#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:51:00 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181301 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/79/2237948.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237948_Fobs loop_ _publ_author_name 'Trifa, Chahrazed' 'Bouhali, Amira' 'Bouacida, Sofiane' 'Boudaren, Chaouki' 'Bataille, Thierry' _publ_section_title ; Poly[1H-imidazol-3-ium [di-\m-nitrato-sodium]] ; _journal_coeditor_code LH5609 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m303 _journal_page_last m304 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.546 _cell_angle_gamma 90.000 _cell_length_a 3.5875 _cell_length_b 24.8548 _cell_length_c 8.8190 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file lh5609Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 132.50 94.46 2.43 o 2 0 0 6395.36 6559.73 95.85 o 3 0 0 148.79 134.87 3.80 o 4 0 0 100.61 91.68 7.09 o 1 1 0 6.49 5.39 0.52 o 2 1 0 240.65 244.32 4.96 o 3 1 0 198.11 195.49 3.45 o 4 1 0 12.57 7.14 1.61 o 1 2 0 498.74 495.25 5.57 o 2 2 0 789.84 770.11 8.99 o 3 2 0 73.09 65.26 2.01 o 4 2 0 1.25 -1.47 1.66 o 1 3 0 8859.42 8032.24 165.71 o 2 3 0 0.00 1.40 0.78 o 3 3 0 98.05 95.86 2.08 o 4 3 0 140.66 146.47 3.71 o 1 4 0 36.24 31.90 1.00 o 2 4 0 206.65 204.60 3.24 o 3 4 0 92.26 85.64 1.96 o 4 4 0 0.74 -0.79 1.63 o 1 5 0 470.55 413.74 5.40 o 2 5 0 143.83 128.10 2.35 o 3 5 0 95.49 107.98 2.47 o 4 5 0 27.43 21.06 1.94 o 1 6 0 74.02 104.61 1.81 o 2 6 0 220.11 206.27 3.22 o 3 6 0 163.91 165.05 3.13 o 4 6 0 166.75 173.39 6.13 o 1 7 0 187.89 170.60 3.37 o 2 7 0 64.88 63.69 1.85 o 3 7 0 10.75 7.85 1.26 o 4 7 0 217.57 225.99 5.92 o 0 8 0 0.36 1.00 1.36 o 2 8 0 359.82 333.78 4.19 o 3 8 0 135.65 133.77 3.01 o 4 8 0 111.03 119.88 4.49 o 1 9 0 218.52 213.21 3.27 o 2 9 0 13.78 10.32 0.95 o 3 9 0 1.92 0.30 0.89 o 4 9 0 2.27 3.98 2.12 o 0 10 0 28.14 8.53 0.72 o 1 10 0 1783.52 1795.94 17.41 o 2 10 0 4.01 6.12 1.37 o 3 10 0 452.53 482.35 7.42 o 4 10 0 15.95 11.61 9.37 o 1 11 0 1191.91 1190.67 11.93 o 2 11 0 941.58 991.10 11.82 o 3 11 0 353.36 379.84 6.24 o 4 11 0 62.12 54.30 3.43 o 0 12 0 1425.15 1491.01 19.67 o 1 12 0 61.16 54.26 1.49 o 2 12 0 551.79 586.73 7.63 o 3 12 0 36.79 36.91 1.82 o 4 12 0 267.40 283.32 7.28 o 1 13 0 29.80 25.11 0.97 o 2 13 0 20.95 24.34 1.77 o 3 13 0 16.54 15.39 1.55 o 4 13 0 1.88 5.91 3.65 o 0 14 0 491.35 495.33 7.27 o 1 14 0 102.28 109.53 1.99 o 2 14 0 17.68 15.73 1.07 o 3 14 0 16.46 13.76 1.96 o 4 14 0 56.87 49.01 3.77 o 1 15 0 122.37 123.86 1.98 o 2 15 0 76.39 78.95 1.79 o 3 15 0 42.65 41.30 2.68 o 4 15 0 0.04 -2.37 2.37 o 0 16 0 904.45 996.35 13.68 o 1 16 0 123.87 115.19 1.95 o 2 16 0 305.56 313.29 4.19 o 3 16 0 40.62 39.08 3.23 o 4 16 0 156.65 166.40 5.96 o 1 17 0 411.33 441.05 5.79 o 2 17 0 93.81 91.43 1.99 o 3 17 0 194.54 191.39 3.69 o 0 18 0 33.46 22.22 1.41 o 1 18 0 197.70 194.23 2.86 o 2 18 0 752.34 774.48 9.21 o 3 18 0 108.17 100.11 2.95 o 1 19 0 37.86 36.13 1.17 o 2 19 0 44.79 44.07 2.13 o 3 19 0 133.42 134.67 3.42 o 0 20 0 525.65 548.53 7.69 o 1 20 0 0.03 -0.66 0.66 o 2 20 0 90.62 81.53 2.71 o 3 20 0 28.23 25.34 1.90 o 1 21 0 358.89 371.99 4.76 o 2 21 0 8.71 7.20 1.46 o 3 21 0 0.77 2.00 1.86 o 0 22 0 54.38 56.84 1.88 o 1 22 0 2197.35 2324.61 22.96 o 2 22 0 29.68 25.64 2.69 o 3 22 0 53.18 49.68 2.98 o 1 23 0 0.09 5.49 1.85 o 2 23 0 17.98 18.07 1.98 o 3 23 0 7.54 6.18 2.07 o 0 24 0 951.11 962.03 12.73 o 1 24 0 438.10 463.33 6.19 o 2 24 0 0.13 -0.83 1.52 o 3 24 0 100.15 88.77 3.52 o 1 25 0 27.82 31.09 1.52 o 2 25 0 123.24 120.16 3.88 o 0 26 0 221.32 218.21 4.75 o 1 26 0 171.64 172.27 3.36 o 2 26 0 101.21 103.75 4.11 o 1 27 0 126.74 122.55 4.27 o 2 27 0 18.41 21.84 3.21 o 0 28 0 181.76 195.97 6.27 o 1 28 0 21.80 17.76 1.63 o 2 28 0 66.10 69.57 3.69 o 1 29 0 2.91 1.80 2.12 o 2 29 0 0.18 3.34 2.62 o 0 30 0 324.86 358.03 8.85 o 1 30 0 73.01 75.96 3.55 o 1 31 0 9.89 8.35 2.64 o 0 32 0 21.43 26.35 4.54 o -4 1 1 0.99 2.64 1.49 o -3 1 1 75.02 71.70 1.94 o -2 1 1 967.64 986.04 13.01 o -1 1 1 1519.85 1534.74 20.22 o 1 1 1 293.15 301.26 3.16 o 2 1 1 998.89 1031.45 12.01 o 3 1 1 68.63 76.91 2.02 o 4 1 1 7.58 6.83 1.76 o -4 2 1 1.04 0.98 1.48 o -3 2 1 48.39 36.27 1.61 o -2 2 1 338.48 358.37 5.16 o -1 2 1 3988.12 3800.31 46.53 o 1 2 1 936.71 873.50 9.02 o 2 2 1 1823.12 1801.46 25.63 o 3 2 1 161.30 170.42 2.88 o 4 2 1 4.27 -0.68 1.62 o -4 3 1 3.36 0.79 1.94 o -3 3 1 1.36 1.80 1.34 o -2 3 1 39.66 40.19 1.30 o -1 3 1 525.41 527.81 6.11 o 1 3 1 1345.74 1375.69 15.12 o 2 3 1 194.83 184.84 2.85 o 3 3 1 91.66 78.72 1.92 o 4 3 1 71.76 58.67 2.74 o -4 4 1 67.29 60.04 2.44 o -3 4 1 468.98 486.61 7.17 o -2 4 1 616.26 608.47 7.29 o -1 4 1 8767.95 8219.11 168.02 o 0 4 1 2684.93 2493.49 24.87 o 1 4 1 1080.79 1014.39 12.22 o 2 4 1 716.87 730.55 8.09 o 3 4 1 258.31 276.31 3.91 o 4 4 1 149.26 154.77 4.35 o -4 5 1 5.38 6.66 2.59 o -3 5 1 85.83 73.37 2.36 o -2 5 1 439.55 465.17 5.81 o -1 5 1 7229.69 7004.83 87.39 o 0 5 1 1577.53 1450.82 12.54 o 1 5 1 1676.69 1700.10 18.21 o 2 5 1 240.95 247.45 3.45 o 3 5 1 149.13 151.83 2.97 o 4 5 1 11.44 13.98 2.04 o -4 6 1 69.67 65.14 3.60 o -3 6 1 364.99 390.12 6.10 o -2 6 1 45.90 39.62 1.46 o -1 6 1 846.55 745.05 8.70 o 0 6 1 38.42 32.83 1.07 o 1 6 1 216.67 198.17 4.42 o 2 6 1 1171.96 1237.11 18.22 o 3 6 1 169.05 162.04 2.79 o 4 6 1 219.31 225.06 5.88 o -4 7 1 90.15 82.35 3.50 o -3 7 1 60.33 54.46 2.60 o -2 7 1 179.48 156.16 2.60 o -1 7 1 860.10 880.74 8.83 o 0 7 1 341.27 368.47 3.78 o 1 7 1 4270.99 4217.07 61.24 o 2 7 1 186.15 192.16 3.12 o 3 7 1 338.42 347.24 5.29 o 4 7 1 2.20 -1.22 3.45 o -4 8 1 1.16 -0.85 1.39 o -3 8 1 293.45 302.79 5.33 o -2 8 1 725.48 715.38 9.34 o -1 8 1 2076.26 1938.44 19.71 o 0 8 1 530.06 463.49 4.51 o 1 8 1 639.37 738.09 10.42 o 2 8 1 444.44 460.81 5.60 o 3 8 1 115.03 102.96 2.45 o 4 8 1 53.54 41.37 3.08 o -4 9 1 0.49 0.41 2.46 o -3 9 1 1.17 1.29 0.92 o -2 9 1 63.66 65.04 1.57 o -1 9 1 134.18 138.26 2.21 o 0 9 1 622.18 572.50 5.29 o 1 9 1 1725.17 1767.33 18.07 o 2 9 1 130.75 125.54 2.54 o 3 9 1 70.95 67.38 1.94 o 4 9 1 34.65 32.35 2.72 o -4 10 1 0.09 0.31 2.28 o -3 10 1 26.25 25.00 1.75 o -2 10 1 695.78 736.09 9.67 o -1 10 1 0.19 7.71 1.40 o 0 10 1 1278.30 1286.94 11.84 o 1 10 1 0.36 -0.10 0.86 o 2 10 1 18.53 15.12 1.13 o 3 10 1 7.85 8.35 2.19 o 4 10 1 85.64 84.34 4.48 o -4 11 1 65.92 55.64 5.03 o -3 11 1 305.45 321.84 5.45 o -2 11 1 862.03 876.99 12.32 o -1 11 1 9.08 3.46 0.60 o 0 11 1 61.17 90.64 3.17 o 1 11 1 951.38 1024.18 11.07 o 2 11 1 119.06 107.19 2.12 o 3 11 1 487.42 509.36 7.22 o 4 11 1 6.28 2.00 2.40 o -4 12 1 31.65 21.34 2.62 o -3 12 1 56.61 55.40 2.14 o -2 12 1 313.31 279.73 4.30 o -1 12 1 625.36 621.39 6.62 o 0 12 1 3356.08 3223.32 30.62 o 1 12 1 36.76 23.49 1.39 o 2 12 1 7.66 3.44 0.91 o 3 12 1 24.47 19.86 1.81 o 4 12 1 0.72 -2.14 2.14 o -4 13 1 29.90 18.20 3.94 o -3 13 1 510.70 548.68 8.17 o -2 13 1 93.71 99.12 2.68 o -1 13 1 2.94 2.11 0.80 o 0 13 1 75.41 116.25 2.41 o 1 13 1 656.27 728.65 8.61 o 2 13 1 31.82 32.55 1.46 o 3 13 1 9.70 10.28 1.60 o 4 13 1 6.49 4.97 2.29 o -4 14 1 102.89 102.76 4.63 o -3 14 1 61.05 54.07 2.16 o -2 14 1 1892.55 1994.96 22.13 o -1 14 1 327.00 366.19 4.31 o 0 14 1 609.74 576.31 5.85 o 1 14 1 40.42 40.94 1.49 o 2 14 1 433.46 428.76 5.21 o 3 14 1 29.49 25.05 1.52 o 4 14 1 72.51 69.39 3.36 o -4 15 1 20.57 22.08 4.46 o -3 15 1 0.20 0.06 1.20 o -2 15 1 101.22 97.05 2.86 o -1 15 1 6.33 6.05 0.71 o 0 15 1 352.32 361.91 4.01 o 1 15 1 592.34 601.10 7.47 o 2 15 1 563.54 619.48 7.07 o 3 15 1 36.93 30.46 1.81 o 4 15 1 353.41 382.94 10.34 o -4 16 1 48.67 42.69 5.16 o -3 16 1 9.53 12.21 1.38 o -2 16 1 1271.38 1333.08 14.59 o -1 16 1 200.88 213.11 2.94 o 0 16 1 642.25 659.91 6.71 o 1 16 1 54.14 55.51 1.29 o 2 16 1 0.20 -0.96 0.96 o 3 16 1 33.16 36.80 2.30 o -3 17 1 12.99 11.34 1.78 o -2 17 1 0.00 -0.09 1.62 o -1 17 1 589.37 592.20 6.60 o 0 17 1 575.72 602.18 6.42 o 1 17 1 49.70 40.39 1.64 o 2 17 1 2.61 2.96 0.79 o 3 17 1 14.12 11.33 1.39 o -3 18 1 0.25 -0.40 1.22 o -2 18 1 563.56 561.82 7.77 o -1 18 1 384.14 388.72 4.49 o 0 18 1 2185.07 2166.21 20.02 o 1 18 1 16.31 12.94 0.88 o 2 18 1 4.24 5.06 0.84 o 3 18 1 23.80 16.84 1.59 o -3 19 1 0.41 2.20 1.12 o -2 19 1 217.16 216.90 4.05 o -1 19 1 921.82 933.58 9.32 o 0 19 1 69.38 74.48 2.10 o 1 19 1 514.51 525.59 6.06 o 2 19 1 70.66 70.66 1.81 o 3 19 1 51.51 38.74 2.33 o -3 20 1 1.39 2.99 1.64 o -2 20 1 81.70 75.56 2.51 o -1 20 1 101.96 109.84 1.92 o 0 20 1 122.87 123.91 1.99 o 1 20 1 82.63 81.51 1.76 o 2 20 1 56.58 57.03 2.01 o 3 20 1 5.04 4.36 1.76 o -3 21 1 47.39 40.23 2.88 o -2 21 1 0.03 1.85 1.56 o -1 21 1 57.34 51.91 1.32 o 0 21 1 243.13 230.41 3.02 o 1 21 1 188.88 194.91 3.14 o 2 21 1 33.60 32.83 1.91 o 3 21 1 17.38 11.38 1.85 o -3 22 1 152.17 160.73 5.13 o -2 22 1 40.57 34.98 2.44 o -1 22 1 153.25 154.66 2.81 o 0 22 1 1089.80 1115.83 10.13 o 1 22 1 283.08 286.94 3.97 o 2 22 1 807.22 849.46 12.97 o 3 22 1 5.49 5.77 1.61 o -3 23 1 2.51 4.63 2.78 o -2 23 1 20.82 17.42 1.93 o -1 23 1 228.00 225.56 3.38 o 0 23 1 13.29 16.77 1.17 o 1 23 1 353.62 373.23 5.19 o 2 23 1 53.09 46.17 2.37 o 3 23 1 187.95 200.68 5.05 o -3 24 1 5.06 8.28 2.59 o -2 24 1 66.06 56.02 2.63 o -1 24 1 13.45 12.54 1.06 o 0 24 1 443.23 437.26 4.75 o 1 24 1 229.00 228.85 3.90 o 2 24 1 2.61 4.74 2.59 o 3 24 1 220.87 232.75 5.61 o -2 25 1 28.60 19.47 2.71 o -1 25 1 423.44 435.37 5.53 o 0 25 1 1.92 1.64 0.86 o 1 25 1 149.67 131.80 2.81 o 2 25 1 27.27 26.79 2.52 o -2 26 1 55.53 45.73 3.85 o -1 26 1 44.29 37.67 1.46 o 0 26 1 13.97 12.28 1.22 o 1 26 1 152.17 160.80 3.44 o 2 26 1 11.47 6.88 2.22 o -2 27 1 38.45 31.77 2.76 o -1 27 1 95.40 88.07 2.61 o 0 27 1 341.38 338.31 5.44 o 1 27 1 1.67 0.39 2.11 o 2 27 1 31.09 21.75 3.49 o -2 28 1 0.10 3.19 2.37 o -1 28 1 0.05 -0.30 1.61 o 0 28 1 63.43 62.99 2.19 o 1 28 1 106.71 107.59 3.90 o 2 28 1 0.50 2.14 2.33 o -2 29 1 1.91 7.09 2.66 o -1 29 1 106.28 102.27 3.91 o 0 29 1 194.90 211.32 4.42 o 1 29 1 17.26 18.52 2.36 o -1 30 1 45.59 40.30 2.94 o 0 30 1 26.70 24.37 2.53 o 1 30 1 23.55 16.01 2.45 o -1 31 1 9.96 9.90 2.83 o 0 31 1 106.14 99.46 3.80 o 1 31 1 73.05 85.02 3.91 o 0 32 1 121.93 124.37 6.92 o -4 0 2 25.73 21.05 2.82 o -3 0 2 1473.57 1546.50 26.24 o -2 0 2 1623.53 1657.72 27.59 o 0 0 2 369.23 341.32 5.16 o 1 0 2 1318.59 1349.09 15.50 o 2 0 2 58.33 55.71 2.19 o 3 0 2 8.52 4.59 1.34 o 4 0 2 82.70 89.16 9.44 o -4 1 2 90.04 82.55 2.81 o -3 1 2 254.13 256.83 4.19 o -2 1 2 281.26 265.29 3.87 o -1 1 2 4285.94 4316.89 71.67 o 0 1 2 3122.31 2958.88 38.14 o 1 1 2 99.32 77.48 1.08 o 2 1 2 483.65 490.97 5.76 o 3 1 2 112.61 104.00 2.08 o 4 1 2 208.59 218.40 7.87 o -4 2 2 205.60 227.25 5.34 o -3 2 2 34.62 29.26 1.46 o -2 2 2 62.28 53.95 1.40 o -1 2 2 125.14 128.42 3.55 o 0 2 2 2281.04 2178.20 19.15 o 1 2 2 35.57 13.98 0.74 o 2 2 2 11.81 5.62 0.74 o 3 2 2 0.22 2.37 1.12 o 4 2 2 144.32 143.85 6.63 o -4 3 2 0.43 1.38 2.04 o -3 3 2 56.86 57.60 1.92 o -2 3 2 432.01 426.49 5.91 o -1 3 2 78.53 68.28 1.84 o 0 3 2 3360.70 3180.01 52.64 o 1 3 2 1745.46 1563.58 13.29 o 2 3 2 56.41 57.66 1.35 o 3 3 2 395.98 425.91 5.31 o 4 3 2 137.94 135.88 5.40 o -4 4 2 287.19 296.77 6.32 o -3 4 2 0.21 -0.94 1.16 o -2 4 2 626.11 629.63 7.70 o -1 4 2 1401.58 1484.81 23.51 o 0 4 2 2145.80 1963.56 18.05 o 1 4 2 52.59 75.61 1.45 o 2 4 2 0.01 -0.11 0.64 o 3 4 2 11.42 10.98 1.12 o 4 4 2 10.16 8.16 2.09 o -4 5 2 10.82 9.61 2.22 o -3 5 2 94.42 98.75 2.51 o -2 5 2 97.68 92.10 2.34 o -1 5 2 2906.67 2836.79 30.26 o 0 5 2 230.49 255.03 2.69 o 1 5 2 836.94 863.67 11.99 o 2 5 2 157.68 139.70 2.39 o 3 5 2 0.53 1.37 0.95 o 4 5 2 198.26 193.80 4.68 o -4 6 2 4.74 4.08 1.73 o -3 6 2 62.58 57.61 3.32 o -2 6 2 245.78 266.70 3.89 o -1 6 2 221.63 209.17 3.45 o 0 6 2 1.54 -0.05 0.35 o 1 6 2 1612.75 1583.77 14.65 o 2 6 2 142.68 153.68 2.75 o 3 6 2 208.72 197.05 3.29 o 4 6 2 5.11 -0.43 2.65 o -4 7 2 4.35 3.88 2.48 o -3 7 2 59.65 49.86 2.50 o -2 7 2 233.97 239.91 3.29 o -1 7 2 6108.35 6019.75 83.06 o 0 7 2 157.72 134.24 1.49 o 1 7 2 425.51 405.21 4.27 o 2 7 2 8.24 4.40 0.71 o 3 7 2 79.35 76.69 2.32 o 4 7 2 51.05 49.61 3.49 o -4 8 2 12.39 5.34 2.29 o -3 8 2 225.43 221.06 4.12 o -2 8 2 0.58 0.01 0.62 o -1 8 2 708.42 735.66 10.03 o 0 8 2 206.80 165.27 1.86 o 1 8 2 458.76 443.48 4.46 o 2 8 2 394.82 396.67 4.71 o 3 8 2 20.10 18.47 1.46 o 4 8 2 0.72 -2.77 2.91 o -4 9 2 7.71 0.98 3.19 o -3 9 2 562.95 581.18 9.47 o -2 9 2 24.84 24.59 1.39 o -1 9 2 2167.85 2206.15 23.86 o 0 9 2 514.32 594.44 6.71 o 1 9 2 1746.66 1708.45 25.55 o 2 9 2 525.00 576.56 6.60 o 3 9 2 229.93 235.63 3.61 o 4 9 2 176.78 175.80 5.47 o -4 10 2 0.26 0.79 3.14 o -3 10 2 24.73 26.11 1.40 o -2 10 2 29.27 30.11 0.92 o -1 10 2 647.49 620.64 6.31 o 0 10 2 4837.51 4848.85 43.27 o 1 10 2 364.40 346.90 5.72 o 2 10 2 959.30 990.89 11.12 o 3 10 2 47.27 48.67 2.34 o 4 10 2 53.51 52.11 3.95 o -4 11 2 74.84 68.00 6.38 o -3 11 2 17.33 18.42 1.42 o -2 11 2 43.45 38.41 1.04 o -1 11 2 1270.61 1263.60 11.99 o 0 11 2 647.71 662.22 8.78 o 1 11 2 4000.65 4229.85 39.87 o 2 11 2 137.56 130.01 2.38 o 3 11 2 336.34 350.47 6.36 o 4 11 2 15.58 8.01 3.70 o -4 12 2 0.41 1.71 4.02 o -3 12 2 90.49 93.00 2.32 o -2 12 2 252.16 256.19 3.77 o -1 12 2 1445.83 1470.10 13.85 o 0 12 2 186.82 185.48 2.42 o 1 12 2 1218.21 1248.94 12.07 o 2 12 2 129.01 126.32 2.40 o 3 12 2 344.34 363.65 5.47 o 4 12 2 65.26 54.51 4.09 o -4 13 2 42.07 25.41 5.02 o -3 13 2 71.52 67.99 2.43 o -2 13 2 575.34 584.94 8.00 o -1 13 2 207.37 205.13 3.27 o 0 13 2 852.81 896.74 8.24 o 1 13 2 567.17 594.88 6.02 o 2 13 2 0.15 0.18 0.62 o 3 13 2 280.55 288.11 5.08 o 4 13 2 146.13 157.10 6.12 o -4 14 2 5.54 1.44 4.41 o -3 14 2 9.83 11.06 1.91 o -2 14 2 51.30 48.64 1.57 o -1 14 2 19.09 21.11 0.83 o 0 14 2 225.86 236.50 2.74 o 1 14 2 160.83 179.42 2.47 o 2 14 2 4.63 3.78 0.73 o 3 14 2 65.23 54.44 2.05 o 4 14 2 29.03 24.71 3.45 o -4 15 2 5.92 7.13 4.59 o -3 15 2 107.50 116.50 3.35 o -2 15 2 176.67 169.77 3.15 o -1 15 2 95.44 94.00 1.73 o 0 15 2 56.66 64.18 1.29 o 1 15 2 119.87 126.10 1.97 o 2 15 2 0.71 1.38 0.62 o 3 15 2 1.21 -0.65 1.25 o -4 16 2 3.69 -2.15 10.26 o -3 16 2 224.22 244.78 4.93 o -2 16 2 248.38 265.14 4.21 o -1 16 2 423.77 443.73 5.26 o 0 16 2 104.38 114.71 1.83 o 1 16 2 1.38 -0.18 0.48 o 2 16 2 32.35 27.69 1.10 o 3 16 2 268.47 286.09 5.21 o -3 17 2 48.75 51.28 3.35 o -2 17 2 0.03 0.66 1.15 o -1 17 2 675.64 676.55 7.43 o 0 17 2 510.44 550.40 5.82 o 1 17 2 5.16 3.83 0.79 o 2 17 2 87.88 76.75 1.78 o 3 17 2 15.33 15.08 2.91 o -3 18 2 490.54 536.51 8.99 o -2 18 2 0.36 0.93 1.16 o -1 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