#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181299 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/77/2237744.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237744_Fobs loop_ _publ_author_name '\H-purine ; _journal_coeditor_code ZQ2196 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o533 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.808 _cell_angle_beta 78.674 _cell_angle_gamma 82.039 _cell_length_a 8.6978 _cell_length_b 8.8318 _cell_length_c 12.1517 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file zq2196Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ip_07_02_slow in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1635.40 1584.55 4.81 o 3 0 0 3006.34 3020.58 10.95 o 4 0 0 287.64 284.27 2.55 o 5 0 0 767.96 789.22 3.19 o 6 0 0 45.14 55.40 1.78 o 7 0 0 38.36 35.46 0.79 o 8 0 0 233.40 224.95 1.56 o 9 0 0 0.18 1.33 0.74 o 10 0 0 0.35 0.00 1.33 o -9 1 0 74.02 70.87 1.15 o -8 1 0 11.83 13.15 0.78 o -7 1 0 45.83 50.01 0.88 o -6 1 0 6.48 5.99 0.41 o -5 1 0 172.80 171.34 0.84 o -4 1 0 638.11 665.27 1.21 o -3 1 0 256.40 217.28 1.78 o -2 1 0 71.10 61.93 0.54 o -1 1 0 952.99 1060.61 8.52 o 1 1 0 383.28 187.46 0.74 o 2 1 0 78.72 74.53 0.48 o 3 1 0 151.16 187.64 3.10 o 4 1 0 8.47 14.23 0.45 o 5 1 0 108.46 98.37 1.63 o 6 1 0 145.80 149.81 8.76 o 7 1 0 314.52 313.01 1.62 o 8 1 0 170.52 178.22 3.26 o 9 1 0 85.10 90.49 1.21 o 10 1 0 4.75 4.37 1.44 o -9 2 0 1.09 2.00 0.78 o -8 2 0 467.46 490.45 6.82 o -7 2 0 2.83 4.44 0.51 o -6 2 0 188.81 194.61 1.69 o -5 2 0 7.19 14.62 0.43 o -4 2 0 967.20 939.18 2.28 o -3 2 0 9.18 5.68 0.35 o -2 2 0 2.83 5.59 0.21 o -1 2 0 5397.64 5379.19 23.43 o 0 2 0 692.81 747.05 4.32 o 1 2 0 1923.66 1950.83 19.11 o 2 2 0 101.20 65.21 1.13 o 3 2 0 485.34 454.24 2.19 o 4 2 0 51.76 51.28 0.59 o 5 2 0 498.14 489.05 11.52 o 6 2 0 9.03 7.70 0.52 o 7 2 0 633.59 605.37 22.37 o 8 2 0 17.26 21.03 0.77 o 9 2 0 165.06 163.72 2.31 o 10 2 0 46.88 47.89 1.80 o -9 3 0 8.00 5.32 1.18 o -8 3 0 248.30 254.42 2.98 o -7 3 0 616.86 609.70 6.98 o -6 3 0 690.85 686.58 4.28 o -5 3 0 172.07 175.44 2.01 o -4 3 0 218.92 184.78 1.45 o -3 3 0 308.76 312.03 1.93 o -2 3 0 44.07 103.89 18.09 o -1 3 0 927.20 872.79 7.84 o 0 3 0 1133.00 1163.19 5.81 o 1 3 0 1589.87 1647.32 18.16 o 2 3 0 142.74 135.73 1.64 o 3 3 0 79.20 71.61 0.46 o 4 3 0 4.77 9.83 0.42 o 5 3 0 110.55 118.46 0.90 o 6 3 0 41.19 43.80 0.72 o 7 3 0 1.46 2.71 1.08 o 8 3 0 94.32 97.63 7.51 o 9 3 0 16.38 18.03 1.39 o 10 3 0 6.82 2.14 1.43 o -8 4 0 78.68 75.10 1.60 o -7 4 0 208.72 205.54 4.35 o -6 4 0 4.10 2.62 0.61 o -5 4 0 21.39 16.54 0.62 o -4 4 0 0.22 2.35 0.29 o -3 4 0 52.25 47.40 0.79 o -2 4 0 117.92 150.90 1.87 o -1 4 0 2793.23 3063.57 13.50 o 0 4 0 1833.77 1813.92 11.93 o 1 4 0 736.64 711.59 2.74 o 2 4 0 1.68 1.17 0.36 o 3 4 0 474.06 434.84 1.87 o 4 4 0 2.22 0.91 0.40 o 5 4 0 177.57 157.73 1.91 o 6 4 0 8.80 7.05 0.40 o 7 4 0 2.34 2.72 0.63 o 8 4 0 125.50 116.47 1.51 o 9 4 0 124.11 144.05 2.35 o -8 5 0 1.33 1.02 1.15 o -7 5 0 18.94 20.27 1.19 o -6 5 0 67.83 60.29 0.94 o -5 5 0 65.14 58.65 1.06 o -4 5 0 154.56 153.08 1.74 o -3 5 0 19.36 20.13 0.42 o -2 5 0 520.51 571.08 1.92 o -1 5 0 61.36 70.16 0.70 o 0 5 0 5.26 4.31 0.33 o 1 5 0 34.69 27.05 0.53 o 2 5 0 237.26 238.21 2.49 o 3 5 0 284.37 308.85 1.23 o 4 5 0 125.80 114.00 2.11 o 5 5 0 199.82 195.63 2.63 o 6 5 0 11.01 9.07 0.67 o 7 5 0 67.38 68.41 1.00 o 8 5 0 85.45 82.59 1.81 o 9 5 0 58.49 63.04 2.00 o -7 6 0 1.64 1.85 1.15 o -6 6 0 0.19 1.05 0.99 o -5 6 0 10.23 12.05 1.07 o -4 6 0 178.81 168.74 1.61 o -3 6 0 156.65 149.71 2.01 o -2 6 0 203.67 187.19 1.17 o -1 6 0 472.85 449.80 1.84 o 0 6 0 344.05 344.73 2.39 o 1 6 0 107.59 106.87 0.69 o 2 6 0 27.64 24.42 0.55 o 3 6 0 82.49 89.45 1.54 o 4 6 0 315.14 293.34 6.06 o 5 6 0 0.04 0.49 0.42 o 6 6 0 58.41 58.73 1.17 o 7 6 0 1.43 0.51 1.02 o 8 6 0 10.93 10.87 1.36 o -6 7 0 16.09 12.97 1.27 o -5 7 0 370.45 376.54 3.19 o -4 7 0 23.04 21.51 1.20 o -3 7 0 2.12 0.00 0.62 o -2 7 0 46.96 48.48 0.68 o -1 7 0 18.54 21.14 0.50 o 0 7 0 12.01 15.18 0.48 o 1 7 0 20.51 19.85 0.51 o 2 7 0 2.76 4.77 0.52 o 3 7 0 220.37 201.58 1.23 o 4 7 0 9.68 8.52 0.58 o 5 7 0 1.29 2.68 0.72 o 6 7 0 12.92 9.73 0.75 o 7 7 0 49.92 63.38 1.65 o 8 7 0 1.91 3.23 1.32 o -5 8 0 29.23 25.69 1.43 o -4 8 0 20.24 19.13 1.26 o -3 8 0 45.56 44.68 1.43 o -2 8 0 129.37 120.88 1.91 o -1 8 0 1.08 1.65 0.65 o 0 8 0 13.06 14.56 0.74 o 1 8 0 25.27 23.31 0.69 o 2 8 0 444.12 474.28 1.78 o 3 8 0 70.20 68.34 2.35 o 4 8 0 18.90 17.68 0.70 o 5 8 0 7.07 5.04 0.70 o 6 8 0 50.37 52.51 1.13 o 7 8 0 1.47 3.17 1.28 o -4 9 0 5.19 3.94 1.25 o -3 9 0 7.28 5.52 1.22 o -2 9 0 1.20 0.17 1.08 o -1 9 0 0.95 0.58 1.04 o 0 9 0 43.96 44.64 1.41 o 1 9 0 313.46 325.08 1.86 o 2 9 0 28.26 28.80 1.19 o 3 9 0 23.50 21.98 1.14 o 5 9 0 14.51 15.00 1.18 o 6 9 0 54.16 61.61 1.16 o -1 10 0 9.10 7.60 1.20 o 0 10 0 17.20 14.20 1.27 o 1 10 0 7.58 10.03 1.16 o 2 10 0 0.55 2.12 1.07 o 3 10 0 165.51 174.66 5.16 o -3 -10 1 103.99 110.51 1.88 o -2 -10 1 57.03 60.88 1.59 o -1 -10 1 48.48 54.54 1.61 o 0 -10 1 33.60 35.87 1.46 o 1 -10 1 23.57 27.16 1.46 o -5 -9 1 50.91 41.75 1.49 o -4 -9 1 19.58 20.94 1.79 o -3 -9 1 127.28 125.21 1.82 o -2 -9 1 72.56 74.07 1.10 o -1 -9 1 120.13 124.94 1.89 o 0 -9 1 0.63 0.79 0.99 o 1 -9 1 11.97 12.42 1.15 o 2 -9 1 0.34 0.00 1.13 o 3 -9 1 4.05 2.34 1.16 o 4 -9 1 14.93 14.91 1.39 o -7 -8 1 0.45 0.84 1.27 o -6 -8 1 58.43 66.02 1.66 o -5 -8 1 0.58 1.05 0.68 o -4 -8 1 52.77 48.84 2.43 o -3 -8 1 25.91 21.95 0.74 o -2 -8 1 57.84 51.16 1.00 o -1 -8 1 1.25 1.14 0.52 o 0 -8 1 2.55 3.17 0.96 o 1 -8 1 75.71 77.52 1.60 o 2 -8 1 371.45 369.87 3.01 o 3 -8 1 14.60 14.87 1.19 o 4 -8 1 21.80 19.42 1.34 o 5 -8 1 24.84 24.50 1.43 o -8 -7 1 27.22 26.99 1.58 o -7 -7 1 28.86 25.28 1.44 o -6 -7 1 1.83 0.41 0.69 o -5 -7 1 49.92 45.49 1.01 o -4 -7 1 6.21 5.27 0.59 o -3 -7 1 28.75 33.04 0.73 o -2 -7 1 26.34 24.59 0.66 o -1 -7 1 20.49 19.56 0.53 o 0 -7 1 19.79 20.51 0.51 o 1 -7 1 10.99 9.68 0.42 o 2 -7 1 89.46 94.75 1.08 o 3 -7 1 181.05 175.44 1.93 o 4 -7 1 73.23 71.71 1.60 o 5 -7 1 31.26 33.82 1.38 o 6 -7 1 48.36 51.40 1.61 o -8 -6 1 80.85 98.48 2.01 o -7 -6 1 215.30 229.39 2.51 o -6 -6 1 1.22 0.60 1.09 o -5 -6 1 5.77 4.66 0.46 o -4 -6 1 7.66 7.10 0.54 o -3 -6 1 32.44 29.91 0.63 o -2 -6 1 130.37 124.85 2.19 o -1 -6 1 275.45 280.41 1.31 o 0 -6 1 11.05 10.28 0.42 o 1 -6 1 1243.44 1203.84 6.42 o 2 -6 1 177.82 183.25 1.47 o 3 -6 1 101.42 96.76 1.17 o 4 -6 1 108.93 115.33 1.70 o 5 -6 1 130.20 129.66 1.89 o 6 -6 1 23.73 22.33 1.22 o 7 -6 1 3.49 3.93 1.13 o -9 -5 1 27.55 29.78 1.61 o -8 -5 1 0.47 0.86 1.22 o -7 -5 1 8.54 8.82 1.20 o -6 -5 1 68.78 75.69 1.56 o -5 -5 1 139.51 132.72 1.75 o -4 -5 1 227.04 228.84 1.71 o -3 -5 1 90.40 91.10 2.41 o -2 -5 1 96.12 97.44 1.16 o -1 -5 1 101.96 114.49 2.01 o 0 -5 1 234.10 241.02 1.20 o 1 -5 1 1793.40 1914.01 2.76 o 2 -5 1 65.62 91.06 0.97 o 3 -5 1 49.31 58.61 0.58 o 4 -5 1 131.55 120.10 1.19 o 5 -5 1 173.91 167.86 1.18 o 6 -5 1 62.84 69.43 1.49 o 7 -5 1 1.26 2.17 0.98 o 8 -5 1 268.97 289.10 2.87 o -9 -4 1 28.80 27.36 1.59 o -8 -4 1 125.46 122.91 2.01 o -7 -4 1 410.79 399.82 3.45 o -6 -4 1 304.78 291.95 2.25 o -5 -4 1 4.43 3.03 0.34 o -4 -4 1 271.59 258.19 1.97 o -3 -4 1 34.48 25.62 1.22 o -2 -4 1 1.96 3.20 0.42 o -1 -4 1 12.00 21.49 0.70 o 0 -4 1 1192.81 1245.82 3.33 o 1 -4 1 1336.12 1326.81 2.10 o 2 -4 1 666.00 581.85 2.62 o 3 -4 1 72.05 75.60 1.60 o 4 -4 1 144.55 126.10 1.70 o 5 -4 1 403.00 382.61 1.59 o 6 -4 1 181.86 184.83 1.08 o 7 -4 1 19.29 18.15 0.78 o 8 -4 1 69.12 72.51 1.15 o -9 -3 1 2.35 4.31 1.45 o -8 -3 1 45.87 47.47 1.48 o -7 -3 1 724.03 760.72 4.73 o -6 -3 1 166.33 154.11 1.08 o -5 -3 1 2.29 1.96 0.41 o -4 -3 1 0.28 0.00 0.37 o -3 -3 1 7.35 6.70 0.33 o -2 -3 1 150.17 113.56 0.77 o -1 -3 1 18.54 34.66 4.49 o 0 -3 1 1103.28 1145.70 2.79 o 1 -3 1 1118.55 1262.34 2.48 o 2 -3 1 27.90 34.12 0.45 o 3 -3 1 26.82 28.97 0.32 o 4 -3 1 119.63 126.30 1.63 o 5 -3 1 66.54 64.77 1.28 o 6 -3 1 25.58 20.19 0.81 o 7 -3 1 261.04 245.36 3.23 o 8 -3 1 70.08 69.96 1.06 o 9 -3 1 1.26 3.02 1.17 o -9 -2 1 1.20 0.09 1.27 o -8 -2 1 104.15 95.74 6.08 o -7 -2 1 137.82 124.10 1.54 o -6 -2 1 95.74 108.36 1.09 o -5 -2 1 164.93 148.36 2.14 o -4 -2 1 170.67 153.10 0.85 o -3 -2 1 37.45 50.18 0.50 o -2 -2 1 1912.50 1848.34 3.40 o -1 -2 1 4339.07 4440.16 21.03 o 0 -2 1 16418.48 17018.89 118.86 o 1 -2 1 19227.86 20386.37 19.87 o 2 -2 1 915.13 832.52 1.35 o 3 -2 1 311.88 330.54 1.60 o 4 -2 1 92.93 91.09 1.23 o 5 -2 1 922.40 950.52 9.64 o 6 -2 1 339.77 338.61 2.56 o 7 -2 1 49.43 53.05 2.19 o 8 -2 1 179.23 168.78 1.36 o 9 -2 1 34.74 43.72 1.42 o -9 -1 1 0.15 0.00 1.17 o -8 -1 1 28.79 33.26 0.84 o -7 -1 1 20.88 25.56 3.22 o -6 -1 1 540.41 550.39 3.57 o -5 -1 1 350.84 368.39 3.68 o -4 -1 1 3.33 1.17 0.27 o -3 -1 1 851.06 860.94 8.84 o -2 -1 1 4.48 3.53 0.28 o -1 -1 1 669.84 632.04 1.08 o 0 -1 1 10.75 8.50 0.34 o 1 -1 1 184.52 174.56 0.84 o 2 -1 1 711.89 789.17 1.59 o 3 -1 1 52.62 53.47 0.48 o 4 -1 1 343.11 343.24 2.08 o 5 -1 1 32.45 26.25 0.76 o 6 -1 1 106.59 111.32 1.51 o 7 -1 1 143.48 139.67 0.93 o 8 -1 1 179.70 189.25 1.92 o 9 -1 1 32.48 29.10 0.94 o 10 -1 1 94.13 115.89 2.64 o -9 0 1 15.52 15.08 1.34 o -8 0 1 122.73 125.53 2.60 o -7 0 1 686.23 680.22 4.31 o -6 0 1 0.98 1.07 0.27 o -5 0 1 39.66 49.61 0.88 o -4 0 1 1.73 2.75 0.25 o -3 0 1 250.21 214.67 1.38 o -2 0 1 19.99 24.07 0.30 o -1 0 1 4954.76 4965.16 204.53 o 2 0 1 2.86 3.74 0.18 o 3 0 1 3.22 3.51 0.26 o 4 0 1 2159.37 2184.18 5.62 o 5 0 1 300.79 326.43 0.84 o 6 0 1 4.42 3.28 0.29 o 7 0 1 13.72 14.21 0.67 o 8 0 1 226.19 245.32 1.66 o 9 0 1 6.99 2.96 0.76 o 10 0 1 25.79 27.32 1.01 o -9 1 1 75.42 78.62 1.18 o -8 1 1 29.99 29.76 0.86 o -7 1 1 1046.10 1097.94 9.40 o -6 1 1 253.25 259.47 1.15 o -5 1 1 0.86 2.34 0.36 o -4 1 1 778.28 799.98 2.37 o -3 1 1 2.19 4.80 0.31 o -2 1 1 1166.97 1246.63 3.07 o -1 1 1 6338.10 6248.76 23.24 o 1 1 1 585.31 460.67 42.56 o 2 1 1 1571.07 1737.41 53.81 o 3 1 1 12.55 8.95 0.97 o 4 1 1 520.95 525.57 1.55 o 5 1 1 375.82 434.65 2.18 o 6 1 1 95.80 97.97 1.35 o 7 1 1 15.27 19.46 0.69 o 8 1 1 32.18 29.72 0.84 o 9 1 1 56.50 48.77 1.99 o 10 1 1 2.38 1.43 0.84 o -9 2 1 1.63 1.01 0.81 o -8 2 1 373.64 377.16 2.02 o -7 2 1 0.07 1.53 0.53 o -6 2 1 387.34 368.27 1.39 o -5 2 1 1.60 3.63 0.34 o -4 2 1 9.36 18.82 0.36 o -3 2 1 40.83 46.76 0.55 o -2 2 1 58.04 76.03 1.61 o -1 2 1 769.64 922.51 1.56 o 0 2 1 6733.74 7247.04 62.52 o 1 2 1 284.75 289.99 0.67 o 2 2 1 572.67 524.17 3.76 o 3 2 1 856.58 850.94 6.29 o 4 2 1 337.57 341.58 3.99 o 5 2 1 27.44 34.42 0.60 o 6 2 1 141.01 147.47 2.10 o 7 2 1 73.21 66.05 0.90 o 8 2 1 10.33 8.87 1.52 o 9 2 1 23.49 22.19 0.87 o 10 2 1 36.47 34.76 1.70 o -8 3 1 33.93 36.83 0.96 o -7 3 1 301.97 313.66 2.11 o -6 3 1 288.56 274.85 1.45 o -5 3 1 89.59 81.23 0.75 o -4 3 1 89.45 99.03 1.51 o -3 3 1 442.06 482.92 1.90 o -2 3 1 1051.16 1111.36 2.27 o -1 3 1 15.40 21.79 0.45 o 0 3 1 142.10 122.93 1.62 o 1 3 1 7.36 12.10 0.34 o 2 3 1 64.13 57.91 1.30 o 3 3 1 1321.97 1421.59 2.17 o 4 3 1 38.34 42.35 0.80 o 5 3 1 9.82 13.64 0.65 o 6 3 1 160.27 149.13 1.45 o 7 3 1 110.79 111.45 4.21 o 8 3 1 46.83 41.80 0.91 o 9 3 1 10.81 8.46 0.84 o 10 3 1 21.14 22.65 1.55 o -8 4 1 95.73 99.92 1.28 o -7 4 1 38.45 39.08 0.91 o -6 4 1 0.68 0.13 0.62 o -5 4 1 141.39 137.06 2.03 o -4 4 1 1.37 2.48 0.27 o -3 4 1 179.57 196.32 1.45 o -2 4 1 747.74 773.16 1.94 o -1 4 1 1524.03 1511.79 12.76 o 0 4 1 385.53 322.95 3.80 o 1 4 1 383.60 371.63 1.16 o 2 4 1 667.99 686.24 2.75 o 3 4 1 218.18 210.86 0.87 o 4 4 1 73.19 66.52 0.93 o 5 4 1 0.11 0.23 0.26 o 6 4 1 35.95 39.02 0.74 o 7 4 1 129.79 128.98 3.31 o 8 4 1 5.73 7.12 1.73 o 9 4 1 11.41 9.62 0.81 o -8 5 1 110.88 111.19 2.03 o -7 5 1 2.31 1.82 0.73 o -6 5 1 110.65 119.12 1.43 o -5 5 1 496.28 460.59 5.30 o -4 5 1 326.41 300.97 4.35 o -3 5 1 2.33 2.69 0.49 o -2 5 1 253.24 252.52 3.24 o -1 5 1 0.31 2.53 0.44 o 0 5 1 355.53 353.88 0.95 o 1 5 1 0.37 0.37 0.29 o 2 5 1 15.72 13.62 0.55 o 3 5 1 91.01 92.61 0.70 o 4 5 1 8.12 5.50 0.34 o 5 5 1 29.45 27.17 0.43 o 6 5 1 73.00 79.60 0.99 o 7 5 1 172.95 179.55 1.96 o 8 5 1 90.96 107.50 3.76 o 9 5 1 56.65 64.57 1.82 o -7 6 1 0.63 0.59 1.13 o -6 6 1 11.39 10.70 1.14 o -5 6 1 3.50 0.75 1.39 o -4 6 1 227.42 216.63 1.42 o -3 6 1 62.62 51.87 0.81 o -2 6 1 0.02 0.00 0.53 o -1 6 1 10.64 13.55 0.58 o 0 6 1 0.00 0.27 0.33 o 1 6 1 6.85 8.08 0.36 o 2 6 1 166.48 181.67 0.99 o 3 6 1 51.15 62.84 0.69 o 4 6 1 72.79 84.08 0.82 o 5 6 1 0.70 0.26 0.39 o 6 6 1 52.89 52.79 0.94 o 7 6 1 88.69 80.76 1.11 o 8 6 1 340.25 361.11 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0.08 0.24 1.40 o -2 0 12 45.08 49.23 1.07 o -1 0 12 98.30 110.94 1.34 o 0 0 12 2.12 2.55 0.64 o 1 0 12 70.66 72.84 0.91 o 2 0 12 8.45 10.25 0.60 o 3 0 12 205.73 194.50 3.64 o 4 0 12 121.41 123.34 1.05 o 5 0 12 5.83 5.89 0.91 o 6 0 12 71.17 68.75 1.17 o 7 0 12 0.79 1.02 1.24 o -3 1 12 3.19 4.42 1.48 o -2 1 12 8.30 9.77 0.71 o -1 1 12 21.19 20.46 0.72 o 0 1 12 7.26 6.34 0.99 o 1 1 12 9.19 11.68 1.60 o 2 1 12 1.73 2.45 0.64 o 3 1 12 70.76 66.73 1.01 o 4 1 12 12.40 9.89 0.76 o 5 1 12 20.41 24.00 1.27 o 6 1 12 0.07 0.00 1.09 o 7 1 12 3.04 5.81 1.23 o -3 2 12 61.43 75.73 1.35 o -2 2 12 23.95 22.23 1.37 o -1 2 12 12.27 13.37 1.22 o 0 2 12 27.96 32.82 1.35 o 1 2 12 4.35 6.89 0.77 o 2 2 12 2.29 0.86 0.87 o 3 2 12 224.52 206.42 1.53 o 4 2 12 62.23 67.28 1.55 o 5 2 12 0.33 1.39 0.73 o 6 2 12 8.93 9.79 0.87 o 7 2 12 0.34 1.64 1.26 o -3 3 12 40.92 45.87 1.75 o -2 3 12 22.47 20.80 1.43 o -1 3 12 1.64 1.52 1.14 o 0 3 12 10.32 16.79 1.26 o 1 3 12 25.87 21.58 0.80 o 2 3 12 25.88 15.67 0.81 o 3 3 12 22.55 17.78 0.84 o 4 3 12 19.50 18.86 0.87 o 5 3 12 3.82 3.84 0.80 o 6 3 12 0.62 0.66 1.06 o 7 3 12 40.67 41.96 1.14 o -2 4 12 38.50 38.45 1.65 o -1 4 12 1.42 1.78 1.26 o 0 4 12 88.55 92.91 1.90 o 1 4 12 26.30 27.18 1.13 o 2 4 12 108.42 103.09 1.67 o 3 4 12 56.01 54.01 1.08 o 4 4 12 28.88 37.39 1.96 o 5 4 12 4.07 3.92 0.85 o 6 4 12 45.86 55.56 2.10 o -1 5 12 2.36 0.36 1.34 o 0 5 12 3.24 2.79 0.81 o 1 5 12 27.89 25.22 1.73 o 2 5 12 0.05 0.45 0.82 o 3 5 12 6.50 6.93 0.95 o 4 5 12 0.00 2.09 0.86 o 5 5 12 0.86 1.54 0.88 o 6 5 12 22.08 18.49 1.04 o 0 6 12 0.11 0.04 0.87 o 1 6 12 24.26 26.10 1.03 o 2 6 12 15.13 15.51 0.96 o 3 6 12 0.29 0.99 0.87 o 4 6 12 16.19 24.77 1.36 o 0 -3 13 3.66 3.95 0.99 o 1 -3 13 14.49 14.27 1.40 o 2 -3 13 1.57 2.96 1.23 o 3 -3 13 4.73 4.11 1.26 o -1 -2 13 3.50 0.98 1.43 o 0 -2 13 3.26 2.20 1.45 o 1 -2 13 1.46 4.23 1.50 o 2 -2 13 0.01 0.84 1.26 o 3 -2 13 6.26 3.40 1.25 o 4 -2 13 0.99 0.16 0.79 o -2 -1 13 0.29 0.42 1.81 o -1 -1 13 39.25 40.18 2.30 o 0 -1 13 1.06 0.69 1.43 o 1 -1 13 23.74 21.50 1.55 o 3 -1 13 0.75 0.48 1.17 o 4 -1 13 78.31 71.63 1.17 o 5 -1 13 18.72 20.66 1.31 o -2 0 13 1.63 0.70 0.86 o -1 0 13 5.54 0.97 0.89 o 0 0 13 34.77 35.48 0.85 o 1 0 13 5.50 7.37 0.79 o 2 0 13 5.32 6.04 1.32 o 3 0 13 166.53 161.45 5.17 o 4 0 13 3.00 4.29 0.68 o 5 0 13 0.00 0.84 0.83 o 6 0 13 0.07 0.15 0.84 o -2 1 13 2.51 0.00 1.59 o -1 1 13 2.47 0.92 1.15 o 0 1 13 28.57 35.17 1.11 o 1 1 13 0.01 1.59 0.84 o 2 1 13 99.57 104.72 1.71 o 3 1 13 33.10 41.74 0.94 o 4 1 13 24.38 24.82 1.25 o 5 1 13 35.71 40.49 1.45 o 6 1 13 0.55 0.00 1.15 o -2 2 13 6.69 7.42 0.99 o -1 2 13 0.15 0.29 1.19 o 0 2 13 13.24 15.05 1.30 o 1 2 13 13.75 12.43 1.21 o 2 2 13 110.86 118.62 1.92 o 3 2 13 0.03 0.65 0.74 o 4 2 13 4.23 5.08 0.87 o 5 2 13 0.61 0.25 1.11 o 6 2 13 52.24 62.38 1.76 o -1 3 13 2.03 2.44 1.30 o 0 3 13 0.12 1.17 1.25 o 1 3 13 0.55 0.90 1.17 o 2 3 13 1.76 1.46 0.80 o 3 3 13 25.11 25.75 0.93 o 4 3 13 2.49 5.23 0.84 o 5 3 13 0.26 0.00 0.81 o 0 4 13 54.21 66.23 1.84 o 1 4 13 20.12 20.20 1.42 o 2 4 13 16.01 16.57 2.05 o 3 4 13 21.58 20.19 0.95 o 4 4 13 28.84 36.32 1.06 o 5 4 13 16.24 19.47 1.01 o 1 5 13 1.73 0.00 1.41 o 2 5 13 3.59 4.53 1.24 o 3 5 13 2.43 9.36 1.06 o 4 5 13 0.19 0.56 0.90 o 1 -1 14 28.74 34.15 1.75 o 3 -1 14 4.81 4.33 1.25 o 0 0 14 3.71 3.82 1.38 o 1 0 14 1.21 1.72 0.98 o 2 0 14 11.67 11.09 1.49 o 3 0 14 0.69 0.00 1.43 o 4 0 14 52.13 52.32 2.02 o 0 1 14 11.50 12.20 2.14 o 1 1 14 1.44 0.70 0.74 o 2 1 14 26.46 18.37 1.53 o 3 1 14 105.53 119.76 2.22 o 4 1 14 1.34 0.77 0.85 o 0 2 14 29.46 38.53 1.56 o 1 2 14 15.18 15.60 1.36 o 2 2 14 10.01 11.00 1.29 o 3 2 14 0.12 0.61 1.19 o 4 2 14 3.26 3.29 1.14 o 1 3 14 8.88 9.89 1.35 o 2 3 14 6.60 4.91 1.32 o 3 3 14 3.04 0.71 0.83 o