#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/77/2237773.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237773_Fobs loop_ _publ_author_name 'Ravichandran, K.' 'Manikannan, R.' 'Muthusubramanian, S.' 'Ramesh, P.' 'Ponnuswamy, M. N.' _publ_section_title ; 4-(2-Hydroxyphenyl)-3,5-dithiaheptanedioic acid ; _journal_coeditor_code BT6906 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o893 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.094 _cell_angle_beta 99.129 _cell_angle_gamma 102.390 _cell_length_a 7.2465 _cell_length_b 7.6533 _cell_length_c 12.0141 _exptl_crystal_F_000 300.00 _reflns_d_resolution_high 0.8417 _[local]_cod_data_source_file bt6906Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' satga in P -1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1173.85 1252.79 4.33 o 2 0 0 17.10 20.03 0.62 o 3 0 0 1735.88 1775.96 7.33 o 4 0 0 181.44 188.65 2.99 o 6 0 0 454.13 432.13 5.78 o 7 0 0 61.75 57.29 1.66 o 8 0 0 3.69 2.31 1.91 o -8 1 0 1.15 0.81 1.69 o -7 1 0 77.91 77.34 2.29 o -6 1 0 447.19 444.15 5.78 o -5 1 0 35.40 35.58 1.13 o -4 1 0 17.83 18.04 0.72 o -3 1 0 952.07 1057.05 5.61 o -2 1 0 9344.87 9763.21 13.58 o -1 1 0 2.31 7.02 0.26 o 0 1 0 697.88 683.55 6.63 o 1 1 0 697.80 691.53 2.30 o 2 1 0 12.42 15.72 0.57 o 3 1 0 1575.95 1577.59 7.38 o 4 1 0 3.35 0.34 1.14 o 6 1 0 254.13 254.96 4.60 o 7 1 0 122.63 124.36 3.34 o -8 2 0 9.52 11.26 1.18 o -7 2 0 44.01 42.18 1.47 o -6 2 0 33.11 29.18 1.24 o -5 2 0 396.15 392.68 4.78 o -4 2 0 23.38 29.28 0.90 o -3 2 0 0.38 -0.09 0.89 o -2 2 0 9990.20 10346.50 15.40 o -1 2 0 6655.81 6600.10 46.96 o 0 2 0 1404.18 1321.59 8.66 o 1 2 0 140.15 131.56 1.36 o 2 2 0 953.63 993.37 5.60 o 3 2 0 223.33 216.00 3.14 o 4 2 0 226.25 224.81 3.65 o 5 2 0 94.84 87.42 2.39 o 6 2 0 65.36 65.65 1.81 o 7 2 0 1.55 0.88 1.73 o -8 3 0 146.10 136.23 3.65 o -7 3 0 125.18 110.55 3.00 o -6 3 0 14.66 12.37 1.07 o -5 3 0 393.30 392.44 4.94 o -4 3 0 3305.11 3359.96 12.54 o -3 3 0 612.92 663.17 5.03 o -2 3 0 462.56 513.15 4.01 o -1 3 0 406.30 390.30 2.38 o 0 3 0 79.91 72.08 1.47 o 1 3 0 69.56 66.83 2.50 o 2 3 0 1657.83 1568.95 8.07 o 3 3 0 3.76 5.94 0.70 o 4 3 0 187.38 180.48 3.60 o 5 3 0 681.89 655.08 7.31 o 6 3 0 7.12 4.93 1.09 o 7 3 0 13.55 13.06 1.34 o -8 4 0 35.63 35.59 1.62 o -7 4 0 15.60 15.83 1.22 o -6 4 0 75.13 68.21 1.97 o -5 4 0 157.47 159.61 3.52 o -4 4 0 26.76 26.97 1.11 o -3 4 0 496.03 537.63 5.03 o -2 4 0 429.38 433.07 4.21 o -1 4 0 161.61 159.00 1.89 o 0 4 0 80.12 85.49 1.45 o 1 4 0 221.09 213.18 2.27 o 2 4 0 377.13 351.53 4.43 o 3 4 0 17.92 13.84 1.03 o 4 4 0 158.40 156.20 3.81 o 5 4 0 175.57 177.28 4.37 o 6 4 0 7.56 10.00 1.18 o -8 5 0 24.60 23.87 1.49 o -7 5 0 0.10 1.17 1.76 o -6 5 0 136.00 120.03 3.52 o -5 5 0 161.37 160.91 3.74 o -4 5 0 141.40 138.22 3.23 o -3 5 0 27.09 32.12 1.18 o -2 5 0 5.82 8.62 0.83 o -1 5 0 601.54 601.32 3.98 o 0 5 0 211.46 206.13 2.53 o 1 5 0 1.27 1.32 0.67 o 2 5 0 213.80 221.41 4.06 o 3 5 0 236.85 201.34 4.25 o 4 5 0 9.10 13.24 1.12 o 5 5 0 72.69 74.62 2.16 o -7 6 0 32.97 28.17 1.61 o -6 6 0 19.15 18.61 1.46 o -5 6 0 0.34 -0.49 1.63 o -4 6 0 8.70 7.50 1.12 o -3 6 0 7.20 5.02 1.10 o -2 6 0 1.74 0.52 1.64 o -1 6 0 21.98 25.58 1.10 o 0 6 0 97.22 96.19 2.03 o 1 6 0 326.27 298.28 3.42 o 2 6 0 29.55 38.99 1.36 o 3 6 0 80.17 77.99 2.44 o 4 6 0 0.96 2.87 1.59 o -6 7 0 58.05 62.23 1.95 o -5 7 0 11.65 13.78 1.28 o -4 7 0 0.62 2.65 1.60 o -3 7 0 86.35 90.74 2.69 o -2 7 0 53.56 53.01 1.61 o -1 7 0 11.12 11.66 1.93 o 0 7 0 80.31 76.21 1.68 o 1 7 0 86.61 90.55 1.96 o 2 7 0 60.12 55.87 1.71 o 3 7 0 138.34 141.39 3.71 o -5 8 0 90.78 91.37 2.86 o -4 8 0 16.61 16.39 1.44 o -3 8 0 51.19 51.73 1.77 o -2 8 0 36.58 37.80 1.62 o -1 8 0 5.40 8.07 0.83 o 0 8 0 0.07 -0.47 1.23 o 1 8 0 164.48 180.66 3.31 o 2 -9 1 188.97 197.80 5.12 o -2 -8 1 57.66 53.34 1.89 o -1 -8 1 98.51 104.14 2.27 o 0 -8 1 1.44 0.50 1.22 o 1 -8 1 10.90 10.74 0.87 o 2 -8 1 211.63 213.53 4.85 o 3 -8 1 2.14 3.01 1.22 o 4 -8 1 98.90 96.15 2.75 o 5 -8 1 163.95 173.51 4.67 o -3 -7 1 33.90 33.53 1.54 o -2 -7 1 21.55 17.92 1.29 o -1 -7 1 1.14 1.37 1.18 o 0 -7 1 8.35 9.27 0.77 o 1 -7 1 128.76 120.80 2.42 o 2 -7 1 449.33 436.54 6.09 o 3 -7 1 2.31 2.34 1.01 o 4 -7 1 33.55 30.44 1.40 o 5 -7 1 71.23 77.53 2.32 o 6 -7 1 0.17 0.53 1.81 o -4 -6 1 5.59 5.00 1.08 o -3 -6 1 322.51 326.72 5.49 o -2 -6 1 28.10 28.38 1.29 o -1 -6 1 11.57 10.52 0.74 o 0 -6 1 33.82 33.55 1.87 o 1 -6 1 509.12 468.66 3.92 o 2 -6 1 95.81 97.20 2.62 o 3 -6 1 210.19 206.48 3.99 o 4 -6 1 302.17 295.53 4.91 o 5 -6 1 106.60 101.24 2.92 o 6 -6 1 101.09 91.17 2.71 o 7 -6 1 266.88 251.67 5.57 o -5 -5 1 188.23 196.61 4.77 o -4 -5 1 57.04 50.87 1.51 o -3 -5 1 184.64 206.15 4.22 o -2 -5 1 106.63 93.31 2.43 o -1 -5 1 0.14 -0.44 0.92 o 0 -5 1 2056.90 2082.41 7.29 o 1 -5 1 1283.26 1254.58 5.90 o 2 -5 1 33.23 37.88 1.16 o 3 -5 1 69.37 61.57 1.81 o 4 -5 1 765.93 774.42 7.10 o 5 -5 1 19.30 21.60 1.24 o 6 -5 1 141.89 141.47 3.85 o 7 -5 1 118.56 129.09 3.46 o -6 -4 1 4.94 10.66 1.15 o -5 -4 1 4.17 5.43 1.06 o -4 -4 1 47.86 44.63 1.39 o -3 -4 1 6.98 5.71 0.92 o -2 -4 1 747.71 741.76 6.30 o -1 -4 1 38.37 30.64 0.67 o 0 -4 1 44.86 41.67 0.86 o 1 -4 1 25.76 16.53 0.51 o 2 -4 1 2.07 -0.71 1.10 o 3 -4 1 167.80 184.23 3.13 o 4 -4 1 416.68 425.13 4.95 o 5 -4 1 339.76 331.55 4.83 o 6 -4 1 7.20 3.39 1.70 o 7 -4 1 122.24 125.59 3.26 o 8 -4 1 0.55 0.00 1.77 o -7 -3 1 178.68 168.00 4.78 o -6 -3 1 18.01 17.15 1.25 o -5 -3 1 0.17 -0.53 1.49 o -4 -3 1 71.66 69.53 2.10 o -3 -3 1 25.00 19.32 0.84 o -2 -3 1 540.12 628.92 5.07 o -1 -3 1 4198.37 4275.02 27.92 o 0 -3 1 2.19 2.31 0.36 o 1 -3 1 98.43 108.63 1.36 o 2 -3 1 567.25 559.54 4.23 o 3 -3 1 589.72 620.57 4.98 o 4 -3 1 12.33 13.71 0.85 o 5 -3 1 317.39 322.33 4.58 o 6 -3 1 14.59 17.42 1.12 o 7 -3 1 48.40 44.16 1.57 o 8 -3 1 1.33 -0.09 1.98 o -7 -2 1 95.84 96.62 3.01 o -6 -2 1 1.20 1.44 1.44 o -4 -2 1 918.33 953.64 7.12 o -3 -2 1 1258.75 1363.56 7.53 o -2 -2 1 99.30 98.98 1.91 o -1 -2 1 621.96 566.10 8.97 o 0 -2 1 122.32 144.53 1.30 o 1 -2 1 72.88 75.19 1.41 o 2 -2 1 1507.13 1620.90 6.29 o 3 -2 1 118.96 129.26 2.24 o 4 -2 1 220.01 248.66 3.44 o 5 -2 1 685.82 687.45 6.30 o 6 -2 1 27.73 26.79 1.27 o 7 -2 1 0.60 -1.58 1.58 o 8 -2 1 68.47 65.57 2.10 o -8 -1 1 16.07 13.66 1.22 o -7 -1 1 118.92 118.37 3.16 o -6 -1 1 39.38 40.06 1.37 o -5 -1 1 6.93 -0.26 0.26 o -4 -1 1 108.20 95.26 2.32 o -3 -1 1 441.79 496.16 4.16 o -2 -1 1 71.29 76.90 1.57 o -1 -1 1 458.82 473.74 5.62 o 0 -1 1 5.88 12.50 0.26 o 1 -1 1 270.47 306.76 1.44 o 2 -1 1 401.76 445.46 3.10 o 3 -1 1 541.92 567.05 4.24 o 4 -1 1 295.81 333.24 3.88 o 5 -1 1 599.78 609.49 5.94 o 6 -1 1 403.92 405.10 5.57 o 7 -1 1 0.44 1.14 1.50 o 8 -1 1 54.26 60.61 1.84 o -8 0 1 12.14 11.86 1.17 o -7 0 1 53.75 54.06 1.81 o -6 0 1 5.12 5.31 0.99 o -4 0 1 123.29 125.64 2.45 o -3 0 1 0.06 0.42 0.85 o -2 0 1 2.39 1.61 0.46 o -1 0 1 927.91 923.58 2.13 o 1 0 1 4.87 5.98 0.25 o 2 0 1 51.52 54.76 1.31 o 3 0 1 278.03 301.55 3.18 o 4 0 1 11.19 15.03 0.70 o 5 0 1 159.12 156.62 3.28 o 6 0 1 87.45 82.21 2.52 o 7 0 1 39.51 37.66 1.41 o 8 0 1 32.52 28.50 1.52 o -8 1 1 32.24 30.08 1.47 o -7 1 1 56.42 58.57 1.80 o -6 1 1 20.44 16.87 1.13 o -5 1 1 147.98 149.63 3.02 o -4 1 1 11.25 15.67 0.69 o -3 1 1 265.21 284.08 2.97 o -2 1 1 40.57 38.41 1.04 o -1 1 1 1068.49 1168.04 6.50 o 0 1 1 71.21 73.80 0.77 o 1 1 1 38.80 35.29 0.66 o 2 1 1 199.00 220.37 2.47 o 3 1 1 29.40 28.64 0.82 o 4 1 1 428.50 433.71 4.69 o 6 1 1 134.69 134.54 3.60 o 7 1 1 146.10 153.30 4.18 o -8 2 1 60.56 62.91 1.91 o -7 2 1 3.16 3.14 1.00 o -6 2 1 18.39 19.49 1.12 o -5 2 1 310.92 317.74 4.31 o -4 2 1 1.42 1.33 0.95 o -3 2 1 20.74 24.30 0.72 o -2 2 1 147.77 157.68 2.10 o -1 2 1 26.28 28.87 0.61 o 0 2 1 206.18 211.71 4.02 o 1 2 1 569.89 581.29 3.60 o 2 2 1 783.95 815.33 5.25 o 3 2 1 736.96 788.72 5.95 o 4 2 1 10.41 8.97 0.86 o 5 2 1 126.37 129.46 3.36 o 6 2 1 54.22 55.27 1.67 o 7 2 1 45.24 46.00 1.73 o -8 3 1 44.31 43.98 1.68 o -7 3 1 59.84 55.78 1.65 o -6 3 1 8.95 9.17 1.02 o -5 3 1 755.79 756.88 6.70 o -4 3 1 675.12 708.21 5.85 o -3 3 1 238.12 250.83 3.22 o -2 3 1 254.31 257.26 2.93 o -1 3 1 697.07 733.97 7.16 o 0 3 1 129.54 149.65 1.59 o 1 3 1 2755.82 2850.90 7.03 o 2 3 1 7.75 6.45 0.64 o 3 3 1 1.21 1.32 0.77 o 4 3 1 136.83 143.56 3.39 o 5 3 1 48.10 52.46 1.62 o 6 3 1 1.85 -0.34 1.62 o -8 4 1 19.23 19.79 1.38 o -7 4 1 66.37 65.05 1.95 o -6 4 1 1.23 2.20 1.45 o -5 4 1 621.21 609.64 6.37 o -4 4 1 44.86 44.92 1.29 o -3 4 1 14.72 16.06 0.81 o -2 4 1 95.73 90.09 2.24 o -1 4 1 635.39 663.87 3.72 o 0 4 1 278.90 284.33 2.52 o 1 4 1 20.27 25.61 0.61 o 2 4 1 286.78 289.58 4.12 o 3 4 1 2.59 0.73 1.38 o 4 4 1 98.53 97.32 2.64 o 5 4 1 185.69 179.28 4.34 o 6 4 1 24.49 28.80 1.50 o -8 5 1 0.69 -1.64 1.86 o -7 5 1 1.58 1.83 1.76 o -6 5 1 489.31 497.59 6.62 o -5 5 1 1.09 0.50 1.63 o -4 5 1 9.52 12.20 1.06 o -3 5 1 240.63 235.48 3.85 o -2 5 1 77.19 87.39 2.50 o -1 5 1 441.65 446.87 5.02 o 0 5 1 126.73 120.97 1.99 o 1 5 1 6.84 5.48 1.26 o 2 5 1 43.18 43.02 1.36 o 3 5 1 10.98 10.24 1.04 o 4 5 1 1.00 -0.08 1.60 o 5 5 1 1.69 -0.45 1.90 o -7 6 1 83.98 73.25 2.21 o -6 6 1 334.88 335.62 5.80 o -5 6 1 18.88 17.45 1.21 o -4 6 1 17.83 17.92 1.16 o -3 6 1 969.55 960.19 8.23 o -2 6 1 8.98 10.99 1.10 o -1 6 1 52.71 48.28 1.32 o 0 6 1 346.40 340.50 3.55 o 1 6 1 122.51 117.22 2.36 o 2 6 1 1.97 -0.28 1.49 o 3 6 1 312.18 314.37 5.65 o 4 6 1 70.18 65.16 2.06 o -6 7 1 77.66 82.49 2.51 o -5 7 1 21.22 23.51 1.39 o -4 7 1 51.01 49.12 1.61 o -3 7 1 168.40 179.18 4.14 o -2 7 1 0.99 0.99 1.65 o -1 7 1 58.62 59.06 1.20 o 0 7 1 190.28 196.31 4.91 o 1 7 1 137.61 137.03 4.05 o 2 7 1 14.42 9.96 1.24 o 3 7 1 28.18 28.27 1.58 o -5 8 1 14.27 12.47 1.43 o -4 8 1 107.45 115.06 3.33 o -3 8 1 69.04 66.75 2.07 o -2 8 1 16.48 17.69 1.43 o -1 8 1 16.62 16.25 0.94 o 0 8 1 71.99 72.21 1.43 o 1 8 1 5.09 4.96 1.10 o 1 -9 2 67.79 72.26 1.59 o 2 -9 2 18.72 20.25 1.53 o -2 -8 2 0.02 1.04 1.05 o -1 -8 2 0.61 1.35 1.24 o 0 -8 2 32.92 35.80 1.39 o 1 -8 2 0.53 1.15 2.95 o 2 -8 2 4.29 2.89 2.08 o 3 -8 2 11.28 11.23 1.36 o 4 -8 2 19.67 20.76 1.51 o 5 -8 2 1.32 -1.01 2.04 o -3 -7 2 124.12 141.18 4.14 o -2 -7 2 0.27 -1.33 1.65 o -1 -7 2 85.45 87.29 2.47 o 0 -7 2 308.23 296.27 3.62 o 1 -7 2 0.14 0.41 1.09 o 2 -7 2 112.99 109.41 2.90 o 3 -7 2 110.59 117.61 3.38 o 4 -7 2 2.77 1.77 1.80 o 5 -7 2 17.20 19.99 1.42 o 6 -7 2 48.96 54.92 1.93 o -4 -6 2 24.69 26.67 1.37 o -3 -6 2 312.93 294.43 5.27 o -2 -6 2 141.16 125.49 3.43 o -1 -6 2 2.14 2.05 1.13 o 0 -6 2 502.90 477.72 4.01 o 1 -6 2 40.80 41.06 1.24 o 2 -6 2 30.14 35.24 1.38 o 3 -6 2 124.01 129.41 3.41 o 4 -6 2 1.81 2.39 1.81 o 5 -6 2 57.53 61.45 1.84 o 6 -6 2 106.58 102.37 3.12 o 7 -6 2 120.76 112.98 3.20 o -5 -5 2 23.55 18.41 1.35 o -4 -5 2 3.61 7.31 0.99 o -3 -5 2 21.10 15.86 1.13 o -2 -5 2 3.37 3.29 0.89 o -1 -5 2 0.08 1.07 0.84 o 0 -5 2 39.43 38.86 0.83 o 1 -5 2 26.12 27.73 0.77 o 2 -5 2 52.87 55.09 1.62 o 3 -5 2 122.60 129.44 3.10 o 4 -5 2 0.03 2.83 1.61 o 5 -5 2 59.48 65.92 2.11 o 6 -5 2 2.10 2.30 1.68 o 7 -5 2 33.37 32.63 1.58 o -6 -4 2 11.59 9.90 1.20 o -5 -4 2 44.80 44.94 1.51 o -4 -4 2 557.34 524.18 6.39 o -3 -4 2 44.04 41.10 1.24 o -2 -4 2 1.68 0.88 1.17 o -1 -4 2 154.48 150.70 1.94 o 0 -4 2 141.31 146.17 1.81 o 1 -4 2 165.22 172.30 3.24 o 2 -4 2 547.02 563.01 4.94 o 3 -4 2 87.18 89.90 2.38 o 4 -4 2 207.26 204.85 3.69 o 5 -4 2 194.60 196.26 3.90 o 6 -4 2 2.78 1.25 1.53 o 7 -4 2 6.81 7.40 1.12 o 8 -4 2 31.49 30.00 1.61 o -7 -3 2 172.26 166.74 4.50 o -6 -3 2 71.17 64.96 1.90 o -5 -3 2 12.29 11.55 1.01 o -4 -3 2 481.35 473.60 5.51 o -3 -3 2 15.08 17.30 0.82 o -2 -3 2 0.84 1.75 0.55 o -1 -3 2 480.78 466.87 2.81 o 0 -3 2 158.87 165.20 2.09 o 1 -3 2 137.58 124.82 2.39 o 2 -3 2 1653.58 1761.59 7.64 o 3 -3 2 1103.43 1253.99 7.12 o 4 -3 2 0.13 -0.40 1.24 o 5 -3 2 198.24 187.68 3.69 o 6 -3 2 33.30 34.21 1.32 o 7 -3 2 15.87 13.65 1.19 o 8 -3 2 92.90 87.44 2.80 o -7 -2 2 63.32 69.18 2.16 o -6 -2 2 6.48 6.66 0.99 o -4 -2 2 1459.27 1444.03 8.79 o -3 -2 2 161.94 170.22 2.79 o -2 -2 2 140.38 154.56 2.35 o -1 -2 2 2475.31 2452.48 28.60 o 0 -2 2 4.93 4.78 0.46 o 1 -2 2 2173.81 2283.85 40.47 o 2 -2 2 318.35 349.83 3.13 o 3 -2 2 43.12 43.30 1.33 o 4 -2 2 47.76 46.22 1.40 o 5 -2 2 433.72 416.88 5.09 o 6 -2 2 58.30 59.75 1.82 o 7 -2 2 0.03 2.33 1.42 o 8 -2 2 39.32 39.59 1.66 o -8 -1 2 41.04 43.36 1.67 o -7 -1 2 22.12 21.63 1.25 o -6 -1 2 0.76 2.09 1.34 o -5 -1 2 2.03 -0.28 0.28 o -4 -1 2 739.67 748.30 5.87 o -3 -1 2 310.27 334.44 3.48 o -2 -1 2 2022.79 2082.91 7.00 o -1 -1 2 8494.88 8053.30 56.10 o 0 -1 2 1014.75 1080.81 7.28 o 1 -1 2 3007.44 3085.99 24.92 o 2 -1 2 669.63 672.39 3.96 o 3 -1 2 518.06 540.77 4.31 o 4 -1 2 3.95 4.52 0.64 o 5 -1 2 122.92 115.52 2.89 o 6 -1 2 1.91 0.92 1.50 o 7 -1 2 63.34 60.73 1.75 o 8 -1 2 0.35 -0.19 1.68 o -8 0 2 29.83 29.44 1.50 o -7 0 2 7.96 10.50 1.07 o -6 0 2 419.93 402.95 5.55 o -4 0 2 95.54 98.67 2.19 o -3 0 2 56.82 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275.79 4.91 o 3 -3 10 297.66 300.94 5.34 o 4 -3 10 5.06 4.86 1.11 o 5 -3 10 5.17 3.85 1.16 o -6 -2 10 108.27 118.89 3.37 o -5 -2 10 9.08 9.89 1.15 o -4 -2 10 2.99 1.54 1.42 o -3 -2 10 276.50 263.34 4.62 o -2 -2 10 10.14 11.49 0.98 o -1 -2 10 286.91 282.46 3.21 o 0 -2 10 1485.24 1440.53 7.06 o 1 -2 10 0.05 0.38 1.01 o 2 -2 10 112.85 109.16 3.23 o 3 -2 10 188.73 180.09 4.36 o 4 -2 10 18.96 19.90 1.37 o 5 -2 10 5.09 6.53 1.12 o -6 -1 10 20.51 20.88 1.39 o -5 -1 10 14.24 15.23 1.22 o -4 -1 10 0.36 -1.46 1.46 o -3 -1 10 170.36 167.34 3.73 o -2 -1 10 7.09 6.38 0.94 o -1 -1 10 310.01 301.69 3.32 o 0 -1 10 68.68 66.83 1.35 o 1 -1 10 196.06 200.65 6.78 o 2 -1 10 0.77 2.28 1.28 o 3 -1 10 114.70 116.83 3.07 o 4 -1 10 77.75 67.39 2.05 o -7 0 10 24.81 23.98 1.49 o -6 0 10 15.47 16.68 1.22 o -5 0 10 96.29 97.29 2.84 o -4 0 10 32.92 34.43 1.31 o -3 0 10 274.22 267.36 4.62 o -2 0 10 844.45 823.74 7.70 o -1 0 10 688.27 672.42 4.93 o 0 0 10 10.02 9.55 0.68 o 1 0 10 96.99 97.12 1.83 o 2 0 10 189.41 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