#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181300 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237813.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237813_Fobs loop_ _publ_author_name 'Such\'a, Veronika' 'Kuch\'ar, Juraj' 'Harms, Klaus' _publ_section_title ; Tetraammine-2\k^4^C-\m-cyanido-1:2\k^2^C:N-tricyanido-1\k^3^C-copper(II)palladium(II) ; _journal_coeditor_code FF2104 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i32 _journal_volume 69 _journal_year 2013 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.5204 _cell_length_b 7.2358 _cell_length_c 10.3955 _exptl_crystal_F_000 668.00 _reflns_d_resolution_high 0.8411 _cod_data_source_file ff2104Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cupd14dab in P n m a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 321.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3529.42 3698.45 117.78 o 4 0 0 52053.29 46727.98 372.96 o 6 0 0 22444.44 20837.09 202.30 o 8 0 0 8104.94 8033.14 111.32 o 10 0 0 19522.96 18035.94 179.71 o 12 0 0 128.48 144.53 54.06 o 14 0 0 2108.07 2046.81 70.24 o 16 0 0 1231.13 1439.97 75.19 o 2 1 0 9126.67 9996.40 96.91 o 4 1 0 1411.42 1495.99 42.83 o 6 1 0 14858.90 14163.24 98.70 o 8 1 0 721.65 756.20 36.03 o 10 1 0 3389.27 3209.48 68.56 o 12 1 0 7313.82 7258.52 135.96 o 14 1 0 493.49 466.78 44.45 o 16 1 0 5761.92 5839.28 145.68 o 0 2 0 103626.13 91179.73 4994.85 o 2 2 0 18243.01 19385.47 223.48 o 4 2 0 42409.76 43900.96 193.96 o 6 2 0 38279.33 38199.63 165.19 o 8 2 0 565.62 614.86 32.67 o 10 2 0 16833.53 16168.45 254.45 o 12 2 0 28.30 27.14 35.56 o 14 2 0 2619.78 2633.78 73.63 o 16 2 0 776.77 739.97 38.33 o 2 3 0 2316.29 2314.84 30.24 o 4 3 0 4180.21 4253.49 54.50 o 6 3 0 21146.74 21803.46 105.57 o 8 3 0 420.11 435.23 30.03 o 10 3 0 2406.51 2451.43 66.42 o 12 3 0 3164.77 3204.97 83.03 o 14 3 0 1645.00 1561.89 43.47 o 16 3 0 4473.52 3939.36 132.81 o 0 4 0 87466.45 81784.30 337.15 o 2 4 0 3554.54 3846.00 37.77 o 4 4 0 22734.04 23043.96 92.15 o 6 4 0 15219.54 15841.37 70.75 o 8 4 0 2173.81 2397.44 42.42 o 10 4 0 11530.77 12017.22 199.35 o 12 4 0 7.48 47.02 42.66 o 14 4 0 1744.73 1728.56 67.74 o 2 5 0 3994.52 4068.85 66.55 o 4 5 0 474.20 446.22 20.84 o 6 5 0 4184.72 4256.15 36.28 o 8 5 0 489.86 510.93 28.02 o 10 5 0 1622.23 1685.07 44.40 o 12 5 0 5096.23 4971.44 58.86 o 14 5 0 69.81 91.08 39.30 o 0 6 0 39419.26 38384.65 256.53 o 2 6 0 1684.28 1801.83 44.25 o 4 6 0 10462.86 10777.49 174.61 o 6 6 0 8348.73 8744.87 174.92 o 8 6 0 1422.12 1404.41 32.04 o 10 6 0 6896.53 6694.69 49.86 o 12 6 0 0.75 8.04 29.03 o 2 7 0 786.60 796.17 23.93 o 4 7 0 761.43 758.43 26.64 o 6 7 0 5476.29 5550.90 192.19 o 8 7 0 124.68 118.43 24.56 o 10 7 0 915.80 783.87 38.17 o 0 8 0 12526.12 12276.29 119.36 o 2 8 0 1635.18 1525.74 156.11 o 4 8 0 5197.25 4813.24 101.59 o 6 8 0 5617.79 4983.67 292.70 o 1 0 1 19505.54 17719.06 274.56 o 2 0 1 1045.27 922.48 113.17 o 3 0 1 36005.39 37446.19 7738.26 o 4 0 1 9267.39 9109.97 335.16 o 5 0 1 18776.60 17955.14 475.48 o 6 0 1 483.75 663.27 41.89 o 7 0 1 18589.15 17043.40 118.74 o 8 0 1 3658.66 3570.28 58.90 o 9 0 1 7286.08 6786.78 71.93 o 10 0 1 2082.00 2092.24 48.65 o 11 0 1 1728.85 1840.07 47.87 o 12 0 1 292.82 282.14 40.75 o 13 0 1 9229.81 9113.30 87.28 o 14 0 1 4149.76 4112.90 62.27 o 15 0 1 218.38 238.23 44.06 o 16 0 1 400.59 412.78 39.70 o 17 0 1 927.78 819.77 52.02 o 0 1 1 5508.46 5907.78 80.49 o 1 1 1 4338.04 4757.29 39.98 o 2 1 1 8628.77 9106.59 86.68 o 3 1 1 1699.20 1768.83 34.89 o 4 1 1 154.35 195.05 29.30 o 5 1 1 2860.97 2900.35 35.90 o 6 1 1 20.80 31.06 27.62 o 7 1 1 512.09 510.56 26.77 o 8 1 1 2391.58 2170.27 41.42 o 9 1 1 12123.23 11138.81 169.68 o 10 1 1 1465.95 1393.14 26.02 o 11 1 1 4.93 26.82 22.82 o 12 1 1 784.41 808.67 26.94 o 13 1 1 5493.92 5386.05 85.81 o 14 1 1 17.42 33.00 30.61 o 15 1 1 4168.08 4206.35 77.02 o 16 1 1 125.83 104.13 29.60 o 17 1 1 746.81 640.94 37.57 o 1 2 1 36167.17 36988.74 167.11 o 2 2 1 486.32 508.45 18.36 o 3 2 1 16970.88 16834.12 87.36 o 4 2 1 16473.88 17716.56 135.85 o 5 2 1 3545.05 3691.49 32.45 o 6 2 1 1479.47 1430.47 24.18 o 7 2 1 22405.96 22018.40 140.35 o 8 2 1 6486.63 6555.07 60.85 o 9 2 1 10135.97 10119.61 84.71 o 10 2 1 565.08 564.23 22.92 o 11 2 1 1377.96 1359.05 25.66 o 12 2 1 86.10 92.87 20.38 o 13 2 1 4935.00 4815.26 73.18 o 14 2 1 1414.12 1405.86 30.31 o 15 2 1 339.46 339.60 33.29 o 16 2 1 78.51 92.17 29.89 o 0 3 1 22.36 25.47 23.20 o 1 3 1 694.55 635.11 16.55 o 2 3 1 1556.39 1504.45 19.10 o 3 3 1 4383.07 4375.86 31.21 o 4 3 1 30.81 41.82 17.34 o 5 3 1 1273.00 1266.64 20.53 o 6 3 1 548.91 558.21 17.15 o 7 3 1 27.30 39.69 22.15 o 8 3 1 3573.40 3660.71 32.09 o 9 3 1 9945.99 9964.19 78.60 o 10 3 1 1385.18 1375.86 27.98 o 11 3 1 281.07 296.83 24.06 o 12 3 1 540.36 544.98 27.45 o 13 3 1 4205.70 4078.71 53.58 o 14 3 1 31.25 41.51 22.03 o 15 3 1 2452.47 2303.00 37.79 o 16 3 1 103.97 90.32 28.12 o 1 4 1 11910.46 12177.16 78.35 o 2 4 1 745.77 690.83 15.51 o 3 4 1 14909.16 14892.90 85.57 o 4 4 1 5824.64 5936.10 34.81 o 5 4 1 4503.24 4791.62 45.07 o 6 4 1 163.48 151.15 18.21 o 7 4 1 11996.89 12184.76 137.37 o 8 4 1 2500.25 2687.04 26.94 o 9 4 1 5204.73 5308.06 71.68 o 10 4 1 795.93 830.05 23.04 o 11 4 1 1115.56 1172.37 26.10 o 12 4 1 24.68 50.78 23.97 o 13 4 1 4966.20 4952.86 84.17 o 14 4 1 1897.27 1757.19 73.82 o 15 4 1 197.56 179.61 23.86 o 0 5 1 3209.18 3252.41 31.29 o 1 5 1 1978.10 1999.87 22.05 o 2 5 1 3960.91 4084.33 38.51 o 3 5 1 529.88 551.81 17.39 o 4 5 1 147.18 147.35 16.83 o 5 5 1 1311.49 1314.85 19.78 o 6 5 1 35.67 35.96 15.81 o 7 5 1 542.67 568.56 17.38 o 8 5 1 651.47 701.63 20.27 o 9 5 1 5018.07 5225.93 57.00 o 10 5 1 628.98 636.74 21.57 o 11 5 1 6.40 19.35 20.64 o 12 5 1 461.80 432.27 28.65 o 13 5 1 3174.94 2845.29 56.54 o 1 6 1 5752.24 5891.18 28.88 o 2 6 1 303.17 315.25 16.85 o 3 6 1 8232.55 8597.60 141.88 o 4 6 1 2577.66 2663.80 29.81 o 5 6 1 2419.27 2573.46 42.58 o 6 6 1 77.82 102.38 18.71 o 7 6 1 6827.72 7322.02 60.31 o 8 6 1 1225.81 1274.23 21.42 o 9 6 1 2865.09 2838.50 43.37 o 10 6 1 435.39 408.08 21.05 o 11 6 1 695.73 643.46 23.56 o 12 6 1 25.48 42.36 24.63 o 0 7 1 123.22 131.50 23.28 o 1 7 1 277.98 285.07 22.03 o 2 7 1 662.28 692.71 21.30 o 3 7 1 886.22 902.73 20.48 o 4 7 1 3.13 9.70 17.78 o 5 7 1 369.63 363.55 19.91 o 6 7 1 122.32 134.01 20.18 o 7 7 1 8.68 17.85 19.19 o 8 7 1 1060.75 1077.19 28.78 o 9 7 1 3344.52 3247.67 36.25 o 1 8 1 3822.07 3623.90 83.71 o 2 8 1 133.65 163.72 22.42 o 3 8 1 3332.25 3228.03 73.95 o 4 8 1 1605.97 1494.77 33.91 o 5 8 1 708.68 678.24 23.13 o 6 8 1 279.14 280.37 20.49 o 2 0 2 15477.22 12893.35 173.58 o 3 0 2 1257.08 1147.76 93.23 o 4 0 2 378.50 357.82 50.17 o 5 0 2 5.44 27.32 46.69 o 6 0 2 11930.72 11429.08 608.58 o 7 0 2 1549.52 1394.12 49.70 o 8 0 2 12325.88 11844.83 177.46 o 9 0 2 1940.02 1897.52 44.04 o 10 0 2 6494.15 6461.57 64.96 o 11 0 2 4658.55 4751.08 138.21 o 12 0 2 2337.34 2315.01 87.69 o 13 0 2 11.69 38.20 34.30 o 14 0 2 2737.74 2743.91 194.88 o 15 0 2 63.70 78.49 35.83 o 16 0 2 1582.86 1467.46 53.52 o 17 0 2 1328.39 1202.42 79.68 o 1 1 2 5283.53 5607.48 55.71 o 2 1 2 708.03 767.12 29.47 o 3 1 2 5827.92 6472.29 61.45 o 4 1 2 1613.17 1647.39 31.01 o 5 1 2 11676.02 11339.52 231.61 o 6 1 2 1333.19 1300.98 29.32 o 7 1 2 1571.53 1474.75 29.83 o 8 1 2 2839.44 2682.97 30.30 o 9 1 2 1650.31 1568.83 32.70 o 10 1 2 4242.68 4060.92 64.37 o 11 1 2 1080.22 1087.49 27.40 o 12 1 2 1213.62 1230.53 33.99 o 13 1 2 1310.53 1316.39 31.87 o 14 1 2 5171.52 4979.97 84.47 o 15 1 2 2272.03 2217.42 54.13 o 16 1 2 1362.97 1287.80 37.62 o 0 2 2 22875.33 23874.35 131.41 o 1 2 2 2468.88 2449.68 27.78 o 2 2 2 985.12 788.20 19.36 o 3 2 2 3745.61 3898.24 37.59 o 4 2 2 17864.33 18123.79 145.62 o 5 2 2 43.43 52.06 17.51 o 6 2 2 5521.99 5525.05 35.75 o 7 2 2 4456.11 4499.53 94.69 o 8 2 2 9414.37 9174.16 57.94 o 9 2 2 2560.17 2524.31 29.68 o 10 2 2 3112.59 3145.89 64.18 o 11 2 2 2510.95 2500.50 39.25 o 12 2 2 3850.00 3877.34 58.99 o 13 2 2 5.25 12.85 23.95 o 14 2 2 3560.93 3369.43 63.31 o 15 2 2 291.92 287.92 33.10 o 16 2 2 595.83 583.52 36.39 o 1 3 2 1787.61 1773.45 20.49 o 2 3 2 335.85 383.52 19.86 o 3 3 2 2394.44 2386.76 21.96 o 4 3 2 1704.80 1764.51 24.80 o 5 3 2 12056.17 12039.55 71.27 o 6 3 2 1083.50 1100.88 22.90 o 7 3 2 1764.60 1803.97 24.87 o 8 3 2 4759.02 4905.48 62.01 o 9 3 2 713.58 765.01 23.95 o 10 3 2 1140.50 1163.35 26.49 o 11 3 2 852.66 854.04 26.60 o 12 3 2 1378.24 1336.80 30.78 o 13 3 2 462.80 460.07 24.43 o 14 3 2 3770.92 3638.43 56.51 o 15 3 2 1570.08 1480.92 30.26 o 0 4 2 10545.74 10841.42 115.71 o 1 4 2 4211.52 4206.12 36.32 o 2 4 2 4851.69 4755.73 34.30 o 3 4 2 1051.69 1101.40 17.75 o 4 4 2 3770.94 3770.60 59.55 o 5 4 2 6.27 12.28 18.99 o 6 4 2 5821.65 5900.30 52.77 o 7 4 2 1737.87 1804.89 24.42 o 8 4 2 6520.69 6862.29 46.45 o 9 4 2 1411.31 1490.29 25.74 o 10 4 2 2967.67 3064.75 26.72 o 11 4 2 2419.55 2454.17 27.34 o 12 4 2 2022.68 1900.35 27.57 o 13 4 2 1.57 7.97 24.77 o 14 4 2 2109.63 1985.58 32.63 o 15 4 2 110.37 85.35 25.27 o 1 5 2 2380.59 2405.64 20.86 o 2 5 2 454.75 516.23 17.51 o 3 5 2 1956.16 2006.21 20.04 o 4 5 2 528.26 512.57 15.99 o 5 5 2 3876.27 3928.86 23.18 o 6 5 2 528.03 557.45 17.83 o 7 5 2 448.59 471.76 18.45 o 8 5 2 783.02 804.13 22.08 o 9 5 2 948.86 999.21 23.89 o 10 5 2 3222.76 3169.83 29.14 o 11 5 2 537.80 540.24 21.94 o 12 5 2 515.17 480.16 25.04 o 13 5 2 969.44 867.85 26.53 o 0 6 2 5476.02 5640.23 141.67 o 1 6 2 2251.65 2322.97 27.36 o 2 6 2 3186.11 3348.80 24.90 o 3 6 2 657.60 662.36 20.52 o 4 6 2 2061.74 2197.77 21.30 o 5 6 2 6.76 17.32 17.17 o 6 6 2 3083.88 3241.15 25.71 o 7 6 2 925.04 971.12 21.92 o 8 6 2 3918.24 3943.99 42.17 o 9 6 2 670.86 664.99 20.09 o 10 6 2 1876.82 1798.83 38.00 o 11 6 2 1520.77 1431.45 36.12 o 12 6 2 1192.27 1056.06 27.40 o 1 7 2 592.25 596.42 19.55 o 2 7 2 6.68 7.71 17.46 o 3 7 2 563.36 567.69 23.40 o 4 7 2 433.96 433.93 21.78 o 5 7 2 3187.16 3171.34 34.38 o 6 7 2 338.96 335.25 19.83 o 7 7 2 442.73 423.82 20.10 o 8 7 2 1426.03 1318.79 27.51 o 9 7 2 263.84 284.29 26.09 o 0 8 2 3080.03 2778.32 33.93 o 1 8 2 590.48 568.39 23.64 o 2 8 2 897.97 929.52 31.20 o 3 8 2 376.00 356.33 23.73 o 4 8 2 2433.02 2430.58 101.11 o 5 8 2 17.97 18.99 20.82 o 1 0 3 30852.26 24492.23 260.46 o 2 0 3 12808.70 11536.66 161.16 o 3 0 3 2540.17 2101.43 92.50 o 4 0 3 4444.61 3956.89 82.94 o 5 0 3 38999.94 34708.11 259.78 o 6 0 3 1971.54 1887.08 91.62 o 7 0 3 1447.48 1425.09 56.96 o 8 0 3 2448.44 2512.83 59.50 o 9 0 3 5505.12 5811.93 72.99 o 10 0 3 524.23 548.69 47.08 o 11 0 3 3640.82 3784.45 60.94 o 12 0 3 1.42 -6.75 34.78 o 13 0 3 91.48 103.58 36.93 o 14 0 3 1688.52 1708.11 46.71 o 15 0 3 3697.54 3663.25 86.71 o 16 0 3 83.24 91.59 44.63 o 0 1 3 1172.25 1259.99 52.48 o 1 1 3 9696.44 9683.10 152.40 o 2 1 3 4856.19 4738.21 65.25 o 3 1 3 1117.96 1218.73 31.38 o 4 1 3 2126.23 2140.14 62.65 o 5 1 3 2242.87 2315.85 78.16 o 6 1 3 544.90 521.26 30.08 o 7 1 3 7920.89 7867.20 130.46 o 8 1 3 3613.67 3559.09 72.47 o 9 1 3 192.33 217.85 27.69 o 10 1 3 34.99 40.85 26.43 o 11 1 3 6618.39 6787.40 118.22 o 12 1 3 1158.32 1212.45 31.33 o 13 1 3 1246.90 1224.28 33.00 o 14 1 3 177.41 197.27 29.01 o 15 1 3 2918.56 2908.81 41.31 o 16 1 3 1.74 0.60 28.68 o 1 2 3 34016.81 33769.10 313.97 o 2 2 3 254.01 261.36 21.09 o 3 2 3 202.77 183.40 19.45 o 4 2 3 1845.15 1848.96 27.94 o 5 2 3 30656.06 29788.91 215.16 o 6 2 3 2379.23 2438.84 29.76 o 7 2 3 973.89 1049.44 25.74 o 8 2 3 144.38 146.51 24.76 o 9 2 3 9224.70 9038.32 151.35 o 10 2 3 492.35 496.62 25.95 o 11 2 3 1933.84 1974.79 25.85 o 12 2 3 137.55 149.57 25.50 o 13 2 3 78.30 85.98 28.97 o 14 2 3 1739.59 1803.35 35.05 o 15 2 3 2718.13 2735.93 46.02 o 16 2 3 133.53 136.24 31.79 o 0 3 3 180.99 240.87 24.33 o 1 3 3 6904.88 6893.93 55.36 o 2 3 3 8944.56 8968.88 41.02 o 3 3 3 57.67 64.28 19.07 o 4 3 3 49.00 82.21 17.88 o 5 3 3 867.49 903.23 24.24 o 6 3 3 733.50 797.32 21.19 o 7 3 3 4888.59 5114.09 33.05 o 8 3 3 3563.67 3689.14 39.48 o 9 3 3 99.90 108.90 21.59 o 10 3 3 43.77 53.62 20.61 o 11 3 3 6497.31 6496.06 49.38 o 12 3 3 324.30 360.38 26.28 o 13 3 3 998.74 963.85 24.68 o 14 3 3 37.21 48.74 24.05 o 15 3 3 1996.69 1839.89 57.82 o 1 4 3 16597.97 16815.45 90.92 o 2 4 3 1751.51 1822.43 19.26 o 3 4 3 796.16 776.63 18.08 o 4 4 3 1515.47 1565.90 24.74 o 5 4 3 18846.33 19062.37 164.27 o 6 4 3 1003.05 1065.36 21.52 o 7 4 3 776.50 799.17 19.41 o 8 4 3 765.36 790.80 20.59 o 9 4 3 4519.31 4775.36 49.22 o 10 4 3 3.83 -0.92 19.64 o 11 4 3 2027.03 2011.24 27.41 o 12 4 3 15.66 19.47 22.56 o 13 4 3 81.51 93.17 24.67 o 14 4 3 1221.45 1170.91 32.02 o 0 5 3 161.07 165.66 23.40 o 1 5 3 3443.48 3579.89 34.75 o 2 5 3 1323.99 1315.37 19.43 o 3 5 3 566.84 612.17 17.03 o 4 5 3 1912.65 1879.90 23.71 o 5 5 3 1068.87 1100.69 22.03 o 6 5 3 119.40 146.90 22.77 o 7 5 3 3706.29 3850.62 70.66 o 8 5 3 1595.79 1654.38 25.12 o 9 5 3 81.66 101.43 23.01 o 10 5 3 71.37 83.50 24.17 o 11 5 3 3052.85 3055.12 65.76 o 12 5 3 901.00 789.92 27.86 o 13 5 3 769.55 636.96 31.49 o 1 6 3 7950.03 8172.43 70.37 o 2 6 3 856.16 893.69 18.03 o 3 6 3 450.63 471.95 18.42 o 4 6 3 997.22 1062.13 24.55 o 5 6 3 10454.94 10613.36 108.15 o 6 6 3 467.00 501.06 19.06 o 7 6 3 561.32 612.16 20.10 o 8 6 3 454.99 472.48 20.28 o 9 6 3 2670.37 2658.89 35.91 o 10 6 3 8.27 7.50 20.47 o 11 6 3 1241.67 1066.69 25.69 o 0 7 3 62.80 70.24 26.54 o 1 7 3 1653.70 1618.84 22.71 o 2 7 3 2060.13 2080.62 29.38 o 3 7 3 38.68 40.75 20.44 o 4 7 3 0.20 13.77 18.43 o 5 7 3 251.87 256.98 20.67 o 6 7 3 235.74 246.81 22.18 o 7 7 3 1702.39 1604.95 48.18 o 8 7 3 1180.11 1069.80 25.73 o 9 7 3 62.18 61.29 19.88 o 1 8 3 4487.79 4083.37 74.32 o 2 8 3 67.71 55.86 19.97 o 3 8 3 129.54 165.26 23.36 o 4 8 3 327.19 279.67 21.11 o 0 0 4 17663.21 14698.41 189.04 o 1 0 4 859.45 774.86 79.88 o 2 0 4 20091.33 15374.17 590.32 o 3 0 4 5439.49 4847.08 157.93 o 4 0 4 11665.01 10972.43 788.97 o 5 0 4 41.86 31.69 46.70 o 6 0 4 3013.62 2789.63 66.81 o 7 0 4 38.34 79.01 69.01 o 8 0 4 21581.95 21950.91 175.77 o 9 0 4 2599.26 2660.84 61.48 o 10 0 4 26.87 59.68 64.29 o 11 0 4 225.44 274.27 54.73 o 12 0 4 4950.10 5230.63 295.19 o 13 0 4 980.06 966.60 128.35 o 14 0 4 775.17 788.72 94.83 o 15 0 4 74.38 66.19 40.74 o 16 0 4 0.03 25.03 45.65 o 1 1 4 6776.60 6409.56 246.64 o 2 1 4 1114.19 1002.88 33.53 o 3 1 4 3653.65 3351.92 118.93 o 4 1 4 9302.63 8749.43 340.70 o 5 1 4 1420.85 1382.13 50.86 o 6 1 4 1287.59 1281.84 41.85 o 7 1 4 3548.38 3514.40 70.93 o 8 1 4 5720.11 5622.40 93.99 o 9 1 4 2512.95 2545.37 91.82 o 10 1 4 2587.06 2631.81 84.09 o 11 1 4 395.73 408.40 30.89 o 12 1 4 104.60 109.27 33.72 o 13 1 4 682.01 705.81 34.58 o 14 1 4 7765.47 7971.94 327.35 o 15 1 4 215.50 205.39 31.99 o 16 1 4 329.56 328.88 44.47 o 0 2 4 2878.05 2933.01 42.65 o 1 2 4 1823.54 1914.51 32.52 o 2 2 4 32882.95 31847.21 195.90 o 3 2 4 38.22 34.33 19.78 o 4 2 4 4826.88 4756.38 68.75 o 5 2 4 2117.69 2135.44 41.15 o 6 2 4 5277.05 5489.48 126.68 o 7 2 4 663.32 713.32 29.46 o 8 2 4 13817.22 13945.02 263.03 o 9 2 4 1527.68 1507.11 32.51 o 10 2 4 4.95 29.48 26.30 o 11 2 4 55.59 65.39 24.03 o 12 2 4 4294.52 4448.04 102.68 o 13 2 4 1096.10 1106.12 36.33 o 14 2 4 723.66 754.40 37.67 o 15 2 4 663.50 679.10 38.08 o 1 3 4 2206.32 2220.35 25.21 o 2 3 4 522.02 526.27 19.85 o 3 3 4 4687.20 4830.81 33.30 o 4 3 4 4457.86 4469.80 65.23 o 5 3 4 2051.53 2168.67 28.22 o 6 3 4 210.33 258.32 31.09 o 7 3 4 2433.34 2581.57 28.87 o 8 3 4 3288.90 3540.44 38.96 o 9 3 4 518.11 572.71 27.20 o 10 3 4 3086.46 3299.31 35.59 o 11 3 4 768.35 783.37 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3413.68 3221.70 79.55 o 0 7 7 3281.75 2963.67 198.60 o 1 7 7 621.28 591.25 21.55 o 2 7 7 1194.63 1052.25 24.10 o 0 0 8 7129.40 6501.63 111.94 o 1 0 8 199.01 181.98 47.50 o 2 0 8 184.30 170.99 46.86 o 3 0 8 125.53 116.79 36.68 o 4 0 8 4732.34 4612.46 67.85 o 5 0 8 188.93 185.88 38.45 o 6 0 8 2079.73 2238.77 94.08 o 7 0 8 2518.05 2639.71 79.40 o 8 0 8 13.17 25.57 50.01 o 9 0 8 98.67 124.47 47.99 o 10 0 8 2169.48 2310.75 64.34 o 11 0 8 2283.66 2505.63 84.18 o 12 0 8 246.21 262.09 53.22 o 13 0 8 955.87 926.86 77.27 o 1 1 8 4404.84 4201.12 53.52 o 2 1 8 1605.93 1570.36 33.81 o 3 1 8 447.05 415.35 31.34 o 4 1 8 2282.29 2199.65 72.89 o 5 1 8 6026.90 5932.99 209.62 o 6 1 8 2755.26 2917.41 120.82 o 7 1 8 840.45 840.65 35.88 o 8 1 8 67.73 97.00 50.02 o 9 1 8 3100.79 3173.09 156.87 o 10 1 8 335.67 378.98 43.68 o 11 1 8 1769.84 1913.42 44.58 o 12 1 8 984.81 1094.32 56.32 o 13 1 8 314.81 326.07 54.52 o 0 2 8 7880.61 7560.72 88.28 o 1 2 8 799.33 743.43 37.30 o 2 2 8 1.37 8.76 31.29 o 3 2 8 88.75 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4 5 8 1041.71 1002.57 26.79 o 5 5 8 3408.29 3413.37 89.93 o 6 5 8 1660.97 1656.57 56.22 o 7 5 8 377.53 405.64 37.01 o 8 5 8 0.66 4.68 31.14 o 0 6 8 2982.61 3153.75 122.78 o 1 6 8 130.38 145.41 19.85 o 2 6 8 17.13 22.21 24.69 o 3 6 8 5.62 2.64 24.76 o 4 6 8 1299.86 1222.74 38.58 o 5 6 8 175.36 179.32 26.72 o 1 0 9 1403.19 1315.36 45.98 o 2 0 9 540.14 525.54 48.84 o 3 0 9 645.82 627.19 40.68 o 4 0 9 2976.11 3047.30 59.46 o 5 0 9 269.36 279.17 37.36 o 6 0 9 337.59 386.18 44.27 o 7 0 9 984.91 993.79 75.58 o 8 0 9 1562.30 1584.56 59.28 o 9 0 9 1027.18 1013.29 55.74 o 10 0 9 970.65 1039.42 77.60 o 11 0 9 0.47 -22.14 72.27 o 0 1 9 343.13 349.83 39.58 o 1 1 9 225.20 207.86 27.61 o 2 1 9 9704.12 8983.34 139.65 o 3 1 9 462.31 423.85 31.57 o 4 1 9 1590.37 1527.93 36.97 o 5 1 9 229.16 235.24 28.99 o 6 1 9 1684.65 1819.70 53.43 o 7 1 9 357.06 373.18 31.58 o 8 1 9 6632.81 6717.51 205.87 o 9 1 9 1346.02 1464.97 72.32 o 10 1 9 124.30 141.12 37.04 o 11 1 9 710.40 682.82 46.67 o 1 2 9 373.81 372.21 28.66 o 2 2 9 804.84 869.52 40.84 o 3 2 9 1848.61 1941.71 105.11 o 4 2 9 3174.54 3345.60 82.12 o 5 2 9 459.41 496.79 29.64 o 6 2 9 423.62 455.11 29.02 o 7 2 9 1000.06 1051.07 81.43 o 8 2 9 2090.74 2141.15 132.98 o 9 2 9 18.35 46.38 44.47 o 10 2 9 402.41 439.45 47.33 o 11 2 9 255.04 282.08 47.28 o 0 3 9 455.28 411.00 50.97 o 1 3 9 292.42 277.32 29.63 o 2 3 9 6667.82 6579.62 298.70 o 3 3 9 0.45 13.88 30.21 o 4 3 9 1954.59 2038.81 39.50 o 5 3 9 783.97 816.93 35.40 o 6 3 9 1173.68 1206.61 71.36 o 7 3 9 371.67 380.25 51.03 o 8 3 9 5518.14 5668.29 315.47 o 9 3 9 1139.25 1202.25 49.34 o 10 3 9 79.94 79.74 40.07 o 1 4 9 630.06 671.12 27.23 o 2 4 9 464.64 467.59 22.10 o 3 4 9 738.37 723.82 22.77 o 4 4 9 2077.17 2217.83 67.41 o 5 4 9 252.60 282.86 31.53 o 6 4 9 224.28 261.66 33.53 o 7 4 9 705.34 712.90 37.21 o 8 4 9 1262.34 1432.27 46.57 o 0 5 9 186.78 175.73 27.48 o 1 5 9 85.23 84.54 24.53 o 2 5 9 5689.86 5426.55 194.16 o 3 5 9 626.58 577.77 34.61 o 4 5 9 725.89 639.97 25.22 o 5 5 9 14.96 25.91 25.77 o 6 5 9 1147.53 981.29 63.31 o 0 0 10 126.39 126.72 46.30 o 1 0 10 1521.98 1471.19 53.58 o 2 0 10 2322.99 2213.77 73.05 o 3 0 10 394.93 357.55 42.43 o 4 0 10 618.57 577.26 47.36 o 5 0 10 875.06 877.59 49.05 o 6 0 10 223.05 239.54 43.84 o 7 0 10 1763.98 1687.95 62.15 o 8 0 10 789.10 843.81 75.97 o 9 0 10 25.67 4.89 75.86 o 10 0 10 262.99 253.49 76.93 o 1 1 10 8016.80 7507.85 161.67 o 2 1 10 2.04 18.57 33.07 o 3 1 10 2434.57 2341.97 51.80 o 4 1 10 404.78 448.10 31.80 o 5 1 10 8691.19 8641.66 170.62 o 6 1 10 27.73 49.85 26.98 o 7 1 10 1321.90 1339.73 61.83 o 8 1 10 399.46 451.40 55.05 o 9 1 10 2049.55 2190.67 158.24 o 0 2 10 138.98 114.13 54.73 o 1 2 10 713.19 730.55 41.48 o 2 2 10 1600.57 1564.19 46.09 o 3 2 10 9.51 22.35 31.06 o 4 2 10 207.21 197.20 30.96 o 5 2 10 112.85 121.02 28.59 o 6 2 10 63.91 86.06 35.77 o 7 2 10 1801.49 1880.15 100.73 o 8 2 10 1678.31 1719.32 99.38 o 9 2 10 5.67 24.76 34.55 o 1 3 10 7499.54 7289.62 161.92 o 2 3 10 56.56 59.49 38.49 o 3 3 10 1406.67 1402.82 57.11 o 4 3 10 493.47 487.06 35.45 o 5 3 10 7306.72 7355.51 340.73 o 6 3 10 230.12 246.90 39.31 o 7 3 10 859.03 803.72 63.53 o 8 3 10 345.34 370.45 44.74 o 0 4 10 1.70 7.18 39.01 o 1 4 10 795.78 762.23 29.41 o 2 4 10 1365.45 1345.99 46.20 o 3 4 10 58.16 60.41 24.88 o 4 4 10 306.84 293.31 29.00 o 5 4 10 330.77 358.27 36.91 o 6 4 10 118.91 140.85 33.63 o 1 5 10 4206.40 3903.28 172.81 o 1 0 11 760.69 743.85 43.24 o 2 0 11 174.71 176.16 48.95 o 3 0 11 230.06 239.41 49.52 o 4 0 11 423.85 395.75 48.20 o 5 0 11 1464.03 1419.23 54.93 o 6 0 11 218.69 246.09 48.63 o 7 0 11 11.57 -0.73 52.71 o 0 1 11 3931.71 3758.21 166.64 o 1 1 11 2619.95 2538.75 76.92 o 2 1 11 3998.64 4060.79 49.07 o 3 1 11 751.67 716.15 33.31 o 4 1 11 2829.78 2826.57 43.75 o 5 1 11 69.38 68.25 28.05 o 6 1 11 2609.89 2793.61 119.37 o 7 1 11 76.34 102.62 42.33 o 1 2 11 433.42 450.81 29.60 o 2 2 11 6.86 -3.80 29.25 o 3 2 11 181.11 189.29 35.43 o 4 2 11 231.59 255.64 29.71 o 5 2 11 2642.42 2587.10 59.48 o 6 2 11 806.64 838.23 40.47 o 0 3 11 2193.27 2102.61 70.64 o 1 3 11 1130.50 1026.42 46.89 o 2 3 11 3589.25 3380.49 130.26 o 3 3 11 392.09 422.80 35.10 o 4 3 11 2922.74 2687.49 55.55 o 5 3 11 162.29 162.28 31.16 o 0 0 12 298.20 310.42 73.89 o 1 0 12 796.07 738.90 46.81 o 2 0 12 318.84 350.62 50.84 o 3 0 12 545.16 563.37 45.25 o 4 0 12 22.02 39.17 45.43 o 1 1 12 1206.86 1185.82 46.55 o 2 1 12 5.79 14.57 35.79 o 3 1 12 4011.64 3806.80 68.36 o 0 2 12 220.42 180.31 44.59 o 1 2 12 26.37 54.44 35.16 o