#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181299 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/77/2237784.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237784_Fobs loop_ _publ_author_name 'Yotnoi, Bunlawee' 'Rujiwatra, Apinpus' _publ_section_title ; catena-Poly[[bis(pyridine-\kN)zinc]-\m-5-carboxybenzene-1,3-dicarboxylato-\k^2^O^1^:O^3^] ; _journal_coeditor_code CQ2004 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m345 _journal_volume 69 _journal_year 2013 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.4850 _cell_length_b 15.7677 _cell_length_c 16.7252 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.7500 _cod_data_source_file cq2004Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S554005_02_0m in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 320.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3965.34 3917.29 72.05 o 4 0 0 17257.12 15755.44 270.18 o 6 0 0 28851.58 30023.11 722.71 o 8 0 0 14194.19 13916.02 351.53 o 10 0 0 3531.75 3371.20 110.26 o 12 0 0 24.92 6.55 28.38 o 14 0 0 6086.38 6355.93 195.42 o 16 0 0 6.09 14.19 42.58 o 2 1 0 81349.34 80243.55 1184.20 o 4 1 0 2071.68 1799.30 31.30 o 6 1 0 13326.60 13034.14 186.78 o 8 1 0 722.43 1073.35 35.89 o 10 1 0 11288.65 10919.59 203.02 o 12 1 0 3429.02 3232.74 79.89 o 14 1 0 23.49 37.43 25.65 o 16 1 0 1843.60 1881.61 70.63 o 0 2 0 62.94 74.24 5.46 o 2 2 0 12712.01 13090.06 128.36 o 4 2 0 12889.55 12808.20 207.34 o 6 2 0 21.61 35.51 8.78 o 8 2 0 2763.44 2910.86 54.20 o 10 2 0 1329.79 1246.95 42.46 o 12 2 0 146.87 154.02 23.93 o 14 2 0 305.08 290.32 32.39 o 16 2 0 4.04 -28.17 28.17 o 2 3 0 45706.02 47710.92 504.83 o 4 3 0 426.58 474.30 14.70 o 6 3 0 198.33 294.53 14.50 o 8 3 0 7.41 2.62 10.84 o 10 3 0 2109.77 2086.36 47.26 o 12 3 0 563.49 470.87 33.17 o 14 3 0 284.12 215.59 31.26 o 16 3 0 13.65 -3.08 29.35 o 0 4 0 286.93 453.91 19.65 o 2 4 0 1929.66 2068.85 25.77 o 4 4 0 31109.62 30795.83 425.03 o 6 4 0 7597.05 7530.85 112.82 o 8 4 0 860.51 733.44 36.49 o 10 4 0 13179.21 13304.42 198.33 o 12 4 0 498.70 490.28 43.12 o 14 4 0 512.40 564.02 40.05 o 16 4 0 107.42 139.87 34.29 o 2 5 0 11475.17 11618.51 126.55 o 4 5 0 10366.19 11413.06 162.83 o 6 5 0 13653.99 12917.36 185.94 o 8 5 0 8750.61 8635.08 131.52 o 10 5 0 11856.35 11469.60 173.96 o 12 5 0 4251.65 4022.65 84.21 o 14 5 0 929.32 924.56 49.39 o 16 5 0 6178.51 6481.78 147.44 o 0 6 0 6556.81 6041.06 100.46 o 2 6 0 794.80 796.75 15.82 o 4 6 0 21181.81 21098.52 294.77 o 6 6 0 6806.02 6657.50 101.89 o 8 6 0 3217.77 3011.91 56.29 o 10 6 0 237.95 249.76 23.22 o 12 6 0 1457.03 1279.92 41.16 o 14 6 0 1812.55 1888.66 66.33 o 16 6 0 430.90 554.24 46.66 o 2 7 0 33830.86 34819.52 479.45 o 4 7 0 681.78 715.94 20.78 o 6 7 0 7974.19 7664.36 115.96 o 8 7 0 5192.96 5214.56 86.32 o 10 7 0 1967.23 1823.87 44.91 o 12 7 0 363.12 332.52 34.85 o 14 7 0 153.59 111.40 28.88 o 16 7 0 288.90 247.62 38.84 o 0 8 0 590.09 640.29 36.03 o 2 8 0 1494.02 1836.35 34.02 o 4 8 0 10690.93 12125.63 174.38 o 6 8 0 2319.05 2295.86 62.01 o 8 8 0 302.41 307.10 19.28 o 10 8 0 1361.33 1361.06 40.25 o 12 8 0 195.18 164.55 22.53 o 14 8 0 208.71 220.98 27.66 o 16 8 0 0.09 -12.01 48.04 o 2 9 0 4837.59 5053.56 77.72 o 4 9 0 97.91 92.59 13.07 o 6 9 0 2391.48 2303.32 50.99 o 8 9 0 2485.70 2444.58 50.40 o 10 9 0 6912.17 6956.07 114.91 o 12 9 0 2062.84 2247.22 58.30 o 14 9 0 340.18 348.21 39.71 o 16 9 0 426.90 342.80 60.04 o 0 10 0 7532.92 7283.72 132.77 o 2 10 0 1759.60 1732.73 34.65 o 4 10 0 9579.31 9464.84 140.13 o 6 10 0 3371.06 3331.70 60.17 o 8 10 0 9309.25 9020.94 183.95 o 10 10 0 1931.94 1948.83 69.51 o 12 10 0 2272.43 2341.30 85.27 o 14 10 0 686.07 715.46 61.14 o 2 11 0 5360.74 5013.02 79.40 o 4 11 0 4363.82 4509.30 74.14 o 6 11 0 6874.72 6988.39 110.07 o 8 11 0 673.48 670.79 33.05 o 10 11 0 2614.30 2654.50 58.77 o 12 11 0 4119.62 4403.34 107.69 o 14 11 0 813.76 772.93 73.14 o 0 12 0 2695.51 2621.14 93.34 o 2 12 0 1815.68 1951.19 52.68 o 4 12 0 1290.00 1301.50 32.96 o 6 12 0 157.19 155.28 16.99 o 8 12 0 4801.43 4792.77 105.46 o 10 12 0 1836.77 1670.22 62.77 o 12 12 0 1129.41 1205.25 80.79 o 14 12 0 1679.82 1912.68 100.44 o 2 13 0 94.32 97.61 14.42 o 4 13 0 1.05 -3.23 15.17 o 6 13 0 728.78 613.51 26.20 o 8 13 0 4.08 -21.61 21.61 o 10 13 0 275.58 227.08 45.85 o 12 13 0 74.19 117.90 43.67 o 14 13 0 326.34 234.72 57.86 o 0 14 0 2771.05 2861.37 66.37 o 2 14 0 9.24 -11.65 11.65 o 4 14 0 27.62 46.50 18.81 o 6 14 0 815.93 747.82 53.49 o 8 14 0 382.33 279.48 43.67 o 10 14 0 613.81 517.47 55.68 o 12 14 0 219.16 352.62 56.77 o 2 15 0 1054.07 1080.25 40.94 o 4 15 0 43.53 41.48 30.57 o 6 15 0 4828.35 4985.84 156.11 o 8 15 0 765.61 713.98 58.95 o 10 15 0 378.69 360.26 54.59 o 12 15 0 185.77 151.75 46.94 o 0 16 0 426.62 409.39 41.48 o 2 16 0 131.50 84.69 22.35 o 4 16 0 7819.58 7867.95 219.43 o 6 16 0 395.20 474.89 49.13 o 8 16 0 1077.86 1010.92 68.78 o 10 16 0 1723.20 1699.79 90.61 o 2 17 0 1148.26 1088.67 57.31 o 4 17 0 799.33 788.66 39.71 o 6 17 0 1902.03 2146.30 92.80 o 8 17 0 943.64 882.10 67.69 o 10 17 0 714.36 795.86 72.05 o 0 18 0 201.30 239.08 40.39 o 2 18 0 31.55 11.90 22.76 o 4 18 0 180.85 217.98 29.53 o 6 18 0 149.47 171.40 42.58 o 8 18 0 177.56 199.78 49.13 o 2 19 0 64.39 85.15 26.25 o 4 19 0 6.13 12.79 25.33 o 6 19 0 23.28 -34.93 37.12 o 0 20 0 1384.46 1519.66 79.69 o 2 20 0 41.38 -0.81 26.56 o 4 20 0 1369.88 1425.94 67.14 o 1 1 1 3387.26 3505.37 77.56 o 2 1 1 202.83 237.89 5.06 o 3 1 1 5603.08 6044.76 50.26 o 4 1 1 2201.50 2217.69 24.11 o 5 1 1 1828.60 1872.89 26.36 o 6 1 1 1290.08 1200.29 20.99 o 7 1 1 19401.96 20410.90 223.71 o 8 1 1 1816.63 1734.77 29.38 o 9 1 1 2801.09 2855.83 46.28 o 10 1 1 2591.90 2451.68 49.79 o 11 1 1 1499.54 1504.91 35.85 o 12 1 1 2340.19 2297.97 51.98 o 13 1 1 620.82 496.42 24.96 o 14 1 1 29.78 62.77 19.19 o 15 1 1 960.98 949.95 36.87 o 16 1 1 227.78 260.70 25.06 o 17 1 1 35.51 41.96 23.40 o 0 2 1 21408.44 20811.43 634.28 o 1 2 1 9901.08 9518.22 217.74 o 2 2 1 13.13 17.53 2.31 o 3 2 1 12734.13 12481.61 106.72 o 4 2 1 8403.88 8123.52 82.75 o 5 2 1 4699.94 4354.80 47.83 o 6 2 1 839.94 859.43 16.10 o 7 2 1 13.49 0.25 6.67 o 8 2 1 13199.05 13376.11 151.25 o 9 2 1 13270.80 13407.80 152.91 o 10 2 1 3378.34 3320.10 49.30 o 11 2 1 292.30 267.34 27.58 o 12 2 1 506.38 451.50 23.17 o 13 2 1 3233.04 3172.29 58.39 o 14 2 1 1526.26 1503.46 40.76 o 15 2 1 458.41 412.66 27.48 o 16 2 1 108.49 113.49 23.52 o 17 2 1 1376.56 1539.74 83.83 o 1 3 1 4254.89 4210.14 31.50 o 2 3 1 60533.90 63135.23 471.41 o 3 3 1 3796.87 3469.36 32.23 o 4 3 1 261.85 227.90 12.86 o 5 3 1 2735.94 2512.63 30.38 o 6 3 1 12705.39 12564.24 127.91 o 7 3 1 11828.71 11540.96 119.29 o 8 3 1 3396.02 3154.67 40.63 o 9 3 1 322.38 349.59 14.09 o 10 3 1 1441.80 1465.26 30.25 o 11 3 1 7103.00 6995.57 89.24 o 12 3 1 943.42 895.21 38.45 o 13 3 1 28.99 22.43 17.26 o 14 3 1 670.80 622.90 29.05 o 15 3 1 1304.79 1428.30 42.35 o 16 3 1 1393.37 1439.39 46.80 o 17 3 1 441.51 517.37 33.13 o 0 4 1 2959.67 2762.25 35.73 o 1 4 1 767.59 758.68 8.15 o 2 4 1 4642.74 4739.45 39.90 o 3 4 1 719.69 664.88 9.68 o 4 4 1 20158.72 20284.40 199.74 o 5 4 1 13217.86 13883.15 139.50 o 6 4 1 684.73 650.30 14.60 o 7 4 1 8.18 0.92 6.88 o 8 4 1 1692.28 1561.68 25.53 o 9 4 1 9935.57 9828.86 106.00 o 10 4 1 301.55 299.59 17.16 o 11 4 1 1256.35 1215.98 28.74 o 12 4 1 2007.19 2020.98 44.06 o 13 4 1 1543.33 1482.39 47.59 o 14 4 1 1999.29 1970.66 47.06 o 15 4 1 46.29 99.22 21.50 o 16 4 1 87.50 61.03 22.44 o 17 4 1 297.36 311.23 30.12 o 1 5 1 3704.45 3729.45 30.41 o 2 5 1 3188.79 3338.57 31.11 o 3 5 1 70.74 65.81 4.47 o 4 5 1 1003.09 1016.91 16.07 o 5 5 1 349.44 376.74 10.74 o 6 5 1 42.66 49.92 7.65 o 7 5 1 614.55 640.23 17.08 o 8 5 1 52.20 39.03 11.31 o 9 5 1 21.39 8.67 9.47 o 10 5 1 875.91 826.90 28.47 o 11 5 1 1545.94 1527.63 29.74 o 12 5 1 567.20 535.08 22.79 o 13 5 1 496.87 448.79 23.39 o 14 5 1 3.39 14.51 18.21 o 15 5 1 469.65 488.67 29.28 o 16 5 1 74.90 114.90 24.11 o 17 5 1 38.34 6.99 23.30 o 0 6 1 1064.08 1074.56 17.72 o 1 6 1 3798.74 3685.33 34.15 o 2 6 1 6.55 7.42 3.67 o 3 6 1 18080.68 19987.03 170.26 o 4 6 1 240.16 187.56 10.87 o 5 6 1 6436.33 6860.11 72.79 o 6 6 1 793.35 932.02 18.09 o 7 6 1 1104.50 1099.87 23.60 o 8 6 1 79.04 71.86 9.54 o 9 6 1 3250.78 3259.76 64.68 o 10 6 1 53.80 58.55 11.88 o 11 6 1 283.66 290.07 16.15 o 12 6 1 1362.33 1297.57 29.21 o 13 6 1 30.40 -0.40 15.26 o 14 6 1 11.58 0.43 16.96 o 15 6 1 181.21 176.48 23.68 o 16 6 1 15.90 16.53 22.54 o 17 6 1 271.92 295.61 56.92 o 1 7 1 11667.42 12161.33 104.93 o 2 7 1 9312.13 9625.28 84.23 o 3 7 1 6705.32 6395.37 62.24 o 4 7 1 3116.51 3160.86 37.20 o 5 7 1 580.87 550.42 13.64 o 6 7 1 1202.86 1059.12 19.71 o 7 7 1 7999.42 7900.08 85.42 o 8 7 1 2499.08 2494.16 35.32 o 9 7 1 751.98 828.39 29.18 o 10 7 1 2402.72 2418.83 44.43 o 11 7 1 102.96 115.48 13.91 o 12 7 1 430.38 427.28 19.86 o 13 7 1 251.83 265.20 19.87 o 14 7 1 93.58 67.06 18.40 o 15 7 1 1143.45 1201.30 40.83 o 16 7 1 697.71 841.09 43.87 o 0 8 1 3273.60 3025.32 37.77 o 1 8 1 3838.10 3698.75 35.45 o 2 8 1 2906.41 3314.06 36.26 o 3 8 1 685.94 601.99 13.46 o 4 8 1 3643.40 3565.98 41.58 o 5 8 1 9057.63 8714.24 91.43 o 6 8 1 1286.56 1235.91 21.78 o 7 8 1 83.07 77.61 9.34 o 8 8 1 3658.74 3643.06 46.63 o 9 8 1 2561.43 2451.88 36.65 o 10 8 1 2114.84 2175.43 35.23 o 11 8 1 599.77 575.62 21.12 o 12 8 1 1548.81 1585.47 32.83 o 13 8 1 1619.15 1626.72 35.11 o 14 8 1 1343.82 1445.74 38.24 o 15 8 1 115.27 90.03 28.68 o 16 8 1 178.60 211.83 32.06 o 1 9 1 745.92 669.73 16.61 o 2 9 1 674.07 505.60 14.08 o 3 9 1 6131.12 5881.49 63.56 o 4 9 1 1442.34 1382.01 21.71 o 5 9 1 4405.87 4758.06 54.28 o 6 9 1 5902.85 5907.85 66.17 o 7 9 1 4447.94 4534.71 54.42 o 8 9 1 1620.42 1612.89 28.25 o 9 9 1 132.23 157.60 13.02 o 10 9 1 328.10 335.80 17.25 o 11 9 1 6986.48 6983.46 106.55 o 12 9 1 501.88 469.43 20.88 o 13 9 1 206.78 197.08 20.45 o 14 9 1 566.93 535.68 35.61 o 15 9 1 1579.21 1540.13 66.45 o 16 9 1 114.99 101.01 39.85 o 0 10 1 1932.34 2074.53 33.38 o 1 10 1 381.15 376.34 11.27 o 2 10 1 1117.26 1164.60 19.41 o 3 10 1 22.44 31.29 7.27 o 4 10 1 897.87 819.67 17.68 o 5 10 1 1607.29 1623.38 29.78 o 6 10 1 2.09 -7.31 8.79 o 7 10 1 502.61 473.49 16.19 o 8 10 1 382.40 383.18 15.94 o 9 10 1 671.60 643.77 24.49 o 10 10 1 756.77 752.01 22.91 o 11 10 1 776.99 725.77 23.76 o 12 10 1 526.12 493.57 24.30 o 13 10 1 517.30 483.47 29.57 o 14 10 1 46.50 42.19 21.46 o 15 10 1 156.95 188.84 32.49 o 1 11 1 2938.75 3004.70 31.96 o 2 11 1 114.84 99.19 8.57 o 3 11 1 48.33 64.75 8.98 o 4 11 1 154.90 168.21 10.39 o 5 11 1 159.47 173.67 11.16 o 6 11 1 119.94 106.00 16.70 o 7 11 1 59.44 62.96 11.50 o 8 11 1 850.95 807.35 25.63 o 9 11 1 57.14 67.41 13.04 o 10 11 1 111.06 108.70 16.28 o 11 11 1 219.46 221.54 19.18 o 12 11 1 2.14 15.41 16.84 o 13 11 1 44.33 49.67 25.80 o 14 11 1 14.50 22.17 29.00 o 15 11 1 61.13 45.18 36.26 o 0 12 1 5273.41 5440.93 74.34 o 1 12 1 1642.87 1665.88 22.69 o 2 12 1 51.95 52.17 9.47 o 3 12 1 281.90 282.83 11.93 o 4 12 1 1470.37 1482.77 26.28 o 5 12 1 816.87 857.27 20.20 o 6 12 1 3.41 -2.86 9.81 o 7 12 1 1072.72 1005.42 22.89 o 8 12 1 1550.32 1598.93 32.98 o 9 12 1 445.52 432.26 20.78 o 10 12 1 314.54 364.67 20.87 o 11 12 1 110.50 109.89 24.79 o 12 12 1 115.51 124.25 25.57 o 13 12 1 43.63 25.50 34.39 o 14 12 1 409.48 341.22 44.21 o 1 13 1 4284.12 4286.89 43.88 o 2 13 1 6733.58 6663.67 67.95 o 3 13 1 4856.81 4744.02 63.14 o 4 13 1 713.89 751.55 18.98 o 5 13 1 343.77 388.51 16.86 o 6 13 1 1341.49 1271.95 28.00 o 7 13 1 740.49 835.24 24.26 o 8 13 1 152.90 171.57 18.64 o 9 13 1 489.12 487.43 29.17 o 10 13 1 862.58 776.05 36.12 o 11 13 1 1128.64 1247.01 70.42 o 12 13 1 915.64 867.98 50.95 o 13 13 1 424.78 448.96 43.61 o 14 13 1 44.61 42.31 35.07 o 0 14 1 2687.81 2476.47 67.31 o 1 14 1 15168.00 15228.43 156.36 o 2 14 1 236.53 203.12 14.48 o 3 14 1 296.68 295.16 26.47 o 4 14 1 830.62 799.49 25.23 o 5 14 1 3994.83 3989.05 62.47 o 6 14 1 1283.81 1242.37 37.58 o 7 14 1 42.39 36.52 18.44 o 8 14 1 1680.63 1701.16 109.72 o 9 14 1 569.28 616.00 39.37 o 10 14 1 449.97 485.25 38.98 o 11 14 1 131.95 160.96 32.75 o 12 14 1 110.22 124.62 34.19 o 13 14 1 942.14 932.11 55.56 o 1 15 1 23.05 25.64 17.96 o 2 15 1 220.09 241.00 17.01 o 3 15 1 1270.54 1299.64 53.13 o 4 15 1 120.27 104.72 46.40 o 5 15 1 320.51 290.13 28.11 o 6 15 1 255.79 279.48 29.30 o 7 15 1 55.73 38.48 25.08 o 8 15 1 451.39 407.34 39.30 o 9 15 1 68.20 43.73 35.48 o 10 15 1 207.22 156.24 31.65 o 11 15 1 387.01 375.05 47.49 o 12 15 1 192.93 199.15 36.26 o 0 16 1 57.10 42.37 22.93 o 1 16 1 245.97 229.78 17.56 o 2 16 1 11.42 23.47 14.29 o 3 16 1 108.80 94.38 16.03 o 4 16 1 5.19 0.17 21.91 o 5 16 1 23.63 12.43 22.68 o 6 16 1 147.65 144.62 27.40 o 7 16 1 174.13 139.74 28.94 o 8 16 1 33.50 80.06 28.94 o 9 16 1 4.21 7.81 28.17 o 10 16 1 0.64 -28.53 28.53 o 11 16 1 8.35 1.77 31.26 o 1 17 1 68.77 56.55 15.90 o 2 17 1 915.08 876.62 28.76 o 3 17 1 9.48 21.52 15.63 o 4 17 1 7.48 -12.86 16.01 o 5 17 1 205.17 203.79 28.53 o 6 17 1 243.74 223.47 30.48 o 7 17 1 61.56 74.05 27.76 o 8 17 1 146.11 119.12 30.43 o 9 17 1 44.72 22.55 28.94 o 10 17 1 3.58 -12.55 30.11 o 0 18 1 579.69 531.90 34.29 o 1 18 1 692.54 706.04 31.20 o 2 18 1 117.50 91.31 17.67 o 3 18 1 1110.40 1085.97 32.41 o 4 18 1 2604.05 2454.84 48.74 o 5 18 1 1124.15 1146.38 46.34 o 6 18 1 2.97 17.18 27.33 o 7 18 1 9.25 -0.60 27.33 o 8 18 1 33.74 15.30 29.71 o 9 18 1 449.99 443.79 41.69 o 1 19 1 428.23 393.47 23.98 o 2 19 1 1187.82 1120.34 33.88 o 3 19 1 476.80 450.39 28.52 o 4 19 1 0.98 -9.16 17.55 o 5 19 1 442.10 435.60 25.01 o 6 19 1 825.64 747.45 44.34 o 7 19 1 515.43 521.96 46.40 o 0 20 1 501.66 475.54 37.39 o 1 20 1 151.50 159.87 25.19 o 2 20 1 1.09 19.06 18.61 o 3 20 1 67.82 71.25 19.59 o 4 20 1 1075.37 1089.33 35.19 o 5 20 1 258.52 262.97 22.86 o 1 0 2 41340.58 42441.27 580.50 o 2 0 2 12494.48 13041.42 127.84 o 3 0 2 4392.21 4233.71 54.45 o 4 0 2 69.70 25.66 8.10 o 5 0 2 790.54 539.07 17.44 o 6 0 2 3990.57 4349.42 69.12 o 7 0 2 17159.89 18589.80 264.30 o 8 0 2 2440.32 3047.35 81.99 o 9 0 2 13292.46 12614.18 186.99 o 10 0 2 656.82 626.34 31.62 o 11 0 2 294.45 276.01 25.44 o 12 0 2 71.43 73.91 21.99 o 13 0 2 1799.87 1996.52 68.23 o 14 0 2 33.21 42.10 24.67 o 15 0 2 1494.20 1482.37 58.67 o 16 0 2 6.75 1.95 34.93 o 17 0 2 1318.81 1237.07 63.30 o 1 1 2 29177.06 30379.77 551.15 o 2 1 2 910.39 881.84 8.16 o 3 1 2 33695.49 34202.79 287.07 o 4 1 2 58.21 49.41 4.52 o 5 1 2 345.74 323.24 9.27 o 6 1 2 3156.06 3641.48 42.41 o 7 1 2 6155.72 5606.75 62.25 o 8 1 2 0.59 -5.10 8.30 o 9 1 2 317.11 343.47 17.21 o 10 1 2 916.51 954.85 25.11 o 11 1 2 4907.21 4700.30 72.32 o 12 1 2 1.45 17.58 14.81 o 13 1 2 1006.73 957.85 32.69 o 14 1 2 389.59 340.87 34.43 o 15 1 2 1603.22 1681.52 44.89 o 16 1 2 41.11 35.02 21.38 o 17 1 2 241.19 256.61 33.42 o 0 2 2 7352.52 7293.60 257.64 o 1 2 2 5227.85 5624.75 41.28 o 2 2 2 13001.49 13390.12 107.27 o 3 2 2 573.24 537.91 8.29 o 4 2 2 492.61 555.14 10.99 o 5 2 2 3345.95 3323.39 41.98 o 6 2 2 5110.26 5559.60 66.40 o 7 2 2 174.06 264.80 11.77 o 8 2 2 41.49 56.41 9.62 o 9 2 2 543.62 450.84 17.25 o 10 2 2 86.06 81.69 12.30 o 11 2 2 23.25 22.49 12.48 o 12 2 2 48.26 47.00 15.42 o 13 2 2 1964.61 1919.20 44.03 o 14 2 2 43.46 45.27 18.21 o 15 2 2 136.32 100.56 20.99 o 16 2 2 14.87 6.61 21.15 o 17 2 2 212.42 197.50 26.23 o 1 3 2 25354.78 26700.70 200.19 o 2 3 2 3483.68 3493.94 31.73 o 3 3 2 2.88 7.78 5.52 o 4 3 2 76.41 78.15 5.44 o 5 3 2 124.21 158.77 7.62 o 6 3 2 3015.81 3259.31 38.91 o 7 3 2 6860.64 6786.84 73.91 o 8 3 2 45.49 29.60 9.32 o 9 3 2 6.07 -5.05 9.29 o 10 3 2 45.28 32.59 11.77 o 11 3 2 2001.69 2080.80 37.87 o 12 3 2 130.94 143.25 15.98 o 13 3 2 258.50 218.29 20.60 o 14 3 2 269.91 252.08 22.92 o 15 3 2 286.26 286.26 26.70 o 16 3 2 1.74 10.72 21.23 o 17 3 2 89.00 94.29 24.50 o 0 4 2 48363.88 50390.27 686.39 o 1 4 2 6502.81 6178.04 63.90 o 2 4 2 13590.78 14655.10 124.52 o 3 4 2 6632.02 6574.09 58.27 o 4 4 2 26.37 37.43 5.58 o 5 4 2 16900.94 16790.88 167.50 o 6 4 2 346.28 366.24 14.89 o 7 4 2 247.93 204.14 10.21 o 8 4 2 372.37 409.41 16.68 o 9 4 2 9309.86 9457.73 112.19 o 10 4 2 0.14 5.50 10.98 o 11 4 2 426.70 403.31 18.99 o 12 4 2 137.93 126.11 16.13 o 13 4 2 2796.26 2794.01 49.29 o 14 4 2 73.84 115.32 20.56 o 15 4 2 72.86 77.92 21.50 o 16 4 2 0.82 12.87 21.19 o 17 4 2 1268.84 1365.13 46.62 o 1 5 2 24516.03 25171.56 211.70 o 2 5 2 2047.64 2257.75 22.44 o 3 5 2 34842.79 35314.48 297.20 o 4 5 2 633.36 577.54 11.31 o 5 5 2 7322.31 7404.80 77.84 o 6 5 2 324.99 317.15 16.03 o 7 5 2 19876.67 19542.69 196.62 o 8 5 2 2.21 4.17 7.79 o 9 5 2 859.95 786.08 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3 1879.99 1848.27 20.36 o 4 3 3 8168.57 8336.19 78.75 o 5 3 3 20573.91 21747.01 235.52 o 6 3 3 8234.37 8063.52 93.15 o 7 3 3 1186.25 1012.57 25.71 o 8 3 3 10640.02 10907.98 125.76 o 9 3 3 189.56 206.71 13.42 o 10 3 3 6771.07 6700.62 84.65 o 11 3 3 3536.86 3549.65 76.25 o 12 3 3 2525.35 2474.48 43.69 o 13 3 3 0.57 -3.63 15.04 o 14 3 3 1425.80 1440.36 40.23 o 15 3 3 1280.86 1273.70 52.63 o 16 3 3 1338.57 1489.51 94.07 o 17 3 3 488.58 502.18 36.08 o 0 4 3 8936.67 9869.83 168.61 o 1 4 3 866.35 748.11 17.62 o 2 4 3 1840.65 1866.49 18.58 o 3 4 3 6133.16 6284.27 55.90 o 4 4 3 2887.91 2588.07 33.22 o 5 4 3 3302.71 3150.57 37.11 o 6 4 3 895.99 936.31 17.58 o 7 4 3 1.49 -7.38 7.38 o 8 4 3 2801.03 2704.02 40.52 o 9 4 3 114.92 114.30 12.15 o 10 4 3 3420.68 3451.55 50.96 o 11 4 3 403.10 408.94 19.52 o 12 4 3 2989.65 3026.03 49.43 o 13 4 3 1684.79 1657.10 36.97 o 14 4 3 1836.00 1814.98 40.66 o 15 4 3 15.10 -2.67 20.14 o 16 4 3 303.94 356.76 30.25 o 17 4 3 328.98 325.18 48.34 o 1 5 3 13098.47 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9 1319.17 1299.01 49.18 o 2 6 9 23.58 29.19 6.06 o 3 6 9 13.58 24.02 7.49 o 4 6 9 251.62 256.52 13.24 o 5 6 9 1723.86 1629.83 34.59 o 6 6 9 572.58 553.53 16.73 o 7 6 9 105.43 110.01 14.98 o 8 6 9 181.66 187.35 16.71 o 9 6 9 411.02 387.08 22.30 o 10 6 9 320.13 301.87 21.39 o 11 6 9 11.51 -17.00 17.00 o 12 6 9 284.03 282.88 23.95 o 13 6 9 758.15 805.25 34.26 o 14 6 9 0.25 21.88 21.96 o 15 6 9 7.18 10.58 22.75 o 1 7 9 431.96 463.47 38.74 o 2 7 9 2600.26 2520.86 39.51 o 3 7 9 9516.30 9186.10 94.84 o 4 7 9 379.79 341.85 22.15 o 5 7 9 214.84 200.61 14.45 o 6 7 9 1603.47 1616.69 44.59 o 7 7 9 6637.90 6639.99 93.62 o 8 7 9 1288.11 1194.59 31.82 o 9 7 9 360.53 354.29 21.34 o 10 7 9 120.00 117.65 18.96 o 11 7 9 4255.97 4270.39 72.41 o 12 7 9 124.60 153.45 25.86 o 13 7 9 34.45 46.88 22.13 o 14 7 9 171.27 172.28 26.14 o 15 7 9 1350.05 1542.34 48.52 o 0 8 9 3634.73 3469.96 78.35 o 1 8 9 5489.13 5521.30 90.97 o 2 8 9 184.37 202.06 12.61 o 3 8 9 1008.62 1051.84 34.77 o 4 8 9 1130.34 1107.91 31.75 o 5 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12 506.74 499.62 23.73 o 3 9 12 1758.11 1729.31 45.36 o 4 9 12 690.98 587.70 36.87 o 5 9 12 1669.51 1601.25 34.68 o 6 9 12 1194.59 1114.43 35.83 o 7 9 12 3.41 -14.55 14.55 o 8 9 12 2.58 11.53 15.96 o 9 9 12 194.69 208.98 28.21 o 10 9 12 185.69 150.77 21.32 o 11 9 12 19.26 29.09 20.82 o 12 9 12 94.72 68.13 22.55 o 13 9 12 14.07 13.58 30.88 o 0 10 12 1370.77 1452.61 52.00 o 1 10 12 181.92 162.21 23.48 o 2 10 12 850.99 793.84 43.54 o 3 10 12 2891.50 2866.70 62.17 o 4 10 12 3813.49 3753.35 58.95 o 5 10 12 1426.55 1372.21 32.29 o 6 10 12 407.35 369.02 20.42 o 7 10 12 320.66 302.49 21.12 o 8 10 12 1193.92 1265.94 36.27 o 9 10 12 191.49 153.73 22.53 o 10 10 12 327.86 303.06 32.27 o 11 10 12 123.75 74.13 21.22 o 12 10 12 701.14 774.05 36.24 o 1 11 12 466.60 506.42 26.05 o 2 11 12 1950.01 2106.00 67.28 o 3 11 12 264.87 268.50 33.98 o 4 11 12 178.80 151.48 23.49 o 5 11 12 544.58 497.82 22.16 o 6 11 12 864.76 881.59 28.69 o 7 11 12 362.17 359.72 22.11 o 8 11 12 244.28 247.35 21.95 o 9 11 12 3.34 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