#------------------------------------------------------------------------------
#$Date: 2016-04-03 06:50:42 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181300 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237886.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2237886_Fobs
loop_
_publ_author_name
'Xu, Shan-Shan'
'Mi, Jun-Long'
'Chen, Hong-Ji'
_publ_section_title
;
Poly[tetraaqua(5-hydroxypyridin-1-ium-3-carboxylato-\kO^3^)tris(\m-oxalato-\k^4^O^1^,O^2^:O^1'^,O^2'^)dieuropium(III)]
;
_journal_coeditor_code HY2623
_journal_issue 5
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m294
_journal_page_last m295
_journal_volume 69
_journal_year 2013
_space_group_IT_number 2
_symmetry_space_group_name_Hall '-P 1'
_symmetry_space_group_name_H-M 'P -1'
_cell_angle_alpha 103.493
_cell_angle_beta 98.589
_cell_angle_gamma 92.240
_cell_length_a 7.5912
_cell_length_b 8.0973
_cell_length_c 10.6706
_exptl_crystal_F_000 442.00
_reflns_d_resolution_high 0.7224
_cod_data_source_file hy2623Isup2.hkl
_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' Eu in P-1'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 152.26
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 942.19 919.68 30.59 o
2 0 0 16405.85 17013.51 258.68 o
3 0 0 7719.46 7679.03 98.28 o
4 0 0 4168.20 4343.01 70.96 o
5 0 0 4210.47 4256.40 73.77 o
6 0 0 43.86 59.21 9.21 o
7 0 0 2202.04 2283.03 57.55 o
8 0 0 1102.57 1082.02 52.11 o
9 0 0 819.99 811.22 68.15 o
-9 1 0 1202.01 1205.40 102.39 o
-8 1 0 2728.56 2702.05 78.76 o
-7 1 0 424.81 387.51 27.56 o
-6 1 0 4696.67 4525.51 104.68 o
-5 1 0 1090.03 1078.40 29.92 o
-4 1 0 3848.84 3775.47 66.61 o
-3 1 0 12131.44 12255.90 194.29 o
-2 1 0 1064.85 1134.50 31.59 o
-1 1 0 20614.42 21310.26 448.49 o
0 1 0 1014.59 1038.00 28.19 o
1 1 0 12656.31 12799.87 221.30 o
2 1 0 4055.27 4143.85 60.03 o
3 1 0 66.60 59.56 5.69 o
4 1 0 8809.85 8688.93 110.83 o
5 1 0 69.31 77.41 7.14 o
6 1 0 4172.45 4229.33 128.15 o
7 1 0 2865.71 2807.09 63.18 o
8 1 0 169.12 171.52 40.14 o
9 1 0 1806.45 1803.08 103.29 o
-9 2 0 2099.15 2101.04 72.86 o
-8 2 0 40.34 27.31 12.89 o
-7 2 0 4785.88 4708.88 131.36 o
-6 2 0 1345.28 1427.12 53.75 o
-5 2 0 4550.54 4565.81 75.27 o
-4 2 0 5428.48 5431.50 89.31 o
-3 2 0 1959.75 2120.24 40.23 o
-2 2 0 13050.76 13025.34 235.43 o
-1 2 0 28.84 25.58 3.56 o
0 2 0 1143.69 1098.42 24.90 o
1 2 0 11933.53 11612.82 202.21 o
2 2 0 893.05 836.44 16.52 o
3 2 0 15645.79 15592.78 247.79 o
4 2 0 2789.63 2944.65 50.30 o
5 2 0 6330.78 6490.21 95.90 o
6 2 0 4124.82 4157.11 77.23 o
7 2 0 153.91 200.15 23.02 o
8 2 0 2526.12 2619.92 123.01 o
9 2 0 172.24 141.88 55.09 o
-9 3 0 47.59 14.49 16.60 o
-8 3 0 1073.60 1066.17 59.56 o
-7 3 0 2186.27 2126.39 92.39 o
-6 3 0 1981.55 1997.83 83.29 o
-5 3 0 4380.20 4515.70 84.76 o
-4 3 0 23.37 37.83 6.01 o
-3 3 0 14368.92 15065.31 235.58 o
-2 3 0 1882.18 1854.79 40.27 o
-1 3 0 8792.43 8703.02 105.99 o
0 3 0 7765.69 7528.48 91.97 o
1 3 0 2067.96 2210.21 32.15 o
2 3 0 11158.59 11230.61 135.05 o
3 3 0 3713.21 3623.31 56.06 o
4 3 0 158.58 137.09 12.51 o
5 3 0 2451.85 2354.16 49.34 o
6 3 0 52.60 46.57 12.27 o
7 3 0 3607.54 3601.49 115.25 o
8 3 0 527.70 481.09 85.16 o
9 3 0 1101.51 1143.24 109.96 o
-9 4 0 2186.39 2323.36 130.42 o
-8 4 0 2512.47 2636.18 113.59 o
-7 4 0 279.11 282.13 34.74 o
-6 4 0 4633.38 4740.95 243.02 o
-5 4 0 97.77 89.17 13.48 o
-4 4 0 12562.02 13016.39 166.02 o
-3 4 0 3442.13 3387.69 80.08 o
-2 4 0 4093.80 4123.77 61.99 o
-1 4 0 7804.81 7452.81 100.13 o
0 4 0 19.88 30.39 3.31 o
1 4 0 6280.17 6316.42 79.42 o
2 4 0 2049.79 2071.83 39.96 o
3 4 0 2668.17 2693.88 39.99 o
4 4 0 2745.71 2751.20 70.12 o
5 4 0 149.24 150.71 15.16 o
6 4 0 4052.62 4215.16 139.19 o
7 4 0 630.74 538.32 42.71 o
8 4 0 1644.88 1742.67 82.39 o
-9 5 0 1240.62 1226.84 112.63 o
-8 5 0 1159.00 1138.65 73.38 o
-7 5 0 2417.95 2488.82 107.63 o
-6 5 0 930.87 971.00 58.10 o
-5 5 0 3068.42 3205.93 87.28 o
-4 5 0 2805.19 2900.89 94.70 o
-3 5 0 614.49 626.47 18.33 o
-2 5 0 5807.18 5805.69 74.82 o
-1 5 0 1344.45 1451.08 29.57 o
0 5 0 6084.19 5940.70 83.62 o
1 5 0 679.75 681.23 16.83 o
2 5 0 4013.90 4102.67 55.44 o
3 5 0 4942.59 4957.15 71.09 o
4 5 0 105.27 127.79 9.33 o
5 5 0 3920.32 3772.30 83.10 o
6 5 0 1649.63 1612.91 69.73 o
7 5 0 447.18 511.39 40.45 o
8 5 0 1516.77 1483.63 133.21 o
-8 6 0 1953.20 2046.39 102.46 o
-7 6 0 3.52 -25.41 25.41 o
-6 6 0 2195.70 2128.16 93.83 o
-5 6 0 2017.93 2078.86 88.32 o
-4 6 0 1177.62 1124.77 41.00 o
-3 6 0 4571.70 4554.47 89.59 o
-2 6 0 160.07 157.02 11.65 o
-1 6 0 5833.98 5911.86 93.47 o
0 6 0 2484.20 2525.75 40.32 o
1 6 0 1661.84 1697.31 32.25 o
2 6 0 1250.10 1198.63 30.08 o
3 6 0 484.86 501.51 19.74 o
4 6 0 1953.52 2025.04 66.34 o
5 6 0 894.42 913.32 45.64 o
6 6 0 393.06 392.52 34.78 o
7 6 0 1905.36 1941.89 85.10 o
-8 7 0 300.73 298.31 58.96 o
-7 7 0 1721.95 1908.49 96.57 o
-6 7 0 1311.94 1381.87 93.28 o
-5 7 0 137.38 127.93 20.65 o
-4 7 0 2264.59 2348.50 91.42 o
-3 7 0 47.04 59.24 13.31 o
-2 7 0 2799.42 2879.17 70.76 o
-1 7 0 2831.26 2859.25 52.31 o
0 7 0 80.86 81.67 5.98 o
1 7 0 1479.66 1466.85 34.08 o
2 7 0 1333.42 1350.88 31.80 o
3 7 0 2038.70 1972.76 78.06 o
4 7 0 2225.53 2257.16 141.08 o
5 7 0 420.71 505.51 44.27 o
6 7 0 2635.29 2493.59 283.00 o
-6 8 0 302.80 238.48 61.82 o
-5 8 0 2727.49 2901.19 184.70 o
-4 8 0 314.16 285.36 54.12 o
-3 8 0 1797.72 1677.76 72.50 o
-2 8 0 1270.93 1289.43 60.59 o
-1 8 0 1185.66 1231.42 58.86 o
0 8 0 2215.91 2276.41 84.18 o
1 8 0 583.81 571.60 41.65 o
2 8 0 2942.84 2903.09 86.60 o
3 8 0 1168.89 1173.41 61.86 o
4 8 0 1182.40 1147.02 67.10 o
5 8 0 2612.62 2533.79 105.58 o
6 8 0 42.02 -16.71 36.06 o
-4 9 0 1424.15 1462.48 117.32 o
-3 9 0 2474.86 2364.47 97.39 o
-2 9 0 331.90 341.12 37.71 o
-1 9 0 1424.46 1426.45 123.58 o
0 9 0 434.35 470.64 52.83 o
1 9 0 2045.78 2157.21 86.28 o
2 9 0 1643.85 1678.48 115.82 o
3 9 0 258.06 280.39 45.79 o
4 9 0 1632.19 1536.12 109.47 o
-3 10 0 327.88 331.33 64.02 o
-2 10 0 1114.09 1061.30 104.46 o
-1 10 0 463.51 479.30 68.11 o
0 10 0 1118.71 1103.26 77.44 o
1 10 0 1534.44 1427.76 115.79 o
2 10 0 89.40 114.80 22.81 o
3 10 0 1551.70 1553.17 94.63 o
1 -11 1 2583.49 2692.46 171.70 o
-3 -10 1 782.92 768.27 65.01 o
-2 -10 1 966.76 972.73 72.55 o
-1 -10 1 84.61 98.22 28.43 o
0 -10 1 3067.59 3105.12 111.29 o
1 -10 1 505.05 519.89 45.08 o
2 -10 1 1159.46 1171.68 66.28 o
-5 -9 1 947.05 1016.36 104.85 o
-4 -9 1 1445.50 1481.22 72.05 o
-3 -9 1 1448.20 1404.65 78.24 o
-2 -9 1 15.00 -9.12 9.12 o
-1 -9 1 2188.51 2251.38 86.05 o
0 -9 1 349.91 344.85 34.09 o
1 -9 1 842.23 850.97 51.25 o
2 -9 1 2070.52 2045.71 83.23 o
3 -9 1 409.21 455.10 52.71 o
4 -9 1 3050.68 3099.18 141.86 o
-6 -8 1 399.50 521.71 82.51 o
-5 -8 1 1565.10 1505.74 80.34 o
-4 -8 1 2604.32 2594.41 83.01 o
-3 -8 1 14.18 -3.79 13.21 o
-2 -8 1 1963.64 1988.15 67.12 o
-1 -8 1 271.68 283.59 34.85 o
0 -8 1 1837.46 1869.25 59.33 o
1 -8 1 3787.84 3686.67 110.03 o
2 -8 1 131.62 106.38 21.42 o
3 -8 1 2792.05 2771.94 120.08 o
4 -8 1 444.87 470.33 65.15 o
5 -8 1 990.84 1085.43 105.11 o
6 -8 1 2150.19 2392.00 171.84 o
-7 -7 1 1429.06 1703.81 150.60 o
-6 -7 1 337.54 390.59 51.37 o
-5 -7 1 1863.70 1732.00 79.14 o
-4 -7 1 138.67 101.85 21.25 o
-3 -7 1 6127.88 5977.32 128.97 o
-2 -7 1 3578.61 3619.97 58.25 o
-1 -7 1 2999.01 3032.71 67.49 o
0 -7 1 10050.78 10053.39 184.23 o
1 -7 1 672.51 700.83 40.32 o
2 -7 1 7783.41 7907.77 148.12 o
3 -7 1 839.05 786.48 42.95 o
4 -7 1 995.83 1003.60 55.66 o
5 -7 1 1312.51 1319.66 96.05 o
6 -7 1 117.88 109.12 27.83 o
7 -7 1 2999.84 3000.63 126.65 o
8 -7 1 163.46 150.43 45.09 o
-8 -6 1 963.06 913.75 112.57 o
-7 -6 1 374.69 345.60 35.64 o
-6 -6 1 2842.93 2807.61 113.40 o
-5 -6 1 168.25 197.45 22.98 o
-4 -6 1 3180.26 3114.80 50.15 o
-3 -6 1 3479.75 3462.46 70.79 o
-2 -6 1 2082.20 2183.22 39.65 o
-1 -6 1 7190.92 7220.23 86.57 o
0 -6 1 364.04 394.97 20.32 o
1 -6 1 6737.97 6634.23 99.73 o
2 -6 1 137.57 152.29 16.84 o
3 -6 1 2376.20 2348.45 58.81 o
4 -6 1 3941.20 4015.16 96.12 o
5 -6 1 3.27 2.09 13.06 o
6 -6 1 3167.93 3253.70 122.13 o
7 -6 1 813.20 849.57 59.05 o
8 -6 1 543.89 528.02 51.59 o
-9 -5 1 1096.18 1057.39 103.34 o
-8 -5 1 488.01 479.43 44.47 o
-7 -5 1 2093.62 2048.62 85.41 o
-6 -5 1 42.76 34.77 17.07 o
-5 -5 1 3176.81 3226.26 94.35 o
-4 -5 1 2858.05 2901.09 74.85 o
-3 -5 1 715.90 725.30 20.96 o
-2 -5 1 8981.21 8979.13 135.16 o
-1 -5 1 525.97 513.65 13.56 o
0 -5 1 5679.69 5529.80 86.60 o
1 -5 1 2803.58 2742.23 45.24 o
2 -5 1 3353.53 3384.72 55.31 o
3 -5 1 10230.26 10440.22 159.36 o
4 -5 1 278.88 264.16 16.75 o
5 -5 1 6824.21 7068.08 156.65 o
6 -5 1 657.04 705.10 54.73 o
7 -5 1 478.97 470.29 69.22 o
8 -5 1 3057.31 3029.10 133.24 o
9 -5 1 12.99 19.35 29.02 o
-9 -4 1 159.85 106.23 46.85 o
-8 -4 1 2855.36 2822.24 106.18 o
-7 -4 1 322.70 304.66 37.94 o
-6 -4 1 2001.37 2107.98 66.68 o
-5 -4 1 2852.94 2832.55 63.82 o
-4 -4 1 1165.96 1083.64 45.02 o
-3 -4 1 8792.19 9067.91 108.74 o
-2 -4 1 316.24 290.87 13.85 o
-1 -4 1 8113.67 8016.84 99.83 o
0 -4 1 7832.18 7695.81 118.72 o
1 -4 1 109.18 88.15 6.64 o
2 -4 1 7295.85 7261.36 91.77 o
3 -4 1 653.96 698.62 23.78 o
4 -4 1 5167.83 5184.58 93.24 o
5 -4 1 1449.88 1452.75 53.46 o
6 -4 1 322.41 279.62 33.31 o
7 -4 1 2459.44 2630.55 131.39 o
8 -4 1 0.69 -10.26 10.84 o
9 -4 1 3006.90 2972.98 106.34 o
-9 -3 1 2530.85 2517.92 121.97 o
-8 -3 1 855.65 796.33 54.19 o
-7 -3 1 2456.20 2514.37 113.58 o
-6 -3 1 6597.78 6782.55 158.28 o
-5 -3 1 162.50 152.91 13.84 o
-4 -3 1 7889.84 8217.70 141.49 o
-3 -3 1 22.70 23.66 9.91 o
-2 -3 1 13843.37 13877.35 220.96 o
-1 -3 1 6298.89 6052.12 75.29 o
0 -3 1 1969.57 1933.29 33.57 o
1 -3 1 12019.83 11328.33 183.06 o
2 -3 1 2021.92 2120.17 37.87 o
3 -3 1 10577.35 10833.71 180.26 o
4 -3 1 2512.07 2507.05 54.02 o
5 -3 1 309.64 307.91 21.57 o
6 -3 1 8830.16 8735.40 236.05 o
7 -3 1 126.07 121.01 24.53 o
8 -3 1 1912.30 1976.27 106.02 o
9 -3 1 1066.66 1053.79 52.04 o
-9 -2 1 544.10 569.58 92.67 o
-8 -2 1 1040.79 1035.25 74.24 o
-7 -2 1 2715.02 2710.85 85.90 o
-6 -2 1 138.95 137.20 7.22 o
-5 -2 1 8494.65 8695.64 163.86 o
-4 -2 1 1770.75 1807.65 34.37 o
-3 -2 1 3327.59 3236.06 55.30 o
-2 -2 1 11249.24 11151.97 300.21 o
-1 -2 1 808.49 841.39 14.17 o
0 -2 1 8841.17 8335.81 107.09 o
1 -2 1 5555.27 5712.62 106.66 o
2 -2 1 13096.69 13011.48 236.21 o
3 -2 1 4724.58 4538.62 73.88 o
4 -2 1 137.43 115.93 9.12 o
5 -2 1 9779.70 10126.53 209.88 o
6 -2 1 1232.11 1211.03 61.32 o
7 -2 1 3277.84 3292.06 105.31 o
8 -2 1 888.96 882.08 43.86 o
9 -2 1 255.87 216.87 24.93 o
-9 -1 1 1003.39 847.64 69.91 o
-8 -1 1 1588.61 1814.50 98.62 o
-7 -1 1 213.08 204.16 15.03 o
-6 -1 1 6563.03 6584.07 113.70 o
-5 -1 1 3385.70 3366.75 61.13 o
-4 -1 1 4518.73 4579.74 72.05 o
-3 -1 1 12915.50 12747.01 347.17 o
-2 -1 1 622.31 672.81 18.65 o
-1 -1 1 18645.68 17026.38 1058.60 o
0 -1 1 2369.79 2467.67 41.31 o
1 -1 1 5140.29 5156.99 118.66 o
2 -1 1 1496.23 1341.80 33.97 o
3 -1 1 270.59 306.12 14.85 o
4 -1 1 6060.03 5788.87 112.66 o
5 -1 1 1160.13 1190.98 34.28 o
6 -1 1 3778.64 3774.86 78.08 o
7 -1 1 2946.20 2905.02 106.32 o
8 -1 1 775.40 749.69 44.74 o
9 -1 1 2185.55 2433.01 130.44 o
-9 0 1 1989.56 2005.84 110.21 o
-8 0 1 82.38 56.02 12.53 o
-7 0 1 2499.17 2545.01 70.36 o
-6 0 1 1143.23 1113.35 32.04 o
-5 0 1 692.81 693.35 20.59 o
-4 0 1 7749.60 7755.23 117.19 o
-3 0 1 450.86 454.21 14.42 o
-2 0 1 878.46 878.07 23.02 o
-1 0 1 3472.84 3738.08 60.49 o
1 0 1 7517.65 7944.58 140.94 o
2 0 1 16984.95 17716.43 239.61 o
3 0 1 5822.82 5744.57 78.02 o
4 0 1 6101.41 6220.90 87.08 o
5 0 1 4693.96 4577.77 72.28 o
6 0 1 5274.41 5326.55 90.27 o
7 0 1 57.14 48.20 10.58 o
8 0 1 3857.96 3894.14 114.97 o
9 0 1 261.89 367.36 47.00 o
-9 1 1 130.29 155.72 31.78 o
-8 1 1 2682.95 2713.11 94.04 o
-7 1 1 1403.01 1424.68 43.99 o
-6 1 1 1430.01 1407.88 36.80 o
-5 1 1 5833.80 5897.43 74.94 o
-4 1 1 56.08 81.55 22.40 o
-3 1 1 12278.45 12268.56 192.86 o
-2 1 1 6142.93 6189.44 133.14 o
-1 1 1 2027.29 2111.72 44.97 o
0 1 1 10122.18 10179.14 138.51 o
1 1 1 490.90 549.71 12.11 o
2 1 1 15442.51 15550.49 201.34 o
3 1 1 7246.00 7678.91 95.04 o
4 1 1 5382.08 5333.63 124.74 o
5 1 1 2340.04 2311.15 44.83 o
6 1 1 184.39 180.56 25.39 o
7 1 1 2004.82 2077.33 53.81 o
8 1 1 971.73 984.43 74.28 o
9 1 1 1145.59 1323.65 89.14 o
-9 2 1 2310.78 2226.24 90.33 o
-8 2 1 1191.44 1210.11 60.06 o
-7 2 1 1297.97 1283.38 65.16 o
-6 2 1 7084.99 7309.48 136.32 o
-5 2 1 14.74 11.82 6.41 o
-4 2 1 5437.80 5190.55 85.21 o
-3 2 1 12587.50 13369.50 190.74 o
-2 2 1 1405.01 1340.84 31.77 o
-1 2 1 3260.24 3173.82 62.67 o
0 2 1 2383.27 2439.99 34.74 o
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2 2 1 1682.80 1647.90 24.50 o
3 2 1 5102.81 5275.50 68.26 o
4 2 1 4341.14 4284.73 59.52 o
5 2 1 155.24 150.17 10.75 o
6 2 1 2125.67 2202.26 47.38 o
7 2 1 921.85 906.79 44.02 o
8 2 1 1191.04 1174.39 81.68 o
9 2 1 1547.28 1595.07 100.12 o
-9 3 1 1485.22 1407.93 72.22 o
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-7 3 1 3700.60 3636.95 127.75 o
-6 3 1 4.78 9.99 8.93 o
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-4 3 1 682.26 654.32 31.30 o
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-1 3 1 39.08 62.83 4.79 o
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1 3 1 11056.03 11217.52 121.60 o
2 3 1 4943.95 4921.59 57.51 o
3 3 1 5005.20 4900.81 62.70 o
4 3 1 3.67 6.78 3.67 o
5 3 1 2948.29 2995.81 48.34 o
6 3 1 515.41 521.65 16.62 o
7 3 1 2424.02 2435.27 78.36 o
8 3 1 866.42 912.44 78.51 o
-9 4 1 270.08 306.72 39.38 o
-8 4 1 2958.81 2901.52 119.74 o
-7 4 1 545.55 487.26 43.03 o
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-5 4 1 1378.29 1389.48 50.99 o
-4 4 1 1721.61 1759.60 47.99 o
-3 4 1 5616.05 5450.41 84.56 o
-2 4 1 1541.77 1663.13 37.27 o
-1 4 1 6020.10 5965.20 84.33 o
0 4 1 6010.59 6134.38 88.33 o
1 4 1 377.52 377.57 17.19 o
2 4 1 9304.65 9428.26 104.88 o
3 4 1 1.86 11.77 6.01 o
4 4 1 2665.47 2662.16 46.94 o
5 4 1 3009.07 3019.31 73.31 o
6 4 1 1746.98 1619.18 60.39 o
7 4 1 889.71 934.02 49.13 o
8 4 1 62.10 62.96 30.20 o
-9 5 1 1688.42 1700.30 137.00 o
-8 5 1 58.80 99.80 38.37 o
-7 5 1 2738.35 2850.48 115.47 o
-6 5 1 4855.73 4814.71 155.16 o
-5 5 1 314.77 333.84 24.20 o
-4 5 1 5587.57 5603.74 175.68 o
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-2 5 1 2514.29 2483.13 39.97 o
-1 5 1 2358.70 2339.78 38.32 o
0 5 1 1116.56 1125.23 24.94 o
1 5 1 880.70 843.14 20.24 o
2 5 1 16.06 18.16 5.86 o
3 5 1 3205.90 3205.33 64.14 o
4 5 1 3026.90 3019.24 52.79 o
5 5 1 1268.46 1264.21 46.10 o
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