#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181300 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237865.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237865_Fobs loop_ _publ_author_name 'McCormick, Cameron A.' 'Nguyen, Vu D.' 'Renfro, Heather E.' 'Koplitz, Lynn V.' 'Mague, Joel T.' _publ_section_title ; 4-Cyano-1-methylpyridinium nitrate ; _journal_coeditor_code HB7076 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o981 _journal_page_last o982 _journal_volume 69 _journal_year 2013 _space_group_IT_number 31 _symmetry_space_group_name_Hall 'P 2ac -2' _symmetry_space_group_name_H-M 'P m n 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1950 _cell_length_b 7.2890 _cell_length_c 6.7210 _exptl_crystal_F_000 188.00 _reflns_d_resolution_high 0.7301 _cod_data_source_file hb7076Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' F12073 - EXOR New: Pmn21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 60.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 -9 13.72 13.76 1.33 o 0 1 -9 14.88 11.59 1.19 o 1 1 -9 3.48 4.80 0.73 o 2 1 -9 7.56 8.99 1.05 o 0 0 -8 16.87 16.51 2.08 o 2 0 -8 1.78 1.47 0.32 o 4 0 -8 5.59 5.50 0.57 o 0 1 -8 1.02 0.59 0.21 o 1 1 -8 26.67 25.25 0.62 o 2 1 -8 9.91 10.05 0.43 o 3 1 -8 9.61 9.11 0.42 o 4 1 -8 16.52 16.18 0.63 o 5 1 -8 0.29 0.31 0.31 o 0 2 -8 36.54 34.58 1.22 o 1 2 -8 19.34 19.67 0.60 o 2 2 -8 44.44 43.99 0.92 o 3 2 -8 5.33 5.91 0.38 o 4 2 -8 60.09 62.71 1.87 o 5 2 -8 0.60 0.37 0.40 o 0 3 -8 1.92 2.42 0.31 o 1 3 -8 4.84 4.10 0.29 o 2 3 -8 17.99 17.56 0.59 o 3 3 -8 23.26 22.02 0.71 o 0 4 -8 16.54 15.97 1.96 o 1 4 -8 1.98 1.73 0.26 o 2 4 -8 11.50 10.46 0.72 o 3 4 -8 83.53 90.63 2.68 o 1 0 -7 154.97 142.61 2.16 o 3 0 -7 65.76 62.43 1.48 o 5 0 -7 101.07 95.38 7.55 o 0 1 -7 60.64 52.24 1.17 o 1 1 -7 2.22 1.89 0.20 o 2 1 -7 25.15 25.99 0.62 o 3 1 -7 11.00 9.84 0.41 o 4 1 -7 134.86 135.31 2.48 o 5 1 -7 3.03 2.85 0.37 o 6 1 -7 7.11 6.17 0.62 o 7 1 -7 0.69 1.21 0.51 o 0 2 -7 20.27 20.14 0.74 o 1 2 -7 8.85 10.37 0.38 o 2 2 -7 21.54 20.43 0.56 o 3 2 -7 28.10 26.91 0.65 o 4 2 -7 37.02 36.20 1.05 o 5 2 -7 8.02 7.89 0.41 o 6 2 -7 8.48 8.69 0.59 o 0 3 -7 32.22 29.55 0.91 o 1 3 -7 31.24 29.84 0.68 o 2 3 -7 17.51 16.47 0.50 o 3 3 -7 125.02 123.10 2.88 o 4 3 -7 87.78 82.85 3.79 o 5 3 -7 48.39 47.20 2.34 o 6 3 -7 3.31 3.45 0.73 o 0 4 -7 5.85 5.00 0.55 o 1 4 -7 0.66 0.38 0.15 o 2 4 -7 48.12 47.90 0.92 o 3 4 -7 2.46 2.94 0.23 o 4 4 -7 99.14 99.76 5.91 o 5 4 -7 3.30 3.14 0.76 o 0 5 -7 54.05 46.60 2.38 o 1 5 -7 14.92 13.93 0.56 o 2 5 -7 6.40 6.68 0.42 o 3 5 -7 7.93 8.33 0.91 o 4 5 -7 4.88 3.59 0.79 o 2 6 -7 0.89 1.02 0.42 o 0 0 -6 17.71 17.62 0.89 o 2 0 -6 75.81 75.13 1.27 o 4 0 -6 110.94 109.64 2.14 o 6 0 -6 21.24 20.31 2.25 o 8 0 -6 13.19 12.49 1.62 o 0 1 -6 33.00 28.54 0.79 o 1 1 -6 1.85 2.05 0.18 o 2 1 -6 45.01 43.14 0.73 o 3 1 -6 526.13 510.98 7.16 o 4 1 -6 37.04 36.22 0.81 o 5 1 -6 134.79 130.63 3.29 o 6 1 -6 18.95 19.45 0.66 o 7 1 -6 18.95 19.82 0.81 o 8 1 -6 13.45 16.63 0.78 o 0 2 -6 32.70 29.32 0.82 o 1 2 -6 82.82 72.80 0.90 o 2 2 -6 1.96 1.72 0.18 o 3 2 -6 121.49 116.24 2.21 o 4 2 -6 2.31 2.40 0.28 o 5 2 -6 74.71 75.62 2.04 o 6 2 -6 29.42 31.50 1.47 o 7 2 -6 27.30 29.37 0.85 o 8 2 -6 4.19 5.03 0.61 o 0 3 -6 30.84 35.60 0.91 o 1 3 -6 95.68 86.63 1.34 o 2 3 -6 13.42 15.09 0.62 o 3 3 -6 53.24 52.85 1.20 o 4 3 -6 10.07 9.50 0.82 o 5 3 -6 0.85 0.90 0.18 o 6 3 -6 11.42 11.23 0.40 o 7 3 -6 79.67 82.24 2.90 o 0 4 -6 7.38 7.62 0.52 o 1 4 -6 16.75 17.89 0.74 o 2 4 -6 0.71 0.41 0.15 o 3 4 -6 1.79 2.00 0.18 o 4 4 -6 2.95 2.88 0.29 o 5 4 -6 2.73 2.76 0.28 o 6 4 -6 1.44 0.98 0.19 o 7 4 -6 12.50 11.69 0.91 o 0 5 -6 0.14 0.19 0.27 o 1 5 -6 59.00 53.05 1.26 o 2 5 -6 3.67 3.58 0.30 o 3 5 -6 2.13 2.27 0.36 o 4 5 -6 5.02 5.20 0.78 o 5 5 -6 5.52 4.65 0.46 o 6 5 -6 0.02 0.08 0.16 o 0 6 -6 2.09 1.58 0.48 o 1 6 -6 1.55 1.52 0.33 o 2 6 -6 18.97 21.26 0.91 o 3 6 -6 20.51 23.55 1.26 o 4 6 -6 52.71 49.36 6.52 o 5 6 -6 9.26 9.69 0.85 o 0 7 -6 1.60 2.34 0.48 o 1 7 -6 5.44 4.32 0.68 o 2 7 -6 0.34 0.09 0.15 o 3 7 -6 6.98 7.91 0.99 o 1 0 -5 56.77 52.79 0.97 o 3 0 -5 177.25 171.58 4.98 o 5 0 -5 56.49 56.22 3.10 o 7 0 -5 5.04 4.43 0.45 o 9 0 -5 46.96 49.45 1.85 o 0 1 -5 220.33 226.66 2.00 o 1 1 -5 217.00 210.27 2.64 o 2 1 -5 130.27 128.06 2.02 o 3 1 -5 217.38 212.15 3.81 o 4 1 -5 485.49 495.26 9.60 o 5 1 -5 129.64 125.62 3.43 o 6 1 -5 19.72 17.52 0.65 o 7 1 -5 62.13 58.89 1.36 o 8 1 -5 14.11 12.03 0.53 o 9 1 -5 45.70 48.12 1.29 o 0 2 -5 6.41 5.46 0.33 o 1 2 -5 4.24 3.91 0.21 o 2 2 -5 6.25 5.93 0.23 o 3 2 -5 37.60 36.06 0.58 o 4 2 -5 14.40 12.82 0.40 o 5 2 -5 21.47 21.65 0.56 o 6 2 -5 2.58 2.31 0.24 o 7 2 -5 6.33 5.68 0.34 o 8 2 -5 5.17 3.77 0.32 o 9 2 -5 11.50 14.36 1.01 o 0 3 -5 253.23 229.06 5.99 o 1 3 -5 9.21 9.83 0.29 o 2 3 -5 4.11 4.57 0.21 o 3 3 -5 59.35 56.18 1.10 o 4 3 -5 106.59 110.22 1.66 o 5 3 -5 17.06 17.40 0.68 o 6 3 -5 33.90 33.38 0.67 o 7 3 -5 0.93 1.05 0.23 o 8 3 -5 38.50 40.20 1.86 o 0 4 -5 24.50 19.85 1.10 o 1 4 -5 55.17 47.49 1.35 o 2 4 -5 20.85 18.25 0.49 o 3 4 -5 58.05 55.47 1.15 o 4 4 -5 19.84 21.12 0.75 o 5 4 -5 54.68 54.85 1.24 o 6 4 -5 23.36 24.85 0.71 o 7 4 -5 24.47 25.31 0.95 o 0 5 -5 47.59 41.72 2.44 o 1 5 -5 0.54 0.45 0.14 o 2 5 -5 0.85 0.75 0.18 o 3 5 -5 25.82 26.67 2.00 o 4 5 -5 16.00 15.35 1.13 o 5 5 -5 3.18 3.67 0.31 o 6 5 -5 4.85 5.12 0.36 o 7 5 -5 1.97 2.42 0.25 o 0 6 -5 0.41 0.10 0.19 o 1 6 -5 17.49 16.63 0.71 o 2 6 -5 8.47 8.14 0.44 o 3 6 -5 15.95 16.84 0.83 o 4 6 -5 14.91 14.68 0.67 o 5 6 -5 3.68 4.10 0.38 o 6 6 -5 1.09 1.17 0.30 o 0 7 -5 32.53 28.73 1.26 o 1 7 -5 2.51 2.17 0.30 o 2 7 -5 37.60 37.83 1.03 o 3 7 -5 15.50 15.72 0.83 o 4 7 -5 27.24 26.27 2.28 o 0 8 -5 34.77 29.60 2.12 o 1 8 -5 15.90 15.57 1.53 o 2 8 -5 17.18 17.67 0.79 o 0 0 -4 6.29 7.03 0.34 o 2 0 -4 22.21 17.38 0.46 o 4 0 -4 52.80 55.62 1.20 o 6 0 -4 18.02 14.28 0.69 o 8 0 -4 0.01 0.26 0.19 o 0 1 -4 9.60 9.64 0.30 o 1 1 -4 561.33 620.16 6.99 o 2 1 -4 1.29 1.04 0.10 o 3 1 -4 109.63 108.89 1.14 o 4 1 -4 7.54 6.75 0.25 o 5 1 -4 7.76 8.06 0.35 o 6 1 -4 4.45 4.55 0.29 o 7 1 -4 224.88 201.94 2.82 o 8 1 -4 0.53 0.50 0.15 o 9 1 -4 8.23 6.58 0.40 o 0 2 -4 2.82 3.44 0.19 o 1 2 -4 49.04 53.14 1.05 o 2 2 -4 12.57 13.26 0.42 o 3 2 -4 129.58 130.43 2.08 o 4 2 -4 47.13 51.67 1.15 o 5 2 -4 29.50 29.12 0.72 o 6 2 -4 8.50 9.05 0.37 o 7 2 -4 4.91 4.58 0.29 o 8 2 -4 2.82 3.57 0.28 o 9 2 -4 19.20 21.16 0.70 o 0 3 -4 70.13 76.13 2.21 o 1 3 -4 14.19 14.07 0.31 o 2 3 -4 204.30 205.22 3.17 o 3 3 -4 473.73 469.06 6.61 o 4 3 -4 305.33 311.88 7.92 o 5 3 -4 149.48 143.74 2.49 o 6 3 -4 26.16 26.56 0.54 o 7 3 -4 4.13 3.78 0.32 o 8 3 -4 21.74 23.27 0.78 o 9 3 -4 22.78 25.57 0.85 o 0 4 -4 25.27 23.23 0.84 o 1 4 -4 12.74 12.51 0.32 o 2 4 -4 20.03 19.43 0.52 o 3 4 -4 63.48 63.13 0.94 o 4 4 -4 54.57 54.46 1.51 o 5 4 -4 3.87 4.18 0.30 o 6 4 -4 7.86 8.10 0.40 o 7 4 -4 16.31 16.30 0.64 o 8 4 -4 6.59 5.88 0.48 o 9 4 -4 9.58 12.09 1.27 o 0 5 -4 33.52 27.79 1.95 o 1 5 -4 64.58 59.00 1.42 o 2 5 -4 92.86 95.78 2.26 o 3 5 -4 3.10 2.90 0.24 o 4 5 -4 174.47 181.51 4.23 o 5 5 -4 1.79 1.93 0.25 o 6 5 -4 11.55 11.67 0.51 o 7 5 -4 36.11 41.34 0.92 o 8 5 -4 9.74 11.36 1.31 o 0 6 -4 57.45 57.63 6.22 o 1 6 -4 96.86 90.81 2.06 o 2 6 -4 14.48 13.21 0.54 o 3 6 -4 17.57 18.13 0.70 o 4 6 -4 32.44 33.35 0.92 o 5 6 -4 29.95 29.91 0.93 o 6 6 -4 9.18 9.85 0.54 o 7 6 -4 70.88 81.58 4.39 o 0 7 -4 62.60 57.87 1.72 o 1 7 -4 7.40 7.63 0.45 o 2 7 -4 0.81 0.71 0.19 o 3 7 -4 11.01 11.10 0.52 o 4 7 -4 12.14 12.71 0.64 o 5 7 -4 9.24 9.07 0.62 o 0 8 -4 150.52 130.41 11.55 o 1 8 -4 39.58 35.51 1.02 o 2 8 -4 24.50 24.12 1.12 o 3 8 -4 0.69 0.97 0.28 o 4 8 -4 0.85 0.58 0.26 o 1 0 -3 72.64 78.62 2.41 o 3 0 -3 340.39 389.84 4.21 o 5 0 -3 121.89 139.14 2.16 o 7 0 -3 5.49 6.66 0.49 o 9 0 -3 6.79 7.14 0.67 o 0 1 -3 989.96 1180.74 26.13 o 1 1 -3 161.91 182.04 2.91 o 2 1 -3 7.96 8.78 0.23 o 3 1 -3 9.64 9.26 0.31 o 4 1 -3 54.59 50.08 2.68 o 5 1 -3 12.85 8.79 1.00 o 6 1 -3 35.64 28.32 0.63 o 7 1 -3 34.39 31.15 0.70 o 8 1 -3 75.25 66.31 1.30 o 9 1 -3 2.04 1.60 0.23 o 10 1 -3 1.32 1.23 0.21 o 0 2 -3 118.70 132.97 2.92 o 1 2 -3 74.91 69.80 1.19 o 2 2 -3 18.85 18.57 0.40 o 3 2 -3 208.66 226.85 3.39 o 4 2 -3 57.04 60.48 1.04 o 5 2 -3 87.72 90.32 1.69 o 6 2 -3 10.94 8.14 0.56 o 7 2 -3 11.99 14.75 0.47 o 8 2 -3 4.70 3.21 0.26 o 9 2 -3 1.42 1.58 0.22 o 10 2 -3 13.06 14.89 1.47 o 0 3 -3 571.74 594.78 21.63 o 1 3 -3 49.96 53.31 1.42 o 2 3 -3 108.98 116.42 2.75 o 3 3 -3 234.25 250.80 4.20 o 4 3 -3 73.29 71.80 1.26 o 5 3 -3 30.42 32.45 1.72 o 6 3 -3 79.48 70.30 4.55 o 7 3 -3 31.70 29.84 0.83 o 8 3 -3 83.82 84.56 1.65 o 9 3 -3 18.34 21.51 0.89 o 0 4 -3 184.30 187.71 4.10 o 1 4 -3 129.11 134.25 3.39 o 2 4 -3 9.48 8.77 0.27 o 3 4 -3 37.24 38.61 0.81 o 4 4 -3 54.86 55.62 1.72 o 5 4 -3 16.54 16.40 0.43 o 6 4 -3 42.77 42.51 1.33 o 7 4 -3 43.93 42.85 3.26 o 8 4 -3 12.14 11.35 1.14 o 9 4 -3 11.42 14.12 0.62 o 0 5 -3 29.30 29.81 0.85 o 1 5 -3 40.87 39.88 0.78 o 2 5 -3 129.94 126.98 2.44 o 3 5 -3 368.77 365.49 5.69 o 4 5 -3 261.13 262.94 5.95 o 5 5 -3 76.56 72.61 3.95 o 6 5 -3 46.13 47.15 1.54 o 7 5 -3 21.70 18.94 1.29 o 8 5 -3 13.21 13.30 0.67 o 0 6 -3 337.17 306.43 10.19 o 1 6 -3 171.50 169.50 1.68 o 2 6 -3 38.70 39.61 0.73 o 3 6 -3 14.25 13.68 0.49 o 4 6 -3 2.09 1.92 0.28 o 5 6 -3 23.27 24.02 0.67 o 6 6 -3 129.37 126.27 5.76 o 7 6 -3 83.85 83.54 1.46 o 8 6 -3 60.10 66.65 2.62 o 0 7 -3 14.69 14.96 0.88 o 1 7 -3 42.80 43.48 1.02 o 2 7 -3 18.62 18.40 0.63 o 3 7 -3 39.32 38.63 0.95 o 4 7 -3 31.55 32.76 1.22 o 5 7 -3 2.06 1.56 0.27 o 6 7 -3 4.41 5.22 0.39 o 7 7 -3 46.30 43.35 2.57 o 0 8 -3 24.44 20.32 1.07 o 1 8 -3 28.79 25.76 0.83 o 2 8 -3 2.15 2.33 0.28 o 3 8 -3 55.35 56.62 1.38 o 4 8 -3 15.49 15.30 0.73 o 5 8 -3 35.64 35.34 2.35 o 0 9 -3 4.85 5.37 0.93 o 1 9 -3 4.40 4.17 0.45 o 2 9 -3 3.07 2.23 0.32 o 3 9 -3 12.94 13.20 1.27 o 0 0 -2 1002.30 1121.30 17.28 o 2 0 -2 249.82 265.29 4.19 o 4 0 -2 899.84 1084.24 60.69 o 6 0 -2 31.33 24.15 6.27 o 8 0 -2 27.39 19.79 5.50 o 10 0 -2 49.32 64.86 1.60 o 0 1 -2 240.04 286.36 8.88 o 1 1 -2 326.78 323.95 5.40 o 2 1 -2 385.38 421.06 4.92 o 3 1 -2 109.76 108.46 4.08 o 4 1 -2 205.72 169.22 24.96 o 5 1 -2 39.93 35.20 6.19 o 6 1 -2 48.59 36.51 6.69 o 7 1 -2 38.84 30.63 5.71 o 8 1 -2 17.51 14.98 2.48 o 9 1 -2 39.80 42.08 0.86 o 10 1 -2 25.29 24.06 1.42 o 0 2 -2 623.74 696.26 15.44 o 1 2 -2 286.78 312.62 8.69 o 2 2 -2 45.21 51.05 1.14 o 3 2 -2 59.15 57.86 2.83 o 4 2 -2 418.88 466.25 18.75 o 5 2 -2 34.12 32.16 0.88 o 6 2 -2 20.98 18.69 2.67 o 7 2 -2 70.49 51.66 6.68 o 8 2 -2 31.70 34.92 0.86 o 9 2 -2 4.23 3.83 0.40 o 10 2 -2 29.85 35.44 1.06 o 0 3 -2 739.39 784.77 73.54 o 1 3 -2 196.72 200.92 2.69 o 2 3 -2 24.13 28.47 0.53 o 3 3 -2 1.54 0.93 0.09 o 4 3 -2 11.49 11.95 0.46 o 5 3 -2 1.38 2.12 0.13 o 6 3 -2 92.22 74.83 6.08 o 7 3 -2 23.89 17.76 1.38 o 8 3 -2 56.19 47.06 4.41 o 9 3 -2 15.06 15.57 0.66 o 10 3 -2 8.12 8.84 1.02 o 0 4 -2 925.11 1030.26 37.04 o 1 4 -2 731.75 794.45 15.16 o 2 4 -2 141.94 147.41 2.45 o 3 4 -2 32.89 32.86 0.65 o 4 4 -2 10.75 9.80 0.52 o 5 4 -2 122.20 120.54 3.54 o 6 4 -2 127.61 130.66 4.63 o 7 4 -2 277.60 283.05 5.38 o 8 4 -2 117.45 108.87 12.24 o 9 4 -2 24.27 23.81 2.46 o 0 5 -2 294.05 301.00 5.75 o 1 5 -2 17.33 15.15 0.39 o 2 5 -2 10.54 9.19 0.28 o 3 5 -2 39.00 37.05 0.74 o 4 5 -2 46.44 49.97 1.42 o 5 5 -2 14.75 15.41 0.43 o 6 5 -2 57.12 56.63 1.16 o 7 5 -2 7.07 6.64 0.30 o 8 5 -2 29.64 28.57 0.95 o 9 5 -2 0.46 0.45 0.19 o 0 6 -2 25.04 24.27 0.81 o 1 6 -2 33.50 35.06 0.69 o 2 6 -2 5.71 5.51 0.27 o 3 6 -2 138.97 133.80 3.00 o 4 6 -2 34.45 35.49 0.85 o 5 6 -2 24.95 22.69 1.24 o 6 6 -2 2.61 2.25 0.26 o 7 6 -2 25.97 26.16 0.66 o 8 6 -2 6.81 6.99 0.43 o 0 7 -2 29.75 27.57 1.15 o 1 7 -2 12.48 12.92 0.47 o 2 7 -2 122.40 117.46 3.35 o 3 7 -2 129.44 130.57 1.77 o 4 7 -2 196.01 191.08 6.71 o 5 7 -2 59.51 59.43 1.83 o 6 7 -2 13.87 13.41 0.60 o 7 7 -2 1.21 1.07 0.54 o 0 8 -2 1.62 2.00 0.42 o 1 8 -2 3.59 3.26 0.32 o 2 8 -2 0.42 0.43 0.14 o 3 8 -2 26.41 26.03 0.73 o 4 8 -2 4.26 4.39 0.37 o 5 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179.16 3.64 o 5 0 5 56.66 58.32 1.05 o 7 0 5 4.95 4.35 0.62 o 9 0 5 47.03 53.39 2.97 o 0 1 5 220.21 234.93 5.86 o 1 1 5 216.84 223.10 3.87 o 2 1 5 130.17 129.38 1.06 o 3 1 5 217.21 209.60 3.72 o 4 1 5 485.18 494.56 8.52 o 5 1 5 129.50 127.08 3.48 o 6 1 5 19.73 19.22 0.46 o 7 1 5 62.04 58.83 1.29 o 8 1 5 14.07 11.73 0.74 o 9 1 5 45.63 46.99 10.08 o 0 2 5 6.46 6.04 0.33 o 1 2 5 4.18 3.88 0.21 o 2 2 5 6.28 5.94 0.26 o 3 2 5 37.82 34.74 1.25 o 4 2 5 14.44 13.01 0.36 o 5 2 5 21.52 22.38 0.70 o 6 2 5 2.61 2.26 0.18 o 7 2 5 6.30 6.29 0.29 o 8 2 5 5.19 4.60 0.29 o 0 3 5 252.99 241.65 2.66 o 1 3 5 9.17 10.20 0.34 o 2 3 5 4.11 4.45 0.25 o 3 3 5 59.29 57.48 0.84 o 4 3 5 106.61 109.49 1.91 o 5 3 5 17.02 17.63 0.43 o 6 3 5 33.84 31.67 2.40 o 7 3 5 0.92 0.87 0.13 o 8 3 5 38.42 40.34 0.82 o 0 4 5 24.57 21.33 0.71 o 1 4 5 55.35 48.67 0.80 o 2 4 5 20.92 19.37 0.56 o 3 4 5 58.08 57.33 1.34 o 4 4 5 19.84 21.94 0.55 o 5 4 5 54.72 55.99 1.15 o 6 4 5 23.43 25.79 0.59 o 7 4 5 24.60 27.48 0.55 o 8 4 5 5.61 8.48 1.13 o 0 5 5 47.58 42.93 1.04 o 1 5 5 0.54 0.51 0.16 o 2 5 5 0.85 0.76 0.19 o 3 5 5 25.88 27.63 0.76 o 4 5 5 15.97 16.85 0.66 o 5 5 5 3.20 3.83 0.28 o 6 5 5 4.86 5.60 0.30 o 7 5 5 1.96 2.85 0.33 o 0 6 5 0.42 0.44 0.21 o 1 6 5 17.49 18.88 0.72 o 2 6 5 8.46 8.68 0.46 o 3 6 5 15.95 16.30 0.69 o 4 6 5 14.86 14.17 0.64 o 5 6 5 3.68 3.78 0.34 o 6 6 5 1.10 1.35 0.24 o 0 7 5 32.51 33.88 1.47 o 1 7 5 2.51 2.45 0.32 o 2 7 5 37.66 38.69 1.10 o 3 7 5 15.56 14.73 0.81 o 4 7 5 27.35 27.06 0.90 o 0 8 5 34.69 33.13 1.51 o 1 8 5 15.92 16.66 1.07 o 2 8 5 17.14 19.64 1.58 o 0 0 6 17.60 19.03 0.95 o 2 0 6 76.02 77.02 2.19 o 4 0 6 111.58 113.61 1.64 o 6 0 6 21.20 21.62 0.83 o 8 0 6 13.15 11.78 1.36 o 0 1 6 32.93 30.87 0.85 o 1 1 6 1.86 1.78 0.21 o 2 1 6 44.89 42.55 1.12 o 3 1 6 525.76 533.06 3.52 o 4 1 6 36.93 36.92 0.72 o 5 1 6 134.67 140.70 1.40 o 6 1 6 18.88 19.30 0.67 o 7 1 6 18.96 20.75 0.55 o 8 1 6 13.41 14.92 0.64 o 0 2 6 32.90 29.69 0.99 o 1 2 6 82.93 73.19 1.00 o 2 2 6 1.96 1.92 0.21 o 3 2 6 121.70 122.53 1.22 o 4 2 6 2.36 2.32 0.22 o 5 2 6 74.82 72.90 3.08 o 6 2 6 29.46 32.91 0.66 o 7 2 6 27.35 30.20 1.54 o 8 2 6 4.25 5.29 0.48 o 0 3 6 30.82 37.30 1.14 o 1 3 6 95.56 87.97 1.26 o 2 3 6 13.40 15.59 0.49 o 3 3 6 53.26 54.10 0.97 o 4 3 6 10.05 10.17 0.40 o 5 3 6 0.86 0.83 0.16 o 6 3 6 11.41 9.79 1.16 o 7 3 6 79.56 83.76 1.37 o 0 4 6 7.47 8.02 0.57 o 1 4 6 16.74 18.66 0.59 o 2 4 6 0.71 0.76 0.19 o 3 4 6 1.79 1.59 0.25 o 4 4 6 2.96 3.28 0.27 o 5 4 6 2.72 2.84 0.26 o 6 4 6 1.45 1.29 0.21 o 7 4 6 12.50 10.43 1.24 o 0 5 6 0.13 0.13 0.17 o 1 5 6 58.94 57.08 1.44 o 2 5 6 3.69 3.68 0.33 o 3 5 6 2.14 2.73 0.29 o 4 5 6 5.03 5.94 0.44 o 5 5 6 5.53 5.61 0.42 o 6 5 6 0.01 0.13 0.19 o 0 6 6 2.11 1.58 0.59 o 1 6 6 1.56 1.34 0.25 o 2 6 6 18.94 21.79 0.76 o 3 6 6 20.53 23.48 0.88 o 4 6 6 52.63 54.49 2.11 o 0 7 6 1.60 2.68 0.79 o 1 7 6 5.45 5.45 0.46 o 2 7 6 0.34 0.17 0.18 o 1 0 7 155.36 157.48 2.98 o 3 0 7 65.75 67.47 1.38 o 5 0 7 101.11 104.63 2.00 o 7 0 7 89.07 107.47 4.13 o 0 1 7 60.55 55.28 1.86 o 1 1 7 2.23 1.96 0.28 o 2 1 7 25.13 28.32 1.00 o 3 1 7 10.98 10.69 0.43 o 4 1 7 134.77 141.08 1.81 o 5 1 7 3.03 2.72 0.25 o 6 1 7 7.11 7.25 0.38 o 7 1 7 0.70 0.85 0.40 o 0 2 7 20.26 20.25 1.15 o 1 2 7 8.81 10.70 0.52 o 2 2 7 21.61 21.55 0.71 o 3 2 7 28.24 28.10 0.75 o 4 2 7 37.14 39.18 0.82 o 5 2 7 8.07 8.51 0.39 o 6 2 7 8.48 8.69 0.42 o 0 3 7 32.21 30.21 1.41 o 1 3 7 31.23 31.23 0.89 o 2 3 7 17.45 17.98 0.72 o 3 3 7 124.87 130.65 1.95 o 4 3 7 87.62 88.61 1.36 o 5 3 7 48.33 48.83 0.93 o 6 3 7 3.30 3.25 0.40 o 0 4 7 5.84 5.09 0.73 o 1 4 7 0.68 0.32 0.17 o 2 4 7 48.13 54.32 1.19 o 3 4 7 2.45 3.15 0.33 o 4 4 7 99.18 104.62 2.22 o 5 4 7 3.27 2.62 0.47 o 0 5 7 53.97 48.06 2.72 o 1 5 7 14.87 15.10 0.74 o 2 5 7 6.39 7.32 0.48 o 3 5 7 7.93 8.49 0.49 o 0 6 7 32.50 34.69 2.37 o 1 6 7 0.16 0.23 0.37 o 2 6 7 0.89 0.84 0.23 o 0 0 8 16.92 15.85 1.53 o 2 0 8 1.79 1.32 0.31 o 4 0 8 5.61 6.61 0.56 o 0 1 8 1.02 0.96 0.51 o 1 1 8 26.66 27.13 1.01 o 2 1 8 9.92 11.07 0.57 o 3 1 8 9.60 9.16 0.47 o 4 1 8 16.52 18.53 0.65 o 5 1 8 0.29 0.40 0.24 o 0 2 8 36.69 35.17 1.63 o 1 2 8 19.40 20.80 1.04 o 2 2 8 44.44 46.97 1.67 o 3 2 8 5.31 6.56 0.44 o 4 2 8 59.98 69.13 1.46 o 5 2 8 0.61 0.53 0.42 o 0 3 8 1.92 2.41 0.71 o 1 3 8 4.85 4.13 0.42 o 2 3 8 17.97 19.06 0.85 o 3 3 8 23.29 22.57 0.81 o 0 4 8 16.53 18.61 1.19 o 1 4 8 1.97 1.73 0.44 o 2 4 8 11.56 10.51 0.73 o 3 4 8 83.56 95.14 3.51 o