#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:50:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181300 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/78/2237895.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237895_Fobs loop_ _publ_author_name 'Li, Yu-Long' 'Xie, Bin' 'Zou, Li-Ke' _publ_section_title ; Tetraphenylphosphonium [\m~3~-(4-methylphenyl)tellurolato]tris[tetracarbonyliron(0)] ; _journal_coeditor_code IM2431 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m328 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.802 _cell_angle_beta 87.964 _cell_angle_gamma 86.312 _cell_length_a 12.3673 _cell_length_b 12.5576 _cell_length_c 13.6260 _exptl_crystal_F_000 1052.00 _reflns_d_resolution_high 0.7591 _cod_data_source_file im2431Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 241.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 20.71 28.87 6.70 o 2 0 0 518.42 519.76 18.00 o 3 0 0 2961.28 2821.75 46.05 o 4 0 0 18580.49 19019.86 170.56 o 5 0 0 4150.35 4153.80 82.55 o 6 0 0 227.62 270.87 22.48 o 7 0 0 431.97 479.97 47.26 o 8 0 0 29.74 37.35 15.02 o 9 0 0 468.03 457.59 80.94 o 10 0 0 8400.48 8297.95 490.08 o 11 0 0 8.93 -1.37 49.97 o 12 0 0 79.81 88.50 38.17 o 13 0 0 1493.79 1231.64 427.64 o 14 0 0 1174.37 1123.70 106.98 o 15 0 0 758.42 544.41 328.11 o 16 0 0 495.14 279.93 191.25 o -15 1 0 557.70 401.76 229.41 o -14 1 0 495.67 490.26 262.63 o -13 1 0 116.31 157.14 65.24 o -12 1 0 240.91 299.07 136.56 o -11 1 0 4670.41 4547.80 308.49 o -10 1 0 2.32 17.53 48.72 o -9 1 0 979.76 849.76 64.05 o -8 1 0 231.63 213.82 53.78 o -7 1 0 1655.29 1663.25 76.47 o -6 1 0 3184.26 3024.74 91.43 o -5 1 0 14367.06 14224.14 227.99 o -4 1 0 11671.52 11476.76 151.06 o -3 1 0 141.14 145.56 13.57 o -2 1 0 11605.26 11468.09 108.87 o -1 1 0 42075.35 40638.48 460.51 o 0 1 0 953.52 656.78 134.14 o 1 1 0 19527.55 18512.88 269.94 o 2 1 0 9453.01 9154.49 122.31 o 3 1 0 16914.58 16808.51 500.48 o 4 1 0 23799.89 24128.81 285.84 o 5 1 0 4751.47 4513.75 112.69 o 6 1 0 835.35 867.57 53.77 o 7 1 0 3947.88 3946.47 139.72 o 8 1 0 1406.38 1468.89 91.84 o 9 1 0 5347.06 5341.67 134.81 o 10 1 0 1.86 21.69 30.41 o 11 1 0 1973.11 2010.35 142.23 o 12 1 0 164.78 149.38 65.78 o 13 1 0 477.59 480.42 106.21 o 14 1 0 1635.10 1743.24 140.32 o 15 1 0 379.84 314.69 171.27 o 16 1 0 945.69 492.58 369.38 o -15 2 0 78.21 64.41 38.29 o -14 2 0 349.49 322.92 204.19 o -13 2 0 297.51 259.89 154.69 o -12 2 0 46.91 -10.20 48.01 o -11 2 0 1557.23 1557.54 394.84 o -10 2 0 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547.84 557.03 134.24 o -7 3 0 1961.04 1949.38 94.62 o -6 3 0 11097.11 11870.37 252.70 o -5 3 0 5724.82 5631.54 93.04 o -4 3 0 8720.35 8320.91 83.16 o -3 3 0 1236.55 1296.38 28.45 o -2 3 0 2975.35 2842.61 37.18 o -1 3 0 16691.51 15659.51 312.20 o 0 3 0 1668.26 1609.38 22.31 o 1 3 0 4640.85 4573.40 73.70 o 2 3 0 7.53 18.55 5.75 o 3 3 0 237.90 281.25 12.37 o 4 3 0 1534.82 1642.17 52.73 o 5 3 0 2845.42 2568.29 100.57 o 6 3 0 11583.07 11863.49 183.52 o 7 3 0 143.79 140.98 66.49 o 8 3 0 638.63 631.29 217.96 o 9 3 0 16389.05 16552.28 731.00 o 10 3 0 43.58 72.81 86.41 o 11 3 0 2306.39 2299.69 343.38 o 12 3 0 1245.49 1251.85 289.41 o 13 3 0 31.31 57.45 37.51 o 14 3 0 1034.88 1097.72 188.26 o 15 3 0 140.57 195.99 58.97 o 16 3 0 308.76 268.64 118.83 o -13 4 0 1791.31 1624.15 275.45 o -12 4 0 243.35 183.02 76.03 o -11 4 0 2114.31 2166.11 201.27 o -10 4 0 4647.01 5105.90 236.16 o -9 4 0 1697.13 1836.41 154.06 o -8 4 0 49.67 73.17 32.54 o -7 4 0 2821.84 2853.34 116.19 o -6 4 0 2024.15 2034.37 92.85 o -5 4 0 7378.35 7697.85 208.79 o -4 4 0 15.25 51.90 10.68 o -3 4 0 1104.85 1019.49 33.69 o -2 4 0 14081.10 13469.55 582.62 o -1 4 0 1371.31 1353.73 34.01 o 0 4 0 24609.84 24871.03 336.88 o 1 4 0 537.18 582.13 20.43 o 2 4 0 1877.92 3075.81 87.46 o 3 4 0 173.56 173.02 12.34 o 4 4 0 2503.67 2514.65 40.47 o 5 4 0 243.31 269.17 40.09 o 6 4 0 1642.27 1280.59 77.51 o 7 4 0 10532.43 10395.41 290.93 o 8 4 0 3008.69 2809.38 160.44 o 9 4 0 1.19 29.61 24.90 o 10 4 0 10920.59 11334.33 361.13 o 11 4 0 553.75 619.09 129.78 o 12 4 0 229.64 192.64 62.86 o 13 4 0 1170.88 1193.00 280.31 o 14 4 0 539.79 441.19 120.59 o 15 4 0 382.16 269.12 126.93 o -12 5 0 2587.07 2977.98 217.96 o -11 5 0 5585.31 6031.96 296.86 o -10 5 0 1582.34 1740.97 92.76 o -9 5 0 1053.47 1175.93 181.59 o -8 5 0 194.86 157.93 33.26 o -7 5 0 1318.78 1305.69 59.12 o -6 5 0 1294.56 1337.52 74.79 o -5 5 0 4063.57 3964.00 115.10 o -4 5 0 6391.09 6480.46 232.80 o -3 5 0 164.17 134.40 18.30 o -2 5 0 79.51 59.29 14.75 o -1 5 0 19004.28 18432.58 375.25 o 0 5 0 117.03 147.10 24.05 o 1 5 0 532.76 570.23 20.20 o 2 5 0 143.97 136.87 25.36 o 3 5 0 1085.82 1196.34 38.51 o 4 5 0 2699.95 2829.73 88.22 o 5 5 0 9974.64 9748.00 202.54 o 6 5 0 11141.49 11361.07 432.08 o 7 5 0 424.93 456.57 62.39 o 8 5 0 4.71 8.19 35.16 o 9 5 0 10893.10 11024.01 340.58 o 10 5 0 971.95 1051.69 139.24 o 11 5 0 2786.16 2620.25 136.23 o 12 5 0 1435.33 1334.89 285.58 o 13 5 0 557.26 632.58 152.12 o 14 5 0 482.02 486.31 160.66 o 15 5 0 38.15 47.48 35.86 o -12 6 0 319.62 227.09 173.89 o -11 6 0 746.94 851.94 234.01 o -10 6 0 4159.12 4551.75 167.81 o -9 6 0 1926.90 2113.73 127.62 o -8 6 0 7.04 17.40 12.90 o -7 6 0 1772.81 1771.62 86.50 o -6 6 0 6294.08 6345.48 143.35 o -5 6 0 3586.44 3507.64 128.87 o -4 6 0 262.82 524.61 66.31 o -3 6 0 422.92 421.61 54.51 o -2 6 0 291.62 272.50 52.32 o -1 6 0 90.90 81.44 18.64 o 0 6 0 9658.48 10317.69 188.71 o 1 6 0 3448.88 3511.72 89.43 o 2 6 0 20.06 40.70 12.07 o 3 6 0 2007.37 2049.17 58.66 o 4 6 0 7324.44 7418.95 165.23 o 5 6 0 12085.01 12347.06 259.59 o 6 6 0 235.60 190.65 33.69 o 7 6 0 6911.88 7360.93 198.20 o 8 6 0 9183.85 9764.76 332.54 o 9 6 0 386.75 369.24 121.48 o 10 6 0 3471.49 3731.56 184.49 o 11 6 0 161.86 198.15 58.52 o 12 6 0 393.97 442.13 198.76 o 13 6 0 765.76 709.81 166.22 o 14 6 0 0.55 61.90 59.58 o 15 6 0 640.33 617.91 163.60 o -12 7 0 90.26 65.24 71.08 o -11 7 0 3065.24 3106.55 603.27 o -10 7 0 423.51 478.87 136.68 o -9 7 0 1.73 14.98 15.79 o -8 7 0 22.21 44.99 25.83 o -7 7 0 3238.03 3140.30 127.42 o -6 7 0 2637.98 2733.77 101.87 o -5 7 0 6226.11 6215.55 230.37 o -4 7 0 507.64 617.94 216.35 o -3 7 0 400.42 429.13 199.00 o -2 7 0 323.52 313.88 82.91 o -1 7 0 8204.94 8556.63 224.75 o 0 7 0 10304.77 10529.01 187.84 o 1 7 0 65.41 105.07 23.63 o 2 7 0 34.88 19.09 7.88 o 3 7 0 3659.14 3779.42 99.18 o 4 7 0 15105.90 16030.93 445.13 o 5 7 0 907.99 746.29 58.03 o 6 7 0 8044.69 7952.83 152.78 o 7 7 0 6241.19 6087.53 166.77 o 8 7 0 221.63 223.27 76.75 o 9 7 0 8868.84 8958.17 392.65 o 10 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110.53 o 1 11 0 129.22 139.72 53.71 o 2 11 0 459.17 476.50 127.27 o 3 11 0 465.79 585.11 144.27 o 4 11 0 1423.23 1317.58 72.31 o 5 11 0 207.96 187.20 71.36 o 6 11 0 207.87 291.88 90.63 o 7 11 0 102.65 107.43 46.98 o 8 11 0 252.68 247.21 77.09 o 9 11 0 1738.19 1764.00 375.22 o 10 11 0 3040.48 3352.39 194.59 o 11 11 0 523.80 278.73 223.81 o 12 11 0 7.57 19.17 26.64 o -10 12 0 18.01 21.65 28.15 o -9 12 0 1627.50 1337.79 551.86 o -8 12 0 1411.12 1677.29 227.33 o -7 12 0 480.47 502.54 255.36 o -6 12 0 3957.99 4167.28 349.10 o -5 12 0 419.10 455.37 262.63 o -4 12 0 100.68 86.83 51.82 o -3 12 0 827.72 1005.44 264.72 o -2 12 0 468.42 356.38 194.65 o -1 12 0 759.90 849.26 245.16 o 0 12 0 377.69 396.63 232.81 o 1 12 0 172.33 182.05 64.12 o 2 12 0 836.31 721.64 261.62 o 3 12 0 3084.48 3088.48 230.85 o 4 12 0 2194.89 2461.84 539.04 o 5 12 0 4.51 3.84 30.81 o 6 12 0 86.53 74.80 40.63 o 7 12 0 20.23 38.09 32.02 o 8 12 0 660.97 555.03 142.26 o 9 12 0 2867.55 2890.54 158.23 o 10 12 0 1042.41 1089.94 149.17 o 11 12 0 496.64 419.23 173.00 o -9 13 0 55.00 56.41 53.61 o -8 13 0 277.96 216.65 127.38 o -7 13 0 4045.02 3575.82 377.37 o -6 13 0 235.39 281.36 105.97 o -5 13 0 374.73 295.79 130.24 o -4 13 0 867.92 775.73 340.87 o -3 13 0 415.65 363.12 202.10 o -2 13 0 891.25 770.24 322.98 o -1 13 0 177.86 151.29 100.07 o 0 13 0 1217.87 1215.12 240.51 o 1 13 0 241.95 207.83 127.38 o 2 13 0 251.65 237.18 80.31 o 3 13 0 1401.14 1684.84 104.81 o 4 13 0 304.84 306.62 90.28 o 5 13 0 7.24 51.93 28.82 o 6 13 0 707.88 595.27 283.56 o 7 13 0 41.28 44.69 31.21 o 8 13 0 346.03 359.14 107.54 o 9 13 0 534.13 411.04 171.65 o 10 13 0 1137.84 801.76 285.76 o -7 14 0 642.56 533.61 257.20 o -6 14 0 1126.94 1172.96 140.62 o -5 14 0 24.60 103.35 69.95 o -4 14 0 235.80 222.50 130.60 o -3 14 0 2.71 53.19 53.19 o -2 14 0 459.15 327.57 148.37 o -1 14 0 1843.58 1824.94 513.51 o 0 14 0 2.96 32.20 36.79 o 1 14 0 32.99 71.86 80.21 o 2 14 0 706.22 827.61 270.20 o 3 14 0 573.80 564.86 353.93 o 4 14 0 1342.24 1120.30 451.20 o 5 14 0 29.07 51.53 27.46 o 6 14 0 27.46 66.08 34.47 o 7 14 0 775.64 502.13 162.38 o 8 14 0 545.10 311.63 140.11 o 9 14 0 753.00 582.03 262.57 o -5 15 0 224.90 206.52 114.44 o -4 15 0 68.32 43.29 52.84 o -3 15 0 42.98 44.55 47.17 o -2 15 0 114.12 139.37 73.59 o -1 15 0 9.41 69.06 62.91 o 0 15 0 2314.06 2579.26 295.55 o 1 15 0 34.41 102.45 98.10 o 2 15 0 17.01 75.68 52.96 o 3 15 0 2412.06 2309.65 639.34 o 4 15 0 21.98 19.20 43.83 o 5 15 0 321.04 186.66 150.88 o 6 15 0 143.83 112.53 79.02 o 7 15 0 70.91 38.94 59.28 o -3 16 0 28.53 80.15 93.63 o -2 16 0 32.47 113.90 100.72 o -1 16 0 3277.94 2925.08 330.91 o 0 16 0 40.87 44.55 51.17 o 1 16 0 598.93 363.06 241.52 o 2 16 0 966.35 775.73 424.96 o 3 16 0 255.09 203.47 128.99 o 4 16 0 791.13 584.06 353.63 o 5 16 0 267.49 172.88 133.70 o -4 -16 1 217.31 143.72 97.38 o -3 -16 1 271.17 239.49 159.17 o -2 -16 1 31.23 30.18 43.95 o -1 -16 1 50.76 67.09 49.44 o 0 -16 1 447.47 278.55 228.88 o 1 -16 1 146.60 130.78 78.00 o 2 -16 1 1147.83 1020.23 393.35 o -7 -15 1 784.01 562.59 268.36 o -6 -15 1 958.72 700.17 438.49 o -5 -15 1 2.99 67.03 59.10 o -4 -15 1 903.43 701.13 306.34 o -3 -15 1 374.36 234.60 203.47 o -2 -15 1 84.19 10.67 64.64 o -1 -15 1 30.59 57.37 50.33 o 0 -15 1 7.08 14.25 43.35 o 1 -15 1 727.22 566.17 329.24 o 2 -15 1 460.18 443.03 259.59 o 3 -15 1 212.15 271.64 138.83 o 4 -15 1 366.61 292.99 170.50 o 5 -15 1 133.00 89.63 91.66 o -9 -14 1 1297.18 692.24 103.35 o -8 -14 1 1466.70 1292.70 125.74 o -7 -14 1 7.36 29.39 29.50 o -6 -14 1 31.69 28.37 23.69 o -5 -14 1 537.12 406.25 145.56 o -4 -14 1 503.65 397.05 201.63 o -3 -14 1 39.67 50.99 45.62 o -2 -14 1 98.43 100.54 85.22 o -1 -14 1 258.71 228.58 140.02 o 0 -14 1 320.66 231.32 112.17 o 1 -14 1 831.81 861.19 284.22 o 2 -14 1 602.47 584.36 313.44 o 3 -14 1 112.76 96.79 65.12 o 4 -14 1 37.81 38.23 50.51 o 5 -14 1 2350.22 2396.60 279.39 o 6 -14 1 1592.04 1312.14 162.62 o 7 -14 1 660.19 518.88 312.31 o -10 -13 1 443.24 349.32 144.90 o -9 -13 1 1521.76 1358.53 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