#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237806.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237806_Fobs loop_ _publ_author_name 'Zhu, Hang' 'Ma, Qing' 'Shi, Hua-Tian' 'Chen, Qun' 'Zhang, Qian-Feng' _publ_section_title ; Aquacarbonyl(ferrocenyldithiophosphonato-\k^2^S,S')bis(triphenylphosphane-\kP)ruthenium(II) dichloromethane monosolvate ; _journal_coeditor_code DS2231 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m343 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.811 _cell_angle_beta 98.278 _cell_angle_gamma 109.759 _cell_length_a 12.1493 _cell_length_b 14.2208 _cell_length_c 14.7100 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.7660 _[local]_cod_data_source_file ds2231Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 249.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3491.83 3585.73 43.37 o 3 0 0 3935.13 4016.85 46.27 o 4 0 0 889.38 828.07 20.58 o 5 0 0 2321.94 2660.29 42.38 o 6 0 0 683.36 639.48 22.40 o 7 0 0 617.29 700.19 25.50 o 8 0 0 3.31 -7.40 7.40 o 9 0 0 2098.78 2210.51 50.64 o 10 0 0 293.30 357.90 25.11 o 11 0 0 990.85 1108.70 41.09 o 12 0 0 656.69 625.11 45.04 o 13 0 0 816.82 859.27 49.75 o 14 0 0 127.94 160.37 35.58 o -14 1 0 21.27 16.33 23.08 o -13 1 0 7.27 10.05 18.69 o -12 1 0 528.56 612.65 40.16 o -11 1 0 2098.78 2325.27 57.34 o -10 1 0 131.13 182.88 20.36 o -9 1 0 1.55 0.59 8.74 o -8 1 0 44.82 44.79 18.10 o -7 1 0 2129.49 1937.59 45.31 o -6 1 0 1282.49 995.51 26.43 o -5 1 0 120.59 109.12 9.65 o -4 1 0 348.60 383.73 13.57 o -3 1 0 7743.38 8926.68 92.80 o -2 1 0 1241.52 1543.68 30.87 o 1 1 0 280.37 357.20 18.18 o 2 1 0 4281.58 5566.13 56.26 o 3 1 0 3826.59 4314.74 51.03 o 5 1 0 331.91 352.83 17.25 o 6 1 0 5780.36 5677.96 89.93 o 7 1 0 4017.90 4704.71 71.14 o 8 1 0 1012.14 1041.59 33.67 o 9 1 0 969.54 952.49 34.29 o 10 1 0 519.38 480.93 28.53 o 11 1 0 20.19 31.68 16.66 o 12 1 0 5.35 25.55 14.67 o 13 1 0 5.06 14.05 16.10 o 14 1 0 86.60 45.88 28.23 o -15 2 0 499.52 534.73 60.39 o -14 2 0 326.91 279.49 44.08 o -13 2 0 398.77 385.69 47.21 o -12 2 0 10.57 2.21 29.37 o -11 2 0 962.72 1053.26 38.31 o -10 2 0 155.41 221.43 19.77 o -9 2 0 5.18 3.05 10.79 o -8 2 0 533.18 576.28 38.45 o -7 2 0 2919.90 3008.57 40.80 o -6 2 0 246.06 214.03 9.64 o -5 2 0 1192.02 1326.46 22.92 o -4 2 0 523.50 600.38 21.73 o -3 2 0 4722.60 4668.04 107.17 o -2 2 0 61398.65 66249.05 2374.85 o -1 2 0 15062.76 16767.80 278.57 o 0 2 0 9.79 13.59 6.66 o 1 2 0 3291.42 3542.96 46.81 o 2 2 0 2451.88 3344.17 48.10 o 3 2 0 2321.37 2633.68 66.59 o 4 2 0 6.80 4.03 7.46 o 5 2 0 1809.20 1353.99 32.27 o 6 2 0 385.58 295.80 18.53 o 7 2 0 834.89 778.60 28.88 o 8 2 0 304.54 236.11 20.00 o 9 2 0 1491.22 1633.30 46.35 o 10 2 0 3276.67 3301.57 69.98 o 11 2 0 943.05 874.67 39.99 o 12 2 0 281.27 231.37 26.51 o 13 2 0 6.79 7.19 15.98 o -15 3 0 205.56 259.80 46.08 o -14 3 0 305.28 318.20 87.72 o -13 3 0 1293.19 1577.73 194.76 o -12 3 0 503.68 687.11 53.86 o -11 3 0 45.16 40.28 19.55 o -10 3 0 488.69 478.70 47.72 o -9 3 0 3247.98 3507.14 60.70 o -8 3 0 1643.55 1547.49 27.65 o -7 3 0 6228.00 6969.95 65.45 o -6 3 0 399.29 393.44 26.16 o -5 3 0 3938.24 4334.35 52.50 o -4 3 0 3.99 -1.84 4.05 o -3 3 0 968.27 1374.97 29.15 o -2 3 0 3459.50 3777.77 50.63 o -1 3 0 5.10 16.29 4.83 o 0 3 0 26543.87 28167.05 433.91 o 1 3 0 1167.34 967.56 20.07 o 2 3 0 15425.59 16164.25 165.41 o 3 3 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0 7277.14 6238.03 69.44 o -3 7 0 794.12 603.66 19.37 o -2 7 0 5.49 0.75 4.75 o -1 7 0 2648.52 2230.31 32.91 o 0 7 0 2686.94 2350.89 31.88 o 1 7 0 4203.51 4033.29 48.95 o 2 7 0 134.94 129.72 11.12 o 3 7 0 859.90 802.09 23.52 o 4 7 0 1.37 2.47 8.85 o 5 7 0 197.34 317.60 28.56 o 6 7 0 1156.51 1089.49 47.07 o 7 7 0 1989.18 1779.43 62.40 o 8 7 0 1602.49 1737.26 64.97 o 9 7 0 868.12 732.96 63.16 o 10 7 0 30.80 43.85 21.12 o 11 7 0 12.72 9.45 22.52 o -15 8 0 380.67 308.45 54.00 o -14 8 0 30.22 24.63 23.55 o -13 8 0 27.93 44.81 28.54 o -12 8 0 519.33 642.77 54.73 o -11 8 0 1303.73 1327.84 121.34 o -10 8 0 1741.01 1772.20 49.48 o -9 8 0 1261.22 1086.29 37.76 o -8 8 0 3.39 13.66 10.44 o -7 8 0 146.59 131.14 15.81 o -6 8 0 1749.64 1671.40 41.96 o -5 8 0 4485.68 4327.03 114.00 o -4 8 0 4354.89 4078.97 55.51 o -3 8 0 1145.35 1069.28 24.03 o -2 8 0 3326.02 3071.58 42.04 o -1 8 0 2050.61 1848.11 31.56 o 0 8 0 422.78 471.89 15.86 o 1 8 0 1430.34 1409.23 30.43 o 2 8 0 863.06 802.16 23.13 o 3 8 0 233.96 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