#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/75/2237574.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237574_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Ashraf, Mohamed' 'Kay, Andrew J.' _publ_section_title ; Bis(2-carboxy-N-{[1-(2-hydroxyethyl)-3,3-dimethylindolin-2-ylidene]methylimino}anilinium) sulfate monohydrate ; _journal_coeditor_code WM2718 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o343 _journal_page_last o344 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.681 _cell_angle_beta 87.688 _cell_angle_gamma 82.627 _cell_length_a 12.2530 _cell_length_b 14.6114 _cell_length_c 23.2442 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.9000 _[local]_cod_data_source_file wm2718Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' APYC P-1 SO4 anion 16Feb Twin -1 0 0 0 -1 0 0 -1 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10373.82 8934.97 265.46 o 3 0 0 1918.58 1650.95 42.56 o 4 0 0 62.65 152.10 17.12 o 5 0 0 6.27 12.30 4.27 o 6 0 0 1463.06 1702.95 43.40 o 7 0 0 70.37 66.67 5.10 o 8 0 0 2584.60 2912.74 139.52 o 9 0 0 185.64 246.43 26.92 o 10 0 0 1966.63 2220.46 119.58 o 11 0 0 127.13 150.39 25.46 o 12 0 0 36.69 38.43 14.14 o 13 0 0 131.65 137.97 23.22 o -13 1 0 3.96 3.67 24.41 o -12 1 0 101.44 114.08 19.70 o -11 1 0 84.09 102.45 32.34 o -10 1 0 709.59 739.40 51.75 o -9 1 0 306.79 343.45 38.98 o -8 1 0 7.57 12.04 11.45 o -7 1 0 2746.07 2748.67 90.18 o -6 1 0 240.31 225.84 27.05 o -5 1 0 511.64 473.69 14.77 o -4 1 0 9827.90 9026.35 214.52 o -3 1 0 7763.13 6316.00 162.68 o -2 1 0 18701.82 15853.64 390.14 o 2 1 0 8837.90 6993.80 166.22 o 3 1 0 295.91 233.70 48.95 o 4 1 0 675.98 687.03 23.59 o 5 1 0 3779.48 3379.87 80.70 o 6 1 0 4102.45 4398.72 111.12 o 7 1 0 910.13 806.64 25.41 o 8 1 0 148.47 160.33 12.38 o 9 1 0 622.33 635.69 45.22 o 10 1 0 158.72 159.35 31.99 o 11 1 0 232.93 182.02 31.95 o 12 1 0 80.10 92.24 21.76 o 13 1 0 0.05 0.05 11.71 o -13 2 0 5.42 2.08 14.87 o -12 2 0 172.27 184.57 22.81 o -11 2 0 39.57 44.83 16.07 o -10 2 0 2.96 3.65 37.87 o -9 2 0 420.76 421.94 46.14 o -8 2 0 334.60 325.67 47.20 o -7 2 0 294.21 318.91 17.49 o -6 2 0 638.49 681.65 72.09 o -5 2 0 4414.79 4493.97 101.78 o -4 2 0 5641.52 5744.20 145.07 o -3 2 0 7572.00 7586.27 220.43 o -2 2 0 4704.93 4516.44 95.86 o -1 2 0 4994.40 4684.07 177.62 o 1 2 0 3189.67 2999.91 81.25 o 2 2 0 3410.13 3857.31 88.32 o 3 2 0 33.19 33.41 8.92 o 4 2 0 8202.01 8600.83 243.63 o 5 2 0 144.14 147.94 9.95 o 6 2 0 1015.17 1221.67 34.73 o 7 2 0 211.55 205.94 12.93 o 8 2 0 2675.08 2605.46 73.74 o 9 2 0 219.16 208.98 21.60 o 10 2 0 539.29 539.63 41.85 o 11 2 0 1.87 1.53 9.08 o 12 2 0 130.31 147.81 20.96 o 13 2 0 61.10 65.48 25.76 o -12 3 0 118.82 102.81 28.92 o -11 3 0 956.09 950.40 66.98 o -10 3 0 46.99 45.82 15.28 o -9 3 0 3.79 3.49 41.09 o -8 3 0 201.51 213.16 29.18 o -7 3 0 319.32 352.80 31.39 o -6 3 0 134.33 139.56 179.87 o -5 3 0 12.64 14.53 28.75 o -4 3 0 10.63 10.57 40.82 o -3 3 0 583.10 549.25 15.90 o -2 3 0 2432.55 2182.19 45.06 o -1 3 0 5693.60 5665.62 119.07 o 0 3 0 476.20 408.53 36.99 o 1 3 0 8.25 7.44 14.28 o 2 3 0 2799.21 2695.56 58.30 o 3 3 0 171.67 149.00 13.16 o 4 3 0 2168.08 2460.14 74.46 o 5 3 0 139.07 137.06 25.56 o 6 3 0 6776.41 7064.51 200.95 o 7 3 0 213.06 205.65 30.48 o 8 3 0 89.25 94.89 11.35 o 9 3 0 466.32 441.17 37.80 o 10 3 0 444.44 418.16 52.71 o 11 3 0 7.69 12.24 20.30 o 12 3 0 1135.97 1130.07 90.25 o 13 3 0 20.12 22.80 25.87 o -12 4 0 5.49 4.92 17.31 o -11 4 0 773.08 766.95 80.62 o -10 4 0 1060.21 978.44 70.51 o -9 4 0 3078.34 3172.69 160.80 o -8 4 0 168.31 168.24 26.46 o -7 4 0 2.89 3.19 10.64 o -6 4 0 3072.15 3457.13 113.83 o -5 4 0 1013.38 978.11 33.72 o -4 4 0 1130.08 1001.58 29.33 o 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1963.57 2102.24 62.04 o 6 5 0 1113.58 1045.58 33.44 o 7 5 0 347.52 343.00 20.85 o 8 5 0 0.83 2.66 5.68 o 9 5 0 2035.96 1969.95 96.81 o 10 5 0 24.34 23.63 25.11 o 11 5 0 20.97 23.62 14.14 o 12 5 0 515.37 457.40 47.92 o 13 5 0 174.06 163.54 42.34 o -11 6 0 68.08 97.47 33.31 o -10 6 0 815.63 849.47 88.94 o -9 6 0 0.04 0.05 35.75 o -8 6 0 1637.22 1622.02 176.89 o -7 6 0 12.46 13.06 101.70 o -6 6 0 1015.01 1160.28 54.90 o -5 6 0 61.98 58.45 29.22 o -4 6 0 452.33 495.86 22.21 o -3 6 0 61.97 68.92 47.90 o -2 6 0 884.11 970.55 31.10 o -1 6 0 2475.74 2534.70 70.03 o 0 6 0 4441.34 4963.04 115.37 o 1 6 0 2426.94 2454.34 67.68 o 2 6 0 10439.15 11405.48 338.63 o 3 6 0 131.24 106.71 9.09 o 4 6 0 978.37 1265.18 35.62 o 5 6 0 2832.98 3193.25 94.81 o 6 6 0 1741.33 1874.42 59.65 o 7 6 0 765.84 827.12 38.89 o 8 6 0 2164.63 2188.15 95.27 o 9 6 0 201.83 205.23 36.14 o 10 6 0 3.01 3.28 21.46 o 11 6 0 420.12 362.68 31.93 o 12 6 0 1497.53 1603.91 91.90 o 13 6 0 4.41 3.82 8.30 o -11 7 0 22.13 30.18 47.09 o -10 7 0 464.52 455.98 71.30 o -9 7 0 20.44 24.24 36.62 o -8 7 0 333.45 385.46 58.21 o -7 7 0 89.04 114.31 45.72 o -6 7 0 264.20 304.16 73.37 o -5 7 0 533.08 532.35 54.27 o -4 7 0 1350.19 1327.53 84.67 o -3 7 0 569.67 581.96 35.29 o -2 7 0 462.89 403.80 20.93 o -1 7 0 32.38 35.50 21.52 o 0 7 0 5395.64 5444.57 166.09 o 1 7 0 3436.27 3362.64 138.81 o 2 7 0 2159.99 1941.49 141.46 o 3 7 0 1065.21 1072.63 112.42 o 4 7 0 1195.29 1069.87 92.87 o 5 7 0 247.34 196.90 14.86 o 6 7 0 1110.77 1092.96 152.18 o 7 7 0 18.27 18.42 17.50 o 8 7 0 1.38 1.43 21.32 o 9 7 0 1294.39 1142.51 62.62 o 10 7 0 27.97 26.55 30.66 o 11 7 0 1601.92 1463.10 71.24 o 12 7 0 7.32 5.99 5.86 o -10 8 0 93.01 99.16 28.18 o -8 8 0 135.18 169.44 54.09 o -7 8 0 34.11 46.90 22.67 o -6 8 0 1973.72 2052.27 156.95 o -5 8 0 1029.95 1220.81 127.20 o -4 8 0 0.08 0.09 39.27 o -3 8 0 16.17 26.42 20.55 o -2 8 0 25.21 24.41 13.16 o -1 8 0 125.32 138.89 9.87 o 0 8 0 194.69 201.90 16.59 o 1 8 0 420.16 514.94 24.71 o 2 8 0 5.31 5.15 5.41 o 3 8 0 3.81 5.28 9.99 o 4 8 0 745.15 894.39 43.48 o 5 8 0 10.58 12.91 28.79 o 6 8 0 335.21 410.99 42.29 o 7 8 0 789.97 818.50 61.31 o 8 8 0 592.52 598.53 52.19 o 9 8 0 147.09 128.13 17.53 o 10 8 0 292.95 317.20 45.13 o 11 8 0 21.91 23.48 12.80 o 12 8 0 110.43 78.27 23.01 o -9 9 0 34.14 41.05 21.46 o -8 9 0 21.41 29.92 68.91 o -7 9 0 17.36 17.64 54.07 o -6 9 0 828.97 850.90 94.65 o -5 9 0 39.46 42.26 35.76 o -4 9 0 583.62 583.54 60.03 o -3 9 0 750.32 843.03 72.89 o -2 9 0 164.99 152.57 30.24 o -1 9 0 20.96 15.74 7.35 o 0 9 0 9.42 7.88 17.95 o 1 9 0 739.80 921.17 66.55 o 2 9 0 4.94 4.63 47.65 o 3 9 0 3.34 2.91 18.31 o 4 9 0 210.44 220.39 55.03 o 5 9 0 52.07 57.47 38.39 o 6 9 0 151.03 151.64 33.15 o 7 9 0 160.73 91.40 94.32 o 8 9 0 1221.77 1322.55 84.01 o 9 9 0 994.03 834.92 63.56 o 10 9 0 143.29 138.65 25.81 o 11 9 0 558.66 606.98 50.55 o -9 10 0 19.36 31.77 32.25 o -8 10 0 197.84 240.95 48.84 o -7 10 0 5.48 7.16 14.82 o -6 10 0 5.29 4.86 33.14 o -5 10 0 168.99 206.39 47.11 o -4 10 0 4.02 5.54 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14 0 272.45 517.58 43.78 o 5 14 0 24.62 59.16 22.67 o 6 14 0 811.20 1012.66 84.68 o 7 14 0 1.88 14.27 13.07 o -1 15 0 65.26 133.93 31.68 o 0 15 0 96.20 135.24 53.21 o 1 15 0 153.87 128.74 57.77 o 2 15 0 219.34 191.17 42.75 o 3 15 0 5.83 4.91 27.83 o 4 15 0 15.11 24.66 33.13 o -3 -15 1 11.86 7.06 12.20 o -2 -15 1 180.03 259.35 51.87 o -1 -15 1 151.88 106.09 31.49 o 0 -15 1 2.34 5.23 16.56 o -6 -14 1 212.57 243.36 52.34 o -5 -14 1 71.72 31.48 21.90 o -4 -14 1 7.17 17.44 19.03 o -3 -14 1 8.06 9.38 33.15 o -2 -14 1 7.29 22.03 24.41 o -1 -14 1 9.34 10.59 45.35 o 0 -14 1 54.91 26.35 39.53 o 1 -14 1 339.94 445.57 57.20 o 2 -14 1 91.31 89.49 34.80 o 3 -14 1 32.96 68.86 24.10 o -8 -13 1 80.40 46.07 21.70 o -7 -13 1 257.92 271.39 67.85 o -6 -13 1 73.24 84.99 20.92 o -5 -13 1 305.97 323.52 58.01 o -4 -13 1 1095.93 1344.63 77.55 o -3 -13 1 1413.76 1855.34 140.56 o -2 -13 1 199.22 212.60 50.59 o -1 -13 1 286.37 328.02 56.71 o 0 -13 1 673.04 764.67 153.13 o 1 -13 1 322.42 249.82 63.72 o 2 -13 1 0.54 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49.47 o 4 -11 1 145.41 175.66 35.75 o 5 -11 1 8.05 7.04 43.62 o 6 -11 1 12.58 18.24 34.88 o 7 -11 1 404.07 544.24 67.62 o 8 -11 1 55.82 57.71 23.09 o -11 -10 1 25.42 25.56 13.72 o -10 -10 1 250.85 317.63 42.60 o -9 -10 1 489.79 591.71 41.48 o -8 -10 1 1029.17 987.77 66.21 o -7 -10 1 487.47 465.28 63.72 o -6 -10 1 12.63 25.31 17.21 o -5 -10 1 7.33 9.66 22.67 o -4 -10 1 114.93 129.49 35.75 o -3 -10 1 33.98 79.41 28.88 o -2 -10 1 122.21 128.91 36.62 o -1 -10 1 1612.82 1689.30 119.39 o 0 -10 1 96.52 103.12 53.17 o 1 -10 1 15.38 16.44 40.99 o 2 -10 1 115.34 7.50 21.81 o 3 -10 1 285.24 338.20 73.98 o 4 -10 1 554.84 659.68 59.37 o 5 -10 1 157.66 187.32 69.62 o 6 -10 1 223.29 283.82 48.01 o 7 -10 1 208.12 217.66 37.51 o 8 -10 1 65.47 92.13 36.62 o 9 -10 1 269.36 363.02 49.06 o -11 -9 1 489.02 562.51 58.79 o -10 -9 1 143.06 126.92 24.02 o -9 -9 1 339.18 327.70 36.65 o -8 -9 1 454.41 516.53 46.67 o -7 -9 1 74.89 54.90 30.52 o -6 -9 1 25.47 24.18 35.77 o -5 -9 1 1133.39 1226.18 90.12 o -4 -9 1 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