#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/74/2237486.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237486_Fobs loop_ _publ_author_name 'Sreenivasa, S.' 'ManojKumar, K.E.' 'Suchetan, P.A.' 'Palakshamurthy, B. S.' 'Gunasekaran, K.' _publ_section_title ; 2-Amino-5-fluorobenzoic acid ; _journal_coeditor_code HB7040 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o387 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.782 _cell_angle_gamma 90.000 _cell_length_a 4.9346 _cell_length_b 11.7542 _cell_length_c 11.9727 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file hb7040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hstp4 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 102.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 170.50 163.29 3.02 o 2 0 0 62.83 58.61 1.07 o 3 0 0 123.17 120.11 1.89 o 4 0 0 10.85 11.79 0.47 o 5 0 0 4.09 4.67 0.88 o 1 1 0 1645.12 1597.16 16.62 o 2 1 0 0.13 0.21 0.10 o 3 1 0 887.35 927.62 9.62 o 4 1 0 2.48 3.11 0.28 o 5 1 0 0.28 0.13 0.22 o 0 2 0 36.19 32.00 1.02 o 1 2 0 263.69 232.23 2.31 o 2 2 0 688.30 673.92 7.42 o 3 2 0 15.57 12.60 0.37 o 4 2 0 23.88 24.51 0.54 o 5 2 0 1.48 1.38 0.26 o 1 3 0 742.00 716.25 6.50 o 2 3 0 20.07 22.24 0.32 o 3 3 0 101.34 93.53 1.29 o 4 3 0 0.66 1.03 0.40 o 5 3 0 0.38 0.29 0.23 o 0 4 0 166.78 158.87 5.04 o 1 4 0 60.69 46.38 0.79 o 2 4 0 6.96 5.40 0.16 o 3 4 0 1.92 1.82 0.18 o 4 4 0 8.22 8.62 0.33 o 5 4 0 35.89 36.54 0.87 o 1 5 0 63.11 61.61 0.71 o 2 5 0 0.10 0.27 0.08 o 3 5 0 51.36 53.45 0.85 o 4 5 0 23.22 23.12 0.61 o 5 5 0 0.25 0.00 0.22 o 0 6 0 2.51 4.67 0.50 o 1 6 0 0.77 1.15 0.09 o 2 6 0 10.11 9.90 0.23 o 3 6 0 182.10 182.69 2.39 o 4 6 0 17.98 20.00 0.51 o 5 6 0 3.51 4.11 0.45 o 1 7 0 151.42 145.42 1.59 o 2 7 0 5.32 5.84 0.19 o 3 7 0 24.14 23.32 0.53 o 4 7 0 21.66 22.06 0.57 o 5 7 0 4.29 5.10 0.50 o 0 8 0 88.51 90.92 1.61 o 1 8 0 31.96 33.57 0.53 o 2 8 0 62.76 59.29 0.77 o 3 8 0 20.81 19.49 0.57 o 4 8 0 2.70 3.12 0.35 o 1 9 0 0.88 0.87 0.14 o 2 9 0 562.71 581.68 7.92 o 3 9 0 4.93 4.78 0.35 o 4 9 0 10.70 9.16 0.51 o 0 10 0 64.87 63.86 3.57 o 1 10 0 280.27 274.11 3.55 o 2 10 0 37.20 37.75 0.84 o 3 10 0 0.41 0.39 0.25 o 4 10 0 0.66 2.43 0.47 o 1 11 0 4.10 4.59 0.29 o 2 11 0 9.15 8.39 0.43 o 3 11 0 4.59 5.13 0.51 o 0 12 0 2.06 2.08 0.37 o 1 12 0 13.17 15.55 0.61 o 2 12 0 5.98 6.11 0.40 o 1 13 0 2.62 2.64 0.30 o 2 13 0 1.42 1.63 0.32 o -5 1 1 3.95 3.66 0.30 o -4 1 1 71.88 72.53 1.09 o -3 1 1 312.52 313.97 3.59 o -2 1 1 29.55 26.81 0.50 o -1 1 1 221.58 212.81 2.38 o 0 1 1 746.49 711.65 9.49 o 1 1 1 322.90 348.66 6.28 o 2 1 1 3006.87 3016.12 42.66 o 3 1 1 46.87 52.93 0.74 o 4 1 1 49.90 51.27 0.86 o 5 1 1 0.26 0.11 0.22 o -5 2 1 9.56 10.28 0.45 o -4 2 1 11.85 13.25 0.46 o -3 2 1 41.33 43.48 0.85 o -2 2 1 630.49 590.00 6.14 o -1 2 1 10414.92 8005.61 264.03 o 0 2 1 918.68 894.41 12.92 o 1 2 1 190.73 167.51 1.89 o 2 2 1 679.95 728.51 8.03 o 3 2 1 4.64 4.18 0.22 o 4 2 1 6.52 7.30 0.32 o 5 2 1 26.80 26.89 0.72 o -5 3 1 0.07 0.00 0.20 o -4 3 1 4.50 4.10 0.25 o -3 3 1 6.01 5.96 0.22 o -2 3 1 2.25 3.21 0.13 o -1 3 1 2298.63 2231.81 22.45 o 0 3 1 54.75 60.28 0.91 o 1 3 1 55.89 56.50 1.00 o 2 3 1 97.94 102.12 1.25 o 3 3 1 31.23 31.86 0.58 o 4 3 1 1.89 1.80 0.22 o 5 3 1 18.86 16.69 0.55 o -5 4 1 4.76 5.76 0.37 o -4 4 1 0.51 0.57 0.18 o -3 4 1 11.58 11.92 0.39 o -2 4 1 15.14 15.73 0.50 o -1 4 1 335.43 308.86 3.16 o 0 4 1 190.07 173.67 2.01 o 1 4 1 122.79 109.49 1.45 o 2 4 1 25.21 37.32 0.58 o 3 4 1 56.83 59.59 0.92 o 4 4 1 18.39 18.16 0.67 o 5 4 1 37.86 41.08 0.92 o -5 5 1 1.95 1.43 0.39 o -4 5 1 9.41 8.56 0.36 o -3 5 1 60.17 57.80 0.91 o -2 5 1 135.08 130.27 1.47 o -1 5 1 266.89 262.09 2.71 o 0 5 1 43.81 38.24 0.62 o 1 5 1 0.01 0.11 0.05 o 2 5 1 109.19 108.51 1.44 o 3 5 1 16.29 16.28 0.41 o 4 5 1 4.99 5.12 0.28 o 5 5 1 0.51 0.00 0.24 o -5 6 1 2.18 1.77 0.33 o -4 6 1 1.66 2.07 0.23 o -3 6 1 140.49 131.26 1.80 o -2 6 1 13.54 13.05 0.27 o -1 6 1 8.21 9.13 0.33 o 0 6 1 4.57 2.74 0.14 o 1 6 1 23.32 21.19 0.32 o 2 6 1 11.82 11.81 0.33 o 3 6 1 10.30 9.80 0.34 o 4 6 1 16.73 15.50 0.64 o 5 6 1 0.03 0.00 0.25 o -5 7 1 3.90 3.64 0.39 o -4 7 1 31.39 30.78 0.86 o -3 7 1 217.40 221.53 2.86 o -2 7 1 20.80 19.25 0.32 o -1 7 1 9.36 7.11 0.23 o 0 7 1 526.18 545.82 6.05 o 1 7 1 36.56 36.12 0.49 o 2 7 1 46.51 46.60 0.68 o 3 7 1 91.95 90.54 1.34 o 4 7 1 17.46 15.20 0.52 o -4 8 1 24.13 23.04 0.77 o -3 8 1 8.20 8.76 0.39 o -2 8 1 77.31 78.02 1.07 o -1 8 1 24.03 25.80 0.57 o 0 8 1 170.37 184.48 4.00 o 1 8 1 125.06 129.06 1.45 o 2 8 1 46.90 42.06 0.65 o 3 8 1 3.86 3.66 0.23 o 4 8 1 3.46 3.70 0.48 o -4 9 1 0.95 1.26 0.31 o -3 9 1 0.44 0.32 0.24 o -2 9 1 196.96 199.54 2.41 o -1 9 1 8.40 8.70 0.31 o 0 9 1 36.79 37.73 0.65 o 1 9 1 3.31 3.68 0.17 o 2 9 1 130.35 130.57 2.36 o 3 9 1 27.32 25.59 0.76 o 4 9 1 3.25 3.57 0.37 o -4 10 1 1.12 0.95 0.40 o -3 10 1 0.60 0.99 0.25 o -2 10 1 18.29 20.04 0.52 o -1 10 1 0.03 0.00 0.15 o 0 10 1 13.12 14.78 0.54 o 1 10 1 4.06 4.73 0.41 o 2 10 1 11.78 11.10 0.53 o 3 10 1 0.00 0.00 0.26 o 4 10 1 40.17 49.80 1.77 o -3 11 1 10.05 11.05 0.55 o -2 11 1 15.92 18.16 0.62 o -1 11 1 16.89 18.24 0.62 o 0 11 1 0.00 0.00 0.25 o 1 11 1 151.61 155.37 2.18 o 2 11 1 0.01 0.00 0.28 o 3 11 1 9.18 9.35 0.88 o -3 12 1 0.02 0.00 0.29 o -2 12 1 5.51 5.61 0.60 o -1 12 1 3.89 4.44 0.47 o 0 12 1 4.79 4.77 0.31 o 1 12 1 31.94 31.80 0.96 o 2 12 1 0.67 0.52 0.42 o -2 13 1 0.00 0.00 0.20 o -1 13 1 3.14 3.12 0.33 o 0 13 1 14.76 13.63 0.88 o 1 13 1 9.60 12.44 0.55 o 2 13 1 1.52 1.58 0.33 o -5 0 2 2.84 2.93 0.37 o -4 0 2 53.19 50.40 1.34 o -3 0 2 731.72 697.53 12.77 o -2 0 2 1154.56 1088.46 14.99 o -1 0 2 81.82 77.65 1.13 o 0 0 2 15.45 15.47 0.27 o 1 0 2 117.48 119.25 1.72 o 2 0 2 197.65 221.81 3.16 o 3 0 2 23.29 28.81 0.73 o 4 0 2 10.43 9.56 0.62 o 5 0 2 4.65 4.56 0.46 o -5 1 2 0.00 0.00 0.18 o -4 1 2 7.70 7.05 0.30 o -3 1 2 3.55 3.08 0.22 o -2 1 2 0.96 0.67 0.11 o -1 1 2 1637.57 1533.39 14.96 o 0 1 2 3548.62 3261.32 38.48 o 1 1 2 390.12 386.28 4.12 o 2 1 2 230.76 254.12 3.05 o 3 1 2 2.86 2.74 0.15 o 4 1 2 9.08 8.62 0.39 o 5 1 2 2.34 1.53 0.27 o -5 2 2 6.50 7.53 0.40 o -4 2 2 19.10 19.34 0.49 o -3 2 2 5.04 4.72 0.20 o -2 2 2 141.59 131.51 1.45 o -1 2 2 8901.72 7876.80 88.19 o 0 2 2 195.33 186.21 2.66 o 1 2 2 32.56 27.94 0.32 o 2 2 2 29.90 32.03 0.53 o 3 2 2 2.91 2.79 0.19 o 4 2 2 87.92 91.38 1.35 o 5 2 2 28.38 30.53 0.80 o -5 3 2 14.09 14.21 0.51 o -4 3 2 32.99 33.88 0.67 o -3 3 2 83.41 85.17 1.03 o -2 3 2 846.84 841.09 9.25 o -1 3 2 123.67 106.87 1.15 o 0 3 2 1.23 0.91 0.05 o 1 3 2 1394.11 1407.24 14.44 o 2 3 2 1122.85 1206.52 14.07 o 3 3 2 40.11 42.88 0.71 o 4 3 2 10.80 11.74 0.40 o 5 3 2 54.69 57.06 1.16 o -5 4 2 2.99 2.48 0.27 o -4 4 2 120.39 122.93 1.74 o -3 4 2 14.33 15.39 0.31 o -2 4 2 178.96 172.89 1.89 o -1 4 2 26.84 21.49 0.28 o 0 4 2 794.55 764.89 9.70 o 1 4 2 2469.67 2435.42 24.50 o 2 4 2 265.06 253.20 3.10 o 3 4 2 115.86 120.10 1.62 o 4 4 2 5.78 4.68 0.27 o 5 4 2 12.02 12.01 0.50 o -5 5 2 3.98 4.36 0.55 o -4 5 2 19.68 21.78 0.58 o -3 5 2 5.20 5.50 0.23 o -2 5 2 87.23 93.69 1.10 o -1 5 2 620.00 684.68 7.75 o 0 5 2 27.93 35.16 0.67 o 1 5 2 0.06 0.06 0.06 o 2 5 2 140.56 130.41 1.70 o 3 5 2 31.26 31.76 0.60 o 4 5 2 15.13 11.73 0.46 o 5 5 2 28.99 27.23 0.80 o -5 6 2 1.37 1.25 0.31 o -4 6 2 6.37 6.71 0.41 o -3 6 2 7.70 7.03 0.39 o -2 6 2 87.96 93.28 1.10 o -1 6 2 50.37 51.12 0.73 o 0 6 2 681.25 711.45 8.02 o 1 6 2 85.68 76.39 0.88 o 2 6 2 34.61 32.38 0.45 o 3 6 2 16.82 15.41 0.41 o 4 6 2 19.92 17.63 0.49 o 5 6 2 9.71 9.33 0.46 o -5 7 2 0.05 0.00 0.26 o -4 7 2 6.38 6.57 0.47 o -3 7 2 521.66 507.30 6.97 o -2 7 2 16.50 15.20 0.33 o -1 7 2 26.16 23.36 0.43 o 0 7 2 11.80 14.13 0.51 o 1 7 2 1.22 1.92 0.12 o 2 7 2 15.65 16.29 0.54 o 3 7 2 1.96 1.69 0.26 o 4 7 2 16.89 16.25 0.53 o -4 8 2 6.14 6.46 0.43 o -3 8 2 64.33 69.04 1.27 o -2 8 2 166.87 157.25 1.94 o -1 8 2 95.95 97.30 1.38 o 0 8 2 155.29 154.36 2.33 o 1 8 2 1.15 1.37 0.12 o 2 8 2 41.46 42.86 0.73 o 3 8 2 0.26 0.24 0.15 o 4 8 2 10.17 10.12 0.53 o -4 9 2 4.81 6.36 0.81 o -3 9 2 0.04 0.00 0.20 o -2 9 2 14.58 12.70 0.37 o -1 9 2 60.65 60.76 1.25 o 0 9 2 12.14 11.85 0.28 o 1 9 2 10.18 10.59 0.29 o 2 9 2 14.13 15.23 0.41 o 3 9 2 0.66 0.41 0.23 o 4 9 2 3.46 4.70 0.73 o -4 10 2 0.00 0.00 0.26 o -3 10 2 1.49 1.88 0.27 o -2 10 2 42.71 42.52 0.79 o -1 10 2 4.88 4.71 0.26 o 0 10 2 6.45 6.31 0.36 o 1 10 2 59.79 60.85 1.00 o 2 10 2 1.73 1.04 0.29 o 3 10 2 15.19 17.49 0.65 o -3 11 2 0.10 0.08 0.26 o -2 11 2 1.15 1.48 0.25 o -1 11 2 0.02 0.00 0.17 o 0 11 2 14.00 14.86 0.50 o 1 11 2 134.55 136.52 2.46 o 2 11 2 0.76 1.59 0.36 o 3 11 2 9.60 12.02 0.75 o -2 12 2 4.25 4.09 0.35 o -1 12 2 0.34 0.30 0.22 o 0 12 2 66.64 70.65 2.12 o 1 12 2 10.72 9.59 0.47 o 2 12 2 0.37 0.09 0.31 o -2 13 2 0.08 0.00 0.24 o -1 13 2 5.07 5.34 0.59 o 0 13 2 25.46 23.75 0.87 o 1 13 2 16.57 16.33 0.62 o -5 1 3 1.35 0.72 0.24 o -4 1 3 2.17 2.24 0.24 o -3 1 3 8.67 9.49 0.29 o -2 1 3 0.01 0.00 0.08 o -1 1 3 1647.32 1654.94 16.10 o 0 1 3 103.49 88.04 0.85 o 1 1 3 2916.78 2997.09 29.20 o 2 1 3 10.43 10.39 0.21 o 3 1 3 0.69 0.72 0.12 o 4 1 3 17.67 18.61 0.89 o 5 1 3 18.70 17.83 0.62 o -5 2 3 16.18 16.86 0.55 o -4 2 3 90.75 88.41 1.43 o -3 2 3 61.04 58.90 0.81 o -2 2 3 18.58 23.66 0.35 o -1 2 3 1575.78 1533.22 14.60 o 0 2 3 1531.65 1492.56 13.55 o 1 2 3 18.80 18.15 0.25 o 2 2 3 128.62 136.53 1.43 o 3 2 3 0.48 0.24 0.14 o 4 2 3 55.03 55.00 1.02 o 5 2 3 8.05 7.21 0.40 o -5 3 3 7.30 6.76 0.38 o -4 3 3 38.81 37.65 0.73 o -3 3 3 14.51 14.74 0.32 o -2 3 3 326.81 332.00 3.74 o -1 3 3 1059.04 1051.48 10.00 o 0 3 3 269.06 279.37 2.93 o 1 3 3 1227.69 1346.81 13.81 o 2 3 3 435.93 472.79 5.28 o 3 3 3 143.65 142.03 1.89 o 4 3 3 55.80 55.55 0.93 o 5 3 3 88.74 89.18 1.56 o -5 4 3 0.27 0.46 0.22 o -4 4 3 61.32 61.36 1.02 o -3 4 3 0.00 0.00 0.13 o -2 4 3 1450.45 1452.84 17.07 o -1 4 3 46.18 50.93 0.67 o 0 4 3 32.97 30.98 0.40 o 1 4 3 102.25 116.39 1.41 o 2 4 3 4.75 5.77 0.21 o 3 4 3 3.75 3.50 0.21 o 4 4 3 2.00 3.72 0.26 o 5 4 3 10.01 11.13 0.49 o -5 5 3 11.44 11.80 0.61 o -4 5 3 281.89 284.82 3.63 o -3 5 3 2.37 2.09 0.16 o -2 5 3 720.08 679.82 8.72 o -1 5 3 435.73 456.92 5.62 o 0 5 3 16.08 17.14 0.27 o 1 5 3 14.30 14.80 0.24 o 2 5 3 2.37 1.59 0.15 o 3 5 3 148.19 154.40 2.06 o 4 5 3 48.83 44.98 0.83 o 5 5 3 0.30 0.22 0.26 o -5 6 3 3.85 4.17 0.38 o -4 6 3 1.30 1.09 0.26 o -3 6 3 182.09 181.20 2.21 o -2 6 3 24.35 24.73 0.44 o -1 6 3 849.08 879.02 9.92 o 0 6 3 31.19 23.38 0.38 o 1 6 3 144.84 165.82 1.69 o 2 6 3 34.58 37.76 0.72 o 3 6 3 17.59 14.47 0.59 o 4 6 3 35.24 36.03 0.77 o -5 7 3 1.09 0.92 0.32 o -4 7 3 0.13 0.25 0.24 o -3 7 3 29.05 30.67 1.04 o -2 7 3 72.07 74.12 1.02 o -1 7 3 0.00 0.10 0.12 o 0 7 3 171.29 177.56 2.31 o 1 7 3 19.61 20.40 0.32 o 2 7 3 0.90 1.10 0.15 o 3 7 3 11.14 8.71 0.33 o 4 7 3 16.61 15.00 0.50 o -4 8 3 2.08 2.53 0.53 o -3 8 3 106.44 107.73 1.79 o -2 8 3 26.86 26.93 0.52 o -1 8 3 96.43 98.88 1.40 o 0 8 3 4.51 3.64 0.20 o 1 8 3 0.15 0.14 0.09 o 2 8 3 21.15 22.21 0.56 o 3 8 3 72.02 70.39 1.13 o 4 8 3 1.40 1.93 0.25 o -4 9 3 6.91 7.37 0.48 o -3 9 3 0.06 0.00 0.21 o -2 9 3 0.03 0.00 0.15 o -1 9 3 4.33 5.54 0.28 o 0 9 3 1.91 1.52 0.20 o 1 9 3 9.22 9.57 0.28 o 2 9 3 0.38 0.82 0.16 o 3 9 3 4.54 5.41 0.38 o 4 9 3 0.02 0.00 0.25 o -4 10 3 0.08 0.00 0.26 o -3 10 3 6.17 6.64 0.41 o -2 10 3 0.04 0.00 0.16 o -1 10 3 18.41 17.57 0.52 o 0 10 3 18.37 16.72 0.41 o 1 10 3 61.52 61.41 0.89 o 2 10 3 4.58 4.77 0.62 o 3 10 3 27.52 29.09 1.63 o -3 11 3 0.46 0.61 0.35 o -2 11 3 32.36 33.10 0.97 o -1 11 3 22.80 21.95 0.60 o 0 11 3 5.02 5.04 0.31 o 1 11 3 40.04 43.37 1.01 o 2 11 3 32.23 31.11 1.05 o 3 11 3 14.20 16.59 1.32 o -2 12 3 0.46 0.16 0.24 o -1 12 3 0.10 0.00 0.17 o 0 12 3 4.63 4.81 0.53 o 1 12 3 11.96 11.19 0.54 o 2 12 3 9.05 8.62 0.61 o -1 13 3 3.74 4.62 0.37 o 0 13 3 27.66 29.82 1.06 o 1 13 3 0.79 1.01 0.32 o -5 0 4 0.71 0.00 0.31 o -4 0 4 4.80 5.76 0.46 o -3 0 4 8.75 7.22 0.32 o -2 0 4 31.00 37.14 0.65 o -1 0 4 155.52 145.90 2.09 o 0 0 4 158.29 143.76 2.09 o 1 0 4 1660.33 1752.03 24.02 o 2 0 4 433.82 398.93 5.59 o 3 0 4 867.62 862.72 11.99 o 4 0 4 376.19 367.33 7.07 o 5 0 4 2.06 1.82 0.37 o -5 1 4 10.07 10.47 0.64 o -4 1 4 14.79 12.98 0.44 o -3 1 4 41.96 40.51 0.66 o -2 1 4 4.69 5.49 0.16 o -1 1 4 98.87 100.12 1.05 o 0 1 4 776.18 760.02 6.96 o 1 1 4 11.76 12.86 0.21 o 2 1 4 58.23 55.45 0.65 o 3 1 4 31.42 30.74 0.48 o 4 1 4 292.74 292.13 4.05 o 5 1 4 0.01 0.24 0.23 o -5 2 4 11.00 14.62 0.54 o -4 2 4 5.00 4.34 0.49 o -3 2 4 21.85 21.96 0.41 o -2 2 4 17.22 17.89 0.31 o -1 2 4 127.28 123.86 1.34 o 0 2 4 321.89 324.40 3.20 o 1 2 4 731.02 812.95 8.85 o 2 2 4 176.44 192.23 1.97 o 3 2 4 22.81 24.26 0.50 o 4 2 4 2.84 2.02 0.36 o 5 2 4 5.58 4.54 0.35 o -5 3 4 40.66 42.28 0.83 o -4 3 4 26.58 28.74 0.59 o -3 3 4 37.04 35.26 0.61 o -2 3 4 0.00 0.48 0.14 o -1 3 4 146.53 145.11 1.46 o 0 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