#------------------------------------------------------------------------------
#$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $
#$Revision: 88054 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237539.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2237539_Fobs
loop_
_publ_author_name
'Shirkhanlou, Mahdi'
'Weil, Matthias'
_publ_section_title
;
 The Mg member of the isotypic series <i>M</i>Te~6~O~13~
;
_journal_coeditor_code           PJ2001
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i18
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   10.1676
_cell_length_b                   10.1676
_cell_length_c                   18.9701
_exptl_crystal_F_000             2568.00
_reflns_d_resolution_high        0.5156
_[local]_cod_data_source_file    pj2001Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' ms_mgte6o13_0m in R-3'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1531.45
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 2 0 3414.85 3754.85 110.86 o
0 3 0 300352.03 305426.66 2826.46 o
-2 4 0 4644.82 5462.39 91.48 o
-4 5 0 150902.47 153304.03 1272.27 o
-1 5 0 1400320.88 1537055.00 20275.93 o
-3 6 0 332086.22 339566.50 3041.53 o
0 6 0 51784.58 51473.43 424.52 o
-5 7 0 121350.34 122969.04 996.52 o
-2 7 0 65444.47 65427.78 589.41 o
-7 8 0 138855.08 140038.75 1193.46 o
-4 8 0 95538.57 94872.97 840.38 o
-1 8 0 148957.41 150318.44 1247.04 o
-6 9 0 191730.92 190666.89 1719.60 o
-3 9 0 4419.25 4717.62 111.98 o
0 9 0 19087.56 19167.13 230.85 o
-8 10 0 223006.72 224703.75 2178.06 o
-5 10 0 51041.94 50424.02 559.10 o
-2 10 0 89923.45 90183.59 868.09 o
-10 11 0 39521.48 39008.20 452.22 o
-7 11 0 6265.57 6446.21 148.98 o
-4 11 0 325382.28 323739.84 3098.06 o
-1 11 0 37322.30 37548.85 436.61 o
-9 12 0 39403.07 37963.67 477.43 o
-6 12 0 53630.18 54268.34 652.40 o
-3 12 0 24631.05 24968.90 316.49 o
0 12 0 120879.51 118657.41 1392.60 o
-11 13 0 2588.17 3032.88 188.03 o
-8 13 0 16135.57 16011.58 282.36 o
-5 13 0 12564.21 11584.86 218.19 o
-2 13 0 25694.92 26292.09 395.29 o
-13 14 0 52200.57 51957.04 822.49 o
-10 14 0 1257.09 1708.07 121.83 o
-7 14 0 2767.24 3372.21 183.61 o
-4 14 0 12759.23 12707.78 241.68 o
-1 14 0 1871.61 2218.00 139.90 o
-12 15 0 22283.83 22179.42 404.28 o
-9 15 0 155839.91 152325.16 1908.32 o
-6 15 0 4133.21 4388.30 176.45 o
-3 15 0 193.20 974.97 151.82 o
0 15 0 15008.59 14685.64 365.98 o
-14 16 0 5304.70 5649.30 249.77 o
-11 16 0 10243.86 10668.37 269.66 o
-8 16 0 2970.89 3199.62 184.98 o
-5 16 0 144844.36 144558.69 1950.41 o
-2 16 0 19293.92 19392.45 450.63 o
-16 17 0 30.17 103.76 142.58 o
-13 17 0 5209.45 5412.57 238.15 o
-10 17 0 10499.28 10093.30 309.40 o
-7 17 0 1337.73 1489.70 151.05 o
-4 17 0 2979.99 3112.52 197.92 o
-1 17 0 28194.08 27130.07 815.71 o
-15 18 0 21892.41 22352.59 651.50 o
-12 18 0 1519.75 2155.22 198.62 o
-9 18 0 4690.69 4752.85 243.24 o
-6 18 0 13.36 345.23 129.81 o
-3 18 0 0.02 147.79 147.16 o
-11 19 0 13031.56 12383.61 393.60 o
-8 19 0 2306.43 2372.06 211.21 o
-5 19 0 15916.41 15905.06 777.15 o
-1 1 1 0.16 -13.70 13.70 o
-3 2 1 51765.12 53331.80 657.35 o
0 2 1 11538.01 11610.70 162.50 o
-5 3 1 11242.79 10807.17 122.34 o
-2 3 1 12.51 -33.43 33.43 o
1 3 1 14907.93 17524.80 166.31 o
-7 4 1 6368.82 5984.81 98.16 o
-4 4 1 130.07 690.41 42.86 o
-1 4 1 8535.22 8179.48 97.84 o
2 4 1 3265.70 3636.76 98.27 o
-9 5 1 23998.68 24263.38 268.78 o
-6 5 1 60382.43 61409.81 532.64 o
-3 5 1 52614.75 53414.84 453.11 o
0 5 1 7368.73 6923.85 129.92 o
3 5 1 45942.51 46210.42 462.61 o
-11 6 1 23022.95 22500.30 301.36 o
-8 6 1 6905.62 7139.46 110.30 o
-5 6 1 8781.31 8331.97 93.87 o
-2 6 1 2770.35 3296.46 54.03 o
1 6 1 36339.10 35198.17 349.37 o
4 6 1 34872.93 34219.42 392.27 o
-13 7 1 22413.68 21634.80 329.86 o
-10 7 1 2170.13 2227.04 78.05 o
-7 7 1 70.46 222.95 28.60 o
-4 7 1 66830.82 66753.30 571.32 o
-1 7 1 7897.80 7987.60 113.45 o
2 7 1 632.69 971.20 51.43 o
5 7 1 4454.46 4576.57 128.63 o
-15 8 1 21664.04 21050.53 378.62 o
-12 8 1 12898.46 12820.61 214.18 o
-9 8 1 10929.93 11067.22 151.29 o
-6 8 1 1651.64 1925.37 57.63 o
-3 8 1 9872.38 9992.63 156.13 o
0 8 1 107943.30 109321.02 1038.77 o
3 8 1 38.88 179.06 46.20 o
6 8 1 11168.15 10903.72 224.09 o
-17 9 1 552.26 784.97 130.83 o
-14 9 1 22435.87 21363.55 308.38 o
-11 9 1 72553.87 71468.60 741.04 o
-8 9 1 57293.09 57043.00 539.87 o
-5 9 1 1852.47 2143.30 68.59 o
-2 9 1 26430.82 26203.42 266.34 o
1 9 1 14.15 190.63 43.80 o
4 9 1 69666.00 68001.42 803.18 o
7 9 1 149.62 216.05 93.16 o
-19 10 1 31016.91 31022.61 745.12 o
-16 10 1 22202.41 21993.29 431.12 o
-13 10 1 17.51 166.20 57.66 o
-10 10 1 7932.95 8312.81 141.25 o
-7 10 1 41576.68 40953.86 468.22 o
-4 10 1 21946.36 22107.38 253.71 o
-1 10 1 1385.14 1404.97 65.16 o
2 10 1 36251.76 36158.60 424.81 o
5 10 1 11090.46 10964.71 262.45 o
8 10 1 34157.91 34405.29 681.51 o
-18 11 1 281.54 219.16 130.61 o
-15 11 1 7007.83 7065.87 235.61 o
-12 11 1 5761.51 5922.05 154.31 o
-9 11 1 8766.90 8601.65 162.27 o
-6 11 1 251.47 495.20 54.08 o
-3 11 1 10205.26 10391.86 172.60 o
0 11 1 4228.46 4632.37 132.29 o
3 11 1 1888.45 1993.40 130.24 o
6 11 1 5783.14 5797.54 225.30 o
-17 12 1 12.71 94.28 116.10 o
-14 12 1 18.36 209.01 87.53 o
-11 12 1 44.69 175.22 66.65 o
-8 12 1 10432.11 9997.04 182.58 o
-5 12 1 69289.19 69425.68 808.03 o
-2 12 1 1263.00 1472.27 89.31 o
1 12 1 16626.51 16740.23 291.90 o
4 12 1 129.87 354.72 108.19 o
7 12 1 24.89 254.58 153.37 o
-19 13 1 24288.00 24342.42 758.62 o
-16 13 1 43564.14 44209.29 788.27 o
-13 13 1 14602.68 14661.85 314.14 o
-10 13 1 1185.80 1293.09 95.57 o
-7 13 1 9.14 98.27 59.09 o
-4 13 1 20137.96 19892.56 285.77 o
-1 13 1 80155.37 79502.13 1023.22 o
2 13 1 1445.25 1621.10 152.20 o
5 13 1 36599.19 37724.29 949.01 o
-18 14 1 122.13 248.87 129.50 o
-15 14 1 31279.64 31978.76 568.76 o
-12 14 1 74093.98 74026.35 1006.05 o
-9 14 1 13924.36 13509.68 331.37 o
-6 14 1 29.63 136.18 71.49 o
-3 14 1 5139.89 5313.00 172.39 o
0 14 1 2316.97 2405.19 171.66 o
3 14 1 46185.98 45960.66 877.46 o
-17 15 1 4513.01 4130.83 264.23 o
-14 15 1 108.57 251.07 110.83 o
-11 15 1 31674.84 31926.98 562.32 o
-8 15 1 33988.26 32651.95 540.70 o
-5 15 1 61.82 149.31 82.91 o
-2 15 1 234.90 511.99 102.50 o
1 15 1 334.27 661.77 142.23 o
-16 16 1 1034.37 1121.00 165.95 o
-13 16 1 604.74 683.35 139.63 o
-10 16 1 6360.91 6649.99 228.83 o
-7 16 1 18889.57 17837.47 364.43 o
-4 16 1 17874.52 16662.52 422.70 o
-1 16 1 3376.52 3891.94 226.58 o
-15 17 1 2757.86 3149.17 224.69 o
-12 17 1 2687.50 2847.30 181.85 o
-9 17 1 22571.21 22421.16 456.07 o
-6 17 1 26603.91 25374.03 540.47 o
-3 17 1 12341.17 12149.73 360.54 o
0 17 1 28442.29 26948.89 835.06 o
-14 18 1 118.89 115.85 162.42 o
-11 18 1 54.28 143.76 120.29 o
-8 18 1 3539.31 3486.44 236.07 o
-5 18 1 16907.68 16637.25 407.31 o
-13 19 1 30729.33 31276.29 967.85 o
-10 19 1 284.04 342.45 149.72 o
-7 19 1 311.46 502.94 154.66 o
0 1 2 11731.92 10876.58 144.82 o
-2 2 2 295596.44 283738.09 5152.21 o
1 2 2 2076388.63 1829441.38 46835.48 o
-4 3 2 128514.25 133786.59 1295.99 o
-1 3 2 33877.67 34073.48 350.06 o
2 3 2 36.61 577.56 81.56 o
-6 4 2 95248.07 95151.99 861.33 o
-3 4 2 243413.64 249742.22 2026.70 o
0 4 2 26970.19 24876.62 235.20 o
3 4 2 14670.77 15130.23 170.15 o
-8 5 2 324156.50 326051.31 3025.88 o
-5 5 2 140136.03 142853.94 1129.74 o
-2 5 2 128781.00 128460.86 1027.46 o
1 5 2 387258.63 395533.34 3461.18 o
4 5 2 299968.81 302556.75 2732.76 o
-10 6 2 2175.21 2633.18 86.29 o
-7 6 2 172825.88 171175.56 1421.45 o
-4 6 2 979121.13 1057377.75 10662.53 o
-1 6 2 6119.01 6446.99 99.12 o
2 6 2 40112.36 39257.27 383.31 o
5 6 2 124266.25 122367.06 1341.95 o
-12 7 2 1706.69 2265.57 101.15 o
-9 7 2 62572.89 62117.76 612.72 o
-6 7 2 197080.34 196008.56 1503.52 o
-3 7 2 89129.72 88764.91 750.62 o
0 7 2 311535.41 315820.44 2572.92 o
3 7 2 40766.28 40176.88 452.35 o
6 7 2 1840.97 2039.18 113.73 o
-14 8 2 224668.98 216926.28 2465.12 o
-11 8 2 46924.94 47800.16 547.48 o
-8 8 2 81745.16 82242.79 724.90 o
-5 8 2 21228.95 21724.66 220.23 o
-2 8 2 265175.59 264307.84 2331.00 o
1 8 2 22828.11 22848.82 266.42 o
4 8 2 14419.95 14575.85 244.02 o
7 8 2 8195.65 8357.33 216.82 o
-16 9 2 14143.48 14059.74 294.89 o
-13 9 2 5165.41 5500.23 140.79 o
-10 9 2 253698.19 255198.56 2173.76 o
-7 9 2 113013.08 111971.02 1000.64 o
-4 9 2 194585.22 193744.42 1723.15 o
-1 9 2 55681.55 56002.16 563.61 o
2 9 2 79347.64 78330.93 816.14 o
5 9 2 7162.10 7452.64 190.13 o
8 9 2 4234.60 4758.71 227.94 o
-18 10 2 287.93 478.21 142.04 o
-15 10 2 699.02 981.72 101.51 o
-12 10 2 5313.45 5253.98 138.13 o
-9 10 2 83576.49 82856.80 801.79 o
-6 10 2 22046.76 21817.05 253.23 o
-3 10 2 34654.22 33674.53 368.14 o
0 10 2 113025.68 113395.76 1156.72 o
3 10 2 136683.58 134939.61 1453.01 o
6 10 2 1789.53 2223.94 137.83 o
9 10 2 1378.31 1679.06 183.02 o
-17 11 2 10323.22 10364.63 309.25 o
-14 11 2 29847.71 30151.18 491.45 o
-11 11 2 82131.14 82432.38 915.37 o
-8 11 2 13491.91 13455.74 199.41 o
-5 11 2 97047.06 97229.80 1051.21 o
-2 11 2 18884.36 19008.58 246.88 o
1 11 2 93.80 298.23 69.16 o
4 11 2 39807.07 39344.14 656.93 o
7 11 2 79403.89 80149.73 1238.91 o
-19 12 2 54030.37 52324.16 1204.22 o
-16 12 2 925.00 1195.57 145.44 o
-13 12 2 37093.58 36381.02 522.81 o
-10 12 2 54205.99 53156.46 651.61 o
-7 12 2 278190.88 276739.16 2834.97 o
-4 12 2 22525.25 21753.28 305.42 o
-1 12 2 8967.03 9411.37 212.53 o
2 12 2 30323.72 30278.89 531.20 o
5 12 2 10075.45 10478.33 433.77 o
-18 13 2 1922.90 2033.22 179.47 o
-15 13 2 82862.81 80847.11 1213.15 o
-12 13 2 23807.73 24205.50 383.73 o
-9 13 2 42770.84 42850.20 572.82 o
-6 13 2 4314.03 4561.27 139.12 o
-3 13 2 188754.91 186296.06 2062.80 o
0 13 2 15536.82 15877.76 314.99 o
3 13 2 1334.98 1782.53 170.98 o
6 13 2 2360.69 2532.98 309.60 o
-17 14 2 8283.85 8818.34 311.23 o
-14 14 2 38.27 16.39 97.71 o
-11 14 2 26088.45 25939.70 412.39 o
-8 14 2 17803.96 17763.72 386.88 o
-5 14 2 29460.60 30338.27 454.21 o
-2 14 2 18474.58 19252.30 362.09 o
1 14 2 39452.45 39131.77 702.21 o
4 14 2 7024.19 6855.61 300.03 o
-16 15 2 9769.55 9769.97 326.03 o
-13 15 2 15966.14 15802.46 362.51 o
-10 15 2 904.76 1098.65 111.77 o
-7 15 2 6797.27 6932.80 225.64 o
-4 15 2 323.82 591.60 105.43 o
-1 15 2 7772.68 7996.55 271.62 o
2 15 2 33038.88 32877.51 666.23 o
-15 16 2 27675.12 27156.14 624.95 o
-12 16 2 70049.45 70076.56 1010.60 o
-9 16 2 677.11 972.67 158.07 o
-6 16 2 162.34 525.82 181.84 o
-3 16 2 33686.18 33296.54 727.74 o
0 16 2 11155.18 12016.73 384.80 o
-17 17 2 1479.38 1357.48 262.56 o
-14 17 2 6492.02 6357.85 299.95 o
-11 17 2 22023.19 22040.91 490.88 o
-8 17 2 119044.33 117443.96 1643.36 o
-5 17 2 3215.79 3170.78 193.86 o
-2 17 2 1563.69 1696.26 198.87 o
-13 18 2 7706.92 7953.44 355.93 o
-10 18 2 367.88 507.92 130.99 o
-7 18 2 606.19 782.55 150.12 o
-4 18 2 50258.74 49025.25 993.94 o
-12 19 2 1791.22 2205.34 218.77 o
-9 19 2 2381.66 2365.00 212.15 o
-6 19 2 917.54 1415.52 222.71 o
1 1 3 10362.53 10349.30 147.24 o
-1 2 3 17622.56 17518.61 230.06 o
2 2 3 474.56 485.84 37.04 o
-3 3 3 40440.25 41128.39 361.32 o
0 3 3 3006.56 2975.96 50.92 o
3 3 3 76263.01 78578.29 862.74 o
-5 4 3 1173.44 1304.53 54.98 o
-2 4 3 3499.21 3740.76 59.36 o
1 4 3 47.59 -23.97 23.97 o
4 4 3 1351.85 1554.47 56.46 o
-7 5 3 68289.38 68192.73 607.16 o
-4 5 3 1512.63 1663.79 40.79 o
-1 5 3 2939.01 3378.46 61.93 o
2 5 3 6837.46 7483.35 96.26 o
5 5 3 10329.05 10429.47 158.27 o
-9 6 3 32938.89 32690.15 358.62 o
-6 6 3 20167.21 19716.60 184.95 o
-3 6 3 4661.98 4611.19 92.62 o
0 6 3 59138.85 58581.25 522.91 o
3 6 3 580.08 756.03 49.38 o
6 6 3 48903.73 48708.81 609.99 o
-11 7 3 17038.57 16693.06 226.02 o
-8 7 3 1955.78 1844.25 50.95 o
-5 7 3 337.07 743.70 47.67 o
-2 7 3 44412.13 43401.09 390.56 o
1 7 3 16237.97 16050.34 198.99 o
4 7 3 65147.31 64216.07 715.81 o
7 7 3 11583.28 11384.19 231.99 o
-13 8 3 6209.88 6548.03 186.07 o
-10 8 3 860.34 1079.28 60.29 o
-7 8 3 42881.49 42326.96 385.12 o
-4 8 3 8888.09 8898.14 109.16 o
-1 8 3 718.86 1072.68 50.10 o
2 8 3 5087.09 5456.17 130.34 o
5 8 3 16650.70 16472.45 267.08 o
8 8 3 10699.54 10022.71 256.41 o
-15 9 3 933.33 982.67 102.13 o
-12 9 3 19955.12 19871.30 265.23 o
-9 9 3 67.71 197.18 41.18 o
-6 9 3 8523.61 9129.09 141.36 o
-3 9 3 40846.05 40921.41 428.83 o
0 9 3 2720.81 2832.40 87.69 o
3 9 3 10506.01 10786.92 194.30 o
6 9 3 75.81 315.14 82.15 o
9 9 3 8684.24 9094.41 297.35 o
-17 10 3 57684.05 56563.45 870.61 o
-14 10 3 69984.74 70945.78 913.51 o
-11 10 3 17041.37 17468.74 257.41 o
-8 10 3 2482.93 2787.32 81.17 o
-5 10 3 8933.29 8555.65 134.84 o
-2 10 3 4339.64 4820.44 148.91 o
1 10 3 70107.96 69625.67 744.74 o
4 10 3 3999.77 4040.65 144.19 o
7 10 3 33149.02 33661.12 574.11 o
-19 11 3 8785.84 8620.95 305.05 o
-16 11 3 1538.98 1713.04 134.37 o
-13 11 3 28514.69 28490.00 414.71 o
-10 11 3 69646.92 69918.16 728.04 o
-7 11 3 20942.94 20725.03 261.85 o
-4 11 3 1967.63 2022.73 77.86 o
-1 11 3 14705.46 15222.38 239.08 o
2 11 3 113.91 145.47 77.67 o
5 11 3 55994.87 55541.03 862.53 o
8 11 3 289.87 313.29 149.48 o
-18 12 3 12986.04 12969.52 368.00 o
-15 12 3 3698.08 3785.83 176.94 o
-12 12 3 7619.49 7667.56 192.83 o
-9 12 3 2947.26 3160.32 111.74 o
-6 12 3 32502.74 32179.15 418.21 o
-3 12 3 3689.06 4015.35 131.42 o
0 12 3 2041.44 2203.17 111.10 o
3 12 3 7706.78 7816.02 267.66 o
6 12 3 3023.09 3127.16 212.60 o
-17 13 3 186.12 354.14 124.50 o
-14 13 3 209.34 194.19 90.29 o
-11 13 3 8417.35 8680.48 196.62 o
-8 13 3 32861.28 32080.56 462.34 o
-5 13 3 4366.06 4497.04 150.84 o
-2 13 3 25551.79 25337.91 403.82 o
1 13 3 3524.15 3761.30 171.74 o
4 13 3 172.49 305.88 120.12 o
-16 14 3 60.10 65.94 125.15 o
-13 14 3 1581.06 1777.15 143.68 o
-10 14 3 483.99 445.08 88.87 o
-7 14 3 24223.72 23159.10 384.99 o
-4 14 3 51110.83 49474.99 708.17 o
-1 14 3 5892.33 6436.71 206.50 o
2 14 3 25402.55 26004.14 542.11 o
-18 15 3 34916.17 34803.34 850.35 o
-15 15 3 59066.82 58464.50 1146.30 o
-12 15 3 2423.02 2818.76 160.17 o
-9 15 3 1936.35 2009.04 137.28 o
-6 15 3 99.23 171.54 88.78 o
-3 15 3 16801.60 16496.41 334.37 o
0 15 3 45329.11 45049.79 831.78 o
3 15 3 1537.52 1706.05 181.96 o
-17 16 3 1971.48 1959.59 215.94 o
-14 16 3 36493.66 36312.47 727.60 o
-11 16 3 53920.96 52546.65 910.81 o
-8 16 3 133.23 170.77 96.24 o
-5 16 3 234.59 536.36 106.07 o
-2 16 3 363.34 349.80 111.83 o
1 16 3 2148.82 2282.65 211.34 o
-16 17 3 0.36 88.59 170.72 o
-13 17 3 126.20 213.17 137.46 o
-10 17 3 25816.25 25481.78 495.51 o
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