#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:51:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181301 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/79/2237905.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237905_Fobs loop_ _publ_author_name 'Okubo, Takashi' 'Anma, Haruho' 'Maekawa, Masahiko' 'Kuroda-Sowa, Takayoshi' _publ_section_title ; Tris(\m~4~-azepane-1-carbodithioato)bis(\m~3~-azepane-1-carbodithioato)-\m~9~-bromido-tetra-\m~2~-bromido-octacopper(I)copper(II) ; _journal_coeditor_code IS5263 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m275 _journal_page_last m276 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.041 _cell_angle_gamma 90.000 _cell_length_a 12.5728 _cell_length_b 19.5997 _cell_length_c 22.9708 _exptl_crystal_F_000 3604.00 _reflns_d_resolution_high 0.7711 _cod_data_source_file is5263Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100709_CuBr2HmMITC_01' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1119.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10575.50 5440.66 165.19 o 3 0 0 578289.69 362905.59 38924.57 o 4 0 0 8233.68 4723.80 453.36 o 5 0 0 21012.64 15583.56 710.05 o 6 0 0 84767.27 71531.32 3978.65 o 7 0 0 15945.94 14153.81 789.17 o 8 0 0 100104.98 99762.94 6344.28 o 9 0 0 2086.04 2647.61 497.80 o 10 0 0 2259.59 2125.33 296.66 o 11 0 0 3848.79 4902.61 645.50 o 12 0 0 103.90 1753.41 1426.74 o 13 0 0 5448.69 7307.88 860.20 o 14 0 0 673.25 557.96 556.23 o 15 0 0 638.53 1539.54 493.39 o 2 1 0 26196.39 19916.25 574.43 o 3 1 0 30078.31 19044.79 1308.79 o 4 1 0 33657.75 22864.32 2112.50 o 5 1 0 6753.25 5066.64 193.58 o 6 1 0 5268.30 4388.28 231.85 o 7 1 0 4144.67 3560.36 212.47 o 8 1 0 201.46 414.12 120.19 o 9 1 0 20022.19 20916.46 852.82 o 10 1 0 14249.97 15253.03 1001.83 o 11 1 0 780.29 927.52 207.34 o 12 1 0 32946.30 41018.69 2381.02 o 13 1 0 10219.05 14222.00 1382.75 o 14 1 0 703.43 1285.76 309.58 o 15 1 0 7964.05 12628.98 1641.78 o 2 2 0 83184.38 89444.53 2998.21 o 3 2 0 327848.81 303507.91 21060.19 o 4 2 0 61918.36 47201.56 1675.39 o 5 2 0 73609.86 53544.98 4887.69 o 6 2 0 203404.34 156456.16 8414.62 o 7 2 0 3324.57 3051.31 194.56 o 8 2 0 4668.39 4420.46 315.49 o 9 2 0 22675.70 23802.63 2035.04 o 10 2 0 16346.46 17631.63 805.96 o 11 2 0 138.04 318.49 187.20 o 12 2 0 25.54 -83.68 155.66 o 13 2 0 552.17 1107.13 243.71 o 14 2 0 14.15 271.39 217.44 o 15 2 0 3525.76 5331.38 1025.82 o 1 3 0 28054.66 31524.19 870.38 o 2 3 0 126515.10 135456.25 5776.62 o 3 3 0 25.14 271.98 41.50 o 4 3 0 725.00 1019.10 71.44 o 5 3 0 98951.39 77524.66 4489.49 o 6 3 0 210.23 191.27 61.01 o 7 3 0 44311.38 31432.57 2539.95 o 8 3 0 12817.26 11361.39 754.90 o 9 3 0 31116.64 29395.32 1561.49 o 10 3 0 662.66 748.39 263.19 o 11 3 0 722.55 868.15 174.74 o 12 3 0 2584.34 3063.44 392.28 o 13 3 0 4734.24 6325.40 640.27 o 14 3 0 3757.55 4699.38 1365.42 o 15 3 0 7518.29 11167.16 994.06 o 0 4 0 22861.05 24459.71 461.55 o 1 4 0 373.84 808.45 61.52 o 2 4 0 106814.23 119924.66 4102.77 o 3 4 0 445.87 392.43 58.72 o 4 4 0 52269.49 48580.02 1750.54 o 5 4 0 252.37 406.99 63.62 o 6 4 0 76350.74 61682.57 3207.38 o 7 4 0 10354.60 8093.43 1022.11 o 8 4 0 29669.39 22397.59 2451.82 o 9 4 0 19145.57 15417.06 1239.02 o 10 4 0 13280.11 14221.74 1190.35 o 11 4 0 2438.19 2522.23 414.37 o 12 4 0 1153.11 1366.64 231.09 o 13 4 0 809.37 1051.92 313.82 o 14 4 0 284.39 598.88 296.77 o 15 4 0 7049.34 9621.83 1590.59 o 1 5 0 15188.16 17958.65 353.32 o 2 5 0 23365.38 25572.76 795.54 o 3 5 0 112987.77 120514.82 4933.08 o 4 5 0 8737.63 8851.25 377.09 o 5 5 0 101422.26 98249.38 4453.29 o 6 5 0 545.38 570.29 115.68 o 7 5 0 18690.60 13788.77 1420.78 o 8 5 0 1561.32 1157.75 196.52 o 9 5 0 400.70 321.10 89.74 o 10 5 0 1003.35 820.23 165.30 o 11 5 0 3470.14 3611.43 315.00 o 12 5 0 12.35 35.66 163.73 o 13 5 0 4861.30 5954.44 1290.09 o 14 5 0 6160.22 9293.40 879.91 o 15 5 0 3392.67 5244.60 898.02 o 0 6 0 86988.39 109146.94 4786.11 o 1 6 0 2833.22 2881.57 73.59 o 2 6 0 22096.71 20717.09 689.80 o 3 6 0 67143.08 69309.45 2072.04 o 4 6 0 145136.83 151030.64 7061.63 o 5 6 0 27244.82 27341.41 1164.25 o 6 6 0 5592.87 5432.58 254.06 o 7 6 0 151049.67 131877.88 7948.13 o 8 6 0 74487.39 62554.89 7914.56 o 9 6 0 7454.65 13068.19 4938.34 o 10 6 0 2608.23 2761.21 425.36 o 11 6 0 8645.55 10334.05 811.51 o 12 6 0 42.45 213.32 214.54 o 13 6 0 986.76 1159.25 250.94 o 14 6 0 5240.40 9226.13 1567.01 o 15 6 0 889.99 1059.63 466.39 o 1 7 0 192083.20 222724.06 10234.61 o 2 7 0 7782.62 7823.87 207.83 o 3 7 0 3923.27 4289.39 132.60 o 4 7 0 36572.58 36652.53 969.52 o 5 7 0 29438.96 30630.96 1213.77 o 6 7 0 808.94 1025.05 131.28 o 7 7 0 768.82 631.66 95.08 o 8 7 0 505.22 630.77 113.36 o 9 7 0 3568.91 3712.29 461.44 o 10 7 0 13.33 27.32 148.58 o 11 7 0 371.82 488.24 340.27 o 12 7 0 1812.40 2459.03 417.94 o 13 7 0 7480.98 10495.81 1244.16 o 14 7 0 1442.78 1886.61 369.45 o 0 8 0 648.63 812.75 59.27 o 1 8 0 46825.87 49908.48 1233.32 o 2 8 0 125313.35 137847.89 5122.52 o 3 8 0 26845.22 27173.38 829.80 o 4 8 0 3448.82 4101.19 160.52 o 5 8 0 82.80 90.89 52.75 o 6 8 0 1730.04 1655.61 137.00 o 7 8 0 21243.86 21268.89 793.33 o 8 8 0 23831.09 23507.32 1397.70 o 9 8 0 64166.10 57865.97 8845.30 o 10 8 0 24288.71 19278.68 2889.34 o 11 8 0 6380.76 5430.26 845.87 o 12 8 0 4811.64 5072.35 599.85 o 13 8 0 102.46 316.16 455.19 o 14 8 0 7298.72 12516.41 1968.16 o 1 9 0 18.57 26.21 37.04 o 2 9 0 203.89 342.93 46.87 o 3 9 0 53380.14 54799.69 1791.45 o 4 9 0 41502.38 41656.88 1225.33 o 5 9 0 159.66 158.24 57.45 o 6 9 0 13069.70 12921.18 516.82 o 7 9 0 1599.26 1606.62 156.08 o 8 9 0 22798.71 21018.15 964.31 o 9 9 0 27440.33 23461.70 2118.35 o 10 9 0 1208.78 1221.41 185.18 o 11 9 0 14879.25 14174.98 1565.86 o 12 9 0 142.86 159.91 214.21 o 13 9 0 22076.92 27797.19 2840.57 o 14 9 0 973.06 1194.80 231.56 o 0 10 0 817.80 1093.12 117.07 o 1 10 0 34432.21 36494.58 828.10 o 2 10 0 43992.84 48452.41 1179.31 o 3 10 0 14051.94 14978.28 425.82 o 4 10 0 19185.02 18576.27 595.37 o 5 10 0 136.13 196.42 88.99 o 6 10 0 904.83 997.17 104.08 o 7 10 0 11210.09 11922.11 753.68 o 8 10 0 135.18 181.91 74.45 o 9 10 0 10135.18 9783.98 527.19 o 10 10 0 6812.17 7450.65 681.46 o 11 10 0 5607.96 5069.76 558.70 o 12 10 0 10213.01 10060.58 1836.45 o 13 10 0 32.15 -93.43 115.35 o 14 10 0 10010.62 14206.79 2945.52 o 1 11 0 78359.24 86502.38 2731.62 o 2 11 0 78102.82 84643.05 2463.87 o 3 11 0 10947.10 11485.12 386.37 o 4 11 0 16321.91 16343.03 727.03 o 5 11 0 2301.81 2725.27 290.50 o 6 11 0 8662.87 9247.31 614.61 o 7 11 0 308.80 336.35 91.09 o 8 11 0 974.39 961.16 132.06 o 9 11 0 876.66 1008.02 147.55 o 10 11 0 251.26 253.16 91.90 o 11 11 0 936.17 956.05 149.93 o 12 11 0 11.61 27.76 80.23 o 13 11 0 21630.13 23574.57 2718.85 o 14 11 0 3152.78 2825.70 716.52 o 0 12 0 161407.88 190114.53 12821.22 o 1 12 0 299322.31 338764.38 21566.80 o 2 12 0 170634.70 187225.42 7917.15 o 3 12 0 11859.88 12022.67 347.88 o 4 12 0 5525.78 5715.74 250.45 o 5 12 0 26427.73 27643.09 982.54 o 6 12 0 43186.75 43393.02 1618.44 o 7 12 0 2987.19 3342.32 276.48 o 8 12 0 2556.54 2507.59 229.15 o 9 12 0 3967.35 3772.19 247.85 o 10 12 0 2397.96 2116.58 235.05 o 11 12 0 9527.57 8703.28 1160.78 o 12 12 0 1163.86 1700.89 254.12 o 13 12 0 2281.22 1696.57 305.38 o 1 13 0 12146.89 12940.95 376.49 o 2 13 0 18164.44 19359.93 511.17 o 3 13 0 4825.62 4558.27 158.01 o 4 13 0 42464.12 44748.25 1652.97 o 5 13 0 2201.24 2331.48 206.38 o 6 13 0 15080.80 16611.66 754.84 o 7 13 0 24916.11 25500.68 1267.53 o 8 13 0 108.58 96.79 98.40 o 9 13 0 12278.67 11935.96 679.61 o 10 13 0 308.78 324.98 145.83 o 11 13 0 2366.61 2180.30 242.42 o 12 13 0 2537.05 2296.93 280.99 o 13 13 0 8651.08 7186.65 1432.37 o 0 14 0 92316.27 102621.23 5522.04 o 1 14 0 83985.49 89780.52 3235.92 o 2 14 0 68156.14 72823.74 2264.17 o 3 14 0 677.49 807.92 76.78 o 4 14 0 30752.79 30989.57 991.89 o 5 14 0 90813.80 96013.72 4282.77 o 6 14 0 116586.79 130911.23 7160.00 o 7 14 0 8080.66 8786.73 434.89 o 8 14 0 2553.40 2585.09 394.49 o 9 14 0 59.22 98.05 106.39 o 10 14 0 354.12 402.49 146.86 o 11 14 0 6968.96 7278.97 696.14 o 12 14 0 91.58 13.85 99.41 o 13 14 0 1253.67 1693.21 887.19 o 1 15 0 891.53 1045.71 100.50 o 2 15 0 1615.20 1778.54 111.47 o 3 15 0 3325.00 3464.29 143.81 o 4 15 0 5451.84 5340.58 224.75 o 5 15 0 2688.29 2794.86 205.52 o 6 15 0 179.75 126.03 89.63 o 7 15 0 33326.18 38639.17 1910.72 o 8 15 0 9846.27 11159.74 711.44 o 9 15 0 1051.45 942.98 197.77 o 10 15 0 172.71 260.90 109.36 o 11 15 0 16.21 66.47 114.92 o 12 15 0 8.59 41.63 114.86 o 0 16 0 31685.44 35176.00 1836.89 o 1 16 0 13579.09 14314.76 454.77 o 2 16 0 8354.35 9077.83 372.03 o 3 16 0 2746.20 2696.09 136.34 o 4 16 0 7982.71 8354.44 333.41 o 5 16 0 3273.00 3553.23 232.44 o 6 16 0 11440.69 12664.39 791.22 o 7 16 0 19069.10 21280.54 913.84 o 8 16 0 792.25 799.74 179.27 o 9 16 0 10157.31 10874.72 742.14 o 10 16 0 970.01 1112.18 227.49 o 11 16 0 135.20 171.16 171.50 o 12 16 0 173.73 169.38 128.71 o 1 17 0 6518.75 6422.38 317.18 o 2 17 0 44936.45 47460.82 1348.24 o 3 17 0 234.38 189.47 72.03 o 4 17 0 4304.81 4568.40 214.24 o 5 17 0 4624.57 4779.96 271.13 o 6 17 0 37258.67 40267.51 1754.90 o 7 17 0 671.85 537.40 153.20 o 8 17 0 9046.80 10318.93 573.03 o 9 17 0 6402.05 7749.24 595.99 o 10 17 0 2684.53 2895.71 328.68 o 11 17 0 726.39 878.44 245.88 o 0 18 0 10007.21 10157.69 518.55 o 1 18 0 1286.38 1389.66 115.34 o 2 18 0 15135.15 15685.27 581.93 o 3 18 0 15909.55 16648.29 574.67 o 4 18 0 4156.22 4885.58 250.73 o 5 18 0 27157.96 28379.90 1169.43 o 6 18 0 15666.82 17494.82 730.84 o 7 18 0 28.49 20.50 83.16 o 8 18 0 845.64 652.73 180.06 o 9 18 0 12332.04 13494.91 894.55 o 10 18 0 1720.50 2095.94 287.28 o 11 18 0 2704.60 3421.68 1364.44 o 1 19 0 16881.40 17815.97 759.83 o 2 19 0 15047.58 15699.04 602.97 o 3 19 0 7093.64 7288.34 368.00 o 4 19 0 7282.13 7489.28 348.09 o 5 19 0 629.26 630.03 111.72 o 6 19 0 796.10 869.08 142.18 o 7 19 0 592.12 642.60 118.55 o 8 19 0 5408.79 6001.38 452.96 o 9 19 0 4777.67 5014.07 530.49 o 10 19 0 2208.98 1979.49 481.43 o 0 20 0 1247.70 1194.74 166.37 o 1 20 0 36178.35 38991.77 1603.44 o 2 20 0 31953.62 35308.63 1681.85 o 3 20 0 15936.79 16602.99 620.16 o 4 20 0 3358.06 3377.75 187.72 o 5 20 0 2301.57 2047.15 165.53 o 6 20 0 185.97 107.43 86.61 o 7 20 0 6245.45 7255.20 406.12 o 8 20 0 13379.45 14645.68 867.45 o 9 20 0 16869.89 18189.83 1082.12 o 1 21 0 11488.94 12309.54 611.64 o 2 21 0 223.64 362.47 111.36 o 3 21 0 1100.70 1251.47 111.22 o 4 21 0 4840.19 5242.51 297.09 o 5 21 0 8804.41 9184.11 469.36 o 6 21 0 778.06 727.88 143.61 o 7 21 0 9088.40 10587.79 569.51 o 8 21 0 2742.04 2589.28 311.06 o 0 22 0 47.03 -17.30 99.82 o 1 22 0 1240.77 1449.11 159.26 o 2 22 0 370.81 290.59 82.61 o 3 22 0 10255.36 10564.84 492.38 o 4 22 0 9093.66 8940.88 416.21 o 5 22 0 8578.43 8413.00 581.40 o 6 22 0 5869.65 6423.86 385.69 o 7 22 0 132.49 66.40 94.07 o 1 23 0 580.99 613.16 132.92 o 2 23 0 3794.63 4261.97 478.29 o 3 23 0 6098.21 6468.20 447.08 o 4 23 0 896.66 909.13 129.12 o 5 23 0 2082.67 1887.82 153.76 o 6 23 0 8972.37 8934.51 477.62 o 0 24 0 788.58 836.00 210.79 o 1 24 0 9386.34 9894.24 442.47 o 2 24 0 2536.03 2438.60 195.41 o 3 24 0 14016.77 14423.38 669.30 o 4 24 0 10.22 41.22 83.30 o 5 24 0 6134.97 5877.37 874.35 o 1 25 0 5143.72 5491.52 327.26 o 2 25 0 2167.08 1825.09 197.76 o -15 1 1 2569.42 3621.16 641.68 o -14 1 1 3308.49 5116.65 956.90 o -13 1 1 629.70 965.96 213.86 o -12 1 1 3482.20 10739.41 4425.95 o -11 1 1 1277.82 2452.96 1076.77 o -10 1 1 967.75 1164.70 204.11 o -9 1 1 1253.88 1203.22 203.85 o -8 1 1 34399.95 32074.95 1331.91 o -7 1 1 1080.60 1057.47 116.90 o -6 1 1 51772.05 39594.49 2849.50 o -5 1 1 1294.66 1060.07 76.10 o -4 1 1 23651.71 16930.39 756.88 o -3 1 1 881.92 639.47 74.74 o -2 1 1 9692.89 9484.14 269.11 o 2 1 1 12298.50 6006.96 481.81 o 3 1 1 1081.65 1498.02 189.09 o 4 1 1 13242.55 9009.29 387.88 o 5 1 1 10254.38 7163.55 511.38 o 6 1 1 1833.99 1813.56 127.38 o 7 1 1 46828.01 40843.53 1561.95 o 8 1 1 1802.14 2027.91 185.65 o 9 1 1 11782.96 12188.52 914.05 o 10 1 1 715.45 767.35 140.16 o 11 1 1 4005.27 4812.60 463.78 o 12 1 1 454.14 346.02 198.31 o 13 1 1 2240.90 3250.13 470.12 o 14 1 1 176.49 431.24 251.16 o 15 1 1 90.52 3.44 213.68 o -15 2 1 1463.04 2375.19 481.49 o -14 2 1 468.35 624.02 373.92 o -13 2 1 388.88 3508.88 2225.74 o -12 2 1 89.17 65.41 129.18 o -11 2 1 1161.78 3851.28 1272.92 o -10 2 1 1479.17 1479.61 310.08 o -9 2 1 34289.68 35695.32 1825.15 o -8 2 1 349.30 495.86 104.33 o -7 2 1 91015.64 72173.84 6042.41 o -6 2 1 634.82 452.13 76.76 o -5 2 1 19484.10 13974.32 675.66 o -4 2 1 23896.45 22329.08 926.12 o -3 2 1 42864.26 40033.16 2720.98 o -2 2 1 21965.53 21406.91 1652.19 o 1 2 1 4736.54 4699.37 159.53 o 2 2 1 1889.35 1610.09 80.15 o 3 2 1 1732.60 1523.69 91.61 o 4 2 1 15369.99 12185.78 725.67 o 5 2 1 7643.15 6102.46 523.25 o 6 2 1 45220.18 33678.10 3294.43 o 7 2 1 135.23 209.04 61.45 o 8 2 1 31610.88 28990.40 2170.83 o 9 2 1 5020.69 5205.50 343.12 o 10 2 1 2502.89 2712.82 413.33 o 11 2 1 9058.55 10338.06 696.00 o 12 2 1 16467.79 21835.98 2033.95 o 13 2 1 689.06 2469.93 1189.92 o 14 2 1 22.91 -11.51 184.36 o 15 2 1 2.93 -157.73 252.56 o -15 3 1 458.42 1084.71 813.26 o -14 3 1 534.05 948.27 235.73 o -13 3 1 1276.64 1787.74 308.18 o -12 3 1 9972.51 12772.16 1063.97 o -11 3 1 478.77 476.81 227.41 o -10 3 1 1340.90 1399.08 180.98 o -9 3 1 2335.13 2326.56 205.00 o -8 3 1 9206.75 8769.30 562.58 o -7 3 1 3188.22 2578.68 346.70 o -6 3 1 22393.81 17085.02 796.93 o -5 3 1 8276.46 6076.13 445.22 o -4 3 1 59066.70 50114.94 3890.82 o -3 3 1 2941.10 2486.50 193.22 o -2 3 1 28950.04 29231.13 611.02 o -1 3 1 4062.42 4332.21 173.98 o 0 3 1 62.40 166.03 17.55 o 1 3 1 135.15 171.46 32.01 o 2 3 1 579.65 611.33 52.03 o 3 3 1 12497.43 11267.50 434.05 o 4 3 1 10387.87 9291.46 495.08 o 5 3 1 15144.55 11558.05 888.30 o 6 3 1 5886.76 3823.88 241.99 o 7 3 1 28385.68 21548.27 2419.21 o 8 3 1 48.58 54.67 70.00 o 9 3 1 29446.75 28026.06 1890.03 o 10 3 1 1768.00 2012.98 227.81 o 11 3 1 2201.84 2294.08 353.66 o 12 3 1 1878.89 2302.49 322.95 o 13 3 1 406.90 780.45 318.05 o 14 3 1 3156.24 4799.69 601.73 o 15 3 1 529.07 458.77 255.82 o -15 4 1 20.82 22.75 173.44 o -14 4 1 5517.40 7870.57 2289.84 o -13 4 1 1573.64 2450.46 453.78 o -12 4 1 835.02 837.22 208.98 o -11 4 1 1471.32 1528.09 201.66 o -10 4 1 1216.72 1174.73 200.77 o -9 4 1 8231.09 7813.27 543.77 o -8 4 1 1055.79 907.08 124.72 o -7 4 1 278.76 301.46 65.44 o -6 4 1 24482.09 22578.59 767.07 o -5 4 1 24307.64 20581.56 1568.50 o -4 4 1 9081.47 7687.98 382.73 o -3 4 1 27552.18 25991.48 727.15 o -2 4 1 67190.06 73013.84 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