#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:05 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181298 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/76/2237603.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237603_Fobs loop_ _publ_author_name 'Rajalakshmi, P.' 'Srinivasan, N.' 'Krishnakumar, R.V.' 'Razak, Ibrahim Abdul' 'Rosli, Mohd Mustaqim' _publ_section_title ; N-Butoxycarbonyl-5-oxo-L-proline ethyl ester ; _journal_coeditor_code BX2436 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o567 _journal_page_last o568 _journal_volume 69 _journal_year 2013 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 26.6884 _cell_length_b 5.7650 _cell_length_c 8.7054 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8508 _cod_data_source_file bx2436Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 144.36 79.64 3.01 o 8 0 0 204.96 190.72 6.28 o 10 0 0 2032.44 1791.79 57.93 o 12 0 0 121.47 121.40 5.49 o 14 0 0 1466.31 1435.11 97.78 o 16 0 0 10.69 14.13 1.40 o 18 0 0 223.62 226.54 15.71 o 22 0 0 445.90 515.78 24.93 o 24 0 0 362.88 420.72 20.40 o 26 0 0 2.09 3.88 0.91 o 28 0 0 9.70 8.73 0.97 o 30 0 0 2.75 8.20 0.64 o 1 1 0 267.80 275.96 14.01 o 3 1 0 1028.93 975.54 80.19 o 5 1 0 372.20 360.38 21.42 o 6 1 0 1293.00 1231.58 31.65 o 7 1 0 548.09 525.56 12.43 o 8 1 0 7447.87 6867.62 166.30 o 9 1 0 45.57 36.44 1.00 o 10 1 0 0.73 5.60 2.13 o 11 1 0 1286.62 1304.85 30.73 o 12 1 0 36.15 42.08 1.21 o 13 1 0 5.08 4.71 0.80 o 14 1 0 102.38 121.05 3.18 o 15 1 0 798.57 707.98 17.65 o 16 1 0 31.31 36.02 1.14 o 17 1 0 222.47 213.56 7.49 o 18 1 0 1.53 1.56 0.60 o 19 1 0 44.96 48.76 3.83 o 20 1 0 79.04 77.76 3.38 o 21 1 0 24.91 26.32 0.98 o 22 1 0 26.32 22.87 1.89 o 23 1 0 0.87 0.63 0.55 o 24 1 0 20.17 21.82 0.92 o 25 1 0 228.87 294.70 8.31 o 26 1 0 7.19 13.23 0.82 o 27 1 0 83.52 109.77 2.84 o 28 1 0 36.73 47.03 1.36 o 29 1 0 17.97 19.34 0.76 o 30 1 0 1.35 1.96 0.34 o 31 1 0 3.68 5.69 0.52 o 0 2 0 23.73 24.72 1.57 o 1 2 0 2.14 5.63 0.56 o 2 2 0 59.74 66.63 2.16 o 3 2 0 3301.27 3523.01 104.27 o 4 2 0 1240.58 1442.16 36.44 o 5 2 0 161.91 155.69 3.72 o 6 2 0 286.22 275.86 6.99 o 7 2 0 23.67 25.39 0.63 o 8 2 0 637.76 706.07 15.59 o 9 2 0 0.44 0.72 0.16 o 10 2 0 41.57 52.75 1.32 o 11 2 0 2291.73 2254.75 45.12 o 12 2 0 372.53 367.43 7.40 o 13 2 0 26.67 23.39 0.96 o 14 2 0 76.54 74.88 1.73 o 15 2 0 112.45 93.34 2.98 o 16 2 0 40.24 29.54 1.09 o 17 2 0 498.30 463.57 13.20 o 18 2 0 119.62 106.31 4.13 o 19 2 0 137.64 140.71 4.20 o 20 2 0 165.45 150.41 3.58 o 21 2 0 0.00 -0.09 0.33 o 22 2 0 1.98 2.52 0.36 o 23 2 0 426.93 458.72 10.22 o 24 2 0 69.05 74.97 1.82 o 25 2 0 167.90 188.38 3.62 o 26 2 0 25.82 22.02 0.75 o 27 2 0 0.34 -0.25 0.24 o 28 2 0 42.15 54.65 2.12 o 29 2 0 0.06 0.51 0.32 o 2 3 0 1755.82 2043.79 55.35 o 3 3 0 741.17 839.19 49.07 o 4 3 0 68.02 74.71 4.28 o 5 3 0 78.07 59.58 1.63 o 6 3 0 431.08 444.89 9.96 o 7 3 0 1.21 0.82 0.17 o 8 3 0 153.59 157.33 3.28 o 9 3 0 20.63 19.49 0.61 o 10 3 0 146.92 156.02 3.12 o 11 3 0 79.11 76.73 1.64 o 12 3 0 489.46 444.94 8.37 o 13 3 0 201.27 177.92 3.55 o 14 3 0 26.54 27.38 0.77 o 15 3 0 79.64 67.27 1.71 o 16 3 0 2.15 1.11 0.44 o 17 3 0 87.14 87.20 2.88 o 18 3 0 157.67 128.88 5.64 o 19 3 0 51.78 45.78 1.36 o 20 3 0 66.39 73.88 1.95 o 21 3 0 128.09 134.00 3.27 o 22 3 0 0.22 0.14 0.53 o 23 3 0 50.63 53.09 1.44 o 24 3 0 164.31 170.16 4.40 o 25 3 0 3.26 2.94 0.65 o 26 3 0 62.14 65.73 1.84 o 27 3 0 4.35 4.93 0.37 o 28 3 0 8.47 14.61 0.67 o 2 4 0 251.89 266.32 18.19 o 4 4 0 548.64 514.60 21.65 o 5 4 0 20.70 18.80 1.16 o 6 4 0 78.83 84.93 2.57 o 7 4 0 54.87 54.35 1.77 o 8 4 0 3.14 2.12 0.28 o 9 4 0 38.60 41.84 1.30 o 10 4 0 75.84 69.58 2.74 o 11 4 0 122.07 109.08 3.51 o 12 4 0 215.91 181.43 4.40 o 13 4 0 8.07 4.79 0.51 o 14 4 0 12.57 14.96 0.89 o 15 4 0 170.55 148.58 3.54 o 16 4 0 8.35 8.63 0.61 o 17 4 0 67.54 58.75 1.71 o 18 4 0 7.50 9.90 0.63 o 19 4 0 45.98 45.51 1.37 o 20 4 0 0.10 -0.13 0.49 o 21 4 0 0.51 1.16 0.75 o 22 4 0 12.95 9.50 1.77 o 23 4 0 83.48 77.36 2.66 o 24 4 0 1.85 1.92 0.72 o 25 4 0 28.90 31.69 1.79 o 4 5 0 9.32 9.73 1.91 o 5 5 0 1.86 3.04 0.95 o 6 5 0 100.78 97.54 4.27 o 7 5 0 6.47 8.04 1.04 o 8 5 0 123.05 131.18 4.52 o 9 5 0 440.19 406.90 12.89 o 10 5 0 77.11 65.42 2.67 o 11 5 0 2.28 1.14 0.62 o 12 5 0 33.55 37.60 1.58 o 13 5 0 279.33 245.78 7.69 o 14 5 0 66.23 52.07 1.95 o 15 5 0 15.93 21.10 1.38 o 16 5 0 8.78 8.48 1.37 o 17 5 0 5.06 7.14 2.42 o 18 5 0 17.98 20.07 1.22 o 19 5 0 14.63 18.88 1.12 o 20 5 0 65.97 69.82 2.80 o 21 5 0 3.44 1.40 0.42 o 7 6 0 26.71 41.38 2.56 o 8 6 0 121.05 118.34 6.04 o 9 6 0 12.11 24.82 1.81 o 10 6 0 110.93 108.06 5.51 o 11 6 0 0.00 2.90 0.83 o 12 6 0 121.97 107.56 5.43 o 13 6 0 1.17 6.91 0.90 o 14 6 0 1.14 1.31 0.63 o 3 0 1 714.27 606.88 24.68 o 5 0 1 2731.14 2397.30 52.66 o 7 0 1 277.09 245.77 6.51 o 8 0 1 212.72 174.66 4.38 o 9 0 1 358.61 290.73 31.31 o 10 0 1 341.67 299.25 6.73 o 11 0 1 5536.76 4806.94 113.50 o 12 0 1 206.61 223.95 6.14 o 13 0 1 2031.47 1871.32 90.08 o 14 0 1 582.87 578.07 27.96 o 15 0 1 135.84 132.90 4.93 o 16 0 1 181.06 181.42 6.65 o 17 0 1 396.51 390.08 13.95 o 18 0 1 153.73 148.85 7.38 o 21 0 1 186.90 221.80 7.86 o 22 0 1 115.09 122.76 3.95 o 23 0 1 34.58 42.41 1.72 o 24 0 1 5.83 10.67 0.84 o 25 0 1 4.53 1.65 0.51 o 26 0 1 45.78 52.01 1.85 o 27 0 1 30.85 39.90 1.47 o 28 0 1 38.47 54.38 1.81 o 29 0 1 66.10 85.51 2.19 o 30 0 1 20.97 29.70 0.86 o 31 0 1 7.34 7.74 0.73 o -30 1 1 5.77 7.46 0.38 o -29 1 1 17.98 23.67 0.78 o -28 1 1 54.91 72.42 1.94 o -27 1 1 58.13 66.60 1.54 o -26 1 1 17.00 24.49 0.81 o -25 1 1 2.46 3.25 0.47 o -24 1 1 171.01 191.91 4.04 o -23 1 1 35.96 37.87 1.09 o -22 1 1 30.14 27.21 1.14 o -21 1 1 450.17 491.42 11.02 o -20 1 1 48.67 49.60 2.19 o -19 1 1 579.35 590.27 24.79 o -18 1 1 276.21 287.92 16.03 o -17 1 1 100.03 98.53 4.53 o -16 1 1 61.19 60.84 2.33 o -15 1 1 83.35 72.48 2.03 o -14 1 1 462.30 428.06 10.76 o -13 1 1 1187.25 1181.89 29.46 o -12 1 1 29.85 29.39 0.88 o -11 1 1 1107.01 1050.41 23.28 o -10 1 1 119.62 115.72 2.90 o -9 1 1 257.98 265.90 6.31 o -8 1 1 208.57 197.42 5.25 o -7 1 1 3217.57 2999.87 71.08 o -6 1 1 1253.19 1109.79 25.07 o -5 1 1 637.62 647.53 14.87 o -4 1 1 8421.36 8518.15 249.86 o -3 1 1 2606.95 2721.60 78.09 o -2 1 1 4517.50 4571.90 128.67 o -1 1 1 411.23 421.49 21.88 o 1 1 1 409.57 442.27 20.82 o 2 1 1 4525.60 4677.86 200.87 o 3 1 1 2608.48 2719.97 119.64 o 4 1 1 8433.30 8647.22 228.44 o 5 1 1 648.63 652.37 15.26 o 6 1 1 1250.40 1175.62 30.36 o 7 1 1 3234.37 3230.06 67.85 o 8 1 1 208.12 202.82 4.96 o 9 1 1 256.39 268.67 6.08 o 10 1 1 120.76 121.27 2.93 o 11 1 1 1110.15 1080.38 24.57 o 12 1 1 30.27 31.76 1.41 o 13 1 1 1190.64 1220.56 36.53 o 14 1 1 461.97 433.71 13.34 o 15 1 1 82.14 73.73 2.50 o 16 1 1 60.63 60.75 3.07 o 17 1 1 102.39 98.57 7.47 o 18 1 1 275.38 302.45 20.51 o 19 1 1 576.91 594.08 41.02 o 20 1 1 48.60 49.51 2.30 o 21 1 1 452.13 491.53 13.04 o 22 1 1 29.76 26.78 1.18 o 23 1 1 35.44 37.28 1.33 o 24 1 1 170.12 191.04 5.28 o 25 1 1 2.35 3.51 0.60 o 26 1 1 16.58 23.35 1.00 o 27 1 1 58.18 64.22 1.97 o 28 1 1 54.79 73.23 2.14 o 29 1 1 18.03 23.60 1.03 o 30 1 1 5.82 7.77 0.52 o -29 2 1 19.84 31.16 0.97 o -28 2 1 30.70 40.39 1.23 o -27 2 1 36.36 52.80 1.30 o -26 2 1 46.29 52.47 1.34 o -25 2 1 41.19 43.24 1.01 o -24 2 1 41.62 39.59 1.04 o -23 2 1 111.22 112.62 2.42 o -22 2 1 163.32 179.82 4.26 o -21 2 1 151.90 153.25 3.62 o -20 2 1 16.84 14.19 0.85 o -19 2 1 92.30 95.51 2.70 o -18 2 1 36.84 34.77 1.59 o -17 2 1 43.91 39.55 1.23 o -16 2 1 27.82 22.99 0.85 o -15 2 1 26.88 19.49 0.85 o -14 2 1 109.22 92.28 2.37 o -13 2 1 290.18 265.47 5.56 o -12 2 1 680.13 653.90 13.40 o -11 2 1 82.12 82.17 1.82 o -10 2 1 160.84 157.39 3.44 o -9 2 1 1252.67 1242.41 26.97 o -8 2 1 43.77 46.07 1.17 o -7 2 1 1229.18 1345.18 32.23 o -6 2 1 459.60 476.94 13.49 o -5 2 1 1397.72 1469.42 43.80 o -4 2 1 449.05 497.72 12.45 o -3 2 1 617.91 648.06 23.34 o -2 2 1 407.86 514.31 37.17 o -1 2 1 1793.88 2107.59 62.47 o 0 2 1 144.04 157.50 8.13 o 1 2 1 1788.29 2122.93 55.10 o 2 2 1 408.76 491.42 26.84 o 3 2 1 613.10 613.43 18.38 o 4 2 1 447.86 475.77 14.37 o 5 2 1 1399.83 1491.68 40.29 o 6 2 1 459.36 479.69 10.25 o 7 2 1 1230.50 1370.93 27.43 o 8 2 1 42.84 46.47 0.98 o 9 2 1 1260.80 1282.76 24.69 o 10 2 1 162.59 165.66 3.09 o 11 2 1 80.72 78.60 1.63 o 12 2 1 681.28 650.74 11.77 o 13 2 1 292.32 265.67 5.06 o 14 2 1 108.97 93.34 2.04 o 15 2 1 26.51 19.24 1.07 o 16 2 1 27.87 22.08 0.82 o 17 2 1 42.65 36.35 1.17 o 18 2 1 36.81 34.21 1.65 o 19 2 1 93.09 98.56 2.95 o 20 2 1 16.98 13.66 1.18 o 21 2 1 151.87 150.83 3.93 o 22 2 1 163.90 178.93 4.04 o 23 2 1 112.60 116.94 2.80 o 24 2 1 42.00 41.23 2.14 o 25 2 1 40.96 43.06 3.94 o 26 2 1 46.04 53.69 2.72 o 27 2 1 36.34 52.82 1.60 o 28 2 1 30.44 39.85 1.64 o 29 2 1 19.85 32.44 1.61 o -27 3 1 62.39 72.96 1.93 o -26 3 1 24.12 27.34 0.83 o -25 3 1 26.54 30.35 0.93 o -24 3 1 3.84 6.11 0.44 o -23 3 1 75.44 75.83 1.86 o -22 3 1 6.14 7.02 0.46 o -21 3 1 19.38 17.92 0.97 o -20 3 1 42.59 40.12 1.21 o -19 3 1 53.83 49.03 1.42 o -18 3 1 40.43 29.48 1.34 o -17 3 1 141.44 140.72 3.70 o -16 3 1 278.03 222.14 5.76 o -15 3 1 174.36 157.14 3.65 o -14 3 1 144.31 133.52 2.87 o -13 3 1 783.79 687.97 14.11 o -12 3 1 12.53 9.88 0.44 o -11 3 1 10.08 8.94 0.41 o -10 3 1 58.41 53.64 1.23 o -9 3 1 680.13 654.53 12.60 o -8 3 1 99.12 86.40 1.95 o -7 3 1 26.59 29.95 0.80 o -6 3 1 31.75 27.98 0.76 o -5 3 1 87.59 101.63 3.32 o -4 3 1 1142.56 1225.73 32.21 o -3 3 1 231.58 321.03 13.23 o -1 3 1 663.02 806.61 26.25 o 0 3 1 55.85 180.94 8.78 o 1 3 1 663.24 752.07 32.24 o 2 3 1 886.09 1007.21 37.23 o 3 3 1 234.11 295.46 12.58 o 4 3 1 1143.82 1163.98 28.25 o 5 3 1 89.47 103.03 2.63 o 6 3 1 32.36 29.17 0.72 o 7 3 1 26.39 28.87 0.75 o 8 3 1 100.64 90.39 1.78 o 9 3 1 680.01 667.49 11.65 o 10 3 1 60.08 56.16 1.23 o 11 3 1 9.69 8.94 0.39 o 12 3 1 12.66 10.65 0.43 o 13 3 1 781.43 682.95 13.07 o 14 3 1 143.55 131.69 3.00 o 15 3 1 173.31 161.26 4.31 o 16 3 1 276.71 221.43 6.23 o 17 3 1 142.20 146.42 6.53 o 18 3 1 39.62 29.07 1.13 o 19 3 1 54.95 52.02 1.48 o 20 3 1 42.72 40.05 1.22 o 21 3 1 19.54 18.70 0.76 o 22 3 1 6.34 7.14 1.08 o 23 3 1 76.31 78.99 2.19 o 24 3 1 3.68 5.55 0.92 o 25 3 1 26.79 31.56 2.86 o 26 3 1 23.57 27.85 1.82 o 27 3 1 62.05 77.66 8.42 o -25 4 1 88.44 104.41 6.00 o -24 4 1 107.01 124.45 3.92 o -23 4 1 0.26 1.01 0.35 o -22 4 1 28.30 31.12 2.20 o -21 4 1 30.62 30.01 3.19 o -20 4 1 16.69 17.35 1.59 o -19 4 1 25.52 24.17 0.92 o -18 4 1 47.05 43.43 1.34 o -17 4 1 50.87 45.51 1.41 o -16 4 1 265.24 253.10 5.80 o -15 4 1 252.71 229.52 5.31 o -14 4 1 46.22 38.62 1.36 o -13 4 1 14.36 11.18 0.65 o -12 4 1 4.43 4.13 0.47 o -11 4 1 192.34 161.91 4.57 o -10 4 1 132.24 126.20 4.91 o -9 4 1 164.70 144.99 5.57 o -8 4 1 21.36 20.01 1.08 o -7 4 1 77.47 67.53 1.92 o -6 4 1 19.20 24.19 0.87 o -5 4 1 324.45 296.00 11.99 o -4 4 1 390.18 378.80 14.89 o -3 4 1 35.57 54.07 4.34 o -2 4 1 10.09 17.80 2.04 o -1 4 1 64.67 67.65 5.18 o 0 4 1 207.88 264.88 14.91 o 1 4 1 63.87 56.86 2.18 o 2 4 1 10.38 14.11 1.15 o 3 4 1 34.92 62.29 4.78 o 4 4 1 389.61 372.23 10.24 o 5 4 1 322.79 302.03 8.31 o 6 4 1 19.05 24.09 0.72 o 7 4 1 77.33 66.79 1.53 o 8 4 1 21.51 20.06 0.68 o 9 4 1 165.56 143.36 7.03 o 10 4 1 133.09 124.55 4.53 o 11 4 1 193.00 164.13 5.30 o 12 4 1 4.51 3.89 0.52 o 13 4 1 13.49 11.18 0.70 o 14 4 1 45.80 39.71 1.88 o 15 4 1 252.86 239.54 5.88 o 16 4 1 265.89 262.91 6.44 o 17 4 1 50.09 45.51 1.41 o 18 4 1 48.08 44.65 1.37 o 19 4 1 25.71 23.64 0.93 o 20 4 1 16.35 16.61 0.98 o 21 4 1 30.61 31.66 2.46 o 22 4 1 27.54 29.20 2.37 o 23 4 1 0.28 -0.23 2.03 o 25 4 1 89.03 83.84 6.16 o -20 5 1 32.39 31.35 2.07 o -19 5 1 2.30 2.56 0.54 o -18 5 1 27.78 26.06 1.38 o -17 5 1 19.74 19.34 1.21 o -16 5 1 1.07 1.48 0.63 o -15 5 1 54.81 50.70 2.33 o -14 5 1 8.06 7.86 0.88 o -13 5 1 1.13 1.38 0.53 o -12 5 1 41.97 34.11 1.76 o -11 5 1 34.05 34.74 1.52 o -10 5 1 128.09 101.94 4.89 o -9 5 1 89.32 85.26 3.18 o -8 5 1 50.88 48.91 2.71 o -7 5 1 163.28 148.75 5.13 o -6 5 1 9.20 9.30 1.30 o -5 5 1 1.05 3.97 1.38 o -4 5 1 355.36 329.48 22.43 o 4 5 1 356.09 340.31 12.40 o 5 5 1 1.07 2.01 0.71 o 6 5 1 9.33 18.78 3.19 o 7 5 1 161.07 155.43 5.91 o 8 5 1 51.04 48.75 2.26 o 9 5 1 87.42 86.41 3.52 o 10 5 1 129.18 108.26 4.26 o 11 5 1 34.33 34.00 1.76 o 12 5 1 41.79 35.48 1.78 o 13 5 1 0.93 1.10 0.64 o 14 5 1 8.42 10.54 1.40 o 15 5 1 54.94 56.99 3.30 o 16 5 1 0.99 1.20 0.95 o 17 5 1 19.60 20.41 1.62 o 19 5 1 2.37 1.29 0.81 o 20 5 1 32.30 30.26 1.37 o -14 6 1 14.25 16.80 1.24 o -13 6 1 2.21 3.73 0.53 o -12 6 1 115.31 123.23 6.16 o -11 6 1 16.47 24.95 1.70 o -10 6 1 37.27 42.21 2.47 o -9 6 1 24.85 26.11 1.83 o -8 6 1 112.45 106.50 5.46 o -7 6 1 76.61 92.49 4.84 o 6 6 1 184.39 203.13 10.04 o 7 6 1 77.08 92.18 4.83 o 8 6 1 112.79 111.91 5.73 o 9 6 1 24.66 23.88 1.77 o 10 6 1 37.49 41.76 2.48 o 11 6 1 16.79 24.55 1.69 o 12 6 1 115.64 124.87 6.23 o 13 6 1 2.31 3.73 0.77 o 14 6 1 13.84 15.30 1.16 o 1 0 2 1604.51 226.20 783.19 o 2 0 2 1943.32 1790.64 46.95 o 3 0 2 43.65 43.91 1.42 o 4 0 2 9655.66 8806.00 189.96 o 5 0 2 270.30 237.98 5.27 o 6 0 2 3719.91 3280.14 59.52 o 7 0 2 3386.76 3022.01 58.55 o 8 0 2 228.10 217.53 5.00 o 9 0 2 1442.06 1203.15 24.49 o 10 0 2 580.10 528.89 16.06 o 11 0 2 519.52 272.67 97.81 o 12 0 2 15.50 19.36 1.63 o 13 0 2 844.53 781.60 23.35 o 14 0 2 894.78 900.27 32.06 o 15 0 2 767.86 758.66 27.07 o 16 0 2 465.82 453.39 16.22 o 17 0 2 229.23 220.59 8.00 o 18 0 2 6.33 9.33 1.32 o 19 0 2 187.71 188.63 10.50 o 20 0 2 205.36 218.19 6.51 o 21 0 2 143.40 163.18 3.70 o 22 0 2 4.68 6.18 0.57 o 23 0 2 28.84 33.24 1.16 o 24 0 2 65.49 81.54 2.17 o 25 0 2 23.73 29.00 1.03 o 26 0 2 58.01 58.64 1.61 o 27 0 2 69.51 81.07 2.07 o 28 0 2 3.26 9.19 0.56 o 29 0 2 7.60 7.26 0.99 o 30 0 2 0.70 0.50 0.23 o -30 1 2 0.65 0.55 0.19 o -29 1 2 19.13 29.20 0.74 o -28 1 2 2.38 2.41 0.29 o -27 1 2 106.24 135.71 2.89 o -26 1 2 66.51 84.51 1.91 o -25 1 2 66.01 77.73 2.00 o -24 1 2 23.95 25.11 0.87 o -23 1 2 51.73 56.01 1.32 o -22 1 2 50.57 57.06 1.53 o -21 1 2 87.04 88.60 2.05 o -20 1 2 88.63 97.34 2.34 o -19 1 2 51.34 48.73 1.89 o -18 1 2 134.85 144.26 7.34 o -17 1 2 69.28 64.81 4.54 o -16 1 2 185.32 192.27 8.23 o -15 1 2 589.80 546.48 18.69 o -14 1 2 286.39 278.77 7.13 o -13 1 2 64.24 63.63 1.81 o -12 1 2 767.09 732.73 16.90 o -11 1 2 1523.70 1442.53 32.26 o -10 1 2 1259.71 1164.97 26.30 o -9 1 2 853.71 810.52 18.43 o -8 1 2 3315.66 3115.58 64.85 o -7 1 2 210.28 189.43 4.46 o -6 1 2 1031.62 983.59 25.25 o -5 1 2 8.31 8.70 0.47 o -4 1 2 2080.50 2273.11 56.17 o -3 1 2 1114.25 1139.63 25.57 o -2 1 2 2532.16 2606.48 72.02 o -1 1 2 500.76 539.79 16.60 o 0 1 2 32.46 43.28 2.04 o 1 1 2 502.95 525.18 12.23 o 2 1 2 2530.07 2593.14 50.05 o 3 1 2 1115.81 1101.73 22.90 o 4 1 2 2061.47 2263.54 48.28 o 5 1 2 8.40 9.03 0.33 o 6 1 2 1034.58 1041.41 20.15 o 7 1 2 208.94 198.90 3.58 o 8 1 2 3326.28 3390.16 59.15 o 9 1 2 855.40 875.64 15.98 o 10 1 2 1260.71 1232.00 24.61 o 11 1 2 1524.79 1490.52 34.38 o 12 1 2 771.28 754.46 19.89 o 13 1 2 64.84 64.57 1.70 o 14 1 2 288.29 284.03 6.75 o 15 1 2 593.85 550.15 14.86 o 16 1 2 185.70 182.32 6.18 o 17 1 2 67.88 56.20 2.65 o 18 1 2 135.13 144.36 10.43 o 19 1 2 52.18 48.45 3.85 o 20 1 2 89.10 95.99 3.16 o 21 1 2 86.74 87.08 2.61 o 22 1 2 50.68 54.18 1.95 o 23 1 2 51.52 54.56 1.62 o 24 1 2 23.73 25.32 0.94 o 25 1 2 66.80 78.36 2.48 o 26 1 2 66.10 84.24 2.29 o 27 1 2 107.66 134.98 3.96 o 28 1 2 2.32 2.65 0.44 o 29 1 2 19.31 27.82 1.15 o 30 1 2 0.72 0.86 0.26 o -29 2 2 2.71 3.01 0.29 o -28 2 2 28.58 39.83 1.20 o -27 2 2 2.23 2.02 0.24 o -26 2 2 28.73 34.44 0.95 o -25 2 2 5.69 8.87 0.42 o -24 2 2 31.18 33.19 0.85 o -23 2 2 250.37 285.73 7.11 o -22 2 2 97.74 100.37 2.16 o -21 2 2 223.55 236.65 4.73 o -20 2 2 77.96 77.80 1.92 o -19 2 2 24.09 23.08 1.03 o -18 2 2 146.74 146.13 4.19 o -17 2 2 261.74 232.56 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48.76 47.98 1.75 o 5 1 9 17.24 22.98 3.30 o 6 1 9 90.37 88.47 2.25 o 7 1 9 53.68 59.85 1.47 o 8 1 9 1.01 3.41 2.77 o 9 1 9 29.56 26.21 0.77 o 10 1 9 35.38 34.64 0.98 o 11 1 9 25.83 25.15 0.88 o 12 1 9 53.93 58.91 1.73 o 13 1 9 14.21 15.70 0.54 o 14 1 9 1.17 1.88 0.53 o -11 2 9 22.07 15.30 1.13 o -10 2 9 47.08 44.27 1.06 o -9 2 9 14.45 19.03 0.73 o -8 2 9 89.96 86.32 1.97 o -7 2 9 40.97 41.62 1.21 o -6 2 9 11.77 13.94 0.66 o -5 2 9 4.51 10.00 0.67 o -4 2 9 29.85 30.56 1.13 o -3 2 9 8.96 25.29 4.29 o -2 2 9 38.47 62.66 5.81 o -1 2 9 145.59 149.18 8.36 o 1 2 9 145.24 141.18 3.60 o 2 2 9 38.17 44.71 5.75 o 3 2 9 8.74 16.79 6.27 o 4 2 9 29.28 28.62 3.62 o 5 2 9 4.52 6.84 2.37 o 6 2 9 11.77 15.55 0.83 o 7 2 9 41.25 43.75 1.59 o 8 2 9 89.84 87.16 2.81 o 9 2 9 14.45 19.83 0.83 o 10 2 9 47.08 45.75 1.66 o 11 2 9 21.77 14.14 0.54 o -5 3 9 134.81 124.39 7.84 o -4 3 9 5.74 28.12 2.17 o -3 3 9 16.81 25.51 2.03 o -2 3 9 34.88 35.58 2.60 o -1 3 9 17.52 22.25 1.84 o 0 3 9 2.01 9.32 1.22 o 1 3 9 17.18 20.60 1.75 o 2 3 9 35.18 33.73 2.47 o 0 0 10 20.67 43.01 1.23 o 1 0 10 76.80 73.80 1.39 o 2 0 10 1.65 33.12 1.45 o 3 0 10 119.82 106.39 2.17 o 4 0 10 11.42 19.99 4.82 o 5 0 10 5.90 12.11 2.11 o 6 0 10 38.71 30.71 0.72 o -4 1 10 4.96 27.29 4.76 o -3 1 10 103.48 104.93 3.39 o -2 1 10 67.47 87.98 2.71 o -1 1 10 30.96 74.02 2.88 o 0 1 10 199.74 186.83 4.75 o 1 1 10 31.12 66.51 4.02 o 2 1 10 66.35 84.73 4.38 o 3 1 10 103.53 98.21 5.04 o 4 1 10 4.68 34.84 2.49 o