#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/76/2237638.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237638_Fobs loop_ _publ_author_name 'Sohail, Muhammad' 'Yao-Feng, Wang' 'Qi, Wang' 'Chen, Fu-Xue' _publ_section_title ; 7-Iodo-3,3-diphenyloctahydrobenzofuran ; _journal_coeditor_code HG5298 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o585 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.306 _cell_angle_beta 71.646 _cell_angle_gamma 64.945 _cell_length_a 11.4082 _cell_length_b 12.5231 _cell_length_c 14.0067 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.7104 _[local]_cod_data_source_file hg5298Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bo1548-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 261.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22315.70 22487.71 150.46 o 3 0 0 89.84 111.26 7.99 o 4 0 0 78.45 113.89 8.03 o 5 0 0 1519.04 1471.05 43.45 o 6 0 0 7995.89 7836.86 131.37 o 7 0 0 4185.54 4184.93 111.15 o 8 0 0 1187.54 1144.96 54.08 o 9 0 0 401.44 415.76 26.56 o 10 0 0 1078.11 962.86 56.92 o 11 0 0 531.04 461.20 63.92 o 12 0 0 0.58 34.96 41.24 o 13 0 0 830.02 780.95 91.70 o 14 0 0 196.97 322.68 80.18 o -13 1 0 95.56 66.29 38.17 o -12 1 0 33.52 51.71 36.22 o -11 1 0 42.49 51.29 38.38 o -10 1 0 263.08 256.33 18.57 o -9 1 0 3336.00 3225.04 109.15 o -8 1 0 1802.92 1780.93 65.22 o -7 1 0 2411.65 2191.23 53.53 o -6 1 0 1740.88 1790.22 56.04 o -5 1 0 884.00 733.53 23.44 o -4 1 0 46.29 42.85 4.61 o -3 1 0 1527.09 1393.12 32.33 o -2 1 0 2308.91 2254.84 34.42 o -1 1 0 36709.56 36344.30 404.71 o 1 1 0 23.41 11.93 4.68 o 2 1 0 11.34 19.30 2.59 o 3 1 0 1443.17 1487.50 36.56 o 4 1 0 1303.85 1254.59 25.51 o 5 1 0 27696.60 29031.15 222.28 o 6 1 0 3182.18 3163.61 72.00 o 7 1 0 4770.22 4788.36 124.60 o 8 1 0 895.93 949.31 69.63 o 9 1 0 29.58 29.21 11.18 o 10 1 0 129.91 144.96 15.85 o 11 1 0 696.04 686.08 44.83 o 12 1 0 634.78 602.51 76.06 o 13 1 0 76.89 109.14 47.87 o 14 1 0 126.41 101.19 39.36 o -13 2 0 51.35 42.99 33.78 o -12 2 0 15.98 26.52 24.91 o -11 2 0 45.47 64.97 32.31 o -10 2 0 467.58 449.78 30.62 o -9 2 0 2145.76 2185.83 107.21 o -8 2 0 530.53 531.65 30.14 o -7 2 0 1651.97 1561.26 45.25 o -6 2 0 277.98 286.54 21.86 o -5 2 0 7.41 9.47 6.38 o -4 2 0 1457.66 1336.69 27.25 o -3 2 0 1168.71 1142.26 25.81 o -2 2 0 30155.24 29954.42 355.09 o -1 2 0 1112.12 1050.26 26.83 o 0 2 0 2835.52 3114.79 64.90 o 1 2 0 277.25 310.13 10.74 o 3 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1188.01 69.68 o 11 3 0 1257.22 1262.23 56.69 o 12 3 0 372.96 449.72 41.89 o 13 3 0 4.45 21.65 17.12 o 14 3 0 2.16 22.25 30.74 o -12 4 0 0.26 27.63 38.17 o -11 4 0 488.21 454.36 69.85 o -10 4 0 20.04 52.55 28.82 o -9 4 0 495.79 520.82 55.55 o -8 4 0 106.12 115.55 38.35 o -7 4 0 284.78 342.36 26.89 o -6 4 0 53.82 54.81 12.15 o -5 4 0 656.69 643.80 55.14 o -4 4 0 1674.52 1537.64 50.10 o -3 4 0 3345.00 3418.96 125.12 o -2 4 0 10855.45 10835.44 233.39 o -1 4 0 854.50 845.83 18.77 o 0 4 0 2741.17 3102.72 51.17 o 1 4 0 0.62 9.28 8.85 o 2 4 0 10313.22 8944.69 200.61 o 3 4 0 70.38 89.11 25.05 o 4 4 0 23161.83 22954.30 238.91 o 5 4 0 199.97 187.79 18.52 o 6 4 0 11221.57 12136.25 217.40 o 7 4 0 3.94 19.14 10.27 o 8 4 0 3195.80 3512.57 111.99 o 9 4 0 987.11 1005.28 52.22 o 10 4 0 3108.54 3059.51 106.04 o 11 4 0 1253.96 1269.81 57.31 o 12 4 0 612.37 613.40 47.37 o 13 4 0 74.96 38.35 15.13 o 14 4 0 42.79 57.56 24.42 o 15 4 0 25.85 39.26 32.59 o -11 5 0 92.16 135.59 49.13 o -10 5 0 556.26 589.60 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257.01 27.77 o -1 6 0 18.45 27.58 4.37 o 0 6 0 3507.62 3331.01 85.03 o 1 6 0 1783.88 1796.89 41.31 o 2 6 0 22884.59 22989.25 267.12 o 3 6 0 162.26 142.71 19.13 o 4 6 0 4033.39 3648.57 188.70 o 5 6 0 46.82 45.28 10.38 o 6 6 0 2110.17 2172.16 70.75 o 7 6 0 578.17 548.69 43.84 o 8 6 0 9953.63 10215.97 326.87 o 9 6 0 1152.69 1089.64 54.12 o 10 6 0 1640.75 1737.23 59.27 o 11 6 0 496.80 534.78 55.88 o 12 6 0 7.20 18.53 11.33 o 13 6 0 19.17 47.28 19.75 o 14 6 0 278.01 232.94 60.48 o 15 6 0 341.30 365.65 107.57 o -10 7 0 44.62 102.16 45.08 o -9 7 0 35.68 24.49 27.36 o -8 7 0 425.64 479.62 40.79 o -7 7 0 183.48 153.39 28.19 o -6 7 0 759.95 784.19 50.35 o -5 7 0 401.82 467.21 34.33 o -4 7 0 1277.65 1234.46 64.97 o -3 7 0 740.82 768.66 48.62 o -2 7 0 13.66 35.87 14.58 o -1 7 0 1649.00 1782.76 58.47 o 0 7 0 1441.11 1470.84 50.44 o 1 7 0 7193.69 6493.76 139.23 o 2 7 0 259.38 194.69 17.00 o 3 7 0 1896.59 1570.49 66.04 o 4 7 0 83.52 98.41 9.60 o 5 7 0 2684.93 3000.59 110.42 o 6 7 0 35.59 45.45 23.09 o 7 7 0 15681.49 16876.49 274.53 o 8 7 0 697.29 772.44 46.42 o 9 7 0 2347.40 2479.70 106.34 o 10 7 0 221.51 292.21 39.42 o 11 7 0 602.29 614.17 58.18 o 12 7 0 330.25 268.28 42.76 o 13 7 0 261.04 304.17 80.36 o 14 7 0 969.71 932.57 101.15 o 15 7 0 3.97 20.34 19.69 o -9 8 0 8.40 38.45 31.40 o -8 8 0 253.49 192.30 73.27 o -7 8 0 583.91 647.55 46.90 o -6 8 0 16.49 25.30 15.83 o -5 8 0 684.10 712.30 41.63 o -4 8 0 44.88 64.77 19.72 o -3 8 0 115.66 118.49 19.62 o -2 8 0 257.09 217.94 37.44 o -1 8 0 884.37 904.09 44.84 o 0 8 0 1756.66 1711.69 53.80 o 1 8 0 1340.48 1382.82 50.58 o 2 8 0 4148.79 4222.68 110.02 o 3 8 0 34.64 44.24 14.21 o 4 8 0 245.99 260.30 16.99 o 5 8 0 161.75 139.48 25.14 o 6 8 0 5902.81 5864.89 226.06 o 7 8 0 295.63 343.80 42.81 o 8 8 0 2417.10 2558.82 110.06 o 9 8 0 351.59 346.83 31.84 o 10 8 0 149.71 204.96 53.54 o 11 8 0 14.51 17.85 11.14 o 12 8 0 1463.79 1444.63 80.05 o 13 8 0 471.02 442.67 99.65 o 14 8 0 424.76 370.96 119.16 o 15 8 0 224.66 154.76 55.16 o -9 9 0 0.36 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261.89 334.40 89.11 o 3 16 0 71.64 69.30 32.59 o 4 16 0 2.49 51.36 34.26 o 5 16 0 60.17 78.65 49.34 o 6 16 0 208.11 321.35 70.34 o 7 16 0 138.43 92.04 34.05 o 8 16 0 2033.47 2055.16 109.69 o 9 16 0 14.80 49.87 23.54 o -8 -16 1 253.58 216.94 44.43 o -7 -16 1 384.73 327.98 122.23 o -6 -16 1 720.45 729.66 124.63 o -5 -16 1 48.07 115.63 46.89 o -4 -16 1 435.85 350.94 77.74 o -3 -16 1 19.05 31.54 30.36 o -2 -16 1 84.08 77.18 36.36 o -10 -15 1 46.15 91.49 45.29 o -9 -15 1 448.98 395.14 56.49 o -8 -15 1 475.61 422.41 44.31 o -7 -15 1 957.27 907.54 82.21 o -6 -15 1 187.05 199.35 34.25 o -5 -15 1 923.41 822.72 109.84 o -4 -15 1 0.01 26.52 31.40 o -3 -15 1 57.41 48.50 29.59 o -2 -15 1 64.88 64.97 43.13 o -1 -15 1 805.21 834.61 136.92 o 0 -15 1 0.31 16.12 26.24 o -12 -14 1 67.67 113.82 41.45 o -11 -14 1 199.30 152.89 32.78 o -10 -14 1 27.22 63.90 28.16 o -9 -14 1 424.85 389.29 42.18 o -8 -14 1 732.01 718.74 115.35 o -7 -14 1 1218.48 1285.63 91.21 o -6 -14 1 1915.26 1995.30 109.15 o -5 -14 1 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