#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237540.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237540_Fobs loop_ _publ_author_name 'Paz-Morales, Evelyn' 'Hern\'andez-Ortega, Sim\'on' 'Morales-Morales, David' _publ_section_title ; Chlorido[2,3,5,6-tetrakis(tert-butylsulfanylmethyl)phenyl-\k^3^S^2^,C^1^,S^6^]palladium(II) dichloromethane monosolvate ; _journal_coeditor_code PK2463 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m139 _journal_page_last m140 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.216 _cell_angle_gamma 90.000 _cell_length_a 15.9173 _cell_length_b 13.7678 _cell_length_c 17.8076 _exptl_crystal_F_000 1480.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file pk2463Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 177MMD12 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 382.07 398.22 25.53 o 4 0 0 40112.75 44982.17 817.31 o 6 0 0 24560.79 25611.32 914.22 o 8 0 0 61495.79 63072.77 1164.64 o 10 0 0 15.28 68.29 28.52 o 12 0 0 1035.96 955.29 83.88 o 14 0 0 3793.26 3553.12 194.52 o 16 0 0 1121.53 1055.34 98.07 o 18 0 0 522.55 596.14 102.44 o 1 1 0 36705.75 42012.27 978.29 o 2 1 0 8232.25 9964.76 283.62 o 3 1 0 8836.03 9278.79 141.15 o 4 1 0 4664.02 5262.98 85.82 o 5 1 0 1449.15 1720.89 90.26 o 6 1 0 19016.40 21289.76 294.32 o 7 1 0 4511.19 4506.16 87.41 o 8 1 0 6053.38 6011.48 112.25 o 9 1 0 2482.21 2143.64 59.92 o 10 1 0 6230.61 5683.21 114.65 o 11 1 0 437.22 455.27 35.14 o 12 1 0 583.69 643.75 40.95 o 13 1 0 4612.51 4616.54 111.73 o 14 1 0 1711.69 1659.38 66.45 o 15 1 0 147.72 164.77 33.32 o 16 1 0 703.90 772.51 92.14 o 17 1 0 140.26 156.83 37.03 o 18 1 0 440.45 326.31 53.37 o 0 2 0 125.59 108.12 9.57 o 1 2 0 7828.61 8067.07 135.26 o 2 2 0 11979.57 13170.95 210.97 o 3 2 0 40046.84 42561.30 563.61 o 4 2 0 2463.75 2708.63 57.26 o 5 2 0 27553.52 29191.32 390.22 o 6 2 0 2.56 6.14 12.51 o 7 2 0 16684.56 17419.91 282.36 o 8 2 0 645.36 745.50 33.19 o 9 2 0 66.32 70.61 18.55 o 10 2 0 31.76 50.15 18.00 o 11 2 0 2220.08 2038.92 97.61 o 12 2 0 120.00 127.75 26.72 o 13 2 0 2.65 5.59 31.30 o 14 2 0 1302.01 1303.74 66.01 o 15 2 0 1237.93 1184.65 58.43 o 16 2 0 51.13 99.96 46.90 o 17 2 0 0.86 37.99 49.93 o 18 2 0 34.63 164.79 49.11 o 1 3 0 8969.68 9423.76 153.94 o 2 3 0 4473.17 5086.26 100.50 o 3 3 0 2104.18 2024.29 88.24 o 4 3 0 316.52 374.20 23.96 o 5 3 0 1206.79 1313.68 35.38 o 6 3 0 1343.42 1173.35 35.02 o 7 3 0 236.15 305.66 21.99 o 8 3 0 7240.00 7417.82 130.37 o 9 3 0 209.89 221.41 24.36 o 10 3 0 1.53 28.85 16.12 o 11 3 0 1272.51 1148.29 47.92 o 12 3 0 452.60 416.44 37.66 o 13 3 0 107.63 147.54 29.58 o 14 3 0 272.08 370.20 40.29 o 15 3 0 74.74 75.14 34.44 o 16 3 0 669.73 717.05 75.81 o 17 3 0 15.29 82.65 35.32 o 0 4 0 5015.44 4557.77 109.99 o 1 4 0 35017.02 36936.73 823.06 o 2 4 0 505.57 544.37 61.80 o 3 4 0 2047.66 1809.86 65.25 o 4 4 0 3152.80 3446.14 118.79 o 5 4 0 217.54 287.46 14.96 o 6 4 0 3.37 29.03 15.73 o 7 4 0 30530.76 31224.37 440.81 o 8 4 0 1648.14 1589.30 98.40 o 9 4 0 597.45 582.14 31.58 o 10 4 0 217.92 232.33 34.37 o 11 4 0 9.23 43.23 19.15 o 12 4 0 261.51 300.87 34.08 o 13 4 0 17.65 28.39 28.44 o 14 4 0 463.81 454.72 54.05 o 15 4 0 2579.06 2285.61 152.41 o 16 4 0 36.92 26.13 33.74 o 17 4 0 7.85 40.77 43.97 o 1 5 0 7070.30 7084.67 114.19 o 2 5 0 5994.99 6305.75 106.82 o 3 5 0 471.67 424.24 33.47 o 4 5 0 597.38 573.19 29.79 o 5 5 0 688.78 626.41 53.86 o 6 5 0 19550.25 20512.43 299.22 o 7 5 0 2009.22 1969.71 98.07 o 8 5 0 831.73 733.18 32.46 o 9 5 0 6113.67 5931.95 118.88 o 10 5 0 896.87 914.44 76.20 o 11 5 0 9.16 -5.39 33.53 o 12 5 0 536.38 577.16 70.20 o 13 5 0 3468.71 3299.25 123.37 o 14 5 0 1585.52 1399.02 101.63 o 15 5 0 178.85 254.53 46.57 o 16 5 0 66.19 154.37 44.80 o 17 5 0 558.16 542.48 78.29 o 0 6 0 46477.93 48219.43 882.32 o 1 6 0 339.93 264.62 35.25 o 2 6 0 1444.29 1318.78 37.06 o 3 6 0 121.23 77.53 17.88 o 4 6 0 12110.63 11922.70 219.75 o 5 6 0 35.62 112.47 21.32 o 6 6 0 1036.90 987.73 47.03 o 7 6 0 133.14 126.76 27.55 o 8 6 0 11874.25 11796.96 240.08 o 9 6 0 560.63 533.33 45.31 o 10 6 0 1152.57 1149.32 92.92 o 11 6 0 116.90 142.91 32.78 o 12 6 0 1718.24 1773.05 186.69 o 13 6 0 0.11 -1.47 33.14 o 14 6 0 3169.19 3232.43 167.92 o 15 6 0 6.22 100.11 83.28 o 16 6 0 465.77 490.64 150.38 o 1 7 0 7105.30 7143.61 210.43 o 2 7 0 4486.55 4314.52 85.43 o 3 7 0 75.25 94.81 59.01 o 4 7 0 400.67 402.38 31.37 o 5 7 0 2619.60 2576.24 79.72 o 6 7 0 3530.92 3475.40 114.75 o 7 7 0 136.24 122.74 27.23 o 8 7 0 139.32 184.67 33.01 o 9 7 0 3000.81 2980.59 100.44 o 10 7 0 626.69 582.16 94.11 o 11 7 0 75.78 91.23 29.57 o 12 7 0 648.79 684.95 54.61 o 13 7 0 1804.79 1590.38 206.85 o 14 7 0 516.06 522.39 77.04 o 15 7 0 572.43 498.50 127.04 o 16 7 0 28.94 -0.36 42.09 o 0 8 0 19272.03 20578.80 426.26 o 1 8 0 6138.41 5954.56 189.97 o 2 8 0 137.57 216.64 30.53 o 3 8 0 689.05 681.79 38.04 o 4 8 0 3.96 10.77 28.50 o 5 8 0 165.60 178.95 45.00 o 6 8 0 1588.18 1768.06 69.52 o 7 8 0 7339.51 7284.62 211.43 o 8 8 0 1692.77 1810.06 76.19 o 9 8 0 171.12 213.65 39.48 o 10 8 0 133.17 144.82 56.26 o 11 8 0 642.90 607.80 101.96 o 12 8 0 14.41 128.26 46.37 o 13 8 0 113.03 170.21 51.88 o 14 8 0 1266.96 1286.07 187.28 o 15 8 0 524.04 605.63 92.72 o 1 9 0 245.80 268.08 26.28 o 2 9 0 978.72 993.39 42.21 o 3 9 0 62.06 74.79 23.33 o 4 9 0 308.80 390.38 42.60 o 5 9 0 1.81 19.41 25.75 o 6 9 0 4187.73 4163.53 117.89 o 7 9 0 1352.51 1386.83 81.32 o 8 9 0 2776.44 2459.66 206.46 o 9 9 0 1.02 -6.50 23.64 o 10 9 0 315.29 328.64 45.94 o 11 9 0 7.47 39.17 37.84 o 12 9 0 1212.41 1080.53 118.13 o 13 9 0 498.42 511.37 76.31 o 14 9 0 348.70 438.49 78.96 o 15 9 0 3.09 30.27 42.41 o 0 10 0 63.35 95.01 35.67 o 1 10 0 3349.32 3121.12 115.09 o 2 10 0 123.06 95.82 42.41 o 3 10 0 1299.42 1353.06 101.99 o 4 10 0 1242.33 1206.82 62.98 o 5 10 0 496.26 564.89 66.29 o 6 10 0 47.91 62.01 27.22 o 7 10 0 8590.11 8324.55 195.44 o 8 10 0 8.78 5.31 25.43 o 9 10 0 1.27 7.45 30.01 o 10 10 0 132.69 135.96 48.55 o 11 10 0 655.24 613.42 104.61 o 12 10 0 4.81 25.42 42.68 o 13 10 0 52.65 87.86 47.44 o 14 10 0 18.45 90.52 84.99 o 1 11 0 1791.70 1782.81 150.85 o 2 11 0 672.21 639.71 83.78 o 3 11 0 481.50 520.83 70.63 o 4 11 0 146.94 149.32 40.09 o 5 11 0 491.47 480.07 63.25 o 6 11 0 1796.61 1737.99 75.76 o 7 11 0 609.95 661.06 50.16 o 8 11 0 672.24 550.14 93.78 o 9 11 0 650.66 717.46 140.49 o 10 11 0 161.81 242.48 57.46 o 11 11 0 2.04 -39.07 39.07 o 12 11 0 28.61 77.51 76.77 o 13 11 0 423.63 468.27 96.92 o 0 12 0 7410.19 7729.17 892.71 o 1 12 0 25.60 70.86 46.66 o 2 12 0 5.08 -20.18 28.06 o 3 12 0 0.16 31.46 25.09 o 4 12 0 516.37 509.66 75.45 o 5 12 0 301.65 360.68 44.58 o 6 12 0 98.29 179.28 49.49 o 7 12 0 298.80 421.49 65.56 o 8 12 0 2443.93 2475.48 123.21 o 9 12 0 52.05 65.81 54.24 o 10 12 0 95.37 142.60 50.37 o 11 12 0 11.76 -5.18 52.04 o 12 12 0 153.74 222.70 66.98 o 1 13 0 1788.24 1910.23 113.07 o 2 13 0 309.16 391.27 144.09 o 3 13 0 36.23 52.89 67.54 o 4 13 0 255.89 263.77 62.00 o 5 13 0 467.13 523.85 51.58 o 6 13 0 3.95 85.38 78.85 o 7 13 0 319.59 354.93 63.58 o 8 13 0 15.40 59.79 48.35 o 9 13 0 630.73 703.72 106.61 o 10 13 0 168.52 305.70 65.77 o 11 13 0 1.09 10.34 243.23 o 0 14 0 2653.76 2867.00 203.01 o 1 14 0 398.49 443.75 86.11 o 2 14 0 39.02 41.95 65.72 o 3 14 0 956.66 981.87 86.22 o 4 14 0 26.93 54.43 35.72 o 5 14 0 66.37 125.35 56.42 o 6 14 0 432.82 506.76 71.20 o 7 14 0 612.03 619.54 78.05 o 8 14 0 527.09 632.19 83.37 o 9 14 0 29.54 83.72 63.18 o 1 15 0 68.40 66.32 46.44 o 2 15 0 1059.09 1194.99 119.52 o 3 15 0 71.37 138.03 98.89 o 4 15 0 82.23 154.98 80.33 o 5 15 0 8.62 -16.92 56.85 o 6 15 0 805.29 669.59 85.73 o 7 15 0 4.78 50.96 43.57 o 0 16 0 70.92 22.09 103.03 o 1 16 0 672.98 824.61 97.99 o 2 16 0 3.21 45.28 76.06 o 3 16 0 104.15 86.88 151.00 o -17 0 1 39.22 84.80 42.89 o -15 0 1 1934.78 1713.81 101.29 o -13 0 1 242.45 308.47 55.08 o -11 0 1 3597.42 3361.06 120.12 o -9 0 1 681.40 558.06 44.31 o -7 0 1 5875.34 5621.75 144.00 o -5 0 1 36260.74 39461.13 726.64 o -3 0 1 1101.05 949.39 37.34 o 1 0 1 3533.57 3339.93 77.39 o 3 0 1 1503.24 1719.04 51.49 o 5 0 1 4420.31 4670.58 154.54 o 7 0 1 40430.30 42711.79 802.36 o 9 0 1 252.50 412.28 56.15 o 11 0 1 78.97 145.20 37.44 o 13 0 1 2878.73 2917.66 186.57 o 15 0 1 1819.49 1595.98 167.75 o 17 0 1 20.13 3.56 75.42 o -18 1 1 275.27 302.26 67.97 o -17 1 1 22.46 59.72 33.41 o -16 1 1 394.37 353.15 51.06 o -15 1 1 135.07 158.18 31.76 o -14 1 1 2387.70 2228.91 150.06 o -13 1 1 2099.82 1991.42 77.33 o -12 1 1 3586.87 3412.04 89.55 o -11 1 1 2028.27 1980.35 63.65 o -10 1 1 2139.60 2035.86 61.64 o -9 1 1 2308.17 2342.98 64.03 o -8 1 1 3720.52 3723.43 89.26 o -7 1 1 4089.57 4273.78 93.28 o -6 1 1 56699.80 63553.93 914.73 o -5 1 1 3132.53 3154.21 67.39 o -4 1 1 668.13 686.65 25.03 o -3 1 1 68.92 91.23 9.17 o -2 1 1 18181.47 21536.10 453.96 o -1 1 1 10491.77 12002.12 289.22 o 1 1 1 4888.45 5808.64 104.68 o 2 1 1 8250.92 8775.67 126.89 o 3 1 1 5236.64 5519.13 107.27 o 4 1 1 5.95 15.16 8.09 o 5 1 1 15339.34 16702.61 234.02 o 6 1 1 17412.22 18582.01 261.99 o 7 1 1 501.39 677.18 33.60 o 8 1 1 14193.36 14915.37 227.39 o 9 1 1 2798.29 2678.45 69.75 o 10 1 1 1530.47 1509.22 53.67 o 11 1 1 447.34 497.43 35.98 o 12 1 1 2806.69 2535.07 105.36 o 13 1 1 2614.12 2469.67 78.78 o 14 1 1 3.71 48.64 26.46 o 15 1 1 360.80 451.47 47.27 o 16 1 1 796.17 823.79 57.69 o 17 1 1 192.11 205.77 44.37 o -18 2 1 10.87 88.01 39.15 o -17 2 1 0.05 47.55 33.25 o -16 2 1 910.96 874.49 53.99 o -15 2 1 968.26 973.27 56.74 o -14 2 1 2106.34 2113.72 72.92 o -13 2 1 66.50 116.10 26.25 o -12 2 1 1427.39 1368.64 54.42 o -11 2 1 132.55 112.01 24.96 o -10 2 1 538.56 531.44 36.78 o -9 2 1 25.42 17.77 15.09 o -8 2 1 21021.62 21344.63 304.11 o -7 2 1 10908.86 11097.00 170.94 o -6 2 1 1502.12 1602.89 42.28 o -5 2 1 57.04 47.23 15.52 o -4 2 1 4128.11 4108.77 69.03 o -3 2 1 3152.63 3249.09 66.43 o -2 2 1 9691.67 11004.37 206.70 o -1 2 1 14698.67 16523.36 248.57 o 0 2 1 19949.79 23907.31 334.90 o 1 2 1 246.71 312.36 13.62 o 2 2 1 4256.71 4719.17 106.08 o 3 2 1 90.53 111.71 12.44 o 4 2 1 2.99 36.81 9.84 o 5 2 1 201.18 209.46 16.08 o 6 2 1 9560.85 10239.34 159.52 o 7 2 1 5197.17 5592.43 163.34 o 8 2 1 56.67 91.45 18.28 o 9 2 1 554.22 519.86 37.10 o 10 2 1 938.86 905.88 41.60 o 11 2 1 56.00 61.98 19.85 o 12 2 1 1073.45 995.77 48.34 o 13 2 1 1891.88 1743.26 102.21 o 14 2 1 2486.56 2371.53 82.18 o 15 2 1 133.81 206.43 41.01 o 16 2 1 25.66 41.41 42.32 o 17 2 1 9.44 -20.97 32.45 o -18 3 1 131.82 209.09 45.96 o -17 3 1 207.98 198.41 64.29 o -16 3 1 107.07 98.72 36.86 o -15 3 1 2.66 41.63 29.48 o -14 3 1 108.59 148.00 29.69 o -13 3 1 5113.70 5005.85 146.79 o -12 3 1 3.21 16.87 19.87 o -11 3 1 145.76 160.29 24.57 o -10 3 1 160.01 197.73 25.10 o -9 3 1 5715.67 5735.96 127.64 o -8 3 1 41.86 72.15 17.17 o -7 3 1 6137.91 5845.21 104.37 o -5 3 1 15802.14 17229.87 247.91 o -4 3 1 1195.08 1204.50 37.64 o -3 3 1 52.72 39.68 11.17 o -2 3 1 14127.81 15525.08 364.40 o -1 3 1 12763.70 13427.11 184.72 o 0 3 1 2944.84 2925.45 55.86 o 1 3 1 13671.13 14532.51 214.01 o 2 3 1 13014.94 13704.91 204.57 o 3 3 1 4258.05 4360.02 75.66 o 4 3 1 363.16 363.72 36.31 o 5 3 1 6874.43 6724.13 115.65 o 6 3 1 172.96 181.37 18.88 o 7 3 1 1038.81 1007.93 42.46 o 8 3 1 291.12 312.53 35.17 o 9 3 1 6024.18 5629.22 116.54 o 10 3 1 139.22 187.86 26.01 o 11 3 1 374.69 374.73 35.05 o 12 3 1 630.59 650.78 53.14 o 13 3 1 3671.08 3603.53 112.02 o 14 3 1 123.37 108.33 39.32 o 15 3 1 1493.16 1411.55 129.21 o 16 3 1 0.12 43.21 42.56 o 17 3 1 188.49 167.88 45.19 o -17 4 1 77.72 209.98 54.05 o -16 4 1 70.99 155.37 49.04 o -15 4 1 259.38 246.54 43.08 o -14 4 1 519.96 616.48 53.41 o -13 4 1 159.86 206.26 38.74 o -12 4 1 1164.66 1245.21 79.35 o -11 4 1 811.29 818.32 39.61 o -10 4 1 6.60 23.48 15.42 o -9 4 1 59.24 49.54 15.90 o -8 4 1 3650.47 3357.00 74.03 o -7 4 1 1324.00 1549.34 43.70 o -6 4 1 2384.21 2365.28 52.80 o -5 4 1 228.66 312.40 26.13 o -4 4 1 204.73 175.41 17.67 o -3 4 1 449.71 399.55 30.58 o -2 4 1 2531.18 2598.25 108.99 o -1 4 1 952.35 913.57 30.14 o 0 4 1 21621.25 23319.39 336.21 o 1 4 1 516.65 463.39 29.65 o 2 4 1 14464.09 14972.73 225.47 o 3 4 1 42.31 70.25 9.89 o 4 4 1 817.13 683.51 25.34 o 5 4 1 18.75 50.09 11.84 o 6 4 1 12892.02 13019.33 202.72 o 7 4 1 2021.01 1899.94 106.04 o 8 4 1 427.87 375.43 31.08 o 9 4 1 23.05 34.65 16.76 o 10 4 1 343.58 307.35 29.54 o 11 4 1 324.16 340.54 34.26 o 12 4 1 44.01 45.39 21.49 o 13 4 1 592.87 618.76 69.06 o 14 4 1 4775.34 4694.46 178.41 o 15 4 1 255.00 234.93 65.44 o 16 4 1 0.03 -27.13 40.99 o 17 4 1 9.78 25.35 35.52 o -17 5 1 74.50 83.19 42.94 o -16 5 1 48.82 72.70 41.19 o -15 5 1 5.19 71.85 40.26 o -14 5 1 2529.09 2377.22 125.09 o -13 5 1 1607.12 1760.33 78.45 o -12 5 1 6.76 59.16 27.44 o -11 5 1 286.81 331.56 40.19 o -10 5 1 590.69 659.29 42.82 o -9 5 1 1732.38 1642.01 101.50 o -8 5 1 258.75 299.79 23.51 o -7 5 1 5290.25 5202.65 123.94 o -6 5 1 5015.15 4749.59 111.57 o -5 5 1 604.17 534.80 29.86 o -4 5 1 38.28 13.01 11.88 o -3 5 1 422.36 402.79 46.26 o -2 5 1 8049.92 8060.96 126.95 o -1 5 1 898.85 845.65 38.01 o 0 5 1 324.57 366.90 18.33 o 1 5 1 10441.84 10998.37 181.00 o 2 5 1 9308.44 9428.25 150.63 o 3 5 1 333.79 338.02 31.28 o 4 5 1 3550.54 3526.33 68.63 o 5 5 1 3108.30 3184.57 66.01 o 6 5 1 5946.58 5601.03 103.91 o 7 5 1 367.34 395.23 28.31 o 8 5 1 6043.47 5769.39 152.77 o 9 5 1 3751.35 3716.19 88.03 o 10 5 1 39.85 71.78 18.78 o 11 5 1 166.35 191.87 36.65 o 12 5 1 2355.95 2104.08 88.89 o 13 5 1 2212.19 2173.61 116.02 o 14 5 1 55.74 82.14 56.52 o 15 5 1 687.67 786.96 141.69 o 16 5 1 690.49 527.60 103.08 o 17 5 1 145.55 312.49 125.16 o -17 6 1 160.21 217.35 57.35 o -16 6 1 22.37 60.99 40.61 o -15 6 1 3005.58 2710.83 135.00 o -14 6 1 90.35 184.35 49.30 o -13 6 1 172.39 199.53 39.14 o -12 6 1 569.22 630.03 51.86 o -11 6 1 14.96 48.12 27.19 o -10 6 1 190.46 203.78 34.20 o -9 6 1 5864.06 5698.89 137.81 o -8 6 1 517.63 497.08 41.25 o -7 6 1 14432.10 13765.03 324.80 o -6 6 1 365.22 411.19 32.64 o -5 6 1 6678.40 6369.80 175.19 o -4 6 1 650.76 606.68 33.11 o -3 6 1 56.23 58.63 27.52 o -2 6 1 1632.72 1542.96 41.08 o -1 6 1 60093.98 63788.26 998.29 o 0 6 1 5020.96 5222.43 96.55 o 1 6 1 4961.53 5408.30 99.33 o 2 6 1 2.49 15.75 17.79 o 3 6 1 12673.44 13087.33 203.51 o 4 6 1 340.44 320.49 43.48 o 5 6 1 80.61 109.66 21.79 o 6 6 1 21.44 49.02 10.95 o 7 6 1 12837.00 12512.23 203.05 o 8 6 1 960.40 867.40 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