#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:49:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181297 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237548.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237548_Fobs loop_ _publ_author_name 'Yang, Xiao-Zhen' 'Hu, Ai-Yun' 'Yuan, Ai-Hua' _publ_section_title ; 4,4'-(Ethene-1,2-diyl)dipyridinium 4-[2-(pyridin-4-yl)ethenyl]pyridinium octacyanidomolybdate(V) tetrahydrate ; _journal_coeditor_code RZ5039 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m132 _journal_volume 69 _journal_year 2013 _space_group_IT_number 68 _symmetry_space_group_name_Hall '-C 2a 2ac' _symmetry_space_group_name_H-M 'C c c a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.4027 _cell_length_b 16.5342 _cell_length_c 15.3695 _exptl_crystal_F_000 1524.00 _reflns_d_resolution_high 0.8304 _cod_data_source_file rz5039Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8 in Ccca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z' 'x, -y+1/2, -z+1/2' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z' 'x+1/2, -y+1, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y-1/2, -z' '-x, y-1/2, z-1/2' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z' '-x+1/2, y, z-1/2' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 5933.52 5572.19 103.38 o 10 0 0 13300.84 13469.25 223.02 o 12 0 0 771.66 430.68 129.52 o 14 0 0 432.32 541.08 118.25 o 4 2 0 18014.30 17621.68 83.89 o 6 2 0 1557.48 1233.05 31.22 o 8 2 0 7058.71 6805.33 96.20 o 10 2 0 10470.29 10463.66 128.92 o 12 2 0 4565.62 4604.49 103.82 o 14 2 0 3699.16 3767.99 102.84 o 0 4 0 860.55 1020.67 23.89 o 2 4 0 30488.96 29824.81 184.05 o 4 4 0 46978.00 47622.18 196.40 o 6 4 0 3841.70 3656.47 40.78 o 8 4 0 4501.07 4092.82 50.34 o 10 4 0 6726.33 6916.42 76.11 o 12 4 0 3426.64 3391.55 85.61 o 14 4 0 4735.74 4762.27 89.24 o 0 6 0 5935.97 4991.95 59.09 o 2 6 0 1952.75 1681.11 31.37 o 4 6 0 30375.03 31294.73 146.76 o 6 6 0 45439.00 46349.14 400.46 o 8 6 0 497.40 389.89 32.47 o 10 6 0 29.60 24.22 5.77 o 12 6 0 11994.22 12291.97 251.43 o 14 6 0 7961.39 7924.34 200.30 o 0 8 0 4937.23 6037.67 74.24 o 2 8 0 11791.25 11388.79 102.17 o 4 8 0 54759.76 56158.22 299.33 o 6 8 0 8052.44 8028.03 82.42 o 8 8 0 136.14 148.36 15.99 o 10 8 0 5940.28 5871.75 90.66 o 12 8 0 8062.35 8393.69 160.17 o 0 10 0 4993.90 5839.74 157.92 o 2 10 0 14184.28 13945.80 128.62 o 4 10 0 8298.36 7710.99 81.08 o 6 10 0 1495.51 1457.45 45.13 o 8 10 0 10811.12 10757.63 115.26 o 10 10 0 11372.69 11724.96 298.09 o 12 10 0 463.41 460.15 60.15 o 0 12 0 10611.50 10244.19 125.57 o 2 12 0 3226.52 3137.40 44.47 o 4 12 0 4553.19 4569.13 78.42 o 6 12 0 15487.64 15752.52 150.59 o 8 12 0 6483.21 6417.28 251.96 o 10 12 0 665.78 546.08 103.00 o 0 14 0 1783.74 1942.19 124.39 o 2 14 0 4519.93 4679.57 112.66 o 4 14 0 9571.58 9449.13 138.88 o 6 14 0 6710.50 6895.55 193.04 o 8 14 0 2514.26 2428.95 86.59 o 10 14 0 2588.21 2537.97 104.27 o 0 16 0 3498.12 3599.93 122.84 o 2 16 0 4965.79 5074.17 102.43 o 4 16 0 4444.24 4617.62 271.05 o 6 16 0 2829.88 2787.04 89.00 o 8 16 0 4058.62 3876.66 84.25 o 0 18 0 7060.20 7014.48 171.63 o 2 18 0 3826.81 4029.83 223.81 o 4 18 0 1577.08 1670.98 66.36 o 6 18 0 2508.07 2394.42 86.76 o 3 1 1 49725.46 48385.46 387.01 o 5 1 1 22672.99 22530.91 75.50 o 7 1 1 526.25 317.92 26.57 o 9 1 1 1974.53 1902.62 29.93 o 11 1 1 17067.89 16942.12 94.74 o 13 1 1 9627.09 9486.68 109.50 o 2 2 1 14824.12 14323.39 56.95 o 4 2 1 4522.91 4282.58 32.54 o 6 2 1 5790.53 6306.60 54.34 o 8 2 1 3840.59 3914.88 33.56 o 10 2 1 1950.76 2000.92 29.50 o 12 2 1 2650.15 2456.97 40.11 o 14 2 1 664.92 501.47 38.00 o 1 3 1 40509.88 39972.39 583.85 o 3 3 1 16124.35 16224.76 57.26 o 5 3 1 3546.56 2988.66 29.99 o 7 3 1 7971.79 7801.02 44.27 o 9 3 1 13421.43 13629.50 73.46 o 11 3 1 4551.10 4616.81 54.00 o 13 3 1 2155.43 2223.28 46.59 o 2 4 1 4034.96 4497.99 22.38 o 4 4 1 3414.85 3449.49 21.28 o 6 4 1 1484.39 1487.66 17.47 o 8 4 1 1599.72 1702.74 22.94 o 10 4 1 311.82 302.32 18.02 o 12 4 1 238.60 250.09 25.34 o 14 4 1 171.80 164.65 19.99 o 1 5 1 1069.70 919.86 10.68 o 3 5 1 39835.44 39708.14 126.25 o 5 5 1 27824.85 27183.90 132.89 o 7 5 1 4536.42 4368.41 31.74 o 9 5 1 2810.82 2936.96 36.58 o 11 5 1 4680.49 4750.53 74.02 o 13 5 1 4453.34 4511.27 60.60 o 2 6 1 1683.29 1986.77 16.73 o 4 6 1 21.54 27.48 4.41 o 6 6 1 9.97 15.44 6.51 o 8 6 1 3.56 4.78 5.43 o 10 6 1 572.75 532.29 31.97 o 12 6 1 73.37 58.52 13.18 o 14 6 1 462.43 361.31 55.02 o 1 7 1 27076.19 27767.92 93.17 o 3 7 1 1621.09 1217.45 14.92 o 5 7 1 8318.43 7668.72 43.31 o 7 7 1 18404.04 18796.90 118.66 o 9 7 1 6066.57 6283.78 82.22 o 11 7 1 2038.26 2096.91 32.30 o 13 7 1 1855.14 1990.21 59.39 o 2 8 1 15185.40 16487.89 88.21 o 4 8 1 543.03 625.54 17.26 o 6 8 1 3935.89 4276.44 37.25 o 8 8 1 684.97 678.09 23.07 o 10 8 1 561.78 497.47 34.17 o 12 8 1 224.95 199.54 24.46 o 1 9 1 11723.91 11234.94 62.84 o 3 9 1 7273.32 7234.24 43.85 o 5 9 1 7569.23 7500.90 56.28 o 7 9 1 9278.07 9401.57 79.35 o 9 9 1 6916.19 6865.12 57.50 o 11 9 1 2584.34 2734.71 49.86 o 13 9 1 1601.91 1584.13 67.38 o 2 10 1 8141.77 8613.88 49.84 o 4 10 1 572.38 564.53 18.70 o 6 10 1 2604.19 2733.93 34.13 o 8 10 1 351.97 300.38 31.51 o 10 10 1 450.73 395.89 34.28 o 12 10 1 39.69 28.19 10.05 o 1 11 1 4554.97 4308.19 33.88 o 3 11 1 13748.46 14008.89 98.51 o 5 11 1 5867.22 6048.06 61.39 o 7 11 1 4098.23 4053.95 43.88 o 9 11 1 7812.20 7794.35 153.01 o 11 11 1 3332.94 3327.92 73.02 o 2 12 1 148.17 170.94 12.66 o 4 12 1 493.16 503.77 30.98 o 6 12 1 215.95 194.77 18.23 o 8 12 1 448.40 339.58 29.99 o 10 12 1 221.50 206.24 35.93 o 1 13 1 8632.10 8264.00 79.78 o 3 13 1 1592.36 1701.74 34.22 o 5 13 1 7091.64 7213.98 90.45 o 7 13 1 12104.79 11878.42 204.05 o 9 13 1 2391.53 2404.26 46.65 o 11 13 1 621.49 573.96 43.33 o 2 14 1 45.11 38.89 9.94 o 4 14 1 39.50 58.72 10.31 o 6 14 1 85.93 93.22 18.86 o 8 14 1 0.67 16.27 8.93 o 10 14 1 106.65 93.00 25.34 o 1 15 1 7522.23 7448.98 109.65 o 3 15 1 1125.82 1261.99 55.72 o 5 15 1 4503.82 4542.17 92.41 o 7 15 1 11099.61 11114.91 121.04 o 9 15 1 2979.41 2932.11 53.59 o 2 16 1 741.36 678.82 43.43 o 4 16 1 16.99 33.51 14.42 o 6 16 1 3.93 9.02 11.02 o 8 16 1 28.98 49.79 12.95 o 1 17 1 1378.09 1473.41 39.83 o 3 17 1 8572.39 8842.20 112.38 o 5 17 1 4849.41 4996.36 101.92 o 7 17 1 1534.07 1429.67 42.92 o 2 18 1 17.26 19.91 17.39 o 4 18 1 570.29 531.59 42.11 o 6 18 1 17.59 15.89 11.90 o 1 19 1 7255.68 7554.36 113.32 o 3 19 1 1317.94 1246.31 41.75 o 2 0 2 19786.03 19285.26 121.74 o 4 0 2 20845.75 20128.35 91.18 o 6 0 2 15002.26 14471.06 80.07 o 8 0 2 6167.16 5991.28 111.66 o 10 0 2 4017.74 4156.94 63.84 o 12 0 2 4704.26 5032.85 76.14 o 14 0 2 4657.52 4319.10 165.73 o 1 1 2 6079.31 5446.32 45.45 o 3 1 2 30115.80 29569.19 101.95 o 5 1 2 53.24 69.64 6.72 o 7 1 2 18465.20 19193.56 82.49 o 9 1 2 77.61 99.59 9.47 o 11 1 2 7166.42 6915.09 59.78 o 13 1 2 304.10 266.26 34.43 o 2 2 2 21011.05 20999.40 81.56 o 4 2 2 2607.92 2204.22 20.70 o 6 2 2 10503.46 9822.45 65.08 o 8 2 2 14204.37 14430.92 83.38 o 10 2 2 6197.44 6413.74 48.93 o 12 2 2 2976.60 3055.17 40.31 o 14 2 2 2909.15 2822.30 62.04 o 1 3 2 2550.67 2956.01 36.57 o 3 3 2 4579.48 4934.25 29.07 o 5 3 2 83.59 152.71 12.27 o 7 3 2 1151.26 1251.93 23.74 o 9 3 2 21.40 24.63 5.38 o 11 3 2 81.28 78.73 9.52 o 13 3 2 145.06 151.90 19.94 o 2 4 2 17829.27 17466.78 57.91 o 4 4 2 14581.59 14732.33 54.41 o 6 4 2 10482.45 9937.34 55.27 o 8 4 2 8983.81 8619.63 62.38 o 10 4 2 4851.52 4940.55 45.98 o 12 4 2 2880.34 3075.80 66.23 o 14 4 2 3583.31 3646.99 65.04 o 1 5 2 47535.52 48656.73 303.65 o 3 5 2 23005.06 24318.06 94.78 o 5 5 2 11475.49 11999.43 62.76 o 7 5 2 1667.88 1752.16 20.20 o 9 5 2 568.38 584.95 23.35 o 11 5 2 12.70 24.73 6.51 o 13 5 2 0.13 15.34 7.29 o 0 6 2 14156.31 14493.59 98.72 o 2 6 2 13747.43 12856.79 50.43 o 4 6 2 11614.13 10899.26 51.60 o 6 6 2 10699.17 10676.69 60.18 o 8 6 2 8255.39 8385.70 54.10 o 10 6 2 4253.80 4167.21 52.23 o 12 6 2 2458.14 2533.93 43.02 o 14 6 2 2892.00 3003.77 79.35 o 1 7 2 1166.04 1102.18 17.94 o 3 7 2 1171.00 1215.58 15.15 o 5 7 2 4585.28 4677.73 31.31 o 7 7 2 1135.51 1130.96 19.82 o 9 7 2 2636.00 2557.91 31.56 o 11 7 2 87.42 76.68 11.82 o 13 7 2 524.79 440.53 46.97 o 0 8 2 18347.75 17415.27 95.99 o 2 8 2 8523.10 8140.88 48.57 o 4 8 2 7307.64 7389.43 42.61 o 6 8 2 12616.01 12927.12 85.68 o 8 8 2 5930.37 5844.86 60.09 o 10 8 2 2998.46 3008.85 39.75 o 12 8 2 4201.80 4243.36 58.47 o 1 9 2 2878.18 3195.88 27.36 o 3 9 2 729.60 892.97 19.39 o 5 9 2 3503.65 3838.75 39.73 o 7 9 2 273.29 329.14 21.62 o 9 9 2 1666.57 1633.26 35.71 o 11 9 2 465.93 376.24 41.15 o 13 9 2 397.76 279.87 36.34 o 0 10 2 5327.31 5036.86 51.19 o 2 10 2 11077.65 10749.14 79.83 o 4 10 2 10987.68 11162.71 77.37 o 6 10 2 3830.52 3907.26 43.76 o 8 10 2 4979.31 4944.43 58.11 o 10 10 2 6158.60 6038.87 118.33 o 12 10 2 2750.28 2832.46 77.86 o 1 11 2 130.93 166.97 13.36 o 3 11 2 319.02 303.31 18.19 o 5 11 2 198.95 187.31 16.55 o 7 11 2 1097.01 1089.61 39.47 o 9 11 2 8.82 17.65 9.00 o 11 11 2 860.83 855.16 42.65 o 0 12 2 9970.34 10419.40 88.80 o 2 12 2 9792.22 9898.12 82.74 o 4 12 2 4161.93 3992.76 49.73 o 6 12 2 1816.98 1716.12 43.29 o 8 12 2 6553.47 6681.05 75.60 o 10 12 2 8342.69 8518.28 217.76 o 1 13 2 1436.05 1489.57 31.68 o 3 13 2 1600.60 1566.48 28.91 o 5 13 2 148.28 176.49 15.26 o 7 13 2 499.53 474.70 31.99 o 9 13 2 42.89 38.32 9.74 o 11 13 2 2.44 17.19 11.59 o 0 14 2 506.74 696.16 71.56 o 2 14 2 3384.99 3461.95 68.01 o 4 14 2 15985.12 16353.75 127.92 o 6 14 2 10065.68 10147.68 122.47 o 8 14 2 77.12 79.39 21.23 o 10 14 2 692.33 618.84 45.98 o 1 15 2 130.72 117.74 18.53 o 3 15 2 228.33 189.81 23.19 o 5 15 2 45.70 42.24 11.61 o 7 15 2 0.83 10.49 10.51 o 9 15 2 320.94 243.48 39.32 o 0 16 2 73.83 42.97 40.56 o 2 16 2 4094.97 4157.40 89.18 o 4 16 2 16384.50 15999.11 170.76 o 6 16 2 4552.32 4571.68 103.23 o 8 16 2 239.10 214.05 42.30 o 1 17 2 249.99 262.75 36.27 o 3 17 2 27.33 30.75 12.59 o 5 17 2 653.80 611.46 41.18 o 7 17 2 54.58 39.86 14.24 o 0 18 2 2367.36 2175.99 91.32 o 2 18 2 4387.23 4409.27 87.29 o 4 18 2 4091.73 4354.74 64.67 o 6 18 2 1512.43 1498.74 56.23 o 1 19 2 185.60 139.58 35.03 o 3 19 2 124.44 84.49 22.69 o 1 1 3 21022.84 19881.35 76.51 o 3 1 3 14984.47 15171.37 119.76 o 5 1 3 16123.17 15639.43 56.87 o 7 1 3 7627.43 7295.23 40.13 o 9 1 3 6605.80 6639.33 57.25 o 11 1 3 9290.38 9374.42 88.73 o 13 1 3 2846.70 2940.58 51.94 o 2 2 3 19978.46 21708.18 123.19 o 4 2 3 6347.03 6717.08 31.40 o 6 2 3 4049.77 4313.77 32.30 o 8 2 3 3249.21 3344.04 30.59 o 10 2 3 425.03 426.45 24.36 o 12 2 3 294.67 288.59 30.18 o 14 2 3 67.81 28.04 10.80 o 1 3 3 766.43 948.23 9.68 o 5 3 3 26962.14 27466.35 100.97 o 7 3 3 776.55 667.81 15.11 o 9 3 3 6153.49 6160.54 56.48 o 11 3 3 7649.37 7512.75 59.22 o 13 3 3 2282.00 2315.83 57.06 o 2 4 3 1844.52 1862.23 14.57 o 4 4 3 567.69 615.62 15.64 o 6 4 3 119.64 177.95 12.31 o 8 4 3 912.91 880.71 15.70 o 10 4 3 1108.96 1092.14 24.69 o 12 4 3 646.39 569.63 54.78 o 14 4 3 619.07 541.29 60.81 o 1 5 3 23547.19 23033.01 74.26 o 3 5 3 3710.83 3379.44 28.22 o 5 5 3 12795.14 12548.93 68.98 o 7 5 3 17770.47 17885.13 82.17 o 9 5 3 4248.34 4299.93 46.11 o 11 5 3 1713.95 1729.19 28.34 o 13 5 3 4025.64 4058.55 92.39 o 2 6 3 5043.90 5024.56 40.13 o 4 6 3 43.06 79.96 7.58 o 6 6 3 51.19 41.36 8.32 o 8 6 3 16.46 21.00 5.05 o 10 6 3 635.13 616.27 33.77 o 12 6 3 8.48 10.60 10.96 o 14 6 3 502.04 429.08 49.89 o 1 7 3 16581.13 15627.56 66.20 o 3 7 3 5036.43 4816.46 32.80 o 5 7 3 13998.20 14091.65 75.53 o 7 7 3 12095.70 12353.01 68.07 o 9 7 3 1858.94 1748.22 31.68 o 11 7 3 2290.86 2317.30 59.13 o 13 7 3 6366.14 6623.88 212.72 o 2 8 3 141.47 214.94 15.42 o 4 8 3 3788.46 4001.13 30.18 o 6 8 3 201.02 224.05 16.33 o 8 8 3 3147.05 3066.61 37.08 o 10 8 3 229.85 197.39 23.44 o 12 8 3 550.40 513.95 56.91 o 1 9 3 24328.84 24871.56 104.91 o 3 9 3 7853.92 7392.77 44.13 o 5 9 3 133.18 124.55 11.98 o 7 9 3 5359.59 5381.49 55.96 o 9 9 3 15919.46 16238.89 220.57 o 11 9 3 3789.81 3744.67 64.67 o 13 9 3 381.88 352.76 48.52 o 2 10 3 5509.54 6114.56 45.73 o 4 10 3 191.67 240.86 16.54 o 6 10 3 2365.73 2387.00 43.33 o 8 10 3 178.24 196.10 19.68 o 10 10 3 533.98 572.82 35.91 o 12 10 3 67.40 71.35 15.11 o 1 11 3 14869.72 15198.35 100.51 o 3 11 3 3745.60 3689.85 32.71 o 5 11 3 4651.58 4612.10 52.24 o 7 11 3 5940.20 5908.78 88.30 o 9 11 3 2929.33 2799.14 54.61 o 11 11 3 3544.67 3520.90 97.56 o 2 12 3 27.06 49.99 6.71 o 4 12 3 613.23 623.64 35.14 o 6 12 3 13.92 26.62 8.09 o 8 12 3 541.54 509.11 38.03 o 10 12 3 71.61 66.24 15.32 o 1 13 3 11460.27 11929.14 121.27 o 3 13 3 3055.90 2975.29 43.25 o 5 13 3 2934.51 2779.07 43.47 o 7 13 3 5707.59 5831.88 83.44 o 9 13 3 4151.98 4073.69 61.21 o 11 13 3 2199.72 2045.72 71.26 o 2 14 3 10299.56 9983.63 148.72 o 4 14 3 339.49 342.47 38.02 o 6 14 3 4195.60 4127.46 79.29 o 8 14 3 542.17 480.47 47.31 o 10 14 3 703.96 564.33 62.40 o 1 15 3 4857.14 4839.00 62.14 o 3 15 3 6476.35 6786.73 90.66 o 5 15 3 2726.28 2817.92 64.95 o 7 15 3 2506.19 2442.55 50.26 o 9 15 3 4973.79 4851.19 112.40 o 2 16 3 216.82 176.63 26.70 o 4 16 3 1.04 15.40 9.94 o 6 16 3 823.34 739.52 34.10 o 8 16 3 6.14 15.38 7.59 o 1 17 3 5306.87 5440.64 79.66 o 3 17 3 1951.03 2103.26 53.91 o 5 17 3 3197.23 3216.77 75.71 o 7 17 3 4977.23 4800.51 95.39 o 2 18 3 0.70 22.44 10.87 o 4 18 3 209.27 157.46 37.25 o 1 19 3 3068.37 3182.43 55.65 o 3 19 3 2728.18 2661.07 62.63 o 0 0 4 10426.74 9822.90 99.96 o 2 0 4 16827.23 16011.38 71.11 o 6 0 4 12444.35 12245.05 103.90 o 8 0 4 12581.88 12542.78 115.41 o 10 0 4 6309.42 6363.85 77.80 o 12 0 4 1787.06 1820.42 106.02 o 14 0 4 1539.68 1365.45 174.12 o 1 1 4 860.19 1030.46 12.32 o 3 1 4 3273.51 3262.14 20.98 o 5 1 4 34.72 43.13 4.23 o 7 1 4 1800.28 1853.00 17.15 o 9 1 4 522.98 541.30 21.51 o 11 1 4 748.10 710.50 22.01 o 13 1 4 687.01 585.67 41.72 o 0 2 4 18758.19 17965.64 80.43 o 2 2 4 9199.56 8931.55 51.36 o 4 2 4 11501.78 11034.99 52.20 o 6 2 4 21378.14 21195.27 99.47 o 8 2 4 12820.79 12686.33 82.45 o 10 2 4 2728.92 2785.23 30.86 o 12 2 4 1391.70 1455.75 59.32 o 14 2 4 3216.49 3245.60 64.11 o 1 3 4 9349.23 9985.43 37.04 o 3 3 4 5500.46 5724.39 29.44 o 5 3 4 3066.33 3068.56 29.41 o 7 3 4 1147.27 1156.36 14.97 o 9 3 4 157.40 132.00 12.20 o 11 3 4 261.89 244.39 21.17 o 13 3 4 96.16 97.40 16.64 o 0 4 4 2627.51 2847.05 28.18 o 2 4 4 7913.22 7498.50 32.14 o 4 4 4 26136.61 25117.33 108.55 o 6 4 4 22449.10 22752.84 92.81 o 8 4 4 5182.51 5206.26 35.58 o 10 4 4 1255.80 1265.09 24.61 o 12 4 4 3420.13 3418.47 73.61 o 14 4 4 5198.71 5303.46 118.47 o 1 5 4 5437.85 5517.92 28.01 o 3 5 4 3889.28 4210.56 29.62 o 5 5 4 3512.70 3519.49 25.53 o 7 5 4 2191.50 2176.08 25.27 o 9 5 4 1809.03 1726.72 24.06 o 11 5 4 987.42 903.61 27.22 o 13 5 4 724.49 735.03 71.98 o 0 6 4 29118.73 29702.78 138.48 o 2 6 4 15873.39 15325.38 62.65 o 4 6 4 2755.53 2415.90 21.54 o 6 6 4 6155.46 6022.35 37.72 o 8 6 4 14112.39 14390.56 118.85 o 10 6 4 6276.16 6358.35 50.63 o 12 6 4 970.14 1053.75 70.69 o 1 7 4 3209.58 3318.26 23.80 o 3 7 4 1636.03 1750.15 18.47 o 5 7 4 620.07 654.07 14.05 o 7 7 4 103.48 116.63 10.46 o 9 7 4 12.78 17.68 5.38 o 11 7 4 45.90 35.88 8.03 o 13 7 4 199.10 169.49 32.03 o 0 8 4 22587.47 23242.34 156.39 o 2 8 4 13328.37 13144.19 70.05 o 4 8 4 5304.84 4909.50 34.28 o 6 8 4 3714.48 3597.05 48.73 o 8 8 4 5231.16 5241.35 47.75 o 10 8 4 6772.79 6787.51 85.11 o 12 8 4 4811.76 4921.71 106.31 o 1 9 4 289.41 259.11 15.83 o 3 9 4 715.52 805.63 16.25 o 5 9 4 1267.31 1324.83 24.23 o 7 9 4 1849.89 1742.28 29.52 o 9 9 4 624.60 600.23 43.97 o 11 9 4 883.92 891.64 83.27 o 0 10 4 26853.24 26422.94 322.44 o 2 10 4 12527.44 12615.16 88.41 o 4 10 4 1927.25 1905.69 24.47 o 6 10 4 1508.65 1467.97 27.95 o 8 10 4 5274.75 5298.75 51.19 o 10 10 4 8494.67 8721.99 100.73 o 12 10 4 4770.61 4644.04 82.81 o 1 11 4 28.41 32.15 6.79 o 3 11 4 25.17 34.30 6.08 o 5 11 4 198.63 157.63 14.14 o 7 11 4 118.26 122.87 15.63 o 9 11 4 198.53 177.44 26.37 o 11 11 4 60.46 45.44 18.32 o 0 12 4 1150.03 1120.48 45.36 o 2 12 4 9062.58 9176.08 95.09 o 4 12 4 16338.65 16906.74 128.52 o 6 12 4 2670.67 2622.54 38.25 o 8 12 4 172.74 154.44 20.02 o 10 12 4 4076.02 4065.16 103.19 o 1 13 4 7675.92 7409.92 91.99 o 3 13 4 3119.38 3060.70 45.27 o 5 13 4 7079.24 6905.25 61.81 o 7 13 4 739.07 670.69 42.03 o 9 13 4 3177.81 3126.99 65.58 o 0 14 4 1338.55 1425.43 105.53 o 2 14 4 5862.78 5968.50 59.18 o 4 14 4 11951.00 11985.78 94.95 o 6 14 4 3472.23 3433.50 67.09 o 8 14 4 421.49 415.61 55.02 o 10 14 4 2649.87 2638.54 83.31 o 1 15 4 1759.99 1688.88 48.35 o 3 15 4 534.70 613.98 57.77 o 5 15 4 1126.39 1166.33 46.92 o 7 15 4 6.39 22.32 11.08 o 9 15 4 134.31 127.73 29.80 o 0 16 4 4210.10 4316.95 127.13 o 2 16 4 4308.62 4477.73 94.20 o 4 16 4 4239.66 4229.00 90.39 o 6 16 4 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6 4.14 14.91 13.06 o 0 8 6 829.49 956.14 28.12 o 2 8 6 12636.28 12458.13 63.14 o 4 8 6 34815.40 35463.63 217.86 o 6 8 6 3267.05 3349.81 38.14 o 8 8 6 380.29 347.44 18.01 o 10 8 6 5196.42 5401.97 130.70 o 12 8 6 6201.55 6037.82 125.24 o 1 9 6 2226.56 2209.80 26.79 o 3 9 6 1522.63 1483.40 25.70 o 5 9 6 1083.44 1098.14 20.98 o 7 9 6 400.04 427.15 20.62 o 9 9 6 337.42 315.26 28.35 o 11 9 6 86.56 95.93 19.59 o 0 10 6 2673.28 2816.11 41.18 o 2 10 6 6761.24 6771.96 48.07 o 4 10 6 16038.29 16240.50 140.88 o 6 10 6 7200.11 7141.48 64.83 o 8 10 6 132.36 113.33 15.49 o 10 10 6 2579.11 2735.15 101.19 o 1 11 6 1602.05 1567.01 26.43 o 3 11 6 983.20 1021.44 35.58 o 5 11 6 1056.13 1019.85 24.12 o 7 11 6 285.37 291.58 27.15 o 9 11 6 205.33 207.33 31.60 o 11 11 6 117.70 109.40 22.19 o 0 12 6 9821.65 9883.01 113.50 o 2 12 6 6371.35 6437.99 58.68 o 4 12 6 4694.28 4814.83 56.19 o 6 12 6 3785.47 3797.36 42.08 o 8 12 6 2286.91 2191.73 46.21 o 10 12 6 3887.56 3907.84 70.31 o 1 13 6 115.35 95.01 11.85 o 3 13 6 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7 7 3915.84 4001.35 78.98 o 2 8 7 194.96 172.13 12.17 o 4 8 7 387.82 399.58 20.60 o 6 8 7 101.97 91.85 9.00 o 8 8 7 182.85 194.85 17.08 o 10 8 7 14.01 5.96 11.97 o 12 8 7 2.46 5.05 19.97 o 1 9 7 13883.29 13851.65 72.29 o 3 9 7 2482.76 2506.49 26.34 o 5 9 7 4084.59 4134.14 49.67 o 7 9 7 9436.40 9579.42 74.24 o 9 9 7 5993.23 6270.37 140.89 o 11 9 7 1811.85 1743.74 68.32 o 2 10 7 550.82 513.89 25.83 o 4 10 7 628.69 635.69 21.09 o 6 10 7 0.49 11.12 5.31 o 8 10 7 989.70 922.54 50.32 o 10 10 7 217.97 242.87 34.72 o 1 11 7 17619.59 17836.02 167.50 o 3 11 7 131.82 149.28 16.09 o 5 11 7 1774.11 1689.21 28.22 o 7 11 7 15854.33 15820.24 165.89 o 9 11 7 6432.97 6577.05 112.43 o 11 11 7 158.48 173.78 31.28 o 2 12 7 1066.66 1036.52 29.23 o 4 12 7 163.53 183.06 16.44 o 6 12 7 1048.48 1040.42 34.98 o 8 12 7 297.22 290.99 38.57 o 10 12 7 719.80 626.74 62.15 o 1 13 7 748.51 847.49 32.12 o 3 13 7 11671.40 11684.53 107.60 o 5 13 7 9991.75 10061.42 162.31 o 7 13 7 2316.64 2298.84 55.79 o 9 13 7 1185.85 1165.48 53.40 o 2 14 7 340.88 353.80 34.99 o 4 14 7 0.00 11.80 6.61 o 6 14 7 23.27 22.06 9.92 o 8 14 7 15.37 34.19 18.58 o 1 15 7 6691.46 6338.25 194.37 o 3 15 7 2729.56 2731.16 51.21 o 5 15 7 1769.45 1890.58 38.51 o 7 15 7 3798.96 3757.82 76.58 o 2 16 7 20.30 36.74 12.35 o 4 16 7 713.14 692.79 30.87 o 6 16 7 73.83 44.60 33.72 o 1 17 7 3743.68 3523.02 75.12 o 3 17 7 2128.34 2224.65 52.90 o 5 17 7 4480.22 4794.03 106.63 o 2 18 7 2850.12 2693.90 68.99 o 0 0 8 2034.97 2681.88 43.41 o 2 0 8 22898.17 22716.48 147.76 o 4 0 8 45231.35 46105.95 333.26 o 6 0 8 244.86 265.72 29.72 o 8 0 8 775.37 740.01 47.82 o 10 0 8 10462.10 10334.79 155.15 o 12 0 8 5197.09 5553.08 162.70 o 1 1 8 2110.05 2216.22 19.43 o 3 1 8 2975.26 3249.84 21.88 o 5 1 8 120.43 133.44 10.77 o 7 1 8 1834.66 1817.48 48.61 o 9 1 8 30.33 35.69 6.39 o 11 1 8 588.10 544.55 38.74 o 13 1 8 83.66 97.03 23.19 o 0 2 8 25254.20 24839.81 160.92 o 2 2 8 9640.50 9214.97 49.43 o 4 2 8 5101.70 5119.06 38.44 o 6 2 8 10792.04 10471.97 156.16 o 8 2 8 4651.87 4668.35 82.67 o 10 2 8 2335.83 2369.07 54.20 o 12 2 8 5837.02 6052.84 181.00 o 1 3 8 86.54 93.04 7.97 o 3 3 8 125.99 155.76 8.20 o 5 3 8 757.65 742.49 18.56 o 7 3 8 101.80 102.84 11.44 o 9 3 8 702.62 659.85 30.88 o 11 3 8 0.14 16.09 7.97 o 13 3 8 270.15 277.23 38.28 o 0 4 8 70171.11 74558.99 482.61 o 2 4 8 8009.26 7912.18 41.68 o 4 4 8 467.00 788.25 22.48 o 6 4 8 10911.88 10904.92 71.02 o 8 4 8 14920.74 15643.02 125.30 o 10 4 8 2924.58 2844.00 80.60 o 12 4 8 1807.78 2075.30 94.23 o 1 5 8 812.21 959.36 18.02 o 3 5 8 563.13 683.77 11.82 o 5 5 8 754.49 882.81 24.11 o 7 5 8 880.64 938.04 29.06 o 9 5 8 470.63 457.14 64.99 o 11 5 8 923.01 782.04 72.89 o 0 6 8 1079.71 940.40 24.64 o 2 6 8 14313.77 14161.76 67.24 o 4 6 8 16164.89 16851.36 110.68 o 6 6 8 1152.06 1173.75 32.34 o 8 6 8 5490.41 5235.32 115.22 o 10 6 8 9220.51 9472.17 127.84 o 12 6 8 1278.18 1285.82 46.95 o 1 7 8 51.89 69.97 7.39 o 3 7 8 357.84 354.03 18.29 o 5 7 8 60.38 76.76 6.85 o 7 7 8 723.35 752.39 33.52 o 9 7 8 10.46 24.05 8.78 o 11 7 8 771.86 696.72 74.43 o 0 8 8 26406.30 26432.92 226.91 o 2 8 8 6332.50 6353.41 42.25 o 4 8 8 230.70 246.41 16.03 o 6 8 8 8191.54 8080.46 65.99 o 8 8 8 14846.34 14880.55 326.15 o 10 8 8 2883.93 2945.55 78.11 o 12 8 8 260.83 252.59 34.62 o 1 9 8 95.80 98.68 9.25 o 3 9 8 0.67 8.56 5.84 o 5 9 8 144.67 129.51 12.92 o 7 9 8 26.40 18.29 3.86 o 9 9 8 22.16 30.08 15.03 o 11 9 8 5.70 14.63 12.24 o 0 10 8 647.17 714.25 43.24 o 2 10 8 2742.96 2807.33 35.69 o 4 10 8 16162.52 16549.75 116.85 o 6 10 8 15573.07 15881.69 114.10 o 8 10 8 614.28 613.75 48.45 o 10 10 8 324.18 303.08 41.97 o 1 11 8 3470.33 3458.72 39.78 o 3 11 8 4841.20 4777.06 58.27 o 5 11 8 1328.23 1325.71 25.71 o 7 11 8 3638.56 3591.23 128.62 o 9 11 8 165.32 128.71 23.35 o 0 12 8 985.58 1014.00 35.19 o 2 12 8 5465.32 5584.76 66.08 o 4 12 8 23240.74 24000.74 176.67 o 6 12 8 3607.00 3504.30 74.14 o 8 12 8 377.58 369.26 54.37 o 10 12 8 3947.34 4067.04 115.27 o 1 13 8 557.79 584.55 34.26 o 3 13 8 209.18 215.24 25.94 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