#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:49:45 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181297 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237573.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237573_Fobs loop_ _publ_author_name 'Guenifa, Fatiha' 'Zeghouan, Ouahida' 'Hadjadj, Nasreddine' 'Bendjeddou, Lamia' 'Merazig, Hocine' _publ_section_title ; catena-Poly[[bis[4-(dimethylamino)pyridine-\kN^1^]cobalt(II)]-di-\m-azido-\k^4^N^1^:N^3^] ; _journal_coeditor_code VM2189 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m175 _journal_volume 69 _journal_year 2013 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6220 _cell_length_b 18.4040 _cell_length_c 9.7340 _exptl_crystal_F_000 804.00 _reflns_d_resolution_high 0.7098 _cod_data_source_file vm2189Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lamia_fa11_0m in C m c m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 296.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z-1/2' '-x, y, z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 88054.34 86882.66 1512.31 o 4 0 0 11061.45 11018.77 182.68 o 6 0 0 40058.13 37962.13 970.19 o 8 0 0 12955.75 11956.98 326.05 o 10 0 0 2030.54 1793.59 79.41 o 12 0 0 1070.57 1080.85 69.96 o 3 1 0 3363.62 3452.69 39.11 o 5 1 0 4883.56 4781.56 96.95 o 7 1 0 5488.02 5235.23 109.72 o 9 1 0 131.64 129.97 18.91 o 11 1 0 297.97 289.11 27.25 o 13 1 0 240.28 223.55 27.82 o 2 2 0 2480.62 2729.13 37.20 o 4 2 0 678.73 892.36 16.51 o 6 2 0 3108.73 2849.35 66.10 o 8 2 0 55.62 21.97 36.92 o 10 2 0 112.66 81.21 18.58 o 12 2 0 283.55 305.93 29.56 o 1 3 0 13723.49 14267.71 177.00 o 3 3 0 1125.37 1087.21 16.14 o 5 3 0 5190.64 5600.08 89.92 o 7 3 0 2772.69 2917.97 69.53 o 9 3 0 56.96 34.97 35.68 o 11 3 0 259.56 244.50 44.74 o 13 3 0 429.20 353.19 31.72 o 2 4 0 201.35 167.56 8.44 o 4 4 0 2000.44 2095.07 34.01 o 6 4 0 4658.77 4398.89 75.24 o 8 4 0 6.86 3.79 11.49 o 10 4 0 0.79 5.23 15.89 o 12 4 0 561.97 602.13 38.26 o 1 5 0 5854.96 5857.09 62.64 o 3 5 0 306.23 344.83 19.09 o 5 5 0 756.04 688.88 18.89 o 7 5 0 706.53 749.24 23.14 o 9 5 0 54.48 21.94 15.92 o 11 5 0 5.89 -10.41 17.53 o 13 5 0 51.49 48.69 21.81 o 0 6 0 1976.40 1857.71 31.96 o 2 6 0 2261.67 2406.00 36.33 o 4 6 0 2817.54 3244.10 48.89 o 6 6 0 237.94 187.84 14.39 o 8 6 0 3.56 1.82 18.58 o 10 6 0 156.67 194.09 23.25 o 12 6 0 1.41 -1.12 19.13 o 1 7 0 68.82 72.69 6.00 o 3 7 0 99.90 164.71 16.74 o 5 7 0 86.44 89.93 11.06 o 7 7 0 0.93 11.27 12.27 o 9 7 0 135.54 100.28 19.11 o 11 7 0 2.81 16.69 20.43 o 13 7 0 9.10 7.16 20.51 o 0 8 0 8684.18 9076.59 165.99 o 2 8 0 5607.02 5462.91 84.19 o 4 8 0 3483.00 3691.19 63.83 o 6 8 0 1767.26 1743.51 42.70 o 8 8 0 929.59 899.10 31.70 o 10 8 0 327.59 294.11 45.44 o 12 8 0 60.63 54.39 40.10 o 1 9 0 4448.05 4467.04 72.59 o 3 9 0 7675.38 7633.25 144.51 o 5 9 0 4074.09 3992.87 70.27 o 7 9 0 941.73 963.76 31.28 o 9 9 0 303.91 332.24 27.23 o 11 9 0 310.74 316.80 29.52 o 0 10 0 933.12 799.25 18.52 o 2 10 0 590.79 569.41 24.99 o 4 10 0 881.56 768.63 30.86 o 6 10 0 968.14 1006.83 32.85 o 8 10 0 92.63 137.25 16.92 o 10 10 0 38.83 66.60 41.27 o 12 10 0 100.26 136.37 24.04 o 1 11 0 3043.63 2858.16 43.64 o 3 11 0 1968.99 1922.81 36.94 o 5 11 0 2615.10 2562.46 51.75 o 7 11 0 733.43 687.10 28.65 o 9 11 0 131.59 130.80 18.17 o 11 11 0 280.60 312.44 28.98 o 0 12 0 4271.15 4345.83 89.74 o 2 12 0 2104.57 2137.91 52.41 o 4 12 0 1417.86 1367.52 31.43 o 6 12 0 1392.16 1337.75 36.87 o 8 12 0 554.92 552.32 27.22 o 10 12 0 316.69 357.98 39.29 o 12 12 0 94.68 69.28 22.12 o 1 13 0 5837.83 5365.19 67.70 o 3 13 0 24.23 29.24 12.96 o 5 13 0 162.97 175.45 16.17 o 7 13 0 1334.54 1467.41 58.38 o 9 13 0 527.94 568.51 28.96 o 11 13 0 5.37 -17.12 24.31 o 0 14 0 2984.65 2985.08 68.73 o 2 14 0 610.73 652.90 22.47 o 4 14 0 86.51 101.51 16.23 o 6 14 0 554.04 535.51 29.31 o 8 14 0 410.45 426.16 25.50 o 10 14 0 132.25 155.20 20.96 o 1 15 0 1007.29 946.83 20.29 o 3 15 0 1167.98 1213.66 41.13 o 5 15 0 976.31 1040.25 34.16 o 7 15 0 194.68 209.12 19.47 o 9 15 0 123.90 118.00 19.70 o 11 15 0 175.30 240.15 26.18 o 0 16 0 111.57 133.30 19.73 o 2 16 0 77.58 107.83 10.91 o 4 16 0 245.60 238.46 22.22 o 6 16 0 86.19 59.03 15.66 o 8 16 0 1.20 10.84 15.35 o 10 16 0 24.57 24.50 17.48 o 1 17 0 91.69 120.79 14.98 o 3 17 0 1002.94 904.98 26.31 o 5 17 0 808.86 801.90 42.67 o 7 17 0 10.73 9.48 20.00 o 9 17 0 15.71 -4.40 16.61 o 0 18 0 0.07 15.48 15.23 o 2 18 0 218.87 219.28 23.92 o 4 18 0 424.95 400.64 30.80 o 6 18 0 10.90 10.87 15.10 o 8 18 0 6.78 20.28 14.64 o 1 19 0 218.35 200.48 18.90 o 3 19 0 134.18 105.98 21.59 o 5 19 0 265.86 256.16 19.52 o 7 19 0 71.64 109.66 16.93 o 9 19 0 1.32 -14.84 14.84 o 0 20 0 477.15 556.74 48.82 o 2 20 0 3.34 5.57 14.28 o 4 20 0 34.49 31.62 16.10 o 6 20 0 141.57 144.19 17.65 o 8 20 0 31.78 25.44 15.79 o 1 21 0 825.36 833.85 74.39 o 3 21 0 3.89 -14.38 14.38 o 5 21 0 230.59 254.13 20.48 o 7 21 0 388.92 420.86 24.25 o 0 22 0 528.04 508.78 50.98 o 2 22 0 79.85 70.72 22.93 o 4 22 0 108.87 114.40 19.68 o 6 22 0 467.41 467.26 25.05 o 1 23 0 754.91 751.87 43.58 o 3 23 0 56.11 81.46 25.74 o 5 23 0 478.90 512.20 61.97 o 0 24 0 432.82 312.27 46.73 o 2 24 0 21.58 -22.74 22.74 o 4 24 0 33.89 30.97 25.84 o 1 25 0 449.50 508.37 40.36 o 3 25 0 37.69 68.26 27.93 o 3 1 1 16667.79 16735.77 121.34 o 5 1 1 5788.05 5714.24 49.34 o 7 1 1 191.60 197.88 11.38 o 9 1 1 0.28 13.57 11.20 o 11 1 1 337.17 328.47 19.73 o 13 1 1 196.81 164.37 18.79 o 0 2 1 59.36 -2.87 2.87 o 2 2 1 4.55 -1.86 1.86 o 4 2 1 510.45 518.56 8.47 o 6 2 1 989.88 1032.46 15.88 o 8 2 1 1.38 -5.02 8.31 o 10 2 1 0.78 -18.56 18.56 o 12 2 1 156.78 151.94 16.68 o 1 3 1 6192.56 6409.02 97.09 o 3 3 1 2467.23 2443.53 36.31 o 5 3 1 3657.91 3584.00 37.02 o 7 3 1 1134.10 1051.42 22.99 o 9 3 1 64.00 82.67 12.40 o 11 3 1 132.64 161.59 16.09 o 13 3 1 112.41 111.27 16.02 o 0 4 1 1216.29 1315.86 16.19 o 2 4 1 27.48 46.75 4.33 o 4 4 1 8.15 24.96 4.51 o 6 4 1 900.37 810.85 14.90 o 8 4 1 269.55 253.08 13.58 o 10 4 1 51.34 52.90 16.09 o 12 4 1 52.17 81.02 15.35 o 1 5 1 15047.07 15562.78 108.66 o 3 5 1 236.34 383.23 8.37 o 5 5 1 693.99 494.54 12.19 o 7 5 1 2420.19 2360.10 34.40 o 9 5 1 359.92 357.94 18.56 o 11 5 1 29.43 23.50 13.70 o 13 5 1 12.82 8.97 13.51 o 0 6 1 12313.30 11962.83 136.76 o 2 6 1 3883.97 3725.01 36.77 o 4 6 1 2367.42 2507.08 55.85 o 6 6 1 3419.77 3395.91 40.31 o 8 6 1 662.19 669.36 21.34 o 10 6 1 246.11 263.59 17.71 o 12 6 1 217.79 235.32 18.75 o 1 7 1 8882.42 8950.99 73.52 o 3 7 1 3343.43 3226.34 55.94 o 5 7 1 4183.97 3936.19 44.49 o 7 7 1 1778.40 1741.89 28.90 o 9 7 1 480.88 494.77 21.36 o 11 7 1 548.40 544.96 34.56 o 13 7 1 171.76 179.93 22.81 o 0 8 1 38382.19 39725.60 495.80 o 2 8 1 8413.44 8370.79 78.15 o 4 8 1 2828.17 2992.69 51.72 o 6 8 1 5492.35 5477.45 60.44 o 8 8 1 2457.73 2387.78 40.25 o 10 8 1 661.40 643.76 25.36 o 12 8 1 236.94 260.73 18.38 o 1 9 1 4884.51 5173.53 44.89 o 3 9 1 586.53 587.78 11.83 o 5 9 1 1757.83 1775.40 28.14 o 7 9 1 1127.94 1046.84 22.67 o 9 9 1 251.06 239.47 15.11 o 11 9 1 119.39 121.67 15.22 o 0 10 1 619.93 542.93 15.23 o 2 10 1 245.37 215.77 7.40 o 4 10 1 300.31 261.41 10.64 o 6 10 1 388.75 426.57 13.72 o 8 10 1 24.34 27.94 9.58 o 10 10 1 14.15 26.18 12.78 o 12 10 1 40.19 24.41 18.47 o 1 11 1 353.80 336.69 10.80 o 3 11 1 206.22 200.18 7.36 o 5 11 1 658.38 709.00 24.43 o 7 11 1 168.32 169.87 11.62 o 9 11 1 0.69 -4.37 10.16 o 11 11 1 43.50 80.59 19.38 o 0 12 1 14.57 3.52 7.29 o 2 12 1 485.14 432.48 10.46 o 4 12 1 2152.77 2170.28 37.55 o 6 12 1 383.15 381.15 15.59 o 8 12 1 41.05 40.13 10.27 o 10 12 1 21.11 26.86 15.17 o 1 13 1 199.44 186.10 7.33 o 3 13 1 15.85 14.02 5.84 o 5 13 1 0.33 -5.58 9.46 o 7 13 1 74.10 91.07 10.51 o 9 13 1 12.74 24.38 11.29 o 11 13 1 2.68 -13.26 25.11 o 0 14 1 431.94 403.15 21.71 o 2 14 1 1339.50 1256.15 21.04 o 4 14 1 2502.59 2486.75 38.15 o 6 14 1 768.70 804.12 21.78 o 8 14 1 28.95 33.25 10.45 o 10 14 1 107.23 110.44 20.88 o 1 15 1 1089.54 1078.81 19.51 o 3 15 1 1106.41 1023.24 21.49 o 5 15 1 1444.68 1476.28 26.01 o 7 15 1 400.97 430.22 21.92 o 9 15 1 49.07 36.14 12.97 o 11 15 1 165.68 185.02 24.00 o 0 16 1 726.11 829.02 29.11 o 2 16 1 269.62 268.36 10.09 o 4 16 1 401.01 396.16 15.44 o 6 16 1 499.13 547.67 17.72 o 8 16 1 27.90 24.95 10.37 o 10 16 1 4.55 30.48 16.96 o 1 17 1 1427.43 1340.41 23.20 o 3 17 1 673.09 708.02 19.48 o 5 17 1 833.12 869.62 22.01 o 7 17 1 551.27 566.81 21.30 o 9 17 1 139.25 125.37 17.59 o 0 18 1 7279.64 6569.03 111.29 o 2 18 1 3168.32 2926.11 42.11 o 4 18 1 1173.14 1182.94 24.25 o 6 18 1 2170.50 2196.73 35.03 o 8 18 1 1439.56 1587.65 35.80 o 1 19 1 1312.67 1246.26 27.72 o 3 19 1 360.16 377.85 20.61 o 5 19 1 619.98 630.94 18.34 o 7 19 1 544.68 572.00 32.97 o 9 19 1 133.55 122.50 18.10 o 0 20 1 614.89 605.60 28.98 o 2 20 1 408.64 465.10 20.57 o 4 20 1 411.77 461.31 21.86 o 6 20 1 291.12 321.36 18.68 o 8 20 1 46.05 28.99 15.42 o 1 21 1 624.80 648.78 24.22 o 3 21 1 39.79 22.52 12.98 o 5 21 1 92.15 82.28 16.42 o 7 21 1 183.19 226.78 18.54 o 0 22 1 93.27 128.47 19.81 o 2 22 1 3.02 7.42 12.93 o 4 22 1 1.99 9.57 12.73 o 6 22 1 32.40 38.63 13.27 o 1 23 1 51.22 74.13 15.07 o 3 23 1 35.25 8.24 14.29 o 5 23 1 46.44 34.23 13.60 o 0 24 1 1.63 -22.47 22.47 o 2 24 1 0.73 -3.25 14.45 o 4 24 1 1.45 -8.58 14.49 o 1 25 1 5.96 15.53 17.63 o 3 25 1 77.69 91.61 17.34 o 2 0 2 47723.28 47452.43 1194.06 o 4 0 2 13673.55 13916.90 158.70 o 6 0 2 4604.44 4488.00 64.96 o 8 0 2 8917.73 8682.53 138.29 o 10 0 2 3233.17 3185.83 77.83 o 12 0 2 43.34 41.85 17.15 o 1 1 2 5116.42 5285.72 81.52 o 3 1 2 17420.76 17898.22 183.21 o 5 1 2 1722.54 1673.77 18.76 o 7 1 2 679.66 672.70 14.98 o 9 1 2 2489.20 2362.08 38.37 o 11 1 2 294.97 321.14 22.51 o 13 1 2 1.30 24.40 24.32 o 0 2 2 5763.04 6047.49 187.33 o 2 2 2 5568.19 5515.09 57.97 o 4 2 2 7782.00 7250.33 78.47 o 6 2 2 6.15 3.82 4.45 o 8 2 2 172.12 139.14 9.52 o 10 2 2 494.75 475.09 25.69 o 12 2 2 17.89 8.74 15.32 o 1 3 2 1324.79 1279.04 18.07 o 3 3 2 15412.88 15804.94 141.53 o 5 3 2 2660.07 2797.36 29.66 o 7 3 2 273.55 281.72 12.74 o 9 3 2 776.62 756.61 20.53 o 11 3 2 281.05 297.18 16.78 o 13 3 2 65.99 60.76 16.85 o 0 4 2 7284.99 7437.63 71.78 o 2 4 2 2272.32 2355.02 24.80 o 4 4 2 6311.10 6616.85 65.74 o 6 4 2 5.39 8.55 3.90 o 8 4 2 6.02 -0.62 6.18 o 10 4 2 238.94 234.30 12.74 o 12 4 2 43.39 39.53 21.05 o 1 5 2 465.92 467.39 6.31 o 3 5 2 2047.56 2016.27 26.70 o 5 5 2 3.35 -2.85 3.21 o 7 5 2 42.59 35.15 6.05 o 9 5 2 129.69 129.21 10.21 o 11 5 2 0.58 12.63 15.08 o 13 5 2 16.19 24.56 19.56 o 0 6 2 2.16 0.87 3.45 o 2 6 2 186.95 200.00 6.16 o 4 6 2 35.35 49.24 4.98 o 6 6 2 147.31 161.96 8.02 o 8 6 2 126.03 121.64 7.65 o 10 6 2 16.41 7.56 19.59 o 12 6 2 75.03 80.79 18.51 o 1 7 2 3090.97 3348.46 30.17 o 3 7 2 256.39 271.01 7.78 o 5 7 2 192.71 198.36 7.92 o 7 7 2 500.25 430.74 11.66 o 9 7 2 12.28 -4.50 11.41 o 11 7 2 3.24 9.64 15.95 o 0 8 2 5295.20 5485.13 60.39 o 2 8 2 1244.61 1246.52 14.67 o 4 8 2 823.04 954.80 16.66 o 6 8 2 1753.65 1808.47 27.92 o 8 8 2 453.53 432.95 16.81 o 10 8 2 59.53 57.26 14.53 o 12 8 2 130.30 151.56 21.21 o 1 9 2 2322.11 2259.40 24.07 o 3 9 2 3747.38 3692.72 38.73 o 5 9 2 2893.60 3069.85 69.01 o 7 9 2 739.28 823.91 21.82 o 9 9 2 60.38 100.19 14.56 o 11 9 2 205.54 201.79 22.26 o 0 10 2 1607.96 1407.15 26.51 o 2 10 2 1506.61 1424.99 19.32 o 4 10 2 1396.48 1328.55 21.02 o 6 10 2 1205.78 1314.30 34.09 o 8 10 2 158.99 171.33 21.61 o 10 10 2 33.64 51.69 15.04 o 12 10 2 185.52 194.84 24.43 o 1 11 2 3758.18 3687.37 34.39 o 3 11 2 4272.63 4155.58 43.07 o 5 11 2 3570.05 3714.89 71.92 o 7 11 2 1241.21 1280.78 41.76 o 9 11 2 283.58 296.86 22.52 o 11 11 2 385.12 442.50 29.25 o 0 12 2 3955.23 4097.65 60.91 o 2 12 2 3097.87 3210.97 38.13 o 4 12 2 1827.09 1797.22 23.96 o 6 12 2 1199.76 1232.59 31.93 o 8 12 2 641.35 686.50 37.60 o 10 12 2 262.47 241.66 20.71 o 1 13 2 1177.45 1142.60 17.01 o 3 13 2 289.88 283.66 10.59 o 5 13 2 143.54 142.28 11.61 o 7 13 2 410.29 474.75 30.04 o 9 13 2 142.23 161.02 17.92 o 11 13 2 34.26 21.67 16.31 o 0 14 2 3253.75 3270.61 59.58 o 2 14 2 1256.36 1232.48 19.57 o 4 14 2 234.28 230.60 12.29 o 6 14 2 680.36 752.34 32.91 o 8 14 2 593.10 610.70 26.55 o 10 14 2 93.40 100.62 18.23 o 1 15 2 1726.07 1631.49 30.19 o 3 15 2 1562.47 1587.91 27.95 o 5 15 2 1272.93 1233.70 28.56 o 7 15 2 571.90 587.41 20.29 o 9 15 2 185.99 187.50 20.08 o 0 16 2 392.65 415.10 43.15 o 2 16 2 119.78 117.82 10.97 o 4 16 2 168.47 155.05 12.16 o 6 16 2 282.34 273.79 19.45 o 8 16 2 12.44 7.63 13.18 o 10 16 2 0.83 0.49 26.93 o 1 17 2 120.84 130.04 10.53 o 3 17 2 199.53 200.73 12.65 o 5 17 2 483.95 466.30 18.15 o 7 17 2 53.04 45.81 12.33 o 9 17 2 22.39 8.08 18.01 o 0 18 2 77.13 67.60 18.64 o 2 18 2 1.36 10.83 9.12 o 4 18 2 7.37 -9.69 9.69 o 6 18 2 100.76 80.28 12.16 o 8 18 2 0.82 23.81 14.73 o 1 19 2 40.94 23.20 11.38 o 3 19 2 434.07 439.29 19.04 o 5 19 2 47.59 35.92 11.81 o 7 19 2 60.55 28.26 15.85 o 9 19 2 21.86 -10.92 19.24 o 0 20 2 23.54 18.16 14.99 o 2 20 2 245.35 235.21 16.66 o 4 20 2 182.37 169.59 21.66 o 6 20 2 0.67 -1.86 13.98 o 8 20 2 55.90 55.01 16.78 o 1 21 2 84.11 65.09 14.13 o 3 21 2 340.52 333.53 21.26 o 5 21 2 48.91 33.90 14.71 o 7 21 2 14.72 15.65 15.72 o 0 22 2 12.83 40.98 17.22 o 2 22 2 277.65 313.49 19.48 o 4 22 2 532.93 551.71 24.33 o 6 22 2 11.78 -3.64 15.15 o 1 23 2 267.76 255.10 17.45 o 3 23 2 940.41 1076.27 32.72 o 5 23 2 329.34 370.60 23.07 o 0 24 2 8.55 -11.28 24.21 o 2 24 2 287.02 283.67 20.17 o 4 24 2 463.47 510.55 26.05 o 1 25 2 140.99 160.09 18.83 o 3 25 2 628.15 590.17 58.88 o 1 1 3 9994.99 10365.52 95.78 o 3 1 3 1294.74 1295.98 24.41 o 5 1 3 156.08 137.75 16.84 o 7 1 3 571.01 553.99 18.08 o 9 1 3 188.19 178.80 23.78 o 11 1 3 27.48 34.27 30.28 o 13 1 3 22.47 18.04 37.09 o 0 2 3 569.80 776.57 20.87 o 2 2 3 2439.04 2381.62 35.34 o 4 2 3 2634.73 2778.16 41.41 o 6 2 3 55.69 49.12 8.49 o 8 2 3 19.70 21.51 6.94 o 10 2 3 49.37 60.09 21.75 o 12 2 3 55.39 97.01 26.49 o 1 3 3 1246.43 1285.08 16.27 o 3 3 3 13895.48 13839.46 305.24 o 5 3 3 3174.76 3125.59 47.73 o 7 3 3 591.99 582.05 15.25 o 9 3 3 806.05 767.11 21.76 o 11 3 3 231.03 184.84 28.52 o 13 3 3 80.00 98.33 28.43 o 0 4 3 366.09 304.90 11.80 o 2 4 3 7827.47 8215.45 80.50 o 4 4 3 4934.13 4766.20 59.27 o 6 4 3 142.63 142.19 7.76 o 8 4 3 938.64 954.72 21.77 o 10 4 3 570.01 561.30 25.87 o 12 4 3 8.78 41.20 24.15 o 1 5 3 13.20 30.47 3.04 o 3 5 3 1279.69 1097.33 19.54 o 5 5 3 178.74 215.99 8.84 o 7 5 3 85.53 102.85 8.56 o 9 5 3 737.02 715.78 20.80 o 11 5 3 3.14 2.63 21.47 o 0 6 3 187.88 144.63 7.11 o 2 6 3 9866.06 10019.18 98.53 o 4 6 3 7372.34 7264.76 74.01 o 6 6 3 299.07 266.35 10.61 o 8 6 3 939.67 917.91 22.64 o 10 6 3 708.64 724.29 26.27 o 12 6 3 30.73 40.38 45.10 o 1 7 3 1969.12 1843.71 19.77 o 3 7 3 12308.95 12622.09 134.98 o 5 7 3 1760.20 1813.39 24.86 o 7 7 3 343.84 359.81 14.29 o 9 7 3 1441.48 1409.18 34.70 o 11 7 3 414.08 379.43 23.31 o 0 8 3 3200.44 3371.25 48.11 o 2 8 3 6301.67 6407.32 57.52 o 4 8 3 3296.61 3293.32 57.53 o 6 8 3 555.14 546.15 15.67 o 8 8 3 1858.91 1782.59 37.99 o 10 8 3 792.06 762.69 28.32 o 12 8 3 20.82 18.08 24.94 o 1 9 3 5154.73 5217.72 51.06 o 3 9 3 8083.43 8072.61 76.65 o 5 9 3 1795.05 1837.93 34.91 o 7 9 3 846.18 780.33 21.70 o 9 9 3 1181.37 1084.27 32.19 o 11 9 3 144.59 117.94 23.85 o 0 10 3 3.01 4.43 5.14 o 2 10 3 1399.65 1333.57 17.91 o 4 10 3 1487.67 1414.59 23.07 o 6 10 3 92.19 108.08 7.94 o 8 10 3 229.45 266.45 19.36 o 10 10 3 159.31 166.15 17.71 o 12 10 3 20.18 46.87 16.72 o 1 11 3 170.13 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