#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:49:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181297 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237554.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237554_Fobs loop_ _publ_author_name 'Fang, Wei' 'Hu, Jun-Ping' 'Wang, Mei' 'Chen, Mu-Zi' _publ_section_title ; (Z)-3-Hydroxy-4-(4-methoxyphenyl)but-3-en-2-one ; _journal_coeditor_code SJ5292 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o359 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.425 _cell_angle_gamma 90.000 _cell_length_a 18.8076 _cell_length_b 5.3007 _cell_length_c 10.1439 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.8257 _cod_data_source_file sj5292Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' g120412b-Mo in P21/c ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1182.43 1095.54 6.81 o 4 0 0 2378.78 2080.11 12.36 o 5 0 0 241.91 219.46 3.96 o 6 0 0 2278.37 2048.35 13.32 o 7 0 0 731.80 720.75 8.58 o 8 0 0 41.05 41.85 2.29 o 9 0 0 1588.68 1477.98 25.34 o 10 0 0 87.52 80.92 5.80 o 11 0 0 82.61 82.23 3.04 o 12 0 0 1.21 1.20 0.63 o 13 0 0 37.36 34.13 3.48 o 14 0 0 2.36 2.25 0.95 o 15 0 0 46.45 45.84 3.29 o 16 0 0 1021.01 1071.17 30.87 o 17 0 0 482.26 522.43 14.43 o 18 0 0 316.91 338.06 9.70 o 19 0 0 87.03 91.79 5.26 o 20 0 0 76.78 81.20 5.07 o 21 0 0 14.59 16.10 2.31 o 22 0 0 16.49 25.51 2.92 o 1 1 0 88.04 89.03 2.14 o 2 1 0 16.33 11.87 0.61 o 3 1 0 144.85 133.91 2.04 o 4 1 0 466.93 435.28 3.76 o 5 1 0 565.87 543.52 4.18 o 6 1 0 1835.43 1807.69 9.35 o 7 1 0 20.87 18.18 0.91 o 8 1 0 320.15 339.72 3.81 o 9 1 0 332.49 350.83 4.15 o 10 1 0 1075.95 1084.67 8.94 o 11 1 0 0.75 1.37 0.53 o 12 1 0 128.31 122.51 2.77 o 13 1 0 0.88 1.99 0.56 o 14 1 0 40.78 41.58 2.12 o 15 1 0 50.39 55.40 2.52 o 16 1 0 26.75 31.05 2.41 o 17 1 0 6.48 8.39 1.29 o 18 1 0 14.44 18.31 1.84 o 19 1 0 60.92 65.90 3.51 o 20 1 0 11.39 13.72 1.76 o 21 1 0 23.79 24.86 2.24 o 0 2 0 94.81 76.19 4.13 o 1 2 0 67.23 69.25 1.86 o 2 2 0 240.58 245.23 3.86 o 3 2 0 8.86 8.48 0.67 o 4 2 0 549.54 564.35 7.89 o 5 2 0 1978.07 2046.93 13.87 o 6 2 0 4.19 6.43 0.62 o 7 2 0 21.72 24.90 1.07 o 8 2 0 103.49 131.90 2.50 o 9 2 0 230.41 243.01 3.51 o 10 2 0 304.90 307.65 3.30 o 11 2 0 93.96 85.88 2.02 o 12 2 0 19.45 17.73 0.97 o 13 2 0 0.63 1.41 0.50 o 14 2 0 232.54 215.75 4.58 o 15 2 0 46.05 45.29 3.52 o 16 2 0 0.41 0.00 0.49 o 17 2 0 15.56 14.14 1.28 o 18 2 0 61.91 57.82 2.53 o 19 2 0 45.11 48.99 2.99 o 20 2 0 2.98 1.88 1.22 o 21 2 0 8.81 9.98 5.62 o 1 3 0 63.15 72.95 2.71 o 2 3 0 200.84 236.56 4.72 o 3 3 0 74.28 74.84 2.63 o 4 3 0 77.73 74.32 2.67 o 5 3 0 4.00 6.18 0.85 o 6 3 0 37.69 31.70 1.58 o 7 3 0 100.31 96.40 3.17 o 8 3 0 133.98 129.44 3.48 o 9 3 0 109.28 99.43 2.85 o 10 3 0 30.34 32.55 1.54 o 11 3 0 0.71 0.60 0.34 o 12 3 0 1.20 0.83 0.53 o 13 3 0 6.92 10.65 1.06 o 14 3 0 165.89 153.62 3.89 o 15 3 0 50.43 48.47 5.17 o 16 3 0 0.08 0.56 0.94 o 17 3 0 3.10 2.16 1.77 o 18 3 0 0.55 0.00 2.19 o 19 3 0 0.00 0.08 1.03 o 0 4 0 711.71 764.55 12.02 o 1 4 0 0.07 1.08 1.01 o 2 4 0 85.64 89.80 3.34 o 3 4 0 9.53 11.29 1.25 o 4 4 0 321.16 341.75 6.53 o 5 4 0 79.38 66.60 5.53 o 6 4 0 85.25 84.51 3.77 o 7 4 0 45.38 44.34 2.77 o 8 4 0 2.52 2.27 0.67 o 9 4 0 79.00 87.81 4.50 o 10 4 0 0.00 0.24 0.50 o 11 4 0 0.05 0.00 0.53 o 12 4 0 0.09 0.00 1.10 o 13 4 0 0.51 0.00 1.35 o 14 4 0 19.44 10.55 3.11 o 15 4 0 20.15 18.40 3.82 o 16 4 0 23.08 22.95 4.28 o 17 4 0 0.04 0.00 1.86 o 1 5 0 4.90 4.45 0.95 o 2 5 0 17.54 21.07 1.88 o 3 5 0 284.19 306.07 6.89 o 4 5 0 102.14 107.39 3.38 o 5 5 0 74.58 70.09 5.76 o 6 5 0 2.77 3.64 1.79 o 7 5 0 2.55 4.01 1.31 o 8 5 0 19.31 20.05 3.39 o 9 5 0 35.26 35.60 4.67 o 10 5 0 105.15 113.63 8.23 o 11 5 0 47.55 49.39 5.80 o 12 5 0 11.26 16.49 3.44 o 13 5 0 90.32 86.54 7.68 o 0 6 0 0.23 0.07 0.99 o 1 6 0 40.72 45.87 3.24 o 2 6 0 18.18 21.27 1.99 o 3 6 0 42.17 41.89 2.70 o 4 6 0 0.95 0.00 0.96 o 5 6 0 0.27 0.00 1.26 o 6 6 0 0.61 0.00 1.98 o 7 6 0 0.78 0.13 1.47 o -22 1 1 6.19 9.84 1.97 o -21 1 1 6.85 4.62 1.27 o -20 1 1 48.52 41.23 2.44 o -19 1 1 76.28 78.33 3.28 o -18 1 1 377.46 406.57 7.17 o -17 1 1 36.83 32.61 2.31 o -16 1 1 47.08 43.12 2.22 o -15 1 1 18.23 15.78 1.30 o -14 1 1 14.46 15.16 1.24 o -13 1 1 143.72 152.79 3.76 o -12 1 1 0.25 1.74 0.49 o -11 1 1 117.70 127.23 2.99 o -10 1 1 204.64 239.66 3.89 o -9 1 1 165.97 159.33 2.96 o -8 1 1 319.69 365.99 4.38 o -7 1 1 663.02 624.03 5.59 o -6 1 1 151.92 146.40 2.38 o -5 1 1 214.71 195.38 3.92 o -4 1 1 184.36 185.53 2.30 o -3 1 1 14.44 12.94 0.49 o -1 1 1 9.03 12.25 2.24 o 0 1 1 1488.28 1492.02 6.48 o 1 1 1 13.63 14.54 0.54 o 2 1 1 663.29 625.92 4.32 o 3 1 1 131.67 123.29 1.50 o 4 1 1 529.80 513.81 4.07 o 5 1 1 15.99 14.94 0.79 o 6 1 1 0.58 0.50 0.29 o 7 1 1 49.02 44.83 1.39 o 8 1 1 508.06 511.52 4.56 o 9 1 1 15.94 27.05 1.13 o 10 1 1 2.01 1.65 0.43 o 11 1 1 219.68 226.85 3.68 o 12 1 1 21.11 21.54 1.49 o 13 1 1 36.26 40.28 2.43 o 14 1 1 222.98 217.54 5.73 o 15 1 1 406.88 407.57 8.02 o 16 1 1 511.12 524.39 15.65 o 17 1 1 8.24 7.79 1.20 o 18 1 1 54.62 60.30 2.89 o 19 1 1 1.98 2.95 0.83 o 20 1 1 8.55 9.75 1.33 o 21 1 1 0.00 0.98 0.68 o -21 2 1 0.13 1.47 1.43 o -20 2 1 6.80 7.34 2.78 o -19 2 1 13.84 12.22 2.28 o -18 2 1 29.03 32.52 2.46 o -17 2 1 0.15 0.49 0.69 o -16 2 1 59.54 52.39 2.97 o -15 2 1 9.08 10.35 1.76 o -14 2 1 17.07 17.72 1.53 o -13 2 1 10.92 13.85 1.19 o -12 2 1 121.83 119.68 3.21 o -11 2 1 61.03 65.70 2.09 o -10 2 1 3.53 10.57 0.65 o -9 2 1 13.72 7.77 0.53 o -8 2 1 528.42 522.17 4.94 o -7 2 1 15.85 21.65 1.12 o -6 2 1 0.13 0.17 0.27 o -5 2 1 34.58 47.25 1.44 o -4 2 1 5.49 10.93 0.89 o -3 2 1 58.67 65.80 1.75 o -2 2 1 867.39 904.68 9.17 o -1 2 1 49.04 46.41 1.79 o 0 2 1 107.00 95.09 2.27 o 1 2 1 594.00 643.56 6.30 o 2 2 1 157.83 176.85 2.43 o 3 2 1 226.65 220.11 2.49 o 4 2 1 113.69 126.03 1.98 o 5 2 1 36.81 32.58 1.22 o 6 2 1 830.71 905.07 8.42 o 7 2 1 296.26 312.25 3.85 o 8 2 1 423.68 432.84 3.96 o 9 2 1 10.51 7.38 0.57 o 10 2 1 0.96 0.90 0.43 o 11 2 1 25.37 19.86 1.06 o 12 2 1 2.63 5.06 0.67 o 13 2 1 1.35 2.76 0.58 o 14 2 1 2.63 2.43 0.47 o 15 2 1 7.02 4.44 0.74 o 16 2 1 10.38 8.77 1.06 o 17 2 1 28.08 32.24 1.96 o 18 2 1 0.00 0.19 0.72 o 19 2 1 2.18 1.66 0.76 o 20 2 1 9.80 12.48 2.27 o -19 3 1 3.87 4.11 2.24 o -18 3 1 3.67 6.99 2.61 o -17 3 1 6.64 8.50 2.55 o -16 3 1 144.04 142.10 9.96 o -15 3 1 22.26 16.18 1.51 o -14 3 1 1.97 0.00 1.10 o -13 3 1 38.92 30.51 1.64 o -12 3 1 42.31 40.11 1.84 o -11 3 1 3.38 3.54 0.63 o -10 3 1 14.12 16.75 1.20 o -9 3 1 50.45 52.76 2.10 o -8 3 1 25.66 24.26 1.34 o -7 3 1 3.63 8.86 1.05 o -6 3 1 25.95 22.27 1.44 o -5 3 1 26.90 33.19 1.74 o -4 3 1 299.49 282.56 7.21 o -3 3 1 31.19 35.75 2.55 o -2 3 1 115.29 123.20 7.71 o -1 3 1 26.71 35.14 1.76 o 0 3 1 289.78 298.09 4.55 o 1 3 1 287.24 335.19 5.42 o 2 3 1 144.31 170.72 4.00 o 3 3 1 291.27 319.07 4.26 o 4 3 1 425.42 442.73 5.49 o 5 3 1 1.00 1.40 0.30 o 6 3 1 13.54 24.46 1.45 o 7 3 1 7.54 5.99 0.72 o 8 3 1 36.71 35.60 1.73 o 9 3 1 0.00 0.28 0.38 o 10 3 1 23.57 19.34 1.32 o 11 3 1 0.00 0.57 0.54 o 12 3 1 91.10 75.88 3.17 o 13 3 1 7.92 8.46 1.07 o 14 3 1 12.70 14.08 1.36 o 15 3 1 5.19 4.68 0.86 o 16 3 1 16.25 16.28 1.75 o 17 3 1 50.63 58.26 3.27 o 18 3 1 5.58 9.64 2.08 o 19 3 1 38.95 39.73 4.09 o -17 4 1 0.05 2.78 1.84 o -16 4 1 12.69 9.60 2.87 o -15 4 1 25.42 21.56 4.15 o -14 4 1 0.00 1.38 1.35 o -13 4 1 26.63 22.82 3.94 o -12 4 1 57.31 48.03 3.18 o -11 4 1 54.60 46.62 2.74 o -10 4 1 2.38 0.90 0.66 o -9 4 1 0.38 0.89 0.81 o -8 4 1 3.59 4.94 1.36 o -7 4 1 292.93 297.23 5.72 o -6 4 1 147.32 144.34 4.02 o -5 4 1 311.83 304.28 9.06 o -4 4 1 223.11 219.46 3.92 o -3 4 1 180.18 186.29 3.96 o -2 4 1 34.52 37.77 2.12 o -1 4 1 14.25 12.74 1.03 o 0 4 1 12.38 14.73 1.26 o 1 4 1 193.82 199.39 4.80 o 2 4 1 5.37 5.55 0.89 o 3 4 1 14.47 16.44 1.12 o 4 4 1 26.39 28.52 1.50 o 5 4 1 62.22 55.85 3.99 o 6 4 1 94.75 102.79 5.78 o 7 4 1 79.43 81.45 3.83 o 8 4 1 69.45 67.14 3.51 o 9 4 1 26.87 26.54 2.25 o 10 4 1 0.48 1.54 1.58 o 11 4 1 136.78 123.80 4.92 o 12 4 1 90.72 85.76 7.37 o 13 4 1 36.47 39.32 5.28 o 14 4 1 85.84 77.11 7.38 o 15 4 1 5.03 2.71 1.66 o 16 4 1 0.12 1.21 1.22 o -14 5 1 0.14 2.51 1.94 o -13 5 1 3.53 2.52 1.60 o -12 5 1 4.18 5.29 2.32 o -11 5 1 3.24 4.30 2.13 o -10 5 1 1.45 0.53 1.29 o -9 5 1 0.52 1.51 1.48 o -8 5 1 6.93 4.26 1.71 o -7 5 1 18.18 15.40 2.95 o -6 5 1 62.06 61.46 3.06 o -5 5 1 62.38 58.51 2.04 o -4 5 1 2.28 2.19 0.52 o -3 5 1 70.11 72.23 2.65 o -2 5 1 116.62 136.81 4.53 o -1 5 1 43.01 44.92 2.59 o 0 5 1 45.84 46.92 2.62 o 1 5 1 65.48 77.52 3.44 o 2 5 1 28.07 31.46 2.77 o 3 5 1 43.25 41.27 2.14 o 4 5 1 11.39 10.34 3.72 o 5 5 1 20.53 15.82 2.02 o 6 5 1 9.11 6.50 1.96 o 7 5 1 4.77 4.24 1.92 o 8 5 1 8.99 10.32 2.57 o 9 5 1 2.40 3.33 1.93 o 10 5 1 0.12 0.82 1.79 o 11 5 1 19.04 17.36 3.50 o 12 5 1 3.16 3.64 2.07 o 13 5 1 13.10 15.32 3.46 o -8 6 1 17.03 17.57 2.60 o -7 6 1 4.39 4.54 1.61 o -6 6 1 10.48 13.32 2.36 o -5 6 1 13.21 10.57 2.07 o -4 6 1 0.24 3.93 2.35 o -3 6 1 3.35 4.38 2.23 o -2 6 1 13.00 14.86 2.86 o -1 6 1 0.33 0.00 1.26 o 0 6 1 1.81 4.11 1.02 o 1 6 1 62.42 66.67 3.86 o 2 6 1 35.15 36.64 2.56 o 3 6 1 34.75 33.13 2.43 o 4 6 1 3.02 1.05 0.92 o 5 6 1 13.88 14.02 2.53 o 6 6 1 5.52 7.77 2.49 o 7 6 1 4.66 3.12 1.34 o -22 0 2 4.87 7.10 3.56 o -21 0 2 76.22 86.13 4.96 o -20 0 2 270.19 279.84 15.13 o -19 0 2 4.21 4.41 1.50 o -18 0 2 0.59 0.67 0.79 o -17 0 2 18.21 15.63 1.94 o -16 0 2 82.09 80.75 4.13 o -15 0 2 145.61 146.90 5.35 o -14 0 2 83.06 84.01 3.27 o -13 0 2 230.29 223.86 6.73 o -12 0 2 1.46 0.34 0.53 o -11 0 2 1.90 4.15 1.07 o -10 0 2 2348.49 2400.03 18.99 o -9 0 2 328.06 313.03 6.53 o -8 0 2 43.95 51.79 2.52 o -7 0 2 0.21 1.00 0.51 o -6 0 2 880.54 827.20 8.58 o -5 0 2 465.22 471.04 9.75 o -3 0 2 1892.83 1671.93 9.16 o -2 0 2 6572.07 6287.92 44.00 o -1 0 2 376.31 365.90 4.53 o 0 0 2 706.87 707.83 13.08 o 1 0 2 582.48 545.59 6.05 o 2 0 2 589.80 587.94 6.75 o 3 0 2 8.26 5.97 1.03 o 4 0 2 2957.24 2856.24 32.14 o 5 0 2 630.39 665.27 10.92 o 6 0 2 3576.80 3752.13 21.54 o 7 0 2 56.62 55.06 2.32 o 8 0 2 28.99 33.77 1.93 o 9 0 2 338.79 372.99 6.76 o 10 0 2 561.91 586.59 26.27 o 11 0 2 88.49 83.36 3.38 o 12 0 2 349.60 374.43 9.09 o 13 0 2 1168.61 1090.53 16.14 o 14 0 2 1548.18 1562.34 45.18 o 15 0 2 0.82 5.91 1.94 o 16 0 2 60.56 60.06 4.16 o 17 0 2 0.02 0.21 1.51 o 18 0 2 43.53 45.87 5.31 o 19 0 2 91.92 91.78 5.73 o 20 0 2 4.18 7.22 1.73 o 21 0 2 10.84 11.25 2.04 o -22 1 2 1.18 2.79 1.13 o -21 1 2 35.32 37.94 2.99 o -20 1 2 83.16 93.12 3.48 o -19 1 2 0.93 0.73 0.89 o -18 1 2 72.85 75.41 2.97 o -17 1 2 6.30 5.65 0.93 o -16 1 2 0.11 1.06 0.49 o -15 1 2 37.67 36.99 2.35 o -14 1 2 3.71 4.67 0.73 o -13 1 2 86.51 81.24 2.47 o -12 1 2 20.65 22.90 1.18 o -11 1 2 3.46 3.99 0.54 o -10 1 2 96.95 103.91 2.28 o -9 1 2 544.12 548.70 6.91 o -8 1 2 10.34 13.12 0.66 o -7 1 2 603.99 572.90 5.05 o -6 1 2 624.96 578.07 4.97 o -5 1 2 97.67 113.38 2.20 o -4 1 2 12898.52 12240.64 323.15 o -3 1 2 5.54 11.43 0.61 o -2 1 2 4615.50 4416.63 31.54 o -1 1 2 282.59 293.04 3.09 o 0 1 2 2859.98 2738.47 9.59 o 1 1 2 384.29 371.32 2.66 o 2 1 2 673.45 653.15 3.77 o 3 1 2 930.74 917.37 5.03 o 4 1 2 1085.17 1015.21 5.21 o 5 1 2 1381.74 1364.05 7.04 o 6 1 2 1258.17 1296.17 7.24 o 7 1 2 869.24 876.73 6.26 o 8 1 2 169.59 180.09 2.98 o 9 1 2 82.11 69.60 2.01 o 10 1 2 217.37 209.66 3.24 o 11 1 2 110.45 105.67 2.40 o 12 1 2 228.50 207.92 4.03 o 13 1 2 7.64 7.08 0.92 o 14 1 2 114.58 121.44 3.79 o 15 1 2 211.76 207.57 5.12 o 16 1 2 34.97 36.40 2.26 o 17 1 2 37.53 35.08 2.24 o 18 1 2 5.63 5.91 1.01 o 19 1 2 1.49 1.54 0.65 o 20 1 2 4.50 4.05 0.93 o -21 2 2 2.51 3.95 1.63 o -20 2 2 121.18 145.98 7.35 o -19 2 2 83.19 109.94 9.19 o -18 2 2 104.62 107.20 8.68 o -17 2 2 1.27 1.15 0.93 o -16 2 2 73.61 69.09 2.81 o -15 2 2 18.68 15.44 1.85 o -14 2 2 97.76 87.41 4.36 o -13 2 2 0.75 0.94 0.26 o -12 2 2 103.74 98.85 2.85 o -11 2 2 69.94 64.92 2.19 o -10 2 2 0.36 0.45 0.34 o -9 2 2 0.26 1.27 0.35 o -8 2 2 7.44 8.75 0.71 o -7 2 2 66.84 60.29 1.69 o -6 2 2 6.17 7.22 0.44 o -5 2 2 5.28 4.07 0.33 o -4 2 2 1014.31 1072.33 6.27 o -3 2 2 11.40 11.56 1.12 o -2 2 2 243.47 247.22 4.28 o -1 2 2 440.46 472.39 4.88 o 0 2 2 2620.08 2700.91 11.00 o 1 2 2 270.87 323.82 3.14 o 2 2 2 1779.54 1836.34 8.23 o 3 2 2 194.07 187.56 2.73 o 4 2 2 205.90 233.14 3.14 o 5 2 2 41.56 38.78 1.16 o 6 2 2 0.82 0.20 0.24 o 7 2 2 6.92 5.07 0.60 o 8 2 2 10.83 11.22 0.73 o 9 2 2 299.49 310.94 3.77 o 10 2 2 44.26 42.47 1.45 o 11 2 2 111.55 107.46 2.72 o 12 2 2 2.30 1.66 0.48 o 13 2 2 18.64 17.46 1.19 o 14 2 2 71.36 65.70 3.18 o 15 2 2 32.95 30.85 1.91 o 16 2 2 2.79 3.20 0.78 o 17 2 2 51.54 53.52 2.63 o 18 2 2 40.11 46.35 2.49 o 19 2 2 34.09 36.82 2.88 o -20 3 2 3.16 5.08 2.56 o -19 3 2 17.75 25.29 4.88 o -18 3 2 5.97 3.86 2.47 o -17 3 2 2.71 3.78 2.39 o -16 3 2 1.23 0.00 1.42 o -15 3 2 2.20 1.37 0.82 o -14 3 2 48.34 41.25 2.96 o -13 3 2 105.89 94.19 4.32 o -12 3 2 67.67 71.49 3.68 o -11 3 2 79.25 81.91 3.83 o -10 3 2 285.03 284.39 6.85 o -9 3 2 590.82 564.36 5.87 o -8 3 2 254.15 255.63 3.94 o -7 3 2 90.49 84.87 2.08 o -6 3 2 0.13 0.34 0.28 o -5 3 2 125.03 107.93 2.27 o -4 3 2 332.19 339.94 6.06 o -3 3 2 33.22 30.44 1.32 o -2 3 2 0.04 1.00 0.41 o -1 3 2 485.01 529.68 5.09 o 0 3 2 830.56 861.72 7.45 o 1 3 2 103.14 88.36 2.86 o 2 3 2 28.28 27.36 1.34 o 3 3 2 51.37 51.27 1.64 o 4 3 2 147.44 166.31 2.96 o 5 3 2 36.32 37.30 1.32 o 6 3 2 2.76 3.05 0.43 o 7 3 2 11.44 9.19 0.94 o 8 3 2 3.43 3.12 0.61 o 9 3 2 28.24 29.51 1.67 o 10 3 2 11.16 12.50 1.30 o 11 3 2 37.13 40.58 2.31 o 12 3 2 218.62 202.69 5.18 o 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