#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/76/2237671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237671_Fobs loop_ _publ_author_name 'Zhong, Kai-Long' _publ_section_title ; Poly[diaquabis(\m-4,4'-bipyridine-\k^2^N:N')bis(ethane-1,2-diol-\kO)bis(\m-sulfato-\k^2^O:O')dicobalt(II)] ; _journal_coeditor_code MW2105 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m207 _journal_page_last m208 _journal_volume 69 _journal_year 2013 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.515 _cell_angle_gamma 90.000 _cell_length_a 11.1243 _cell_length_b 22.7920 _cell_length_c 12.0663 _exptl_crystal_F_000 1608.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file mw2105Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 545.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 7257.04 7402.74 164.12 o 8 0 0 18101.93 18504.40 167.28 o 10 0 0 20018.79 20617.14 309.12 o 12 0 0 19733.02 20112.13 731.97 o 3 1 0 2847.19 2418.89 30.97 o 5 1 0 1871.32 2200.56 35.38 o 7 1 0 34.11 29.86 9.09 o 9 1 0 674.06 598.39 24.04 o 11 1 0 2914.59 2727.88 50.70 o 13 1 0 1320.53 1371.22 72.95 o 2 2 0 10800.46 11142.44 51.80 o 4 2 0 4673.59 4592.48 51.63 o 6 2 0 729.42 739.21 26.61 o 8 2 0 189.95 193.65 16.67 o 10 2 0 1.66 20.01 12.35 o 12 2 0 313.76 348.73 34.12 o 1 3 0 338.49 288.11 9.46 o 3 3 0 7680.40 7471.50 44.25 o 5 3 0 1891.49 2161.36 33.90 o 7 3 0 328.75 357.45 20.03 o 9 3 0 87.40 93.97 12.87 o 11 3 0 12.32 23.93 12.90 o 13 3 0 103.16 84.36 30.68 o 2 4 0 4739.62 4855.96 108.33 o 4 4 0 58458.06 60915.04 456.69 o 6 4 0 43119.89 48516.37 275.77 o 8 4 0 22249.82 24104.78 108.11 o 10 4 0 8425.74 8658.41 109.10 o 12 4 0 2318.93 2324.73 134.29 o 14 4 0 557.20 445.00 52.43 o 1 5 0 76.90 90.82 10.42 o 3 5 0 6840.07 6363.54 78.68 o 5 5 0 3064.26 3546.56 36.78 o 7 5 0 37.93 46.36 9.96 o 9 5 0 2749.98 2719.72 46.69 o 11 5 0 966.77 935.27 44.32 o 13 5 0 1498.32 1441.31 93.44 o 0 6 0 21264.56 19759.41 126.22 o 2 6 0 4449.95 3882.76 119.90 o 4 6 0 4463.96 4089.60 86.61 o 6 6 0 505.51 487.16 16.32 o 8 6 0 628.66 643.51 19.15 o 10 6 0 7.54 30.83 11.44 o 12 6 0 145.67 154.67 49.85 o 14 6 0 0.66 -8.95 23.00 o 1 7 0 203.91 218.35 12.02 o 3 7 0 5511.90 5836.72 51.75 o 5 7 0 1711.93 1745.82 49.45 o 7 7 0 1099.86 1129.71 21.54 o 9 7 0 408.38 409.62 15.05 o 11 7 0 878.17 881.41 23.23 o 13 7 0 171.11 236.48 54.97 o 0 8 0 146847.34 136032.69 2487.50 o 2 8 0 17071.06 16512.17 84.37 o 4 8 0 26093.88 25896.71 390.69 o 6 8 0 17844.32 18507.59 144.33 o 8 8 0 12995.31 13152.57 127.57 o 10 8 0 5615.35 5705.54 63.70 o 12 8 0 3384.56 3686.42 146.23 o 1 9 0 1.65 15.16 10.54 o 3 9 0 5725.59 5390.84 299.85 o 5 9 0 116.27 135.03 12.18 o 7 9 0 361.13 338.96 11.87 o 9 9 0 1164.86 1127.22 56.48 o 11 9 0 905.06 837.98 76.76 o 13 9 0 605.49 576.75 69.06 o 0 10 0 14043.86 13555.02 141.31 o 2 10 0 1501.88 1743.31 33.46 o 4 10 0 6547.32 6334.37 99.36 o 6 10 0 106.03 103.77 9.75 o 8 10 0 4319.33 4488.48 108.29 o 10 10 0 79.26 42.18 58.80 o 12 10 0 998.21 1038.86 89.56 o 1 11 0 165.23 155.54 15.49 o 3 11 0 435.84 497.00 23.45 o 5 11 0 4859.64 4891.28 67.04 o 7 11 0 3186.34 3133.27 94.37 o 9 11 0 532.77 537.14 69.06 o 11 11 0 1425.34 1331.25 101.12 o 13 11 0 88.19 93.31 44.74 o 0 12 0 47551.41 46652.47 393.90 o 2 12 0 5671.19 4805.70 57.12 o 4 12 0 24037.50 22441.93 682.19 o 8 12 0 15036.66 15194.56 383.12 o 10 12 0 5380.31 5725.00 231.47 o 12 12 0 1701.32 1611.87 110.10 o 1 13 0 1.01 23.95 14.83 o 3 13 0 1127.44 1101.69 30.46 o 5 13 0 379.07 389.71 22.53 o 7 13 0 387.28 373.79 65.85 o 9 13 0 431.55 359.32 72.89 o 11 13 0 1015.74 996.68 88.28 o 0 14 0 10194.16 10132.64 132.58 o 2 14 0 394.68 423.16 21.61 o 4 14 0 13403.22 13774.85 113.90 o 6 14 0 96.58 96.56 16.73 o 8 14 0 9120.08 9371.01 271.44 o 10 14 0 8.84 57.51 62.62 o 12 14 0 755.08 709.85 88.25 o 1 15 0 205.03 215.87 18.25 o 3 15 0 1847.75 1782.71 38.34 o 5 15 0 5044.31 4757.10 194.93 o 7 15 0 3955.00 4022.45 75.83 o 9 15 0 4085.40 4180.84 199.03 o 11 15 0 228.97 324.70 63.92 o 0 16 0 35929.27 36721.80 367.42 o 2 16 0 20234.17 20327.69 138.05 o 4 16 0 1333.97 1179.97 31.31 o 6 16 0 644.21 675.04 50.53 o 8 16 0 1205.36 1159.57 94.71 o 10 16 0 3039.45 3501.67 160.27 o 12 16 0 1004.66 1028.55 97.23 o 1 17 0 203.67 198.00 24.92 o 3 17 0 95.13 83.10 15.00 o 5 17 0 3185.94 3057.35 106.19 o 7 17 0 701.62 699.34 21.49 o 9 17 0 11.37 67.74 75.41 o 11 17 0 168.13 126.55 42.18 o 0 18 0 5574.22 5796.29 113.36 o 2 18 0 616.38 598.68 33.99 o 4 18 0 4028.06 4184.11 66.85 o 6 18 0 864.50 768.93 78.04 o 8 18 0 2176.72 2189.54 128.12 o 10 18 0 727.81 723.92 90.81 o 1 19 0 40.72 43.42 12.95 o 3 19 0 102.37 97.81 16.04 o 5 19 0 2063.77 2127.36 54.25 o 7 19 0 1755.61 1678.17 33.34 o 9 19 0 463.03 438.58 89.51 o 11 19 0 791.70 795.56 89.53 o 0 20 0 1983.17 2247.28 72.40 o 2 20 0 10891.20 11591.96 167.17 o 4 20 0 1550.14 1670.87 59.42 o 6 20 0 21276.46 22433.31 316.52 o 8 20 0 3861.57 3893.65 169.40 o 10 20 0 5091.80 5158.50 195.24 o 1 21 0 80.12 91.96 22.34 o 3 21 0 131.71 125.64 22.81 o 5 21 0 3427.03 3276.28 85.07 o 7 21 0 721.79 789.17 85.70 o 9 21 0 18.54 2.56 35.79 o 0 22 0 6731.97 6137.64 184.92 o 2 22 0 4780.74 4641.17 81.60 o 4 22 0 1221.78 1190.83 53.44 o 6 22 0 2704.68 2815.44 71.38 o 8 22 0 544.02 679.02 95.91 o 1 23 0 10.96 28.17 20.46 o 3 23 0 19.57 16.00 12.06 o 5 23 0 205.54 153.58 38.29 o 7 23 0 355.96 355.43 115.07 o 9 23 0 23.82 62.63 40.90 o 0 24 0 3053.39 2856.14 138.51 o 2 24 0 9509.23 9411.58 403.37 o 4 24 0 787.18 790.81 63.31 o 6 24 0 4999.60 5141.27 208.12 o 8 24 0 1714.36 1634.81 139.54 o 1 25 0 15.77 30.33 27.88 o 3 25 0 2.96 35.30 26.16 o 5 25 0 964.14 882.73 56.93 o 7 25 0 237.11 272.29 71.59 o 0 26 0 897.57 967.13 227.71 o 2 26 0 1553.76 1687.41 104.97 o 4 26 0 51.98 50.32 26.05 o 6 26 0 706.99 494.95 148.36 o 1 27 0 0.43 29.14 27.65 o 3 27 0 11.05 37.70 22.59 o 5 27 0 129.58 162.33 54.96 o 0 28 0 341.57 256.98 51.14 o 2 28 0 4280.66 4585.74 114.59 o 4 28 0 268.80 251.84 57.53 o 1 29 0 0.32 36.21 29.40 o -13 1 1 786.71 658.74 57.56 o -11 1 1 245.90 253.59 22.54 o -9 1 1 1254.92 1204.33 29.75 o -7 1 1 9071.73 9350.32 162.18 o -5 1 1 18513.29 20371.19 146.83 o -3 1 1 8597.95 8334.20 44.24 o 3 1 1 3232.41 3011.78 33.80 o 5 1 1 729.77 617.69 27.35 o 7 1 1 4468.34 4614.29 58.45 o 9 1 1 1518.46 1599.98 37.18 o 11 1 1 359.15 332.90 20.70 o 13 1 1 184.34 175.90 26.38 o -12 2 1 4512.07 4606.81 71.01 o -10 2 1 496.68 462.28 27.31 o -8 2 1 24440.26 25993.21 313.54 o -6 2 1 24494.31 25955.87 186.41 o -4 2 1 11103.73 9555.03 61.36 o -2 2 1 668.66 618.38 13.70 o 2 2 1 51.81 112.29 9.81 o 4 2 1 85726.61 97988.48 1031.65 o 6 2 1 26137.25 27728.27 177.82 o 8 2 1 15913.92 16837.58 185.42 o 10 2 1 10401.08 10556.12 157.39 o 12 2 1 3114.32 3087.36 63.54 o -13 3 1 348.75 317.07 48.58 o -11 3 1 302.16 271.30 16.55 o -9 3 1 470.69 517.61 24.14 o -7 3 1 10246.58 10648.27 202.13 o -5 3 1 7975.48 8889.46 81.40 o -3 3 1 3509.02 3740.03 52.58 o -1 3 1 663.51 776.99 26.74 o 1 3 1 1805.01 1991.96 32.63 o 3 3 1 10151.39 10389.65 59.22 o 5 3 1 3241.45 3060.29 38.38 o 7 3 1 13987.44 14394.13 117.59 o 9 3 1 2272.35 2245.84 43.68 o 11 3 1 3448.12 3517.35 71.12 o 13 3 1 1399.13 1456.52 88.31 o -12 4 1 239.60 217.12 19.47 o -10 4 1 360.02 385.38 23.35 o -8 4 1 4736.05 4641.87 155.40 o -6 4 1 2921.44 3023.31 38.04 o -4 4 1 16236.63 16859.33 226.94 o -2 4 1 8682.55 9080.68 123.59 o 0 4 1 2670.20 2677.02 39.67 o 2 4 1 598.84 580.89 15.79 o 4 4 1 19.29 17.40 7.56 o 6 4 1 1122.51 1088.58 34.03 o 8 4 1 227.10 256.50 20.05 o 10 4 1 18.10 22.81 10.79 o 12 4 1 8.70 9.11 11.64 o 14 4 1 39.79 106.08 46.01 o -13 5 1 344.85 336.25 52.42 o -11 5 1 2106.36 1997.23 34.20 o -9 5 1 67.50 64.87 8.77 o -7 5 1 1189.03 1266.80 20.29 o -5 5 1 0.63 21.66 16.54 o -3 5 1 1983.73 2004.64 52.24 o -1 5 1 158.94 154.99 11.12 o 1 5 1 31.10 40.85 7.85 o 3 5 1 2383.72 2382.55 35.34 o 5 5 1 3877.11 4219.94 50.79 o 7 5 1 114.30 130.55 20.11 o 9 5 1 1361.89 1319.11 31.95 o 11 5 1 203.61 205.69 15.91 o 13 5 1 115.02 138.05 49.85 o -14 6 1 105.13 93.31 35.79 o -12 6 1 2732.97 3061.09 124.34 o -10 6 1 848.37 834.03 17.50 o -8 6 1 1789.35 1595.18 21.17 o -6 6 1 13905.53 13509.79 183.60 o -4 6 1 6044.43 7784.01 269.86 o -2 6 1 20372.94 21761.95 181.81 o 0 6 1 112351.37 110149.55 2483.64 o 2 6 1 1870.69 1912.58 35.51 o 4 6 1 26805.98 25825.33 267.29 o 6 6 1 188.56 110.10 11.51 o 8 6 1 2513.00 2388.14 37.95 o 10 6 1 8623.87 9055.50 108.05 o 12 6 1 4472.44 4499.91 151.54 o -13 7 1 402.48 442.39 57.54 o -11 7 1 519.92 465.49 65.22 o -9 7 1 227.67 242.77 30.27 o -7 7 1 2767.99 2996.23 77.82 o -5 7 1 3026.44 3215.30 72.74 o -3 7 1 475.44 433.10 30.03 o -1 7 1 2721.14 2426.36 31.46 o 1 7 1 2442.99 2192.12 35.71 o 3 7 1 2619.35 2310.55 36.24 o 5 7 1 770.39 864.26 26.53 o 7 7 1 1569.88 1574.68 45.31 o 9 7 1 504.62 544.29 25.69 o 11 7 1 932.64 912.79 29.72 o 13 7 1 881.03 961.95 80.59 o -12 8 1 1321.73 1471.84 94.71 o -10 8 1 46.81 45.75 19.33 o -8 8 1 2447.35 2453.57 77.57 o -6 8 1 132.11 156.37 31.62 o -4 8 1 4959.27 4903.70 54.84 o -2 8 1 70.59 69.61 9.89 o 0 8 1 3731.38 3316.55 37.33 o 2 8 1 1665.12 1745.16 32.12 o 4 8 1 806.58 800.46 21.10 o 6 8 1 600.33 557.84 24.74 o 8 8 1 335.85 339.17 18.16 o 10 8 1 330.79 326.22 22.56 o 12 8 1 70.90 51.13 34.51 o -13 9 1 387.76 432.15 70.32 o -11 9 1 295.92 268.48 52.42 o -9 9 1 457.70 413.06 46.12 o -7 9 1 1216.91 1248.39 56.70 o -5 9 1 1305.07 1365.74 73.03 o -3 9 1 631.30 791.38 23.36 o -1 9 1 548.91 633.57 19.99 o 1 9 1 1814.80 2010.68 36.49 o 3 9 1 2577.21 2834.30 64.91 o 5 9 1 314.22 346.50 17.72 o 7 9 1 3.94 14.30 13.33 o 9 9 1 894.54 908.99 49.50 o 11 9 1 680.12 757.18 81.86 o 13 9 1 245.74 277.40 62.64 o -12 10 1 6359.78 6166.60 216.15 o -10 10 1 6812.81 6993.50 204.86 o -8 10 1 12936.56 12885.23 205.65 o -6 10 1 33168.07 36185.29 438.95 o -4 10 1 8453.66 8260.55 81.52 o -2 10 1 52396.70 54648.96 294.95 o 0 10 1 193933.83 184713.08 6670.52 o 2 10 1 34266.90 34546.41 331.26 o 4 10 1 51082.61 54701.23 691.70 o 6 10 1 14620.41 15376.88 122.50 o 8 10 1 13848.69 14098.49 131.73 o 10 10 1 17229.96 17804.64 239.99 o 12 10 1 10017.84 10217.06 302.17 o -13 11 1 100.11 134.21 46.01 o -11 11 1 1118.79 1074.88 90.85 o -9 11 1 407.22 395.12 70.33 o -7 11 1 947.55 1060.10 90.23 o -5 11 1 1913.00 1989.55 33.66 o -3 11 1 4195.44 4218.14 59.54 o -1 11 1 8314.01 8376.67 106.75 o 1 11 1 6565.98 6627.12 67.58 o 3 11 1 6517.98 6256.69 64.12 o 5 11 1 186.74 204.22 16.34 o 7 11 1 833.79 844.03 29.20 o 9 11 1 156.16 154.78 14.19 o 11 11 1 934.98 979.98 89.55 o 13 11 1 770.77 862.05 88.25 o -12 12 1 3536.92 3896.81 155.21 o -10 12 1 173.86 209.64 52.41 o -8 12 1 5486.83 5571.35 200.82 o -6 12 1 2.07 19.07 32.14 o -4 12 1 5765.10 5679.23 135.00 o -2 12 1 446.17 425.40 21.14 o 0 12 1 7140.66 6848.16 70.53 o 2 12 1 5.93 27.06 13.19 o 4 12 1 6168.51 6010.10 64.20 o 6 12 1 873.08 794.36 29.62 o 8 12 1 947.79 944.43 51.86 o 10 12 1 1399.87 1419.62 103.69 o 12 12 1 3.43 1.28 37.06 o -11 13 1 87.71 95.86 39.62 o -9 13 1 63.04 149.54 51.13 o -7 13 1 1134.69 1131.54 98.56 o -5 13 1 0.39 12.11 8.27 o -3 13 1 631.09 650.33 22.00 o -1 13 1 1351.83 1303.14 41.74 o 1 13 1 585.19 529.72 26.86 o 3 13 1 344.65 293.09 21.38 o 5 13 1 1354.27 1290.45 29.97 o 7 13 1 290.55 287.53 19.90 o 9 13 1 2141.35 2357.60 129.41 o 11 13 1 1105.49 1252.67 122.84 o -12 14 1 376.62 462.83 75.43 o -10 14 1 6859.92 7483.22 216.35 o -8 14 1 6520.73 6832.69 221.61 o -6 14 1 25569.34 25499.43 912.16 o -4 14 1 5922.36 5652.92 57.65 o -2 14 1 8217.96 7968.03 90.99 o 0 14 1 20708.62 20670.64 150.34 o 2 14 1 14354.98 13965.47 114.73 o 4 14 1 19753.34 20362.01 131.46 o 6 14 1 24664.45 25938.03 256.86 o 8 14 1 10866.57 11448.05 112.98 o 10 14 1 5995.43 6090.12 196.83 o 12 14 1 5031.98 5096.60 192.66 o -11 15 1 3.05 28.12 43.45 o -9 15 1 1089.34 1031.40 92.13 o -7 15 1 617.46 683.02 74.19 o -5 15 1 3123.11 3139.26 56.29 o -3 15 1 150.67 137.27 16.50 o -1 15 1 1856.30 1917.29 39.42 o 1 15 1 1900.59 1996.65 41.89 o 3 15 1 471.50 462.96 31.16 o 5 15 1 687.73 709.83 35.03 o 7 15 1 163.12 176.09 18.48 o 9 15 1 49.52 126.53 67.74 o 11 15 1 65.74 53.68 47.29 o -12 16 1 1709.94 1705.20 121.62 o -10 16 1 280.60 232.67 66.48 o -8 16 1 1519.17 1547.95 106.27 o -6 16 1 1273.13 1308.59 24.73 o -4 16 1 2926.45 3033.73 48.82 o -2 16 1 7.01 45.74 17.63 o 0 16 1 11576.57 11823.42 101.86 o 2 16 1 261.26 305.52 20.24 o 4 16 1 358.18 390.92 26.83 o 6 16 1 252.35 251.63 18.79 o 8 16 1 41.57 31.53 8.83 o 10 16 1 760.71 849.31 92.09 o -11 17 1 450.67 378.47 80.55 o -9 17 1 2290.29 2220.44 128.13 o -7 17 1 116.86 148.27 47.29 o -5 17 1 214.83 222.87 19.89 o -3 17 1 5737.28 5643.15 73.52 o -1 17 1 1597.03 1625.64 45.63 o 1 17 1 861.29 911.64 31.55 o 3 17 1 2569.15 2531.69 49.09 o 5 17 1 2333.62 2289.68 50.76 o 7 17 1 1872.56 1876.47 49.70 o 9 17 1 1665.23 1586.38 112.67 o 11 17 1 2329.98 2348.09 138.35 o -10 18 1 7956.74 8417.75 246.10 o -8 18 1 1826.74 1805.76 117.82 o -6 18 1 19017.58 19453.21 273.06 o -4 18 1 2179.17 2183.59 110.12 o -2 18 1 10940.85 10868.19 147.88 o 0 18 1 8099.92 8141.31 141.67 o 2 18 1 16848.15 17060.07 153.90 o 4 18 1 4794.13 5150.75 77.96 o 6 18 1 16678.55 17454.61 365.77 o 8 18 1 6054.47 6080.69 71.01 o 10 18 1 3260.34 3275.01 157.72 o -11 19 1 221.59 255.66 60.08 o -9 19 1 49.19 66.46 56.24 o -7 19 1 113.78 134.21 47.29 o -5 19 1 34.54 43.66 21.14 o -3 19 1 544.10 513.12 34.20 o -1 19 1 661.89 620.87 29.62 o 1 19 1 909.30 812.79 34.10 o 3 19 1 1082.53 943.14 38.24 o 5 19 1 2200.97 2220.57 53.73 o 7 19 1 134.72 114.02 33.46 o 9 19 1 1221.67 1367.98 113.89 o -10 20 1 852.22 842.95 88.26 o -8 20 1 2946.63 3155.23 160.26 o -6 20 1 2376.64 2338.58 72.78 o -4 20 1 3558.33 3785.28 72.97 o -2 20 1 377.03 371.52 32.12 o 0 20 1 1331.82 1492.62 42.65 o 2 20 1 2296.85 2223.43 52.32 o 4 20 1 1301.31 1231.04 43.88 o 6 20 1 5149.90 5362.71 108.05 o 8 20 1 1453.96 1559.08 133.12 o 10 20 1 1057.16 983.84 95.95 o -9 21 1 0.13 26.84 28.12 o -7 21 1 4.42 46.01 66.46 o -5 21 1 942.79 911.21 53.13 o -3 21 1 491.58 372.11 28.48 o -1 21 1 57.45 63.21 19.33 o 1 21 1 9.97 18.00 15.04 o 3 21 1 63.87 47.72 20.58 o 5 21 1 752.38 800.75 40.60 o 7 21 1 627.01 599.81 76.73 o 9 21 1 1066.22 1068.31 98.52 o -8 22 1 982.52 1026.03 102.35 o -6 22 1 7734.38 8033.47 228.13 o -4 22 1 1549.60 1382.17 55.70 o -2 22 1 13118.73 12393.05 197.98 o 0 22 1 15960.46 14347.55 282.43 o 2 22 1 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23004.60 23482.53 157.52 o 6 12 4 6784.40 6682.69 96.01 o 8 12 4 2173.94 2272.93 52.44 o 10 12 4 4127.59 4256.12 92.50 o 12 12 4 444.66 386.14 65.21 o -11 13 4 13.74 17.89 40.90 o -9 13 4 3.01 43.45 63.90 o -7 13 4 381.52 347.80 58.82 o -5 13 4 11.84 38.45 12.97 o -3 13 4 246.95 296.03 20.80 o -1 13 4 494.83 509.70 29.55 o 1 13 4 2741.82 2709.47 50.55 o 3 13 4 6609.49 6523.94 76.55 o 5 13 4 199.45 164.62 19.54 o 7 13 4 1485.74 1388.90 43.69 o 9 13 4 1518.31 1438.17 69.90 o 11 13 4 341.33 324.74 67.76 o -12 14 4 44.68 74.13 56.24 o -10 14 4 2637.38 2696.73 157.65 o -8 14 4 160.77 159.79 57.52 o -6 14 4 12368.93 12575.06 271.56 o -4 14 4 3329.68 3324.87 45.11 o -2 14 4 23921.51 24431.87 222.12 o 0 14 4 1670.42 1670.89 40.14 o 2 14 4 8561.37 8592.42 91.20 o 4 14 4 446.84 486.41 28.85 o 6 14 4 1025.13 996.42 58.70 o 8 14 4 786.04 814.39 43.91 o 10 14 4 1142.14 1292.38 106.21 o -11 15 4 2776.57 2476.18 140.98 o -9 15 4 716.58 571.75 143.26 o -7 15 4 13.31 46.01 40.90 o -5 15 4 856.77 949.89 37.75 o -3 15 4 15288.19 15815.89 103.98 o -1 15 4 977.56 920.40 32.16 o 1 15 4 2021.29 2035.09 46.61 o 3 15 4 4912.07 4905.98 73.43 o 5 15 4 350.43 335.70 26.60 o 7 15 4 3.16 39.21 17.80 o 9 15 4 5634.84 5660.00 105.34 o 11 15 4 16.03 62.63 42.18 o -10 16 4 729.48 796.83 92.09 o -8 16 4 7760.87 8199.77 300.45 o -6 16 4 153.98 141.89 48.58 o -4 16 4 10747.98 11445.66 121.39 o -2 16 4 509.04 500.27 27.41 o 0 16 4 4221.54 4454.04 64.70 o 2 16 4 1299.03 1212.55 42.02 o 4 16 4 5578.53 5883.29 90.20 o 6 16 4 72.95 69.61 15.60 o 8 16 4 27.20 51.14 18.22 o 10 16 4 1526.10 1619.24 111.36 o -11 17 4 1342.31 1128.74 364.73 o -9 17 4 120.66 90.75 46.02 o -7 17 4 130.31 193.01 85.64 o -5 17 4 0.66 32.55 16.73 o -3 17 4 4915.05 4865.68 75.05 o -1 17 4 382.26 394.77 26.07 o 1 17 4 986.01 976.57 35.81 o 3 17 4 47.74 54.52 16.61 o 5 17 4 12.98 52.88 30.18 o 7 17 4 128.04 127.96 19.06 o 9 17 4 777.55 972.11 94.65 o -10 18 4 1264.47 1213.14 101.10 o -8 18 4 8.28 38.34 69.02 o -6 18 4 4281.87 4320.44 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