#------------------------------------------------------------------------------
#$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $
#$Revision: 88054 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237561.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2237561_Fobs
loop_
_publ_author_name
'Campos-Gaxiola, Jos\'e J.'
'Almaral-Sanchez, Jorge L.'
'Cruz-Enr\'iquez, Adriana'
'H\"opfl, Herbert'
'Parra-Hake, Miguel'
_publ_section_title
;
 (1<i>RS</i>,2<i>RS</i>)-4,4'-(1-Azaniumyl-2-hydroxyethane-1,2-diyl)dipyridinium
 tetrachloridoplatinate(II) chloride
;
_journal_coeditor_code           SU2560
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m157
_journal_page_last               m158
_journal_volume                  69
_journal_year                    2013
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                88.689
_cell_angle_beta                 84.240
_cell_angle_gamma                70.148
_cell_length_a                   7.6361
_cell_length_b                   8.0824
_cell_length_c                   14.5988
_exptl_crystal_F_000             560.00
_reflns_d_resolution_high        0.8409
_[local]_cod_data_source_file    su2560Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' ppchm in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            245.87
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 4686.31 4287.24 351.53 o
3 0 0 9744.36 10287.90 460.62 o
4 0 0 7380.50 7807.45 358.92 o
5 0 0 4095.10 4036.09 439.04 o
6 0 0 198.83 211.85 37.55 o
7 0 0 5118.23 5221.58 381.95 o
8 0 0 4957.95 5199.60 391.67 o
-8 1 0 1653.58 1757.40 172.83 o
-7 1 0 2069.95 2302.76 200.95 o
-6 1 0 619.68 723.44 88.46 o
-5 1 0 12946.62 14789.29 671.54 o
-4 1 0 11248.41 11548.48 719.21 o
-3 1 0 603.92 565.40 60.74 o
-1 1 0 18517.27 19013.51 1032.17 o
0 1 0 10532.57 12410.92 710.70 o
1 1 0 534.09 578.40 24.15 o
2 1 0 2614.69 2567.45 94.89 o
3 1 0 1944.85 1961.45 132.50 o
4 1 0 3359.40 3308.21 181.63 o
5 1 0 9.57 12.89 17.58 o
6 1 0 5612.19 5725.18 276.71 o
7 1 0 5234.27 5938.89 424.25 o
8 1 0 105.03 114.10 49.01 o
-7 2 0 134.17 173.99 56.03 o
-6 2 0 2866.95 2844.17 230.53 o
-5 2 0 4812.09 5040.78 258.03 o
-4 2 0 811.07 740.52 62.53 o
-3 2 0 163.06 160.28 32.89 o
-2 2 0 421.88 317.04 53.07 o
-1 2 0 10448.05 11365.30 742.87 o
0 2 0 5676.91 6120.37 283.96 o
1 2 0 2910.19 3660.94 131.69 o
2 2 0 16074.06 16961.27 585.36 o
3 2 0 899.08 953.20 43.65 o
4 2 0 74.75 77.89 13.44 o
5 2 0 1449.31 1504.47 88.19 o
6 2 0 5936.62 5847.42 281.59 o
7 2 0 4074.28 4298.95 220.38 o
8 2 0 396.13 526.44 81.96 o
-7 3 0 204.43 251.35 70.12 o
-6 3 0 4836.11 4050.15 311.76 o
-5 3 0 7614.51 7829.38 540.61 o
-4 3 0 40.97 26.61 20.91 o
-2 3 0 8638.94 8046.11 378.86 o
-1 3 0 2795.49 3163.08 299.27 o
0 3 0 1351.18 1457.42 79.85 o
1 3 0 34212.20 36162.04 2171.93 o
2 3 0 23648.67 24826.35 851.31 o
3 3 0 4114.83 4042.27 150.55 o
4 3 0 189.05 184.41 19.75 o
5 3 0 13394.41 13265.99 470.55 o
6 3 0 14059.56 13548.35 1343.38 o
7 3 0 718.18 687.47 59.90 o
8 3 0 2447.69 2748.34 228.78 o
9 3 0 3194.69 3849.79 309.79 o
-6 4 0 3987.44 4019.76 315.85 o
-5 4 0 128.24 117.09 43.46 o
-4 4 0 2605.48 2515.90 199.78 o
-3 4 0 9473.71 8047.45 786.48 o
-2 4 0 3548.99 3424.91 250.47 o
-1 4 0 473.84 401.36 55.15 o
0 4 0 9993.59 10807.28 488.17 o
1 4 0 30123.71 32893.73 1440.94 o
2 4 0 14333.81 16368.22 688.32 o
3 4 0 225.08 245.18 22.91 o
4 4 0 6737.73 6929.87 253.98 o
5 4 0 4499.01 4314.91 167.67 o
6 4 0 411.78 451.81 37.66 o
7 4 0 174.69 218.74 38.50 o
8 4 0 2798.28 2927.52 233.01 o
-5 5 0 70.25 61.43 41.05 o
-4 5 0 4467.42 4553.14 333.96 o
-3 5 0 5880.43 4999.30 269.20 o
-2 5 0 937.82 927.71 75.16 o
-1 5 0 2402.72 2528.53 141.92 o
0 5 0 5655.15 6130.01 231.72 o
1 5 0 6432.19 6427.31 301.89 o
2 5 0 148.42 209.78 24.19 o
3 5 0 292.07 320.30 36.88 o
4 5 0 898.04 842.62 47.98 o
5 5 0 1861.42 1827.45 100.28 o
6 5 0 101.57 109.01 27.64 o
7 5 0 2872.76 2830.37 223.81 o
8 5 0 3483.57 3366.37 262.23 o
-4 6 0 4109.63 4096.17 310.81 o
-3 6 0 219.56 200.73 64.57 o
-2 6 0 11.28 18.04 25.28 o
-1 6 0 2255.33 2295.42 136.51 o
0 6 0 3131.64 3200.60 139.08 o
1 6 0 1886.80 1626.97 81.69 o
2 6 0 2007.78 2099.81 104.36 o
3 6 0 10867.95 10877.27 694.88 o
4 6 0 3953.46 3997.41 287.51 o
5 6 0 169.75 134.91 47.11 o
6 6 0 2683.43 2636.58 212.20 o
7 6 0 6065.48 6022.74 420.52 o
8 6 0 2793.05 3032.56 246.24 o
-3 7 0 452.12 422.42 87.14 o
-2 7 0 4115.27 3953.87 262.74 o
-1 7 0 7846.62 7635.03 374.86 o
0 7 0 1386.44 1296.56 130.97 o
1 7 0 1781.32 1858.71 163.40 o
2 7 0 8830.05 8753.55 576.04 o
3 7 0 9753.64 9664.86 631.70 o
4 7 0 1401.22 1284.80 127.54 o
5 7 0 30.25 -0.58 31.34 o
6 7 0 5516.33 5324.58 380.86 o
7 7 0 6295.09 6379.13 448.65 o
8 7 0 420.94 492.47 86.05 o
-1 8 0 1048.72 904.67 115.85 o
0 8 0 140.01 141.56 58.14 o
1 8 0 2097.73 2122.85 188.75 o
2 8 0 6306.43 6341.08 442.87 o
3 8 0 4914.96 4881.70 354.64 o
4 8 0 24.46 52.01 40.61 o
5 8 0 2258.09 2106.92 189.33 o
6 8 0 928.67 953.90 117.46 o
7 8 0 264.99 368.51 78.89 o
0 9 0 307.78 386.70 86.70 o
1 9 0 2495.41 2437.89 217.82 o
2 9 0 1231.28 1345.35 146.38 o
3 9 0 9.48 22.72 38.64 o
4 9 0 962.44 974.43 118.70 o
5 9 0 492.72 509.64 89.63 o
-5 -9 1 923.15 930.53 120.31 o
-4 -9 1 2909.18 2910.57 243.39 o
-3 -9 1 1866.05 1814.81 175.60 o
-2 -9 1 10.82 22.42 40.61 o
-1 -9 1 60.16 70.20 50.26 o
0 -9 1 474.27 501.60 91.09 o
-7 -8 1 296.51 316.14 72.53 o
-6 -8 1 62.52 80.72 48.58 o
-5 -8 1 1362.48 1287.43 136.81 o
-4 -8 1 3767.63 3745.33 287.43 o
-3 -8 1 2633.91 2528.18 211.76 o
-2 -8 1 569.40 553.25 85.02 o
-1 -8 1 3221.20 3423.06 268.81 o
0 -8 1 2225.23 2262.73 200.14 o
1 -8 1 446.40 410.66 83.13 o
2 -8 1 1762.36 1871.06 200.07 o
-7 -7 1 32.66 46.68 43.61 o
-6 -7 1 2706.53 2574.05 213.37 o
-5 -7 1 7597.34 7250.42 491.45 o
-4 -7 1 5883.99 5913.03 409.27 o
-3 -7 1 780.66 771.58 94.74 o
-2 -7 1 10666.60 10150.03 659.67 o
-1 -7 1 7075.56 7364.08 495.83 o
0 -7 1 1157.90 1113.41 86.85 o
1 -7 1 334.62 355.88 50.40 o
2 -7 1 6405.94 6122.41 396.20 o
3 -7 1 5804.29 5025.75 399.85 o
-8 -6 1 470.14 445.14 79.04 o
-7 -6 1 2223.99 2037.82 177.72 o
-6 -6 1 2255.60 2217.81 185.24 o
-5 -6 1 2633.81 2769.74 215.85 o
-4 -6 1 161.72 182.61 49.16 o
-3 -6 1 3966.92 4204.17 234.95 o
-2 -6 1 11907.92 11843.63 540.66 o
-1 -6 1 3363.31 3209.64 168.95 o
0 -6 1 453.35 478.37 52.61 o
1 -6 1 448.62 419.20 57.09 o
2 -6 1 3876.85 3709.31 207.74 o
3 -6 1 1513.16 1473.17 116.42 o
4 -6 1 529.02 556.02 100.51 o
-8 -5 1 10.32 15.19 33.97 o
-7 -5 1 1671.35 1637.02 147.84 o
-6 -5 1 1820.94 1743.74 150.33 o
-5 -5 1 551.19 562.79 40.78 o
-4 -5 1 376.19 360.33 30.95 o
-3 -5 1 14228.95 15188.21 532.93 o
-2 -5 1 4914.13 5369.79 238.01 o
-1 -5 1 65.59 70.54 17.97 o
0 -5 1 909.18 933.71 76.71 o
1 -5 1 316.91 390.35 84.55 o
2 -5 1 4124.46 4283.64 259.57 o
3 -5 1 414.66 361.18 55.01 o
4 -5 1 3306.75 3203.19 278.89 o
5 -5 1 5437.85 5378.85 395.54 o
-8 -4 1 3699.90 4459.86 343.68 o
-7 -4 1 7720.10 8167.94 391.06 o
-6 -4 1 714.38 733.84 61.59 o
-5 -4 1 1346.22 1314.16 65.33 o
-4 -4 1 5627.16 5649.33 209.49 o
-3 -4 1 13473.38 13674.13 567.17 o
-2 -4 1 6455.10 7095.10 268.10 o
-1 -4 1 2427.94 2322.41 144.76 o
0 -4 1 14268.39 15290.04 684.33 o
1 -4 1 13605.68 14350.76 746.89 o
2 -4 1 199.71 175.70 32.68 o
3 -4 1 5392.42 4742.12 278.30 o
4 -4 1 14516.76 9898.75 700.07 o
5 -4 1 4389.86 3911.22 296.71 o
6 -4 1 93.46 86.27 46.53 o
-8 -3 1 5801.08 6114.27 445.58 o
-7 -3 1 7376.81 7876.61 375.80 o
-6 -3 1 1.84 19.43 20.02 o
-5 -3 1 3710.20 3885.78 193.64 o
-4 -3 1 12164.78 12174.51 428.89 o
-3 -3 1 14505.56 15137.91 527.12 o
-2 -3 1 2240.01 2108.56 82.46 o
-1 -3 1 32152.10 35335.88 1277.48 o
0 -3 1 8290.41 8885.35 401.67 o
1 -3 1 1495.32 1518.65 212.01 o
2 -3 1 87.52 88.15 24.53 o
5 -3 1 607.92 588.24 77.57 o
6 -3 1 681.92 691.45 92.04 o
7 -3 1 1336.63 1480.05 154.05 o
-8 -2 1 6377.41 5971.76 435.94 o
-7 -2 1 568.02 540.10 75.97 o
-6 -2 1 2160.91 2114.02 118.82 o
-5 -2 1 4541.99 4663.89 224.92 o
-4 -2 1 653.27 699.63 48.93 o
-3 -2 1 352.44 346.17 22.56 o
-2 -2 1 3653.96 3738.56 136.14 o
-1 -2 1 17811.11 19373.22 663.00 o
0 -2 1 15119.52 16173.00 711.82 o
1 -2 1 20.44 43.93 16.63 o
2 -2 1 1206.20 996.10 78.56 o
4 -2 1 666.60 536.40 62.65 o
5 -2 1 175.26 195.63 46.93 o
6 -2 1 1536.34 1557.69 145.87 o
7 -2 1 1545.80 1462.59 148.28 o
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-7 -1 1 293.94 298.10 59.90 o
-6 -1 1 2785.16 3016.28 158.63 o
-5 -1 1 3480.12 3394.44 169.18 o
-4 -1 1 742.21 688.45 47.72 o
-3 -1 1 6801.03 6563.16 297.22 o
-2 -1 1 16834.26 17188.28 751.07 o
-1 -1 1 16276.48 17038.69 581.67 o
0 -1 1 1070.45 951.34 48.54 o
1 -1 1 6311.03 5639.21 436.08 o
2 -1 1 5867.94 5632.54 383.71 o
3 -1 1 6118.92 5842.03 286.45 o
4 -1 1 83.00 101.74 24.77 o
5 -1 1 9930.90 11188.63 522.60 o
6 -1 1 9651.63 11264.20 636.96 o
7 -1 1 2752.18 3082.08 250.18 o
8 -1 1 224.32 294.88 69.83 o
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-7 0 1 4361.38 4520.13 338.78 o
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-2 0 1 46692.27 50320.91 2187.26 o
-1 0 1 2055.93 2226.63 101.16 o
1 0 1 15114.98 15596.00 649.03 o
2 0 1 22474.27 21801.44 908.54 o
3 0 1 2272.81 2148.09 111.93 o
4 0 1 8890.02 9433.26 432.68 o
5 0 1 19988.12 22465.46 1439.54 o
6 0 1 5198.95 5733.41 308.03 o
7 0 1 26.16 48.58 37.84 o
8 0 1 482.95 481.88 82.83 o
-8 1 1 1862.91 2073.54 194.45 o
-7 1 1 7166.24 7425.29 526.95 o
-6 1 1 6487.68 6650.42 468.51 o
-5 1 1 451.27 455.66 65.59 o
-4 1 1 6955.11 7609.02 381.99 o
-1 1 1 590.45 657.20 36.77 o
0 1 1 11557.55 13098.18 572.26 o
1 1 1 32612.22 35217.38 1422.31 o
2 1 1 4815.34 4832.30 172.34 o
3 1 1 817.19 863.30 41.59 o
4 1 1 4976.44 5076.85 240.09 o
5 1 1 10031.78 10339.86 810.69 o
6 1 1 510.58 470.31 49.15 o
7 1 1 258.79 274.85 42.44 o
8 1 1 1227.10 1375.67 140.76 o
-7 2 1 2621.34 2421.38 212.56 o
-6 2 1 581.57 654.78 87.87 o
-5 2 1 2097.25 1807.29 156.39 o
-4 2 1 3538.51 4011.39 205.66 o
-3 2 1 327.43 285.63 33.43 o
-2 2 1 1104.18 973.96 132.25 o
-1 2 1 1328.13 1730.30 123.23 o
0 2 1 20226.45 21250.19 929.97 o
1 2 1 3648.48 4354.61 156.15 o
2 2 1 2618.53 2736.87 101.92 o
3 2 1 8182.09 8373.13 296.33 o
4 2 1 6210.29 6039.67 220.79 o
5 2 1 1513.06 1468.12 69.16 o
6 2 1 1822.02 1676.47 101.49 o
7 2 1 3430.30 3704.21 196.05 o
8 2 1 1899.37 2130.52 189.33 o
-7 3 1 316.77 377.72 77.87 o
-6 3 1 827.03 792.69 101.09 o
-5 3 1 2124.44 2179.90 185.61 o
-4 3 1 4086.10 3935.18 286.92 o
-3 3 1 1334.63 862.59 105.19 o
-2 3 1 696.41 712.71 56.05 o
-1 3 1 24117.54 26279.45 1151.83 o
0 3 1 30121.57 31970.52 1398.66 o
1 3 1 10.31 19.36 9.06 o
2 3 1 6224.12 7191.89 255.49 o
3 3 1 7221.22 7812.78 279.23 o
4 3 1 6913.96 6996.86 254.14 o
5 3 1 10.30 30.93 13.26 o
6 3 1 6174.89 6113.72 232.34 o
7 3 1 13260.21 14043.66 836.12 o
8 3 1 2627.69 2891.12 165.80 o
-6 4 1 3644.41 4347.96 338.57 o
-5 4 1 11868.11 13164.25 884.73 o
-4 4 1 3886.81 3836.49 285.32 o
-3 4 1 1575.61 1361.57 189.63 o
-2 4 1 9730.40 9958.07 375.98 o
-1 4 1 12392.87 12876.68 607.08 o
0 4 1 5546.79 6098.58 352.69 o
1 4 1 1421.47 1488.06 81.97 o
2 4 1 21673.83 24873.42 854.64 o
3 4 1 11108.64 11608.87 409.68 o
4 4 1 767.20 727.64 42.59 o
5 4 1 3666.65 3415.71 192.29 o
6 4 1 15016.38 15215.94 543.07 o
7 4 1 2635.61 2607.43 209.86 o
8 4 1 2.99 -26.44 30.68 o
-5 5 1 2241.87 2422.70 210.44 o
-4 5 1 1.89 10.08 28.93 o
-3 5 1 1120.24 1166.39 110.81 o
-2 5 1 2554.21 2488.38 146.73 o
-1 5 1 2646.63 2637.06 146.57 o
0 5 1 579.60 684.25 50.52 o
2 5 1 5118.99 5369.49 201.79 o
3 5 1 59.33 70.70 15.85 o
4 5 1 250.15 237.72 31.75 o
5 5 1 1039.18 916.29 63.91 o
6 5 1 3631.33 3600.73 178.70 o
7 5 1 776.27 835.88 67.83 o
8 5 1 853.02 840.10 104.53 o
-4 6 1 765.40 826.07 101.31 o
-3 6 1 2198.11 2383.55 194.45 o
-2 6 1 236.00 286.71 45.65 o
-1 6 1 36.73 55.64 27.50 o
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2 6 1 5532.61 5894.35 489.59 o
3 6 1 9.06 8.95 16.47 o
4 6 1 2432.84 2505.05 171.40 o
5 6 1 5596.24 5471.91 379.76 o
6 6 1 1827.44 1796.55 106.66 o
7 6 1 959.22 970.48 113.00 o
8 6 1 4504.11 4642.48 346.75 o
-3 7 1 3655.78 3797.49 290.57 o
-2 7 1 399.99 413.22 79.55 o
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0 7 1 9587.16 10274.21 671.43 o
1 7 1 18157.14 18527.18 1159.67 o
2 7 1 5.49 22.13 32.58 o
3 7 1 4660.62 4812.16 342.00 o
4 7 1 7630.10 7199.94 487.07 o
5 7 1 1643.06 1628.48 153.83 o
6 7 1 35.80 61.80 43.46 o
7 7 1 3517.02 3442.85 272.46 o
8 7 1 6084.12 5998.86 432.65 o
-1 8 1 3253.64 3144.17 259.17 o
0 8 1 2722.75 2796.11 233.89 o
1 8 1 1436.29 1499.84 150.11 o
2 8 1 1567.11 1490.86 146.82 o
3 8 1 4708.28 4532.18 334.11 o
4 8 1 1265.31 1019.93 117.31 o
5 8 1 212.91 195.40 62.53 o
6 8 1 570.00 538.93 87.58 o
7 8 1 3424.01 3060.17 255.51 o
0 9 1 655.67 722.13 109.64 o
1 9 1 15.19 11.03 40.83 o
2 9 1 3107.27 3114.80 259.24 o
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4 9 1 54.96 67.13 47.41 o
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-5 -9 2 2799.84 2706.77 233.75 o
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-2 -9 2 1024.33 1080.56 127.98 o
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-7 -8 2 1329.31 1301.89 143.32 o
-6 -8 2 524.26 577.35 91.23 o
-5 -8 2 9.75 8.98 39.08 o
-4 -8 2 1852.99 1844.62 170.78 o
-3 -8 2 3734.99 3751.10 286.78 o
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0 -8 2 1773.26 1689.98 165.37 o
1 -8 2 6606.88 6638.09 628.56 o
2 -8 2 2037.99 1920.12 140.94 o
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-5 -7 2 868.62 800.07 99.34 o
-4 -7 2 12447.32 12598.15 807.59 o
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-2 -7 2 364.06 368.95 67.27 o
-1 -7 2 3157.76 2981.27 175.49 o
0 -7 2 7399.85 7489.53 365.94 o
1 -7 2 1696.71 1531.78 109.60 o
2 -7 2 322.13 359.67 57.77 o
3 -7 2 2519.46 2382.99 167.28 o
-8 -6 2 5914.44 6013.54 423.44 o
-7 -6 2 2113.09 2177.92 187.22 o
-6 -6 2 865.11 906.20 104.82 o
-5 -6 2 6426.08 6664.23 449.23 o
-4 -6 2 7797.23 7532.08 497.37 o
-3 -6 2 2310.03 2229.79 177.43 o
-2 -6 2 587.20 601.87 54.93 o
-1 -6 2 1448.99 1512.55 96.25 o
0 -6 2 4714.87 4462.07 228.67 o
1 -6 2 1627.75 1610.53 107.64 o
2 -6 2 4028.26 4070.32 317.02 o
3 -6 2 5128.76 4728.81 267.34 o
4 -6 2 1274.54 1103.42 143.53 o
-7 -5 2 0.65 -5.77 28.34 o
-6 -5 2 325.51 332.54 45.42 o
-5 -5 2 1536.81 1538.83 101.10 o
-4 -5 2 3513.66 3299.29 236.67 o
-3 -5 2 100.71 131.08 28.96 o
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-1 -5 2 4488.77 4536.37 174.30 o
0 -5 2 209.16 256.60 38.17 o
1 -5 2 1837.14 1676.01 106.56 o
2 -5 2 4601.12 4252.11 227.10 o
3 -5 2 2688.31 2381.23 156.70 o
4 -5 2 1263.90 1113.88 104.13 o
5 -5 2 123.44 130.70 36.50 o
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