.22 1.36 0.86 o 1 2 13 18.35 20.15 1.25 o 2 2 13 5.34 6.89 1.08 o 3 2 13 2.35 2.98 1.47 o 4 2 13 8.00 8.19 1.84 o 0 3 13 3.57 1.59 1.12 o 1 3 13 19.56 20.69 1.16 o 2 3 13 17.39 21.12 1.66 o 3 3 13 9.89 10.17 1.74 o 0 4 13 2.38 1.05 1.28 o 1 4 13 10.85 12.35 0.95 o 2 4 13 8.78 8.87 1.58 o 3 4 13 56.77 57.27 3.05 o 0 5 13 1.73 1.87 1.54 o 1 5 13 32.45 33.30 1.76 o 2 5 13 18.32 14.45 3.30 o 0 0 14 56.52 55.63 2.22 o 1 0 14 13.96 17.78 1.65 o 2 0 14 110.07 111.72 3.17 o 3 0 14 30.29 31.48 6.35 o 0 1 14 14.02 14.50 1.15 o 1 1 14 25.91 25.93 1.29 o 2 1 14 8.22 6.75 1.12 o 3 1 14 18.60 18.53 3.57 o 0 2 14 36.58 35.26 1.65 o 1 2 14 155.70 162.98 3.36 o 2 2 14 10.25 13.20 1.69 o 3 2 14 26.21 25.27 2.97 o 0 3 14 53.00 55.96 2.40 o 1 3 14 34.72 37.20 1.68 o 2 3 14 48.21 54.05 2.60 o 0 4 14 9.56 10.72 1.76 o 1 4 14 31.09 30.46 1.95 o 1 0 15 1.67 -0.41 1.44 o 2 0 15 0.79 0.80 2.59 o 0 1 15 27.17 31.17 1.56 o 1 1 15 18.05 18.66 1.31 o 2 1 15 19.25 24.85 2.58 o 0 2 15 6.61 6.17 1.53 o 1 2 15 4.55 5.09 1.37 o 2 2 15 12.68 11.86 2.42 o 0 3 15 1.50 1.72 1.55 o 1 3 15 9.89 9.38 1.90 o 0 0 16 73.59 80.89 9.29 o 0 1 16 10.93 9.88 2.13 o