#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:49:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181297 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237551.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237551_Fobs loop_ _publ_author_name 'Hu, Ai-Yun' 'Yu, Deng-Yong' 'Yuan, Ai-Hua' _publ_section_title ; Tris(3,4,7,8-tetramethyl-1,10-phenanthrolin-1-ium) hexacyanidocobaltate(III) pentahydrate ; _journal_coeditor_code RZ5042 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m142 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 97.216 _cell_angle_beta 110.934 _cell_angle_gamma 112.179 _cell_length_a 12.8360 _cell_length_b 14.4580 _cell_length_c 16.6450 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file rz5042Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yah225 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 617.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8929.16 8168.96 190.70 o 2 0 0 12979.79 13476.97 166.17 o 3 0 0 10482.40 10702.60 175.01 o 4 0 0 43.07 26.21 8.30 o 5 0 0 976.21 955.46 27.75 o 6 0 0 1389.23 1362.56 35.36 o 7 0 0 597.48 632.41 28.66 o 8 0 0 577.31 514.16 28.66 o 9 0 0 582.02 599.17 42.49 o 10 0 0 298.65 338.76 44.36 o 11 0 0 0.29 0.00 28.23 o 12 0 0 0.17 0.00 28.23 o -13 1 0 442.62 350.85 56.46 o -12 1 0 764.82 738.00 72.59 o -11 1 0 697.14 673.48 64.52 o -10 1 0 500.84 548.44 40.33 o -9 1 0 351.93 356.23 27.09 o -8 1 0 1217.02 1212.02 39.58 o -7 1 0 798.80 863.80 30.99 o -6 1 0 2698.97 2522.92 53.61 o -5 1 0 25.95 12.10 8.30 o -4 1 0 65.68 46.62 11.41 o -3 1 0 3631.48 3529.95 64.11 o -2 1 0 612.05 595.81 13.97 o -1 1 0 1217.68 1153.38 32.26 o 0 1 0 27.67 51.02 4.03 o 1 1 0 11.92 24.51 5.70 o 2 1 0 1122.13 1133.71 77.83 o 3 1 0 136.52 106.04 18.15 o 4 1 0 537.94 638.53 24.11 o 5 1 0 1586.78 1692.85 37.71 o 6 1 0 112.62 130.42 15.12 o 7 1 0 155.43 186.37 19.31 o 8 1 0 1073.84 1064.97 68.56 o 9 1 0 58.74 67.37 24.11 o 10 1 0 460.06 532.33 56.46 o 12 1 0 66.17 76.62 48.39 o -13 2 0 37.09 20.16 32.26 o -12 2 0 12.98 44.36 32.26 o -11 2 0 110.59 88.72 32.26 o -10 2 0 66.47 120.98 32.26 o -9 2 0 964.48 1086.05 40.31 o -8 2 0 81.75 89.72 16.97 o -7 2 0 584.96 569.46 52.43 o -6 2 0 9.40 20.78 10.68 o -5 2 0 8152.73 7953.34 118.97 o -4 2 0 3551.82 3356.47 52.74 o -3 2 0 192.95 136.44 16.00 o -2 2 0 1067.43 1036.47 20.96 o -1 2 0 129.22 104.84 16.13 o 0 2 0 12404.28 12275.59 150.97 o 1 2 0 712.66 711.17 40.33 o 2 2 0 3445.92 3772.70 54.71 o 3 2 0 3302.67 3510.52 54.23 o 4 2 0 2686.76 2516.22 102.84 o 5 2 0 451.97 496.04 26.84 o 7 2 0 28.17 12.10 24.20 o 8 2 0 1540.42 1576.83 96.79 o 9 2 0 198.16 221.58 32.70 o 10 2 0 278.29 326.66 48.39 o 11 2 0 41.96 72.59 40.33 o 12 2 0 6.84 0.00 40.33 o -13 3 0 375.18 330.69 56.46 o -12 3 0 327.60 314.56 48.39 o -11 3 0 217.90 237.50 32.70 o -10 3 0 3820.99 3806.97 133.08 o -9 3 0 767.86 823.29 44.13 o -8 3 0 1688.49 1682.74 44.98 o -7 3 0 860.75 876.20 30.99 o -6 3 0 1002.58 865.55 29.43 o -5 3 0 814.40 817.82 25.40 o -4 3 0 1296.03 1454.75 30.99 o -3 3 0 2788.87 2600.48 44.12 o -2 3 0 1187.58 1249.06 26.32 o -1 3 0 277.12 315.33 31.19 o 0 3 0 65.83 73.14 8.73 o 1 3 0 586.96 575.23 16.50 o 2 3 0 767.14 870.93 37.11 o 3 3 0 0.73 1.55 6.29 o 4 3 0 1987.40 2225.69 42.26 o 5 3 0 583.55 500.87 23.36 o 6 3 0 17.23 38.78 18.37 o 7 3 0 609.16 523.39 60.49 o 8 3 0 65.41 26.99 17.10 o 9 3 0 600.31 452.97 42.49 o 10 3 0 73.34 132.91 32.70 o 11 3 0 50.11 100.82 44.36 o -14 4 0 133.06 237.94 52.43 o -13 4 0 67.81 120.98 40.33 o -12 4 0 9.38 35.62 23.82 o -11 4 0 144.74 95.06 50.41 o -10 4 0 2349.28 2605.20 104.85 o -9 4 0 86.97 157.28 36.30 o -8 4 0 492.83 551.52 28.66 o -7 4 0 1181.05 1250.39 44.13 o -6 4 0 1645.40 2185.19 45.75 o -5 4 0 1181.43 1382.92 33.32 o -4 4 0 3285.44 3747.38 75.53 o -3 4 0 74.19 56.46 13.42 o -2 4 0 106.19 176.61 13.58 o -1 4 0 520.12 432.18 18.80 o 0 4 0 413.79 580.86 38.94 o 1 4 0 313.58 410.95 15.20 o 2 4 0 210.65 142.54 9.74 o 3 4 0 2257.61 2210.67 41.14 o 4 4 0 935.31 847.99 25.28 o 5 4 0 1390.71 1358.42 52.24 o 6 4 0 163.65 195.15 26.98 o 7 4 0 101.13 128.71 26.98 o 8 4 0 1126.23 1228.52 72.59 o 9 4 0 89.63 121.65 56.46 o 10 4 0 8.97 35.79 20.75 o 11 4 0 2.81 0.00 40.33 o -14 5 0 26.36 0.00 32.26 o -13 5 0 73.50 34.68 28.09 o -12 5 0 422.08 379.02 40.69 o -11 5 0 10.46 19.93 44.36 o -10 5 0 1084.44 967.57 51.09 o -9 5 0 1.74 0.00 24.20 o -8 5 0 46.61 65.46 18.37 o -7 5 0 202.49 213.21 22.94 o -6 5 0 946.17 837.82 30.27 o -5 5 0 638.52 804.66 27.94 o -4 5 0 3072.48 3301.51 69.82 o -3 5 0 1555.71 1662.98 56.43 o -2 5 0 1133.82 1267.49 39.62 o -1 5 0 1387.97 1437.33 31.57 o 0 5 0 471.37 461.82 19.50 o 1 5 0 614.32 565.55 19.07 o 2 5 0 2044.87 2120.67 38.64 o 3 5 0 130.04 158.71 24.20 o 4 5 0 341.21 343.93 48.39 o 5 5 0 157.77 173.87 26.09 o 6 5 0 166.56 144.73 26.09 o 7 5 0 734.71 791.37 56.46 o 8 5 0 12.24 0.00 24.11 o 9 5 0 598.23 562.38 51.33 o 10 5 0 2.24 5.19 29.84 o -14 6 0 9.58 0.00 42.34 o -13 6 0 5.38 9.55 40.33 o -12 6 0 47.40 102.55 30.25 o -11 6 0 92.83 114.91 44.36 o -10 6 0 79.29 121.89 29.04 o -9 6 0 45.13 32.77 22.28 o -8 6 0 12.49 29.16 22.18 o -7 6 0 160.56 186.91 22.81 o -6 6 0 81.63 85.40 18.37 o -5 6 0 212.29 209.60 18.03 o -4 6 0 2226.82 2113.53 58.85 o -3 6 0 3403.28 3307.38 57.04 o -2 6 0 1208.71 1144.91 31.14 o -1 6 0 3314.28 3151.76 55.75 o 0 6 0 1453.51 1360.94 31.44 o 1 6 0 380.48 370.33 18.59 o 2 6 0 42.44 64.52 17.10 o 3 6 0 741.34 711.56 41.65 o 4 6 0 139.21 138.02 25.19 o 5 6 0 42.75 41.08 22.28 o 6 6 0 94.70 108.02 54.44 o 7 6 0 27.30 21.06 25.19 o 8 6 0 172.08 63.79 30.98 o 9 6 0 0.55 0.58 52.43 o -14 7 0 1.14 0.00 26.84 o -13 7 0 30.06 12.90 24.86 o -12 7 0 498.33 596.60 76.62 o -11 7 0 128.49 206.42 33.86 o -10 7 0 1241.35 1265.40 57.99 o -9 7 0 388.35 361.74 40.33 o -8 7 0 632.82 504.50 35.26 o -7 7 0 2999.98 3291.52 66.64 o -6 7 0 1045.31 1393.37 41.09 o -5 7 0 2064.99 2094.02 48.08 o -4 7 0 4315.90 4292.51 72.78 o -3 7 0 197.16 180.20 25.02 o -2 7 0 56.73 64.89 13.58 o -1 7 0 631.73 766.20 27.57 o 0 7 0 464.83 518.54 23.01 o 1 7 0 168.80 174.60 15.20 o 2 7 0 89.66 109.83 22.28 o 3 7 0 33.35 0.00 19.36 o 4 7 0 68.68 45.78 24.20 o 5 7 0 1.10 15.88 22.28 o 6 7 0 15.54 19.93 30.25 o 7 7 0 258.75 285.75 39.54 o 8 7 0 303.65 266.37 40.69 o 9 7 0 453.77 540.40 88.72 o -14 8 0 3.72 7.33 36.30 o -13 8 0 0.05 12.10 26.84 o -12 8 0 3.45 9.98 24.38 o -11 8 0 3.82 0.00 20.13 o -10 8 0 31.15 64.52 36.30 o -9 8 0 398.41 435.43 38.42 o -8 8 0 823.59 757.86 37.11 o -7 8 0 363.85 325.90 25.40 o -6 8 0 1041.54 1021.98 42.22 o -5 8 0 156.38 114.52 16.97 o -4 8 0 1052.94 928.51 34.77 o -3 8 0 1742.55 1718.34 42.96 o -2 8 0 135.49 299.75 21.19 o -1 8 0 6858.79 7142.50 108.65 o 0 8 0 2.41 0.00 11.17 o 1 8 0 898.52 876.68 52.43 o 2 8 0 1205.65 1265.08 54.25 o 3 8 0 34.80 21.35 23.13 o 4 8 0 51.72 38.98 25.19 o 5 8 0 179.02 174.92 32.26 o 6 8 0 690.66 809.64 57.17 o 7 8 0 264.85 375.05 44.57 o 8 8 0 92.41 88.72 56.46 o -14 9 0 33.97 68.56 46.38 o -13 9 0 311.19 333.36 43.58 o -12 9 0 77.70 47.82 72.59 o -11 9 0 37.94 78.24 26.84 o -10 9 0 55.01 53.49 58.48 o -9 9 0 794.88 769.93 48.23 o -8 9 0 219.93 243.83 26.09 o -7 9 0 712.15 696.37 34.77 o -6 9 0 1852.78 1782.65 49.64 o -5 9 0 609.45 580.53 30.99 o -4 9 0 4198.66 4193.24 82.49 o -3 9 0 90.02 134.57 18.80 o -2 9 0 935.82 849.47 33.51 o -1 9 0 3.53 0.00 15.61 o 0 9 0 8.05 28.23 20.13 o 1 9 0 75.41 65.00 23.13 o 2 9 0 4.04 32.03 23.13 o 3 9 0 51.35 0.00 24.20 o 4 9 0 2.62 14.71 24.11 o 5 9 0 170.20 141.15 33.86 o 6 9 0 50.14 46.09 44.36 o 7 9 0 24.64 52.43 52.43 o -14 10 0 55.82 36.65 30.53 o -13 10 0 0.63 0.00 26.09 o -12 10 0 157.23 189.33 36.74 o -11 10 0 218.81 223.42 35.56 o -10 10 0 158.68 150.81 29.84 o -9 10 0 108.85 117.37 32.26 o -8 10 0 89.33 105.72 32.26 o -7 10 0 33.42 47.80 18.01 o -6 10 0 181.76 122.26 20.70 o -5 10 0 222.72 248.97 23.99 o -4 10 0 417.97 396.21 34.88 o -3 10 0 119.50 89.27 19.16 o -2 10 0 599.13 611.49 31.93 o -1 10 0 278.66 356.70 34.88 o 0 10 0 428.96 455.85 52.43 o 1 10 0 273.45 238.71 34.88 o 2 10 0 1688.61 1841.79 71.55 o 3 10 0 89.60 76.20 30.25 o 4 10 0 1048.43 997.71 61.00 o 5 10 0 433.23 496.81 49.36 o 6 10 0 178.63 137.12 56.46 o -14 11 0 221.21 160.43 38.31 o -13 11 0 595.59 565.70 52.24 o -12 11 0 22.04 25.81 26.84 o -11 11 0 386.24 323.97 39.62 o -10 11 0 689.40 575.96 48.39 o -9 11 0 201.85 190.19 31.97 o -8 11 0 720.74 796.57 51.09 o -7 11 0 368.69 357.08 30.09 o -6 11 0 1630.12 1615.47 51.76 o -5 11 0 6.64 39.28 26.37 o -4 11 0 1180.86 1190.27 44.43 o -3 11 0 124.80 116.27 21.19 o -2 11 0 38.33 100.69 20.29 o -1 11 0 204.28 234.40 31.97 o 0 11 0 311.12 319.21 42.34 o 1 11 0 26.16 16.37 24.11 o 2 11 0 32.36 68.13 30.25 o 3 11 0 31.06 19.95 26.09 o 4 11 0 85.08 97.84 32.70 o 5 11 0 5.51 12.10 48.39 o -13 12 0 2.78 79.31 32.82 o -12 12 0 419.06 339.55 50.41 o -11 12 0 248.10 264.68 52.43 o -10 12 0 388.88 428.07 72.59 o -9 12 0 28.87 39.48 26.09 o -8 12 0 52.77 108.24 28.09 o -7 12 0 14.34 4.36 20.08 o -6 12 0 40.20 16.30 19.91 o -5 12 0 270.68 349.66 38.71 o -4 12 0 586.51 631.02 37.35 o -3 12 0 514.16 509.08 33.96 o -2 12 0 1.86 0.00 40.33 o -1 12 0 1894.67 1894.32 72.67 o 0 12 0 1011.71 989.79 61.00 o 1 12 0 7.39 0.00 23.82 o 2 12 0 352.14 366.13 44.57 o 3 12 0 68.67 126.79 34.88 o 4 12 0 278.23 403.28 80.66 o -13 13 0 251.59 278.23 43.58 o -12 13 0 307.45 329.28 46.38 o -11 13 0 758.07 891.31 62.54 o -10 13 0 29.59 20.57 28.09 o -9 13 0 162.60 231.15 60.49 o -8 13 0 509.39 503.72 98.80 o -7 13 0 90.94 152.52 26.67 o -6 13 0 6.26 0.00 19.91 o -5 13 0 1201.20 1198.53 47.66 o -4 13 0 303.48 324.26 31.61 o -3 13 0 10.78 0.00 32.26 o -2 13 0 30.64 59.89 28.09 o -1 13 0 94.87 88.49 38.31 o 0 13 0 0.87 56.03 30.25 o 1 13 0 43.25 0.00 28.09 o 2 13 0 78.88 77.63 32.82 o 3 13 0 2.99 0.00 44.36 o -12 14 0 0.09 14.11 29.84 o -11 14 0 11.37 25.93 29.04 o -10 14 0 110.40 141.10 58.48 o -9 14 0 12.57 10.49 26.84 o -8 14 0 290.25 399.59 74.61 o -7 14 0 578.67 569.07 39.44 o -6 14 0 260.84 259.19 37.79 o -5 14 0 74.87 80.20 23.56 o -4 14 0 192.15 167.23 33.86 o -3 14 0 1135.26 1129.44 76.62 o -2 14 0 23.36 0.00 25.66 o -1 14 0 176.85 188.26 36.56 o 0 14 0 58.71 62.07 31.97 o 1 14 0 179.30 161.31 64.52 o 2 14 0 282.28 250.03 72.59 o -12 15 0 67.94 84.34 68.56 o -11 15 0 587.92 649.51 55.55 o -10 15 0 817.15 740.95 57.99 o -9 15 0 12.71 1.81 28.09 o -8 15 0 1968.79 2005.66 78.38 o -7 15 0 96.20 128.69 28.43 o -6 15 0 196.11 205.59 30.09 o -5 15 0 161.41 222.43 37.79 o -4 15 0 156.60 175.85 56.46 o -3 15 0 26.65 19.36 28.09 o -2 15 0 477.63 512.83 60.49 o -1 15 0 13.98 21.08 29.84 o 0 15 0 9.80 0.00 52.43 o -11 16 0 91.44 69.64 35.77 o -10 16 0 36.50 0.00 36.30 o -9 16 0 27.11 0.00 29.84 o -8 16 0 273.15 273.04 94.77 o -7 16 0 38.58 0.00 42.34 o -6 16 0 0.12 0.00 29.84 o -5 16 0 9.03 0.00 30.25 o -4 16 0 5.95 7.01 32.70 o -3 16 0 300.15 386.91 48.39 o -2 16 0 15.86 16.83 31.97 o -9 17 0 234.60 248.09 44.13 o -8 17 0 158.06 84.69 48.39 o -7 17 0 438.77 500.07 68.56 o -6 17 0 597.49 570.75 82.67 o -5 17 0 159.23 166.69 41.65 o -4 17 0 190.01 204.06 44.57 o 4 -17 1 14.97 63.90 36.74 o 5 -17 1 113.66 99.67 50.41 o 6 -17 1 3.57 0.00 32.82 o 7 -17 1 186.89 165.35 56.46 o 8 -17 1 6.59 2.02 31.37 o 9 -17 1 13.59 32.26 44.36 o 1 -16 1 39.11 8.59 58.48 o 2 -16 1 8.50 22.18 34.28 o 3 -16 1 827.03 840.69 64.85 o 4 -16 1 86.47 19.29 31.97 o 5 -16 1 238.56 266.76 42.49 o 6 -16 1 254.27 329.51 52.43 o 7 -16 1 145.29 82.14 59.53 o 8 -16 1 448.98 434.04 48.23 o 9 -16 1 416.30 494.90 58.48 o 10 -16 1 527.45 460.44 51.09 o -1 -15 1 170.25 239.72 54.44 o 0 -15 1 78.99 22.00 30.98 o 1 -15 1 102.58 96.79 33.86 o 2 -15 1 329.81 378.32 47.48 o 3 -15 1 31.55 77.13 33.86 o 4 -15 1 20.24 0.00 28.09 o 5 -15 1 11.14 41.06 30.98 o 6 -15 1 11.34 1.09 22.35 o 7 -15 1 164.84 168.25 30.66 o 8 -15 1 228.88 151.18 48.39 o 9 -15 1 58.39 122.83 33.86 o 10 -15 1 138.75 213.13 39.62 o 11 -15 1 3.23 6.66 31.97 o 12 -15 1 76.58 80.04 44.36 o -2 -14 1 20.89 40.50 33.86 o -1 -14 1 76.13 93.59 34.28 o 0 -14 1 2.15 0.00 24.11 o 1 -14 1 39.92 45.71 29.84 o 2 -14 1 613.38 704.41 98.80 o 3 -14 1 574.51 627.53 53.29 o 4 -14 1 43.49 87.76 29.84 o 5 -14 1 51.59 92.49 25.40 o 6 -14 1 513.40 608.01 51.09 o 7 -14 1 165.83 149.68 27.16 o 8 -14 1 1222.94 1179.20 62.54 o 9 -14 1 703.08 772.53 88.72 o 10 -14 1 434.18 502.45 49.36 o 11 -14 1 197.39 218.90 90.74 o 12 -14 1 112.43 141.46 36.74 o -4 -13 1 403.56 439.58 84.69 o -3 -13 1 458.41 463.77 51.33 o -2 -13 1 353.11 326.67 50.41 o -1 -13 1 73.76 99.21 38.31 o 0 -13 1 748.67 822.09 80.66 o 1 -13 1 112.12 152.00 44.36 o 2 -13 1 2980.21 3358.92 99.77 o 3 -13 1 1.45 0.00 36.30 o 4 -13 1 190.79 189.65 26.92 o 5 -13 1 65.86 36.64 21.91 o 6 -13 1 928.70 984.61 47.08 o 7 -13 1 95.92 122.56 25.40 o 8 -13 1 121.45 119.62 30.98 o 9 -13 1 11.63 47.99 28.09 o 10 -13 1 43.65 16.94 36.30 o 11 -13 1 47.35 10.28 42.34 o 12 -13 1 4.17 0.00 26.84 o 13 -13 1 276.39 232.35 41.65 o -5 -12 1 2.43 40.33 52.43 o -4 -12 1 78.99 94.10 33.86 o -3 -12 1 13.81 50.96 30.98 o -2 -12 1 10.30 53.00 29.04 o -1 -12 1 3.11 0.00 24.11 o 0 -12 1 366.90 382.33 40.69 o 1 -12 1 215.18 223.80 56.46 o 2 -12 1 654.11 636.44 80.66 o 3 -12 1 577.40 595.35 44.32 o 4 -12 1 291.09 302.90 29.78 o 5 -12 1 99.11 69.63 39.67 o 6 -12 1 471.40 562.58 52.75 o 7 -12 1 9.05 33.24 22.35 o 8 -12 1 376.29 422.90 44.36 o 9 -12 1 26.30 0.95 23.13 o 10 -12 1 1135.35 1128.65 59.68 o 11 -12 1 151.83 188.12 36.74 o 12 -12 1 431.87 393.16 45.36 o 13 -12 1 127.18 199.94 38.71 o -6 -11 1 1.65 0.00 48.39 o -5 -11 1 363.83 364.91 46.25 o -4 -11 1 120.86 121.66 32.82 o -3 -11 1 336.84 367.51 41.65 o -2 -11 1 119.45 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