#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/77/2237781.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237781_Fobs loop_ _publ_author_name 'Kannan, Piskala Subburaman' 'Yuvaraj, PanneerSelvam' 'Manivannan, Karthikeyan' 'Reddy, Boreddy S. R.' 'SubbiahPandi, A.' _publ_section_title ; Methyl 2-(5-chloro-1-methyl-2-oxo-2,3-dihydro-1H-indol-3-ylidene)acetate ; _journal_coeditor_code BX2438 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o856 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.228 _cell_angle_gamma 90.000 _cell_length_a 8.4709 _cell_length_b 17.1658 _cell_length_c 7.9481 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7431 _[local]_cod_data_source_file bx2438Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' YUVI in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 318.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 615.13 628.75 22.76 o 2 0 0 5755.20 6170.44 100.82 o 3 0 0 935.11 948.99 14.34 o 4 0 0 257.70 246.05 7.17 o 5 0 0 45.90 56.96 1.80 o 6 0 0 209.79 210.25 4.14 o 7 0 0 90.21 95.04 2.39 o 8 0 0 500.23 522.50 9.43 o 9 0 0 80.22 91.50 3.48 o 10 0 0 51.62 51.47 3.96 o 1 1 0 9.55 10.30 0.25 o 2 1 0 779.49 725.92 8.46 o 3 1 0 6.62 6.28 0.29 o 4 1 0 1987.55 2111.49 22.20 o 5 1 0 377.32 376.49 4.32 o 6 1 0 10.76 10.56 0.96 o 7 1 0 11.89 13.56 0.85 o 8 1 0 4.31 4.84 0.64 o 9 1 0 110.48 111.75 2.58 o 10 1 0 0.16 1.32 1.40 o 0 2 0 6334.88 6477.06 243.95 o 1 2 0 2760.36 2817.20 32.14 o 2 2 0 1789.16 1852.71 19.10 o 3 2 0 2458.55 2598.60 28.38 o 4 2 0 858.13 985.20 11.52 o 5 2 0 46.76 44.26 1.06 o 6 2 0 148.27 146.29 2.12 o 7 2 0 331.48 337.22 4.42 o 8 2 0 107.60 113.18 3.14 o 9 2 0 2.55 3.74 0.96 o 10 2 0 0.13 1.24 0.84 o 1 3 0 3353.80 3440.00 44.72 o 2 3 0 4142.23 4294.34 45.61 o 3 3 0 448.85 507.45 5.73 o 4 3 0 438.91 466.75 5.41 o 5 3 0 15.03 17.41 0.55 o 6 3 0 55.41 59.73 1.12 o 7 3 0 273.69 270.42 3.86 o 8 3 0 107.27 106.49 2.34 o 9 3 0 10.88 13.16 1.24 o 10 3 0 6.59 9.13 1.24 o 0 4 0 2349.69 2346.17 60.28 o 1 4 0 499.91 526.88 6.19 o 2 4 0 979.44 1016.34 11.16 o 3 4 0 1529.67 1533.83 18.52 o 4 4 0 508.99 576.67 6.56 o 5 4 0 575.20 663.60 7.90 o 6 4 0 302.79 317.20 3.88 o 7 4 0 373.37 380.48 5.95 o 8 4 0 51.18 48.34 1.91 o 9 4 0 16.70 14.03 1.24 o 10 4 0 29.06 29.88 1.76 o 1 5 0 1168.93 1151.10 13.36 o 2 5 0 527.18 600.50 8.07 o 3 5 0 0.73 0.94 0.25 o 4 5 0 94.58 93.90 1.54 o 5 5 0 70.77 91.42 1.74 o 6 5 0 24.95 27.36 0.72 o 7 5 0 255.26 244.08 5.22 o 8 5 0 41.25 41.91 1.90 o 9 5 0 33.32 31.43 1.75 o 10 5 0 1.26 1.70 0.96 o 0 6 0 2102.31 2050.84 38.50 o 1 6 0 658.40 673.68 8.74 o 2 6 0 39.90 29.00 0.52 o 3 6 0 4862.98 5020.41 58.74 o 4 6 0 0.97 0.53 0.30 o 5 6 0 919.65 911.71 14.06 o 6 6 0 253.50 248.44 4.72 o 7 6 0 191.30 174.06 4.05 o 8 6 0 35.10 24.64 1.52 o 9 6 0 66.80 63.02 2.29 o 10 6 0 0.01 -0.93 0.93 o 1 7 0 4537.62 4889.34 86.29 o 2 7 0 2247.55 2335.21 32.99 o 3 7 0 173.69 184.47 2.65 o 4 7 0 7.75 5.68 0.31 o 5 7 0 79.36 79.33 1.93 o 6 7 0 3.72 1.98 0.76 o 7 7 0 15.44 17.91 1.40 o 8 7 0 1.56 1.98 0.93 o 9 7 0 29.19 30.35 2.33 o 10 7 0 36.23 37.64 3.63 o 0 8 0 70.19 117.16 4.28 o 1 8 0 159.20 196.77 2.73 o 2 8 0 59.56 60.78 1.02 o 3 8 0 272.60 300.81 3.80 o 4 8 0 386.39 370.89 5.27 o 5 8 0 22.62 24.32 0.82 o 6 8 0 30.27 24.43 1.87 o 7 8 0 1.34 0.33 0.99 o 8 8 0 27.68 26.83 1.87 o 9 8 0 23.46 22.35 2.31 o 10 8 0 1.23 1.98 1.40 o 1 9 0 723.60 626.84 8.11 o 2 9 0 2487.86 2589.30 32.60 o 3 9 0 231.40 251.06 3.59 o 4 9 0 1277.10 1222.60 16.31 o 5 9 0 0.06 0.85 0.57 o 6 9 0 290.82 278.25 7.23 o 7 9 0 65.14 58.81 2.53 o 8 9 0 1.18 0.66 0.93 o 9 9 0 19.64 16.99 1.87 o 10 9 0 56.28 57.79 3.01 o 0 10 0 776.44 690.97 13.52 o 1 10 0 20.86 31.62 0.77 o 2 10 0 69.18 67.60 1.28 o 3 10 0 169.30 164.36 2.52 o 4 10 0 33.95 38.51 1.10 o 5 10 0 20.28 19.80 0.90 o 6 10 0 30.55 32.67 3.30 o 7 10 0 2.25 1.65 0.93 o 8 10 0 2.90 0.33 0.93 o 9 10 0 0.49 0.66 1.10 o 1 11 0 1034.74 1108.17 14.20 o 2 11 0 16.76 13.12 0.59 o 3 11 0 36.51 36.03 0.87 o 4 11 0 443.54 415.78 6.91 o 5 11 0 0.04 2.31 0.93 o 6 11 0 95.85 90.59 3.96 o 7 11 0 7.15 7.50 1.40 o 8 11 0 1.09 0.53 1.10 o 9 11 0 44.79 44.60 2.80 o 0 12 0 1113.06 1071.32 18.58 o 1 12 0 234.25 242.67 3.74 o 2 12 0 86.43 84.76 1.74 o 3 12 0 216.14 201.16 3.71 o 4 12 0 277.96 271.82 4.72 o 5 12 0 97.69 91.76 3.27 o 6 12 0 0.93 0.66 1.32 o 7 12 0 5.64 5.28 1.40 o 8 12 0 152.02 150.42 4.88 o 9 12 0 24.65 24.58 2.06 o 1 13 0 362.90 341.70 5.42 o 2 13 0 618.87 631.32 10.38 o 3 13 0 769.96 749.58 11.97 o 4 13 0 979.45 939.89 20.71 o 5 13 0 0.30 1.98 1.32 o 6 13 0 0.19 0.66 1.32 o 7 13 0 131.43 121.11 4.20 o 8 13 0 22.60 24.02 2.06 o 9 13 0 55.31 63.35 4.62 o 0 14 0 36.32 41.31 1.87 o 1 14 0 256.41 232.20 3.74 o 2 14 0 81.71 87.85 2.63 o 3 14 0 5.23 4.78 0.71 o 4 14 0 63.52 62.20 2.53 o 5 14 0 152.94 142.89 4.62 o 6 14 0 20.35 17.13 2.31 o 7 14 0 14.46 12.28 1.98 o 8 14 0 0.75 -0.53 1.10 o 1 15 0 1259.72 1136.21 18.26 o 2 15 0 0.93 0.82 0.66 o 3 15 0 11.65 10.57 0.84 o 4 15 0 3.88 5.36 0.93 o 5 15 0 3.92 5.74 1.10 o 6 15 0 46.64 50.98 2.53 o 7 15 0 47.31 46.85 2.53 o 8 15 0 8.33 6.37 1.40 o 0 16 0 9.98 18.86 1.40 o 1 16 0 4.67 8.22 1.10 o 2 16 0 31.94 33.45 1.51 o 3 16 0 127.79 137.96 6.93 o 4 16 0 2.96 3.71 0.99 o 5 16 0 49.55 52.87 2.53 o 6 16 0 84.84 88.21 3.48 o 7 16 0 43.50 42.62 2.53 o 1 17 0 24.99 22.47 1.24 o 2 17 0 143.90 122.24 3.48 o 3 17 0 12.02 7.92 1.40 o 4 17 0 28.70 29.46 1.87 o 5 17 0 8.51 10.90 1.40 o 6 17 0 1.54 2.64 1.65 o 7 17 0 0.79 1.98 1.40 o 0 18 0 23.04 32.33 2.64 o 1 18 0 30.42 30.72 1.87 o 2 18 0 11.37 9.90 1.98 o 3 18 0 128.68 123.42 4.20 o 4 18 0 19.04 19.43 1.98 o 5 18 0 75.18 75.23 3.27 o 6 18 0 64.81 69.63 3.27 o 1 19 0 120.41 126.51 3.95 o 2 19 0 22.48 19.14 2.64 o 3 19 0 12.91 12.22 1.40 o 4 19 0 15.55 13.86 1.58 o 5 19 0 0.25 1.72 1.10 o 6 19 0 4.32 3.30 1.40 o 0 20 0 11.60 19.14 1.98 o 1 20 0 0.22 1.98 1.32 o 2 20 0 0.05 -1.32 1.32 o 3 20 0 88.06 106.27 3.73 o 4 20 0 32.48 34.72 2.33 o 5 20 0 10.26 13.92 2.31 o 1 21 0 45.24 51.47 3.96 o 2 21 0 3.46 1.98 1.98 o 3 21 0 13.29 18.69 1.98 o 4 21 0 28.56 33.99 2.33 o 1 22 0 4.77 5.94 1.98 o 2 22 0 17.77 17.82 2.64 o 3 22 0 105.09 125.26 4.95 o -11 1 1 6.57 10.07 1.87 o -10 1 1 10.27 12.54 1.87 o -9 1 1 9.56 18.27 3.37 o -8 1 1 162.49 159.20 2.50 o -7 1 1 47.66 42.59 1.53 o -6 1 1 182.35 200.78 2.81 o -5 1 1 228.17 187.46 2.53 o -4 1 1 384.60 378.34 4.67 o -3 1 1 47.84 52.93 0.90 o -2 1 1 86.92 102.50 1.49 o -1 1 1 0.96 4.05 0.29 o 0 1 1 1237.90 1280.35 15.94 o 1 1 1 50.87 60.70 0.69 o 2 1 1 422.70 473.53 5.11 o 3 1 1 661.26 654.25 6.83 o 4 1 1 219.25 272.03 3.01 o 5 1 1 217.00 214.24 2.66 o 6 1 1 400.05 421.89 5.57 o 7 1 1 114.58 131.20 2.62 o 8 1 1 52.00 62.42 1.79 o 9 1 1 56.54 60.12 1.79 o 10 1 1 0.00 -1.32 1.32 o -11 2 1 33.44 35.02 2.80 o -10 2 1 24.36 31.89 2.64 o -9 2 1 1028.05 1072.82 19.70 o -8 2 1 17.06 17.41 1.21 o -7 2 1 326.28 344.55 4.78 o -6 2 1 252.51 265.71 3.52 o -5 2 1 153.44 158.01 2.12 o -4 2 1 1650.30 1628.90 18.79 o -3 2 1 599.02 600.29 7.11 o -2 2 1 4719.31 4766.34 60.43 o -1 2 1 92.47 93.96 1.17 o 0 2 1 2345.68 2336.92 26.63 o 1 2 1 1937.58 2060.87 26.08 o 2 2 1 2953.25 3121.19 33.63 o 3 2 1 481.36 593.62 5.93 o 4 2 1 504.77 540.27 5.65 o 5 2 1 532.84 509.02 5.79 o 6 2 1 31.48 44.65 1.14 o 7 2 1 2389.80 2435.95 33.60 o 8 2 1 6.83 9.54 0.78 o 9 2 1 164.67 170.13 3.52 o 10 2 1 63.76 69.29 3.96 o -11 3 1 0.00 0.00 2.64 o -10 3 1 1.02 1.65 1.40 o -9 3 1 26.85 45.62 2.53 o -8 3 1 1.69 1.98 0.76 o -7 3 1 0.44 1.26 0.43 o -6 3 1 3.89 7.79 0.64 o -5 3 1 718.15 720.17 8.17 o -4 3 1 54.43 59.17 0.97 o -3 3 1 0.57 0.66 0.25 o -2 3 1 2031.65 2027.74 25.61 o -1 3 1 77.64 82.60 1.12 o 0 3 1 4576.65 4796.52 54.21 o 1 3 1 218.06 219.62 4.16 o 2 3 1 152.73 194.90 2.81 o 3 3 1 2543.67 2842.34 29.25 o 4 3 1 260.38 345.99 3.80 o 5 3 1 33.55 31.86 0.74 o 6 3 1 10.41 11.66 0.59 o 7 3 1 208.60 205.84 5.77 o 8 3 1 2.27 3.51 0.66 o 9 3 1 7.20 9.11 1.14 o 10 3 1 3.69 1.98 1.32 o -10 4 1 2.67 5.06 1.14 o -9 4 1 173.15 170.96 4.27 o -8 4 1 1.66 1.32 0.76 o -7 4 1 609.76 612.51 10.93 o -6 4 1 976.33 997.83 14.05 o -5 4 1 561.96 620.72 7.79 o -4 4 1 877.48 886.07 10.44 o -3 4 1 0.36 1.20 0.30 o -2 4 1 147.00 141.78 2.27 o -1 4 1 10.84 18.31 0.37 o 0 4 1 55.83 63.29 1.03 o 1 4 1 142.51 157.62 2.32 o 2 4 1 1607.84 1700.36 21.90 o 3 4 1 179.07 207.90 2.51 o 4 4 1 3084.81 3336.49 33.08 o 5 4 1 1088.95 1124.89 13.84 o 6 4 1 19.70 26.66 0.84 o 7 4 1 337.98 329.36 5.10 o 8 4 1 15.96 18.37 1.21 o 9 4 1 1.35 0.88 0.83 o 10 4 1 93.54 96.35 4.62 o -10 5 1 74.46 71.21 2.52 o -9 5 1 92.83 92.47 2.90 o -8 5 1 144.65 143.28 3.67 o -7 5 1 70.40 61.08 1.54 o -6 5 1 2.11 2.76 0.43 o -5 5 1 202.76 175.29 2.66 o -4 5 1 1.68 1.48 0.26 o -3 5 1 40.35 51.19 0.92 o -2 5 1 2011.87 1946.50 23.97 o -1 5 1 76.49 81.21 1.20 o 0 5 1 2267.15 2329.87 28.29 o 1 5 1 341.91 378.67 4.92 o 2 5 1 2.32 2.61 0.27 o 3 5 1 310.29 307.34 3.91 o 4 5 1 23.78 17.84 0.50 o 5 5 1 220.28 203.13 3.35 o 6 5 1 388.08 389.37 6.00 o 7 5 1 153.67 144.58 2.94 o 8 5 1 365.05 346.60 7.15 o 9 5 1 201.72 221.98 5.20 o 10 5 1 0.03 1.32 1.32 o -10 6 1 6.21 4.62 1.14 o -9 6 1 9.23 7.12 1.28 o -8 6 1 0.02 0.44 0.76 o -7 6 1 13.10 13.99 2.05 o -6 6 1 153.36 140.75 2.38 o -5 6 1 363.92 395.77 5.47 o -4 6 1 81.05 82.49 1.33 o -3 6 1 187.92 188.51 2.46 o -2 6 1 89.83 93.94 1.37 o -1 6 1 1034.54 1086.45 13.69 o 0 6 1 179.12 186.34 2.44 o 1 6 1 523.56 525.22 6.07 o 2 6 1 3.42 3.96 0.40 o 3 6 1 872.20 1025.25 12.55 o 4 6 1 181.07 158.24 2.29 o 5 6 1 19.80 19.32 1.14 o 6 6 1 0.61 -0.65 0.65 o 7 6 1 21.57 19.47 1.40 o 8 6 1 14.19 12.54 1.40 o 9 6 1 13.53 13.57 1.98 o 10 6 1 0.73 0.00 1.98 o -10 7 1 34.65 32.45 2.33 o -9 7 1 34.01 31.43 1.75 o -8 7 1 101.02 95.72 2.90 o -7 7 1 7.63 7.01 0.96 o -6 7 1 6.24 5.63 0.63 o -5 7 1 277.81 254.81 3.58 o -4 7 1 0.47 0.29 0.29 o -3 7 1 219.50 189.29 2.53 o -2 7 1 1691.19 1783.95 22.02 o -1 7 1 180.42 201.07 2.91 o 0 7 1 2525.71 2739.78 34.19 o 1 7 1 196.93 190.85 2.90 o 2 7 1 15.53 7.37 0.52 o 3 7 1 256.41 245.57 3.29 o 4 7 1 0.04 1.40 0.40 o 5 7 1 15.62 15.69 0.78 o 6 7 1 217.28 211.72 4.88 o 7 7 1 37.96 38.74 2.31 o 8 7 1 146.14 130.35 4.20 o 9 7 1 64.60 68.63 2.80 o -10 8 1 15.78 18.86 1.87 o -9 8 1 46.41 44.88 2.33 o -8 8 1 25.92 25.75 1.87 o -7 8 1 75.67 75.02 2.97 o -6 8 1 594.93 547.18 9.88 o -5 8 1 17.19 18.06 0.84 o -4 8 1 444.24 410.43 5.39 o -3 8 1 214.52 220.97 2.92 o -2 8 1 35.14 39.47 0.85 o -1 8 1 3093.52 3566.62 47.45 o 0 8 1 326.16 350.70 4.72 o 1 8 1 150.61 158.20 1.98 o 2 8 1 554.77 547.57 7.35 o 3 8 1 85.39 87.43 1.43 o 4 8 1 1424.08 1375.88 18.80 o 5 8 1 171.81 169.62 4.02 o 6 8 1 36.22 32.51 1.36 o 7 8 1 146.54 144.94 4.42 o 8 8 1 117.26 117.08 5.94 o 9 8 1 0.01 -0.66 0.93 o -10 9 1 82.78 79.50 5.28 o -9 9 1 0.05 -0.66 1.32 o -8 9 1 71.68 74.72 3.30 o -7 9 1 300.94 285.04 7.43 o -6 9 1 99.92 99.66 3.27 o -5 9 1 52.14 52.02 1.44 o -4 9 1 65.17 57.21 1.14 o -3 9 1 375.27 416.25 5.75 o -2 9 1 0.16 0.11 0.27 o -1 9 1 176.85 195.26 2.73 o 0 9 1 3.98 3.05 0.30 o 1 9 1 708.91 853.95 10.10 o 2 9 1 7.54 6.73 0.46 o 3 9 1 11.56 12.67 0.48 o 4 9 1 159.36 140.29 2.73 o 5 9 1 588.14 549.13 9.03 o 6 9 1 60.95 61.45 1.85 o 7 9 1 13.27 14.64 1.40 o 8 9 1 283.51 266.06 10.56 o 9 9 1 7.03 8.92 1.40 o -10 10 1 24.60 27.12 2.33 o -9 10 1 11.20 13.04 1.58 o -8 10 1 1.72 3.30 1.40 o -7 10 1 1.57 3.63 1.40 o -6 10 1 40.22 38.89 2.31 o -5 10 1 570.52 564.27 11.12 o -4 10 1 48.89 48.18 1.04 o -3 10 1 6.54 9.29 0.44 o -2 10 1 211.41 231.15 3.78 o -1 10 1 2520.54 2620.14 32.99 o 0 10 1 89.83 117.84 1.81 o 1 10 1 32.17 39.14 0.68 o 2 10 1 8.94 11.36 0.39 o 3 10 1 1632.11 1647.41 25.31 o 4 10 1 9.57 9.14 0.52 o 5 10 1 31.16 30.77 1.50 o 6 10 1 10.68 7.32 1.65 o 7 10 1 41.74 46.23 2.33 o 8 10 1 30.56 33.67 2.33 o 9 10 1 0.66 0.26 1.10 o -9 11 1 10.96 11.56 1.87 o -8 11 1 118.84 118.47 4.20 o -7 11 1 690.34 628.59 16.52 o -6 11 1 1425.40 1322.57 28.84 o -5 11 1 732.16 721.02 14.13 o -4 11 1 8.63 10.44 0.71 o -3 11 1 237.90 238.97 3.59 o -2 11 1 58.68 63.97 1.44 o -1 11 1 20.20 23.99 0.76 o 0 11 1 51.79 61.36 1.31 o 1 11 1 166.78 134.24 1.96 o 2 11 1 422.66 426.05 5.47 o 3 11 1 1185.11 1141.07 17.80 o 4 11 1 1389.43 1292.89 20.07 o 5 11 1 2017.51 1880.92 31.65 o 6 11 1 225.95 218.82 9.24 o 7 11 1 7.98 9.51 2.31 o 8 11 1 55.22 57.17 2.80 o 9 11 1 24.82 26.39 3.30 o -9 12 1 13.33 10.90 1.87 o -8 12 1 6.60 7.69 1.98 o -7 12 1 0.09 1.32 0.93 o -6 12 1 7.63 10.90 1.40 o -5 12 1 27.57 26.10 1.87 o -4 12 1 224.87 208.88 4.79 o -3 12 1 95.23 79.46 1.59 o -2 12 1 9.54 8.80 0.59 o -1 12 1 84.03 110.70 1.88 o 0 12 1 10.26 11.33 0.57 o 1 12 1 203.64 181.64 2.59 o 2 12 1 331.30 307.11 5.95 o 3 12 1 5.01 3.70 0.57 o 4 12 1 76.59 74.06 1.92 o 5 12 1 24.91 26.22 1.44 o 6 12 1 18.33 19.34 1.58 o 7 12 1 46.85 35.83 2.64 o 8 12 1 8.58 10.72 1.40 o -9 13 1 6.22 7.26 1.58 o -8 13 1 5.86 6.66 1.40 o -7 13 1 22.30 16.88 1.58 o -6 13 1 220.96 196.07 5.60 o -5 13 1 0.12 0.99 0.93 o -4 13 1 29.56 26.89 1.52 o -3 13 1 767.46 767.40 11.25 o -2 13 1 18.22 19.67 0.79 o -1 13 1 3.09 5.57 0.79 o 0 13 1 1.25 1.54 0.34 o 1 13 1 1313.16 1384.20 20.13 o 2 13 1 0.43 0.82 0.58 o 3 13 1 2.90 3.26 0.76 o 4 13 1 411.82 382.70 7.16 o 5 13 1 39.05 35.97 1.87 o 6 13 1 6.71 6.96 1.98 o 7 13 1 2.61 1.58 1.10 o 8 13 1 32.62 35.99 2.33 o -8 14 1 1.31 0.33 1.40 o -7 14 1 43.53 49.15 2.64 o -6 14 1 20.88 20.54 1.87 o -5 14 1 91.75 102.29 3.73 o -4 14 1 65.48 59.92 2.53 o -3 14 1 480.27 472.78 13.65 o -2 14 1 103.61 100.11 2.09 o -1 14 1 117.13 119.69 2.58 o 0 14 1 47.93 42.14 0.99 o 1 14 1 446.16 454.19 8.67 o 2 14 1 144.76 122.27 3.08 o 3 14 1 190.62 188.73 3.88 o 4 14 1 19.86 23.09 1.24 o 5 14 1 185.16 184.25 5.13 o 6 14 1 0.61 1.98 0.93 o 7 14 1 46.72 38.03 3.96 o 8 14 1 50.68 56.16 2.80 o -8 15 1 50.19 50.29 2.80 o -7 15 1 55.05 55.28 5.28 o -6 15 1 37.33 36.96 2.33 o -5 15 1 184.22 176.58 5.13 o 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