#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237501.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237501_Fobs loop_ _publ_author_name 'El-Agrody, Ahmed M.' 'Fouda, Ahmed M.' 'Al-Omar, Mohamed A.' 'Amr, Abd El-Galil E.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; Ethyl 2-amino-4-(4-bromophenyl)-6-methoxy-4H-benzo[h]chromene-3-carboxylate ; _journal_coeditor_code HG5295 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o435 _journal_page_last o436 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.628 _cell_angle_gamma 90.000 _cell_length_a 13.1543 _cell_length_b 16.8110 _cell_length_c 9.3672 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.7680 _[local]_cod_data_source_file hg5295Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 284.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1807.01 1727.20 59.65 o 3 0 0 2812.30 2727.40 65.34 o 4 0 0 1231.55 1206.51 42.14 o 5 0 0 1883.50 2014.54 60.85 o 6 0 0 378.77 437.92 30.62 o 7 0 0 364.58 406.80 31.33 o 8 0 0 5.51 17.14 8.45 o 9 0 0 658.23 692.16 54.15 o 10 0 0 1080.66 1314.09 58.95 o 11 0 0 47.79 86.23 14.64 o 12 0 0 2006.60 2383.15 94.11 o 13 0 0 281.32 301.31 73.76 o 14 0 0 1544.69 1777.91 189.80 o 15 0 0 59.68 113.52 55.95 o 16 0 0 149.44 225.98 82.35 o 17 0 0 37.32 86.95 47.77 o 2 1 0 4374.10 3986.93 59.66 o 3 1 0 14245.89 13562.25 244.00 o 4 1 0 8686.24 8146.11 137.35 o 5 1 0 6869.85 6710.59 144.70 o 6 1 0 5666.33 5746.86 135.75 o 7 1 0 1570.71 1559.21 42.48 o 8 1 0 767.16 734.42 33.47 o 9 1 0 1028.42 1109.59 38.09 o 10 1 0 321.53 316.37 27.81 o 11 1 0 0.61 2.66 4.56 o 12 1 0 146.37 131.84 14.99 o 13 1 0 226.18 296.01 34.78 o 14 1 0 3.09 2.71 21.43 o 15 1 0 0.51 47.65 27.51 o 16 1 0 3.22 -4.69 40.41 o 1 2 0 3851.46 3726.19 73.85 o 2 2 0 11187.85 10763.94 176.06 o 3 2 0 5601.16 5420.71 59.88 o 4 2 0 5990.56 5721.88 191.37 o 5 2 0 113.38 103.62 10.40 o 6 2 0 30.16 36.57 6.81 o 7 2 0 2.16 1.62 3.08 o 8 2 0 1348.97 1311.56 71.89 o 9 2 0 365.53 368.45 18.83 o 10 2 0 502.62 517.06 48.61 o 11 2 0 460.59 577.72 46.76 o 12 2 0 317.84 353.35 40.20 o 13 2 0 66.44 96.41 20.52 o 14 2 0 35.23 62.56 29.62 o 15 2 0 12.87 43.67 21.09 o 16 2 0 5.85 38.83 37.93 o 1 3 0 325.22 314.28 25.98 o 2 3 0 1646.46 1633.20 74.83 o 3 3 0 3873.83 3591.69 65.47 o 4 3 0 3712.35 3761.50 52.20 o 5 3 0 164.49 158.03 12.54 o 6 3 0 9008.56 9830.10 185.59 o 7 3 0 555.46 556.79 34.55 o 8 3 0 2504.42 2660.91 94.58 o 9 3 0 249.43 287.28 23.65 o 10 3 0 177.34 177.08 21.45 o 11 3 0 14.93 23.88 13.29 o 12 3 0 83.32 119.29 22.15 o 13 3 0 0.40 13.31 20.69 o 14 3 0 1.49 9.56 12.96 o 15 3 0 12.21 19.73 33.32 o 16 3 0 13.01 52.43 71.17 o 0 4 0 8580.28 7659.84 153.11 o 1 4 0 510.83 390.93 33.76 o 2 4 0 3428.07 2931.37 93.32 o 3 4 0 9.15 18.98 11.29 o 4 4 0 1160.10 1268.17 44.82 o 5 4 0 1.33 5.04 3.01 o 6 4 0 671.47 780.54 31.95 o 7 4 0 973.32 1070.34 56.49 o 8 4 0 2268.54 2436.10 78.93 o 9 4 0 425.82 529.10 43.87 o 10 4 0 141.90 199.29 27.76 o 11 4 0 2.91 0.49 8.56 o 12 4 0 85.09 185.63 30.56 o 13 4 0 7.78 3.03 21.51 o 14 4 0 12.67 41.35 16.09 o 15 4 0 0.37 -10.00 27.55 o 16 4 0 8.60 15.19 51.89 o 1 5 0 313.89 291.00 24.21 o 2 5 0 550.92 549.44 43.79 o 3 5 0 1144.04 1079.20 49.03 o 4 5 0 2146.97 2152.06 66.67 o 5 5 0 3848.36 4185.52 80.63 o 6 5 0 207.11 200.45 17.45 o 7 5 0 703.53 652.53 28.72 o 8 5 0 101.20 95.49 15.16 o 9 5 0 316.75 397.64 47.60 o 10 5 0 217.96 280.51 42.45 o 11 5 0 172.36 133.30 24.06 o 12 5 0 144.70 145.21 27.15 o 13 5 0 69.90 66.12 18.98 o 14 5 0 19.76 35.34 12.44 o 15 5 0 19.50 46.25 28.65 o 16 5 0 0.17 2.81 17.98 o 0 6 0 1139.64 1271.34 73.94 o 1 6 0 59.02 91.57 12.45 o 2 6 0 99.65 66.38 11.64 o 3 6 0 1.60 41.34 18.78 o 4 6 0 1.79 -2.61 4.17 o 5 6 0 6.13 2.99 4.54 o 6 6 0 898.12 959.93 47.24 o 7 6 0 405.32 416.56 46.75 o 8 6 0 812.98 838.33 40.88 o 9 6 0 54.50 114.75 29.51 o 10 6 0 11.35 18.39 10.68 o 11 6 0 1.44 -12.95 12.95 o 12 6 0 2.91 -4.40 16.08 o 13 6 0 1.33 -10.12 10.97 o 14 6 0 5.15 0.77 12.21 o 15 6 0 19.78 -15.23 20.50 o 16 6 0 0.89 -30.06 32.98 o 1 7 0 873.16 782.34 32.04 o 2 7 0 132.00 145.04 13.13 o 3 7 0 17.23 15.89 5.38 o 4 7 0 400.44 424.52 36.18 o 5 7 0 92.72 68.35 11.31 o 6 7 0 2172.33 2047.76 62.29 o 7 7 0 136.13 197.05 23.17 o 8 7 0 219.33 189.01 22.35 o 9 7 0 186.63 111.23 38.49 o 10 7 0 78.18 29.81 15.85 o 11 7 0 7.46 22.36 17.49 o 12 7 0 379.21 378.44 55.26 o 13 7 0 46.37 -8.95 22.84 o 14 7 0 1.20 21.99 28.91 o 15 7 0 3.39 -33.23 70.14 o 16 7 0 0.39 -16.69 68.75 o 0 8 0 358.07 433.22 37.28 o 1 8 0 2056.50 2020.53 64.11 o 2 8 0 1016.39 1023.40 37.97 o 3 8 0 5516.81 5181.11 159.51 o 4 8 0 1061.73 881.15 72.76 o 5 8 0 85.54 134.89 21.59 o 6 8 0 45.27 28.74 7.58 o 7 8 0 606.56 556.54 38.26 o 8 8 0 0.78 45.92 14.06 o 9 8 0 4.37 6.81 10.08 o 10 8 0 36.67 25.80 21.66 o 11 8 0 540.52 462.07 83.77 o 12 8 0 12.35 -5.54 13.09 o 13 8 0 27.49 19.77 31.84 o 14 8 0 0.79 4.51 26.26 o 15 8 0 25.30 -39.67 39.67 o 1 9 0 89.76 97.16 15.45 o 2 9 0 2615.06 2572.19 74.88 o 3 9 0 902.45 867.20 40.23 o 4 9 0 94.28 90.33 11.40 o 5 9 0 440.72 431.42 36.14 o 6 9 0 993.06 936.21 47.45 o 7 9 0 1316.02 1242.02 62.16 o 8 9 0 634.94 618.84 42.42 o 9 9 0 210.60 140.35 27.65 o 10 9 0 55.75 48.74 18.05 o 11 9 0 317.26 253.01 70.03 o 12 9 0 53.46 85.01 40.70 o 13 9 0 81.32 65.62 33.37 o 14 9 0 24.72 10.04 18.70 o 15 9 0 12.46 29.36 31.09 o 0 10 0 1891.79 1430.61 104.50 o 1 10 0 1596.01 1384.72 71.74 o 2 10 0 121.93 62.13 11.80 o 3 10 0 3561.05 3282.38 82.88 o 4 10 0 2178.14 1950.93 54.95 o 5 10 0 451.44 429.93 37.05 o 6 10 0 5.94 -7.89 7.89 o 7 10 0 137.38 174.93 24.76 o 8 10 0 0.59 3.51 3.90 o 9 10 0 91.64 107.16 18.43 o 10 10 0 228.07 240.03 20.59 o 11 10 0 139.07 88.24 40.84 o 12 10 0 3.08 19.01 26.21 o 13 10 0 67.67 100.64 49.62 o 14 10 0 56.18 69.16 29.66 o 15 10 0 167.49 110.36 38.43 o 1 11 0 1.11 7.65 7.05 o 2 11 0 41.52 81.38 20.02 o 3 11 0 1625.34 1597.87 56.19 o 4 11 0 223.96 292.30 23.48 o 5 11 0 2116.43 2023.61 99.92 o 6 11 0 753.65 767.71 48.05 o 7 11 0 386.58 390.63 39.38 o 8 11 0 198.97 180.57 26.46 o 9 11 0 900.92 866.97 75.61 o 10 11 0 231.83 245.67 34.41 o 11 11 0 141.71 170.90 61.43 o 12 11 0 1.12 11.21 22.55 o 13 11 0 30.87 47.05 40.55 o 14 11 0 6.90 1.69 17.64 o 0 12 0 489.65 484.69 113.64 o 1 12 0 1158.15 1050.19 49.58 o 2 12 0 863.06 828.87 43.48 o 3 12 0 1680.15 1551.24 57.13 o 4 12 0 547.94 469.02 31.91 o 5 12 0 31.98 68.85 17.71 o 6 12 0 19.92 41.79 11.37 o 7 12 0 74.01 35.81 10.95 o 8 12 0 385.98 397.16 36.35 o 9 12 0 60.62 55.37 21.31 o 10 12 0 133.16 168.24 51.94 o 11 12 0 419.93 464.17 98.88 o 12 12 0 94.02 104.41 55.37 o 13 12 0 40.54 79.40 46.15 o 14 12 0 28.92 24.93 38.28 o 1 13 0 782.16 747.02 43.81 o 2 13 0 808.49 844.46 45.76 o 3 13 0 2057.67 2035.27 90.24 o 4 13 0 30.16 33.72 14.73 o 5 13 0 333.35 340.10 23.81 o 6 13 0 163.24 208.92 35.85 o 7 13 0 906.83 907.46 57.92 o 8 13 0 65.57 78.58 22.18 o 9 13 0 343.99 330.67 78.90 o 10 13 0 76.29 50.83 20.79 o 11 13 0 66.69 4.42 15.85 o 12 13 0 14.57 -20.33 20.33 o 13 13 0 15.95 32.09 23.95 o 0 14 0 151.94 211.23 34.09 o 1 14 0 476.20 518.07 38.19 o 2 14 0 691.81 695.50 48.73 o 3 14 0 1087.00 1125.14 69.47 o 4 14 0 1080.96 1044.96 61.01 o 5 14 0 51.00 27.72 8.59 o 6 14 0 41.21 67.49 25.54 o 7 14 0 274.51 354.39 48.91 o 8 14 0 19.02 -16.13 18.72 o 9 14 0 534.12 599.66 113.62 o 10 14 0 15.88 39.25 22.65 o 11 14 0 154.50 229.43 54.13 o 12 14 0 155.04 159.01 46.33 o 13 14 0 64.30 30.69 27.77 o 1 15 0 408.76 417.33 40.50 o 2 15 0 201.48 252.36 30.55 o 3 15 0 216.50 147.52 25.52 o 4 15 0 194.24 259.37 31.52 o 5 15 0 499.95 551.06 97.49 o 6 15 0 314.02 425.43 88.05 o 7 15 0 133.11 206.38 61.05 o 8 15 0 29.14 4.95 24.78 o 9 15 0 2.25 4.85 14.12 o 10 15 0 3.13 -1.50 27.08 o 11 15 0 103.27 148.44 48.36 o 12 15 0 64.84 40.26 25.88 o 0 16 0 54.97 180.43 51.27 o 1 16 0 76.07 92.30 20.02 o 2 16 0 24.30 42.28 13.39 o 3 16 0 7.03 1.10 19.63 o 4 16 0 20.57 17.32 19.95 o 5 16 0 1.88 -25.51 26.50 o 6 16 0 14.01 1.49 22.56 o 7 16 0 112.92 235.06 70.20 o 8 16 0 92.73 181.53 63.94 o 9 16 0 155.14 211.42 53.97 o 10 16 0 76.97 105.74 41.70 o 11 16 0 57.77 16.98 44.90 o 1 17 0 90.49 93.35 27.58 o 2 17 0 76.69 43.12 20.37 o 3 17 0 121.10 113.14 47.18 o 4 17 0 3.84 15.01 25.09 o 5 17 0 79.03 79.52 40.73 o 6 17 0 57.13 64.20 33.00 o 7 17 0 21.26 -30.98 30.98 o 8 17 0 24.40 8.99 21.39 o 9 17 0 5.07 -3.21 48.89 o 10 17 0 177.57 157.47 47.20 o 0 18 0 9.74 16.20 13.21 o 1 18 0 1.23 27.75 11.52 o 2 18 0 1.46 16.20 16.97 o 3 18 0 58.92 39.72 15.92 o 4 18 0 10.63 1.43 18.50 o 5 18 0 37.25 1.88 14.31 o 6 18 0 67.61 58.79 36.97 o 7 18 0 32.89 44.80 44.67 o 8 18 0 47.10 30.32 33.56 o 9 18 0 4.81 15.18 20.40 o 1 19 0 10.92 -3.11 12.73 o 2 19 0 3.18 -11.78 15.76 o 3 19 0 0.54 23.01 30.61 o 4 19 0 26.65 42.93 27.95 o 5 19 0 6.92 -22.74 25.68 o 6 19 0 12.18 21.88 35.33 o 7 19 0 1.60 3.47 29.84 o 8 19 0 10.79 -24.48 24.48 o 0 20 0 63.44 41.29 29.58 o 1 20 0 41.80 -2.39 16.60 o 2 20 0 16.53 49.13 36.55 o 3 20 0 18.77 60.82 41.37 o 4 20 0 0.54 5.72 19.87 o 5 20 0 47.90 15.19 18.84 o 6 20 0 117.83 192.03 75.72 o 1 21 0 2.51 -9.36 16.08 o 2 21 0 0.02 15.15 40.06 o 3 21 0 32.66 48.01 41.41 o 4 21 0 26.05 28.66 34.16 o -17 1 1 2.84 27.18 22.97 o -16 1 1 18.77 6.64 16.00 o -15 1 1 8.65 19.27 34.44 o -14 1 1 6.40 25.01 26.30 o -13 1 1 186.78 193.55 31.90 o -12 1 1 1736.24 1833.41 58.99 o -11 1 1 95.36 120.45 16.74 o -10 1 1 7.26 12.49 7.75 o -9 1 1 1.76 -9.55 13.38 o -8 1 1 216.78 242.33 20.38 o -7 1 1 86.13 107.42 10.04 o -6 1 1 8.34 9.96 3.75 o -5 1 1 2062.19 2213.71 44.15 o -4 1 1 1658.40 1682.39 36.45 o -3 1 1 1445.66 1291.59 33.09 o -2 1 1 8355.42 7981.40 124.41 o 1 1 1 8352.48 8009.65 115.01 o 2 1 1 8468.17 8782.49 105.93 o 3 1 1 18594.75 18811.74 316.57 o 4 1 1 2.74 4.04 10.18 o 5 1 1 263.75 284.37 24.20 o 6 1 1 7.15 -0.63 5.10 o 7 1 1 34.94 16.80 5.26 o 8 1 1 6.78 8.50 3.76 o 9 1 1 5.36 10.17 4.95 o 10 1 1 115.22 121.39 15.01 o 11 1 1 0.73 -7.08 7.16 o 12 1 1 0.22 16.63 11.58 o 13 1 1 260.73 296.02 30.50 o 14 1 1 5.81 -2.58 17.72 o 15 1 1 11.04 18.59 53.02 o 16 1 1 10.35 61.67 34.87 o -17 2 1 0.16 6.09 16.62 o -16 2 1 8.02 -1.31 30.67 o -15 2 1 76.61 86.06 33.56 o -14 2 1 59.59 55.17 17.10 o -13 2 1 215.84 203.65 20.05 o -12 2 1 21.65 16.32 4.68 o -11 2 1 97.34 91.92 14.19 o -10 2 1 322.28 333.78 21.59 o -9 2 1 735.18 695.54 30.40 o -8 2 1 366.53 362.31 22.92 o -7 2 1 484.06 425.92 19.77 o -6 2 1 93.88 78.45 7.95 o -5 2 1 83.31 96.04 8.63 o -4 2 1 2405.71 2412.54 47.80 o -3 2 1 8279.76 8121.76 254.09 o -2 2 1 10410.89 9851.21 203.04 o -1 2 1 723.08 587.29 43.58 o 0 2 1 1692.90 1567.32 65.57 o 1 2 1 31863.14 31227.13 308.52 o 2 2 1 921.15 965.26 25.07 o 3 2 1 458.10 439.33 25.34 o 4 2 1 97.76 95.24 10.73 o 5 2 1 242.81 186.72 18.48 o 6 2 1 1370.09 1323.65 48.83 o 7 2 1 85.00 43.75 8.60 o 8 2 1 1239.93 1242.73 46.09 o 9 2 1 672.87 669.67 36.11 o 10 2 1 142.40 128.75 26.29 o 11 2 1 10.03 -2.53 8.56 o 12 2 1 121.30 124.14 22.63 o 13 2 1 210.85 261.48 33.14 o 14 2 1 116.97 158.72 41.86 o 15 2 1 135.86 178.14 48.84 o 16 2 1 8.87 -6.34 19.35 o -16 3 1 10.98 -19.15 50.38 o -15 3 1 139.20 136.11 85.87 o -14 3 1 6.93 3.84 12.23 o -13 3 1 14.36 20.21 14.99 o -12 3 1 296.50 289.49 22.25 o -11 3 1 38.98 38.31 7.49 o -10 3 1 174.95 179.21 15.99 o -9 3 1 364.17 360.90 18.23 o -8 3 1 440.52 412.95 19.78 o -7 3 1 304.24 282.31 16.39 o -6 3 1 701.49 827.88 26.90 o -5 3 1 164.78 179.16 11.99 o -4 3 1 1908.09 2019.73 45.77 o -3 3 1 10385.18 10333.90 150.82 o -2 3 1 5717.44 5787.36 95.43 o -1 3 1 11204.61 11008.54 96.22 o 0 3 1 9324.28 9333.77 207.38 o 1 3 1 240.96 226.99 14.77 o 2 3 1 9140.11 9308.90 167.91 o 3 3 1 3837.68 3948.58 55.09 o 4 3 1 449.41 454.76 23.31 o 5 3 1 867.13 1000.91 38.18 o 6 3 1 151.32 174.93 17.35 o 7 3 1 1.32 2.01 10.06 o 8 3 1 450.12 491.45 34.05 o 9 3 1 325.53 341.53 28.56 o 10 3 1 2.30 -11.67 12.29 o 11 3 1 83.07 80.74 16.51 o 12 3 1 221.33 247.09 31.90 o 13 3 1 1.04 15.90 12.29 o 14 3 1 123.85 139.44 35.36 o 15 3 1 3.40 13.34 14.73 o 16 3 1 27.66 18.67 23.74 o -16 4 1 0.53 7.42 28.88 o -15 4 1 27.44 27.98 20.65 o -14 4 1 16.12 26.81 15.09 o -13 4 1 0.11 -10.10 14.76 o -12 4 1 27.92 10.11 9.96 o -11 4 1 17.02 22.06 9.86 o -10 4 1 369.92 337.64 31.79 o -9 4 1 1729.52 1694.32 38.98 o -8 4 1 2927.59 2943.00 69.69 o -7 4 1 29.45 27.52 5.03 o -6 4 1 6368.39 6309.65 139.96 o -5 4 1 1782.22 1540.40 32.54 o -4 4 1 10585.14 10669.55 170.40 o -3 4 1 6649.59 6302.49 118.29 o -2 4 1 56.67 69.12 7.31 o -1 4 1 3.39 5.00 3.46 o 0 4 1 467.93 414.84 22.01 o 1 4 1 878.36 830.55 29.81 o 2 4 1 5686.98 5579.03 92.14 o 3 4 1 616.46 587.86 19.50 o 4 4 1 2923.11 2938.74 52.56 o 5 4 1 1876.28 1922.93 52.00 o 6 4 1 6280.82 6888.20 187.76 o 7 4 1 195.65 175.04 17.16 o 8 4 1 595.29 574.75 40.71 o 9 4 1 800.45 764.73 101.05 o 10 4 1 420.94 462.36 61.06 o 11 4 1 71.06 55.65 14.67 o 12 4 1 0.15 -7.81 9.41 o 13 4 1 50.30 31.65 21.83 o 14 4 1 0.17 -5.17 12.87 o 15 4 1 18.59 9.08 71.28 o 16 4 1 16.95 20.77 23.12 o -16 5 1 19.21 -9.51 78.51 o -15 5 1 103.98 86.70 34.44 o -14 5 1 53.79 19.38 9.82 o -13 5 1 35.36 23.15 21.44 o -12 5 1 368.53 373.03 67.03 o -11 5 1 236.33 242.66 34.17 o -10 5 1 547.27 553.63 31.43 o -9 5 1 1537.67 1677.33 78.85 o -8 5 1 317.12 356.77 35.35 o -7 5 1 193.96 240.09 22.59 o -6 5 1 234.98 343.90 39.46 o -5 5 1 3979.21 4253.54 93.76 o -4 5 1 2145.73 2108.62 64.16 o -3 5 1 3914.42 3951.44 130.77 o -2 5 1 1736.59 1685.31 54.37 o -1 5 1 14599.30 13169.80 297.24 o 0 5 1 11463.30 11152.29 151.75 o 1 5 1 3281.66 3177.43 58.03 o 2 5 1 4352.83 4070.23 59.21 o 3 5 1 7880.20 7673.01 176.49 o 4 5 1 1479.13 1592.55 36.55 o 5 5 1 551.10 514.57 20.43 o 6 5 1 807.85 902.97 38.23 o 7 5 1 3099.26 3553.05 90.61 o 8 5 1 24.03 15.75 8.99 o 9 5 1 654.05 708.54 87.11 o 10 5 1 146.79 112.01 25.42 o 11 5 1 129.65 169.50 34.98 o 12 5 1 25.43 -5.84 12.26 o 13 5 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