#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181300 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237808.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237808_Fobs loop_ _publ_author_name 'Ballestero-Mart\'inez, Ernesto' 'Campos-Fern\'andez, Cristian Saul' 'Soto-Tellini, Victor Hugo' 'Gonzalez-Montiel, Simplicio' 'Mart\'inez-Otero, Diego' _publ_section_title ; catena-Poly[[[diaquabis[1,2-bis(pyridin-4-yl)diazene]copper(II)]-\m-1,2-bis(pyridin-4-yl)diazene] bis(perchlorate)] ; _journal_coeditor_code FB2274 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m317 _journal_page_last m318 _journal_volume 69 _journal_year 2013 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 96.629 _cell_angle_gamma 90 _cell_length_a 20.5028 _cell_length_b 9.5882 _cell_length_c 18.7797 _exptl_crystal_F_000 1740 _reflns_d_resolution_high ? _cod_data_source_file fb2274Isup3.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title sgm_46_1d _shelx_refln_list_code 4 _shelx_f_calc_maximum 572.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 14508.50 14445.60 69.87 o 6 0 0 5550.92 4541.26 30.48 o 8 0 0 1649.51 1699.11 20.96 o 10 0 0 19.49 48.10 5.84 o 12 0 0 16285.40 16014.60 82.82 o 14 0 0 3070.80 3148.39 39.96 o 16 0 0 12776.90 12417.40 114.07 o 18 0 0 970.24 907.14 33.52 o 20 0 0 874.65 883.01 40.09 o 22 0 0 1801.60 1790.42 70.40 o 24 0 0 832.42 882.14 52.28 o 3 1 0 7231.75 7548.57 31.25 o 5 1 0 344.00 319.51 6.18 o 7 1 0 4746.18 4694.05 24.94 o 9 1 0 438.16 421.32 8.48 o 11 1 0 83.47 103.99 5.24 o 13 1 0 30.66 42.03 4.44 o 15 1 0 121.43 116.71 7.74 o 17 1 0 509.48 504.81 16.12 o 19 1 0 45.28 63.36 9.71 o 21 1 0 6.96 -13.15 12.39 < 23 1 0 53.60 45.70 11.78 o 25 1 0 0.13 -5.88 15.66 < 0 2 0 353501.00 327761.00 436.41 o 2 2 0 47608.30 50379.30 98.55 o 4 2 0 9109.32 9560.02 40.16 o 6 2 0 1569.89 1489.27 15.16 o 8 2 0 12516.30 13788.60 51.81 o 10 2 0 27.97 29.41 4.07 o 12 2 0 3211.29 2946.36 26.57 o 14 2 0 3340.76 3298.18 27.37 o 16 2 0 5014.46 4776.20 44.17 o 18 2 0 804.92 736.72 21.70 o 20 2 0 568.82 461.85 21.30 o 22 2 0 1130.92 1155.81 40.13 o 24 2 0 530.54 564.34 34.25 o 1 3 0 1211.85 1124.36 16.49 o 3 3 0 29308.80 30527.50 84.83 o 5 3 0 2493.16 2787.99 23.74 o 7 3 0 1264.67 1211.19 16.96 o 9 3 0 537.03 586.97 12.02 o 11 3 0 182.43 170.52 7.08 o 13 3 0 85.76 53.91 5.34 o 15 3 0 0.54 1.74 5.74 < 17 3 0 487.34 569.71 15.79 o 19 3 0 15.11 37.36 8.11 o 21 3 0 7.51 6.54 11.08 < 23 3 0 62.00 34.88 14.45 < 0 4 0 13958.00 14422.20 88.46 o 2 4 0 19276.20 19571.70 71.34 o 4 4 0 15510.60 16510.60 70.07 o 6 4 0 826.95 701.14 12.95 o 8 4 0 45.78 119.51 6.34 o 10 4 0 859.17 791.24 14.76 o 12 4 0 5273.57 4933.37 40.23 o 14 4 0 5170.05 5116.31 48.27 o 16 4 0 2868.34 2698.69 38.59 o 18 4 0 1866.53 1856.98 37.36 o 20 4 0 635.93 587.00 28.54 o 22 4 0 728.33 735.62 43.93 o 1 5 0 348.90 372.28 11.78 o 3 5 0 3819.73 4225.19 36.85 o 5 5 0 110.25 158.74 8.35 o 7 5 0 1104.51 1235.43 19.66 o 9 5 0 139.65 163.84 8.15 o 11 5 0 26.49 15.96 5.54 < 13 5 0 113.90 69.60 7.48 o 15 5 0 26.52 50.94 8.38 o 17 5 0 2.94 16.96 8.98 < 19 5 0 6.53 -19.13 13.02 < 21 5 0 160.91 168.92 26.94 o 23 5 0 4.19 27.37 19.20 < 0 6 0 968.62 865.58 27.01 o 2 6 0 3125.01 3053.89 30.78 o 4 6 0 4641.43 4968.12 39.73 o 6 6 0 14.83 13.59 5.21 < 8 6 0 100.46 92.10 6.98 o 10 6 0 314.53 301.28 12.05 o 12 6 0 2135.93 1819.09 27.77 o 14 6 0 442.68 431.20 17.59 o 16 6 0 1067.99 1052.66 31.95 o 18 6 0 642.93 761.16 42.20 o 20 6 0 291.24 281.25 28.28 o 22 6 0 72.05 27.37 24.04 < 1 7 0 354.73 362.54 13.19 o 3 7 0 36.84 55.95 6.14 o 5 7 0 1.08 -1.97 5.74 < 7 7 0 298.18 251.21 10.42 o 9 7 0 191.68 178.03 10.35 o 11 7 0 257.24 270.30 13.82 o 13 7 0 3.43 11.88 7.28 < 15 7 0 8.56 19.70 11.12 < 17 7 0 43.74 48.07 14.65 o 19 7 0 9.73 7.38 15.32 < 0 8 0 3934.75 4317.39 90.97 o 2 8 0 7910.49 8071.28 77.28 o 4 8 0 1179.99 1187.93 27.81 o 6 8 0 2452.85 2554.25 44.67 o 8 8 0 57.63 50.34 8.08 o 10 8 0 768.57 710.59 22.37 o 12 8 0 588.98 473.97 26.91 o 14 8 0 599.99 603.86 26.77 o 16 8 0 346.80 425.66 29.58 o 18 8 0 886.46 1276.22 59.29 o 1 9 0 122.91 116.57 13.69 o 3 9 0 6.08 -13.35 9.15 < 5 9 0 45.29 41.80 10.08 o 7 9 0 39.96 27.97 10.18 < 9 9 0 115.09 111.46 17.53 o 11 9 0 287.83 349.65 27.17 o 13 9 0 15.69 20.30 12.39 < 15 9 0 9.19 10.62 15.66 < 0 10 0 1581.31 1550.33 87.86 o 2 10 0 878.95 1004.89 43.13 o 4 10 0 204.55 210.68 22.57 o 6 10 0 42.60 51.74 14.52 o 8 10 0 14.63 -13.62 12.85 < 10 10 0 212.15 191.02 22.53 o 12 10 0 83.01 65.83 14.65 o 14 10 0 93.96 131.66 20.46 o 1 11 0 9.90 -31.45 15.92 < 3 11 0 6.81 11.48 15.92 < 5 11 0 23.01 -0.67 15.82 < 7 11 0 2.21 -11.72 16.36 < 9 11 0 45.98 38.59 15.86 < -25 1 1 215.38 235.38 26.91 o -23 1 1 720.10 773.41 33.15 o -21 1 1 176.42 195.22 16.02 o -19 1 1 413.59 456.81 17.76 o -17 1 1 6284.52 6116.45 49.94 o -15 1 1 2654.03 2777.71 27.57 o -13 1 1 7120.01 7318.40 40.03 o -11 1 1 7933.50 7423.59 37.72 o -9 1 1 14205.30 12781.00 44.90 o -7 1 1 5410.60 5347.92 26.94 o -5 1 1 5876.49 6739.78 28.14 o -3 1 1 12184.80 13455.90 40.33 o 3 1 1 1475.32 2343.37 17.73 o 5 1 1 46677.20 49568.30 81.55 o 7 1 1 8487.69 8453.18 37.86 o 9 1 1 5826.86 5533.39 34.62 o 11 1 1 4033.78 3330.50 29.71 o 13 1 1 8359.26 8180.44 46.94 o 15 1 1 7034.52 6999.93 48.20 o 17 1 1 1212.65 1517.35 29.84 o 19 1 1 709.46 815.84 25.04 o 21 1 1 2542.23 2971.53 62.83 o 23 1 1 950.09 1064.14 40.19 o 25 1 1 503.11 564.14 35.05 o -24 2 1 34.77 -11.52 13.75 < -22 2 1 0.75 -2.70 9.75 < -20 2 1 23.22 24.04 10.25 < -18 2 1 167.83 215.95 11.45 o -16 2 1 51.24 50.21 5.51 o -14 2 1 1089.69 1057.57 16.66 o -12 2 1 160.41 181.70 7.28 o -10 2 1 1060.53 1081.33 15.62 o -8 2 1 239.07 218.82 6.64 o -6 2 1 2.55 9.01 3.17 < -4 2 1 1136.10 970.97 13.59 o -2 2 1 839.81 1252.49 17.09 o 0 2 1 13505.20 12393.60 44.97 o 2 2 1 52589.50 50695.50 94.41 o 4 2 1 71599.20 72402.50 107.16 o 6 2 1 105.27 135.57 5.64 o 8 2 1 1632.12 1857.62 18.73 o 10 2 1 569.20 565.94 11.52 o 12 2 1 174.53 158.17 6.84 o 14 2 1 46.84 62.03 6.08 o 16 2 1 2189.16 2364.73 32.18 o 18 2 1 57.03 90.43 9.88 o 20 2 1 49.49 26.17 10.28 < 22 2 1 0.43 -8.38 11.52 < 24 2 1 156.28 203.47 22.50 o -23 3 1 496.38 506.82 29.64 o -21 3 1 687.84 723.74 29.84 o -19 3 1 224.40 227.04 14.29 o -17 3 1 1839.33 1860.05 28.14 o -15 3 1 3005.66 3398.26 34.58 o -13 3 1 6285.68 6614.99 44.67 o -11 3 1 6201.49 6318.52 41.70 o -9 3 1 9257.38 7843.91 44.33 o -7 3 1 514.52 440.95 10.18 o -5 3 1 23247.90 22576.00 68.10 o -3 3 1 21896.60 19053.60 68.47 o -1 3 1 16018.00 16200.30 66.63 o 1 3 1 169.50 207.14 7.11 o 3 3 1 37697.40 37590.70 93.24 o 5 3 1 415.22 475.17 11.18 o 7 3 1 5839.98 5822.92 37.12 o 9 3 1 2785.80 2522.20 25.67 o 11 3 1 11969.20 11736.00 56.48 o 13 3 1 5837.20 6169.53 42.33 o 15 3 1 7024.20 6945.15 50.54 o 17 3 1 414.02 489.73 17.96 o 19 3 1 1522.89 1498.02 33.42 o 21 3 1 761.98 939.72 34.15 o 23 3 1 390.93 477.21 31.85 o -24 4 1 5.24 94.17 22.00 o -22 4 1 17.62 56.12 18.16 o -20 4 1 8.84 -2.64 11.98 < -18 4 1 331.07 415.11 16.26 o -16 4 1 23.37 18.19 6.91 < -14 4 1 26.32 3.84 5.88 < -12 4 1 100.99 70.74 6.24 o -10 4 1 554.36 586.20 12.79 o -8 4 1 1627.24 1718.51 21.03 o -6 4 1 7963.92 8068.71 46.27 o -4 4 1 10416.10 10730.50 58.12 o -2 4 1 1546.29 1442.00 23.33 o 0 4 1 41.83 45.00 4.81 o 2 4 1 946.18 989.77 16.46 o 4 4 1 3063.15 3198.94 30.41 o 6 4 1 1346.26 1666.10 22.83 o 8 4 1 5330.94 6074.73 41.93 o 10 4 1 958.39 942.76 16.02 o 12 4 1 504.97 518.80 13.29 o 14 4 1 106.40 99.38 7.95 o 16 4 1 441.92 566.64 17.46 o 18 4 1 60.58 83.22 10.72 o 20 4 1 0.19 2.90 11.58 < 22 4 1 23.24 -11.92 15.82 < -23 5 1 214.28 171.15 24.84 o -21 5 1 478.15 418.35 39.73 o -19 5 1 285.68 305.22 27.07 o -17 5 1 282.92 294.04 15.76 o -15 5 1 1348.51 1506.13 30.51 o -13 5 1 2964.99 2950.93 37.46 o -11 5 1 3817.67 4220.31 36.95 o -9 5 1 1590.97 1536.41 22.00 o -7 5 1 2045.75 1882.79 23.20 o -5 5 1 9071.00 8447.10 55.32 o -3 5 1 10858.90 10251.10 74.38 o -1 5 1 1675.55 1690.87 28.54 o 1 5 1 779.57 786.23 14.49 o 3 5 1 2986.13 3278.09 30.95 o 5 5 1 7594.72 7739.19 51.18 o 7 5 1 1026.01 1271.55 22.13 o 9 5 1 6929.69 6666.63 46.97 o 11 5 1 2544.90 2585.83 30.18 o 13 5 1 5231.07 5519.04 49.64 o 15 5 1 3088.18 3076.89 42.00 o 17 5 1 805.60 838.37 25.97 o 19 5 1 635.85 595.75 31.08 o 21 5 1 216.23 278.75 39.79 o -22 6 1 14.53 60.06 21.73 < -20 6 1 38.00 33.98 15.02 < -18 6 1 129.01 113.10 16.09 o -16 6 1 0.12 -0.80 8.81 < -14 6 1 20.47 2.34 7.64 < -12 6 1 384.93 367.41 14.09 o -10 6 1 50.81 36.69 6.01 o -8 6 1 518.32 563.70 15.52 o -6 6 1 134.08 75.75 7.51 o -4 6 1 35.49 30.81 7.31 o -2 6 1 413.24 452.30 15.59 o 0 6 1 1850.28 1972.32 32.72 o 2 6 1 140.92 150.66 8.45 o 4 6 1 176.08 166.75 8.35 o 6 6 1 294.04 253.34 10.75 o 8 6 1 34.35 58.59 6.41 o 10 6 1 55.14 43.40 6.31 o 12 6 1 183.66 134.16 8.75 o 14 6 1 43.56 44.93 7.54 o 16 6 1 47.46 34.75 8.98 o 18 6 1 41.10 23.74 13.65 < 20 6 1 77.38 132.03 24.40 o -19 7 1 437.24 541.10 39.02 o -17 7 1 270.13 257.82 23.50 o -15 7 1 717.50 688.82 30.11 o -13 7 1 975.82 833.47 22.73 o -11 7 1 3539.95 3545.35 45.27 o -9 7 1 633.40 720.07 21.83 o -7 7 1 4108.19 4288.92 49.97 o -5 7 1 4694.62 4835.96 56.75 o -3 7 1 2391.14 2363.30 40.23 o -1 7 1 2690.00 2740.46 38.46 o 1 7 1 467.87 434.61 16.06 o 3 7 1 183.83 170.62 9.45 o 5 7 1 337.63 306.45 12.65 o 7 7 1 44.21 44.77 6.81 o 9 7 1 1854.68 1795.16 29.71 o 11 7 1 1887.72 1967.81 33.88 o 13 7 1 1305.50 1479.86 29.31 o 15 7 1 2177.35 2181.76 52.74 o 17 7 1 581.28 737.79 36.62 o 19 7 1 218.09 204.37 26.27 o -18 8 1 11.10 17.66 17.09 < -16 8 1 0.16 -0.50 13.22 < -14 8 1 23.70 -11.95 10.85 < -12 8 1 84.93 54.41 11.15 o -10 8 1 113.95 91.20 10.88 o -8 8 1 142.65 132.86 11.08 o -6 8 1 11.73 11.48 8.48 < -4 8 1 0.68 20.43 7.71 < -2 8 1 154.86 139.77 10.35 o 0 8 1 43.92 71.71 9.85 o 2 8 1 65.81 67.83 10.05 o 4 8 1 125.53 126.79 9.65 o 6 8 1 31.75 19.26 6.71 < 8 8 1 8.55 0.10 6.51 < 10 8 1 19.98 24.57 8.45 < 12 8 1 1150.70 924.50 32.51 o 14 8 1 104.71 112.40 13.99 o 16 8 1 3.71 25.40 15.92 < 18 8 1 41.06 14.86 15.52 < -15 9 1 150.01 183.37 22.90 o -13 9 1 326.57 233.11 20.86 o -11 9 1 646.67 608.97 31.48 o -9 9 1 674.52 766.80 37.19 o -7 9 1 416.88 415.35 24.54 o -5 9 1 743.17 790.10 27.71 o -3 9 1 774.99 855.07 27.74 o -1 9 1 564.66 459.38 18.23 o 1 9 1 243.17 268.63 19.40 o 3 9 1 307.66 304.85 19.73 o 5 9 1 6.46 -9.48 9.58 < 7 9 1 17.64 21.13 10.45 < 9 9 1 417.42 495.57 30.28 o 11 9 1 399.55 463.69 30.48 o 13 9 1 483.71 629.53 29.34 o 15 9 1 328.95 305.99 27.01 o -14 10 1 10.70 18.96 14.15 < -12 10 1 15.14 39.42 16.36 < -10 10 1 10.75 -8.25 12.35 < -8 10 1 141.30 141.84 19.60 o -6 10 1 52.41 34.05 13.05 < -4 10 1 4.30 3.44 13.59 < -2 10 1 343.64 326.55 25.74 o 0 10 1 1.55 16.22 12.95 < 2 10 1 152.25 131.63 17.79 o 4 10 1 76.98 74.54 15.62 o 6 10 1 78.98 100.18 16.69 o 8 10 1 18.51 18.86 13.42 < 10 10 1 301.57 290.93 25.54 o 12 10 1 136.90 50.17 15.02 o -9 11 1 131.23 189.38 23.37 o -7 11 1 96.02 56.25 18.86 < -5 11 1 14.22 31.31 18.83 < -3 11 1 988.71 1219.44 59.49 o -1 11 1 279.03 227.84 27.84 o 1 11 1 218.96 256.08 33.85 o 3 11 1 2.18 -5.27 16.02 < 5 11 1 35.36 15.69 14.72 < 7 11 1 125.13 179.97 24.77 o 9 11 1 87.52 156.30 26.21 o -24 0 2 332.46 439.62 48.87 o -22 0 2 83.49 32.82 21.47 < -20 0 2 175.95 164.74 16.69 o -18 0 2 7739.61 8264.47 85.66 o -16 0 2 8517.46 8921.97 78.45 o -14 0 2 15630.60 14764.10 86.56 o -12 0 2 19645.50 19943.50 92.70 o -10 0 2 5885.37 5435.35 44.17 o -8 0 2 5890.16 5744.10 37.76 o -6 0 2 2616.01 3412.89 28.51 o -4 0 2 16827.90 18297.20 59.62 o 2 0 2 57722.00 61468.80 165.54 o 4 0 2 249211.00 256072.00 306.79 o 6 0 2 12879.20 12922.50 71.77 o 8 0 2 23450.80 22069.50 107.56 o 10 0 2 53461.10 52266.40 186.07 o 12 0 2 294.94 356.89 15.76 o 14 0 2 3658.08 3526.45 48.20 o 16 0 2 2020.43 2107.49 45.27 o 18 0 2 1550.07 1253.52 39.83 o 20 0 2 3178.30 3158.88 89.37 o 22 0 2 1877.88 1493.88 75.55 o 24 0 2 899.83 837.34 52.81 o -25 1 2 9.23 -3.91 17.96 < -23 1 2 26.85 44.77 14.62 o -21 1 2 12.84 -3.71 8.85 < -19 1 2 4.69 10.72 6.74 < -17 1 2 50.00 29.58 6.31 o -15 1 2 24.04 13.89 4.71 < -13 1 2 149.26 129.83 5.91 o -11 1 2 244.45 250.40 7.04 o -9 1 2 288.63 406.17 8.38 o -7 1 2 6369.97 6313.85 29.38 o -5 1 2 13789.10 13421.40 47.24 o -3 1 2 548.04 456.98 9.78 o -1 1 2 1427.76 1647.84 20.56 o 1 1 2 5213.88 5933.08 33.02 o 3 1 2 13743.90 14667.40 49.24 o 5 1 2 22624.10 22594.70 53.35 o 7 1 2 112.50 122.95 5.81 o 9 1 2 353.89 291.40 8.65 o 11 1 2 2005.13 2130.29 25.80 o 13 1 2 134.13 127.25 7.04 o 15 1 2 74.30 72.67 7.18 o 17 1 2 19.27 17.23 6.81 < 19 1 2 372.86 327.85 16.76 o 21 1 2 0.48 -42.56 13.19 < 23 1 2 6.45 11.12 12.82 < 25 1 2 28.54 -10.32 17.06 < -24 2 2 247.10 271.04 24.50 o -22 2 2 15.83 41.86 12.79 o -20 2 2 64.08 102.25 11.58 o -18 2 2 2837.69 2932.04 35.85 o -16 2 2 3667.12 3858.38 34.85 o -14 2 2 13785.10 13430.90 55.42 o -12 2 2 5421.57 5403.06 34.58 o -10 2 2 3080.97 2861.70 24.14 o -8 2 2 2089.73 2260.75 20.53 o -6 2 2 222.25 272.37 6.88 o -4 2 2 40595.20 42671.20 85.53 o -2 2 2 9116.16 8679.41 53.05 o 0 2 2 6173.60 7047.00 45.03 o 2 2 2 22544.10 22551.10 60.22 o 4 2 2 73595.30 76518.10 119.44 o 6 2 2 4655.40 4502.00 29.68 o 8 2 2 1456.55 1219.87 15.82 o 10 2 2 10927.30 11195.20 50.54 o 12 2 2 51.73 53.61 5.27 o 14 2 2 451.21 398.99 13.22 o 16 2 2 708.36 761.23 20.86 o 18 2 2 1037.51 932.45 24.57 o 20 2 2 1900.04 1940.31 45.57 o 22 2 2 848.22 749.71 33.68 o 24 2 2 735.14 671.23 43.10 o -23 3 2 78.47 119.31 16.96 o -21 3 2 56.24 65.20 12.92 o -19 3 2 138.75 192.15 11.98 o -17 3 2 57.74 20.20 6.51 o -15 3 2 0.16 -7.18 5.57 < -13 3 2 260.92 212.15 8.75 o -11 3 2 297.94 247.03 9.08 o -9 3 2 2008.67 2420.08 24.77 o -7 3 2 3768.27 3754.32 30.58 o -5 3 2 2747.55 2656.47 26.37 o -3 3 2 9640.96 10585.60 57.25 o -1 3 2 772.71 862.74 20.50 o 1 3 2 173.23 145.08 6.41 o 3 3 2 127.35 99.55 5.07 o 5 3 2 1939.27 1985.81 21.67 o 7 3 2 15464.10 15412.00 59.39 o 9 3 2 6825.77 7133.66 43.56 o 11 3 2 997.31 950.07 16.59 o 13 3 2 1.43 2.84 4.81 < 15 3 2 954.64 982.96 23.77 o 17 3 2 20.54 54.61 8.41 o 19 3 2 601.20 524.68 19.73 o 21 3 2 0.08 -10.42 12.89 < 23 3 2 42.40 96.64 18.19 o -24 4 2 172.38 205.07 26.57 o -22 4 2 780.25 805.43 45.93 o -20 4 2 388.79 508.05 33.22 o -18 4 2 662.36 660.98 18.99 o -16 4 2 3213.80 3311.43 46.47 o -14 4 2 11015.80 10659.00 72.07 o -12 4 2 9849.60 10202.80 59.49 o -10 4 2 2700.44 2728.07 27.61 o -8 4 2 2883.78 2628.06 27.94 o -6 4 2 2658.29 2563.93 28.78 o -4 4 2 5528.10 5935.19 49.11 o -2 4 2 15889.70 16153.60 99.35 o 0 4 2 17807.90 16937.00 71.64 o 2 4 2 36666.60 36079.20 96.38 o 4 4 2 28450.60 28013.20 92.07 o 6 4 2 25588.80 24230.50 88.16 o 8 4 2 1518.10 1606.41 23.27 o 10 4 2 5881.71 6297.76 42.20 o 12 4 2 2567.34 2650.12 30.28 o 14 4 2 1461.50 1388.52 25.40 o 16 4 2 1061.73 1057.70 24.24 o 18 4 2 2016.74 2033.31 42.03 o 20 4 2 700.93 835.40 39.22 o 22 4 2 479.14 506.45 38.02 o -23 5 2 0.83 -19.70 17.73 < -21 5 2 0.26 -5.54 14.19 < -19 5 2 51.77 66.30 13.05 o -17 5 2 157.81 129.36 12.82 o -15 5 2 0.79 -9.25 6.74 < -13 5 2 59.87 55.18 7.31 o -11 5 2 29.10 24.60 5.54 o -9 5 2 409.45 397.55 12.12 o -7 5 2 186.49 240.92 10.08 o -5 5 2 26.85 43.03 6.74 o -3 5 2 2348.13 2449.93 36.19 o -1 5 2 1498.93 1462.70 25.84 o 1 5 2 1402.85 1446.54 23.10 o 3 5 2 1105.75 1122.09 20.13 o 5 5 2 290.85 241.59 9.78 o 7 5 2 5178.15 5015.99 44.33 o 9 5 2 220.27 230.64 10.28 o 11 5 2 180.17 128.19 7.84 o 13 5 2 65.39 79.15 7.78 o 15 5 2 468.53 489.39 17.79 o 17 5 2 303.77 407.80 18.66 o 19 5 2 6.44 23.00 13.59 < 21 5 2 2.56 -4.07 19.60 < -22 6 2 209.17 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