#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/79/2237968.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237968_Fobs loop_ _publ_author_name 'Selvanayagam, S.' 'Sridhar, B.' 'Kathiravan, S.' 'Raghunathan, R.' _publ_section_title ; Methyl 9-(4-methoxyphenyl)-19-methyl-3,12-diazapentacyclo[10.7.0.0^2,10^.0^3,8^.0^13,18^]nonadeca-1(19),13(18),14,16-tetraene-10-carboxylate ; _journal_coeditor_code NG5324 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o776 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.487 _cell_angle_gamma 90.000 _cell_length_a 22.6716 _cell_length_b 8.8049 _cell_length_c 24.4314 _exptl_crystal_F_000 1840.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ng5324Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AI63m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 503.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1483.31 1481.22 55.66 o 4 0 0 3294.73 3485.62 73.65 o 6 0 0 12216.21 11745.39 218.28 o 8 0 0 2661.68 2489.28 58.09 o 10 0 0 2171.39 2263.78 56.11 o 12 0 0 931.41 1107.89 38.25 o 14 0 0 7.82 -0.55 13.55 o 16 0 0 350.00 303.79 43.83 o 18 0 0 2.55 -13.77 58.75 o 20 0 0 2245.56 2081.99 107.08 o 22 0 0 4.08 59.66 36.41 o 24 0 0 2.30 119.25 52.57 o 1 1 0 528.55 534.10 10.82 o 2 1 0 8327.48 9050.97 126.35 o 3 1 0 59517.70 62905.59 792.23 o 4 1 0 3405.21 3773.46 53.45 o 5 1 0 3241.97 3417.27 53.14 o 6 1 0 20207.19 21191.78 273.29 o 7 1 0 12555.38 12971.14 171.69 o 8 1 0 263.63 406.36 14.66 o 9 1 0 2.93 -2.58 6.56 o 10 1 0 18.20 -1.38 8.03 o 11 1 0 0.00 -0.29 8.10 o 12 1 0 3882.73 3998.78 69.05 o 13 1 0 275.63 357.77 17.57 o 14 1 0 1580.89 1676.66 36.56 o 15 1 0 206.44 209.46 22.76 o 16 1 0 28.21 34.80 15.23 o 17 1 0 125.59 102.13 23.66 o 18 1 0 246.71 266.43 31.94 o 19 1 0 147.25 193.76 38.38 o 20 1 0 121.49 135.08 28.24 o 21 1 0 40.35 52.05 24.38 o 22 1 0 80.07 136.94 30.39 o 23 1 0 7.92 26.31 24.54 o 24 1 0 150.26 190.16 33.80 o 25 1 0 3.36 36.15 29.90 o 0 2 0 1791.24 1671.92 46.20 o 1 2 0 16154.29 16963.73 233.25 o 2 2 0 12990.30 13055.67 169.83 o 3 2 0 68.70 104.80 8.19 o 4 2 0 17762.14 18379.29 237.99 o 5 2 0 4368.58 4510.78 76.24 o 6 2 0 2451.65 2604.28 42.41 o 7 2 0 151.40 208.71 11.93 o 8 2 0 1666.01 1634.32 33.76 o 9 2 0 12386.45 13164.01 177.70 o 10 2 0 380.04 506.03 18.93 o 11 2 0 186.98 224.35 14.54 o 12 2 0 254.78 265.18 16.02 o 13 2 0 54.66 51.44 11.39 o 14 2 0 254.75 252.74 19.52 o 15 2 0 194.32 230.78 21.67 o 16 2 0 92.03 108.81 20.90 o 17 2 0 208.82 170.44 24.32 o 18 2 0 28.32 19.99 21.42 o 19 2 0 27.31 7.21 21.65 o 20 2 0 677.39 616.11 48.59 o 21 2 0 19.73 5.81 44.19 o 22 2 0 11.07 31.27 23.93 o 23 2 0 1.05 19.32 23.85 o 24 2 0 39.79 80.20 30.00 o 1 3 0 1541.32 1505.23 26.91 o 2 3 0 15294.68 16284.43 212.92 o 3 3 0 1182.98 1066.95 24.40 o 4 3 0 3016.65 3211.98 50.57 o 5 3 0 14854.00 15725.75 207.88 o 6 3 0 21.15 31.31 8.38 o 7 3 0 1180.80 1217.62 27.23 o 8 3 0 15145.02 16279.13 217.97 o 9 3 0 1382.49 1344.43 30.46 o 10 3 0 2609.95 2861.89 59.00 o 11 3 0 13.29 7.81 10.20 o 12 3 0 69.78 68.85 12.93 o 13 3 0 2877.05 2853.97 58.07 o 14 3 0 359.18 379.91 23.44 o 15 3 0 84.14 88.35 18.23 o 16 3 0 130.86 141.90 20.72 o 17 3 0 575.86 529.24 35.73 o 18 3 0 576.33 538.89 37.84 o 19 3 0 0.27 16.49 24.99 o 20 3 0 26.62 7.15 22.94 o 21 3 0 228.12 194.70 32.31 o 22 3 0 0.11 5.51 23.41 o 23 3 0 12.31 64.94 26.28 o 24 3 0 22.29 58.11 32.14 o 0 4 0 145.89 217.41 25.44 o 1 4 0 418.56 422.64 16.68 o 2 4 0 5118.93 5650.50 82.34 o 3 4 0 175.85 210.96 11.86 o 4 4 0 2341.21 2960.96 55.09 o 5 4 0 4904.20 5524.59 82.63 o 6 4 0 2273.06 2260.13 41.78 o 7 4 0 72.11 85.14 11.57 o 8 4 0 2171.51 2343.74 44.40 o 9 4 0 267.23 200.68 15.32 o 10 4 0 160.83 129.93 14.27 o 11 4 0 42.77 95.47 14.17 o 12 4 0 38.41 30.30 14.45 o 13 4 0 0.35 9.42 13.28 o 14 4 0 1329.93 1275.69 38.66 o 15 4 0 122.54 119.65 20.26 o 16 4 0 762.30 704.70 36.68 o 17 4 0 1088.63 944.22 41.84 o 18 4 0 338.37 340.80 33.02 o 19 4 0 43.68 50.91 22.00 o 20 4 0 13.49 58.31 24.79 o 21 4 0 154.20 136.71 37.02 o 22 4 0 0.24 23.55 25.15 o 23 4 0 52.36 91.96 28.07 o 1 5 0 7159.67 6763.87 106.86 o 2 5 0 3.21 -2.49 9.70 o 3 5 0 1645.60 1436.88 34.69 o 4 5 0 1417.30 1371.05 30.55 o 5 5 0 199.22 187.47 13.64 o 6 5 0 146.18 186.03 14.54 o 7 5 0 1133.24 1081.66 31.96 o 8 5 0 40.74 40.68 11.98 o 9 5 0 16.21 17.12 11.60 o 10 5 0 266.17 244.45 18.41 o 11 5 0 67.40 75.20 14.40 o 12 5 0 7.50 6.33 14.49 o 13 5 0 117.10 127.50 18.82 o 14 5 0 1570.77 1436.56 46.66 o 15 5 0 379.45 345.28 35.15 o 16 5 0 178.59 140.75 24.70 o 17 5 0 99.86 111.97 23.51 o 18 5 0 13.03 25.06 20.63 o 19 5 0 197.60 196.94 32.96 o 20 5 0 152.23 213.00 47.31 o 21 5 0 52.14 97.05 33.55 o 22 5 0 33.76 109.37 32.14 o 0 6 0 1171.20 1106.70 53.89 o 1 6 0 149.02 163.86 20.11 o 2 6 0 952.13 1015.78 37.71 o 3 6 0 40.04 64.27 17.78 o 4 6 0 360.30 347.13 25.69 o 5 6 0 13.52 -7.21 14.49 o 6 6 0 238.06 267.84 25.58 o 7 6 0 169.51 164.36 21.67 o 8 6 0 378.06 383.73 27.66 o 9 6 0 427.72 356.91 27.72 o 10 6 0 190.22 167.75 23.85 o 11 6 0 99.75 94.43 27.07 o 12 6 0 74.02 66.40 21.10 o 13 6 0 60.31 95.98 22.25 o 14 6 0 24.04 45.72 19.37 o 15 6 0 18.77 -3.41 18.90 o 16 6 0 242.96 212.75 28.96 o 17 6 0 141.25 166.21 27.74 o 18 6 0 0.79 20.68 21.43 o 19 6 0 4.79 51.59 32.14 o 20 6 0 5.27 60.17 27.33 o 1 7 0 46.96 31.81 18.02 o 2 7 0 0.49 -20.86 16.23 o 3 7 0 5.77 44.87 18.65 o 4 7 0 651.19 574.73 46.33 o 5 7 0 291.41 263.23 26.96 o 6 7 0 3554.86 3175.18 74.62 o 7 7 0 12.76 -15.80 18.17 o 8 7 0 261.19 199.29 25.53 o 9 7 0 1455.99 1283.18 51.49 o 10 7 0 1093.42 1069.50 49.92 o 11 7 0 40.55 -11.32 20.39 o 12 7 0 2.53 13.53 20.16 o 13 7 0 455.57 444.07 40.62 o 14 7 0 58.32 20.94 24.50 o 15 7 0 84.68 91.62 27.57 o 16 7 0 1.71 43.88 27.23 o 17 7 0 41.00 131.97 30.63 o 18 7 0 3.94 138.44 36.15 o 0 8 0 344.06 420.31 59.71 o 1 8 0 939.05 937.31 56.93 o 2 8 0 695.58 894.61 42.88 o 3 8 0 15.14 18.61 28.34 o 4 8 0 590.69 609.28 37.05 o 5 8 0 130.91 143.37 24.48 o 6 8 0 583.47 502.91 35.70 o 7 8 0 115.19 102.22 22.25 o 8 8 0 128.72 103.39 23.51 o 9 8 0 3.81 -15.21 22.24 o 10 8 0 2.39 17.38 22.07 o 11 8 0 29.62 37.06 23.63 o 12 8 0 10.76 18.98 21.98 o 13 8 0 80.07 126.43 29.20 o 14 8 0 287.69 369.69 40.79 o 15 8 0 135.00 269.77 37.94 o 16 8 0 28.83 161.47 32.59 o 1 9 0 50.58 71.46 23.89 o 2 9 0 48.87 32.66 21.30 o 3 9 0 247.17 206.10 27.34 o 4 9 0 52.94 64.37 23.54 o 5 9 0 615.38 538.79 38.41 o 6 9 0 169.43 121.89 25.32 o 7 9 0 30.56 57.00 27.89 o 8 9 0 11.29 68.11 25.15 o 9 9 0 2.81 84.05 25.07 o 10 9 0 15.14 78.59 27.70 o 11 9 0 33.12 26.85 25.88 o 12 9 0 1.26 59.44 47.76 o 0 10 0 781.33 922.56 74.59 o 1 10 0 0.09 23.87 23.05 o 2 10 0 13.76 23.91 22.59 o 3 10 0 87.91 159.44 28.12 o 4 10 0 13.85 79.67 22.86 o 5 10 0 48.91 81.38 27.80 o 6 10 0 168.83 203.02 38.34 o 7 10 0 54.66 123.93 32.41 o -25 0 1 65.79 34.74 66.48 o -23 0 1 128.55 187.70 44.79 o -21 0 1 274.23 282.64 52.34 o -19 0 1 403.54 340.09 49.16 o -17 0 1 343.77 222.25 41.37 o -15 0 1 2144.31 1989.67 58.11 o -13 0 1 279.39 329.29 23.78 o -11 0 1 908.48 916.40 33.22 o -9 0 1 1.08 1.86 8.80 o -7 0 1 1647.79 1623.25 39.80 o -5 0 1 32.43 42.20 8.70 o -3 0 1 735.29 601.57 18.39 o -1 0 1 72.34 -3.28 2.19 o 1 0 1 52.89 53.81 8.31 o 3 0 1 5581.38 5096.08 109.97 o 5 0 1 980.84 940.69 26.09 o 7 0 1 1544.57 1341.51 45.53 o 9 0 1 1001.88 893.02 30.29 o 11 0 1 2074.65 2151.44 59.58 o 13 0 1 283.61 251.07 21.20 o 15 0 1 451.50 468.12 36.85 o 17 0 1 2.30 -39.94 44.84 o 19 0 1 30.50 36.76 29.46 o 21 0 1 340.60 393.02 58.92 o 23 0 1 373.34 435.57 63.30 o -25 1 1 87.90 106.73 30.90 o -24 1 1 55.42 113.30 35.71 o -23 1 1 17.10 61.20 25.75 o -22 1 1 18.58 63.57 25.61 o -21 1 1 19.67 3.36 22.22 o -20 1 1 248.57 259.20 33.91 o -19 1 1 601.86 614.23 49.54 o -18 1 1 69.05 96.82 24.89 o -17 1 1 221.60 196.51 23.75 o -16 1 1 31.60 40.00 17.25 o -15 1 1 762.05 761.22 30.81 o -14 1 1 116.09 135.98 13.47 o -13 1 1 1073.81 1005.84 28.33 o -12 1 1 1065.45 1052.27 25.95 o -11 1 1 749.91 633.57 20.14 o -10 1 1 2101.63 1940.12 36.19 o -9 1 1 754.34 678.32 18.70 o -8 1 1 45.77 47.48 7.84 o -7 1 1 2530.96 2235.55 36.80 o -6 1 1 306.72 351.47 14.86 o -5 1 1 491.40 529.36 14.37 o -4 1 1 1823.77 1536.37 26.93 o -3 1 1 309.72 258.47 8.26 o -2 1 1 218.36 271.16 7.28 o -1 1 1 6.17 12.16 3.23 o 0 1 1 57.57 54.95 4.23 o 1 1 1 247.25 219.04 6.53 o 2 1 1 18.32 45.43 4.36 o 3 1 1 93.97 72.04 6.10 o 4 1 1 3813.92 3335.40 48.54 o 5 1 1 1594.68 1638.83 27.98 o 6 1 1 273.62 245.29 10.76 o 7 1 1 1334.08 1103.56 22.86 o 8 1 1 45.79 29.52 7.37 o 9 1 1 2223.10 2131.50 37.89 o 10 1 1 547.54 469.43 22.76 o 11 1 1 12.40 6.02 8.18 o 12 1 1 939.67 849.72 24.13 o 13 1 1 2302.65 2204.29 43.00 o 14 1 1 153.94 170.41 16.37 o 15 1 1 115.86 85.23 15.05 o 16 1 1 2034.31 1787.12 54.58 o 17 1 1 38.09 41.79 20.31 o 18 1 1 665.56 607.95 45.59 o 19 1 1 329.58 264.04 33.85 o 20 1 1 228.03 219.09 33.48 o 21 1 1 247.11 272.09 35.37 o 22 1 1 440.44 420.98 42.73 o 23 1 1 1.98 20.92 24.25 o 24 1 1 43.91 83.16 30.00 o -25 2 1 47.74 95.82 30.87 o -24 2 1 130.71 174.79 45.08 o -23 2 1 0.09 49.84 25.72 o -22 2 1 336.70 394.54 41.79 o -21 2 1 21.27 44.03 25.10 o -20 2 1 59.54 80.70 26.22 o -19 2 1 256.54 261.74 33.97 o -18 2 1 1134.29 1029.08 46.88 o -17 2 1 0.21 -22.68 18.46 o -16 2 1 197.74 213.60 21.79 o -15 2 1 227.28 283.04 22.92 o -14 2 1 123.47 103.66 13.69 o -13 2 1 251.27 241.86 15.72 o -12 2 1 45.95 44.10 10.11 o -11 2 1 50.54 59.07 10.39 o -10 2 1 2571.92 2511.15 44.67 o -9 2 1 168.94 192.89 13.03 o -8 2 1 203.05 210.32 12.88 o -7 2 1 49.98 34.45 8.65 o -6 2 1 267.86 280.14 12.42 o -5 2 1 1244.73 1176.31 27.76 o -4 2 1 210.67 183.23 10.52 o -3 2 1 125.42 152.29 9.28 o -2 2 1 473.87 432.66 12.81 o -1 2 1 168.92 128.29 9.36 o 0 2 1 12.86 20.69 7.55 o 1 2 1 311.57 336.31 10.94 o 2 2 1 87.93 68.02 7.44 o 3 2 1 147.54 144.26 9.54 o 4 2 1 31.12 4.64 6.23 o 5 2 1 470.44 499.40 15.52 o 6 2 1 214.32 209.02 11.48 o 7 2 1 2057.16 2004.97 36.05 o 8 2 1 685.04 682.90 19.73 o 9 2 1 2301.31 2596.83 45.28 o 10 2 1 1209.62 1263.33 28.76 o 11 2 1 6.57 5.64 8.96 o 12 2 1 86.68 93.34 11.85 o 13 2 1 286.28 300.50 20.12 o 14 2 1 754.15 762.90 28.90 o 15 2 1 265.15 282.11 21.24 o 16 2 1 479.63 470.86 35.74 o 17 2 1 73.59 73.04 18.24 o 18 2 1 7.21 12.04 21.15 o 19 2 1 340.02 355.17 37.97 o 20 2 1 1067.18 938.25 57.37 o 21 2 1 22.80 69.64 26.89 o 22 2 1 6.37 33.63 27.23 o 23 2 1 195.55 230.62 35.70 o 24 2 1 164.57 205.66 40.17 o -24 3 1 245.66 207.37 54.01 o -23 3 1 210.75 210.62 32.32 o -22 3 1 17.92 47.43 23.96 o -21 3 1 0.07 35.81 23.63 o -20 3 1 235.54 143.80 33.83 o -19 3 1 68.35 83.38 22.55 o -18 3 1 191.12 133.82 24.25 o -17 3 1 49.42 75.49 18.50 o -16 3 1 348.68 402.25 28.16 o -15 3 1 493.46 536.00 30.31 o -14 3 1 548.92 626.45 30.81 o -13 3 1 233.15 265.77 19.46 o -12 3 1 409.79 416.77 20.18 o -11 3 1 92.27 126.10 13.04 o -10 3 1 32.92 33.00 9.99 o -9 3 1 1140.39 1107.84 28.58 o -8 3 1 3659.77 3457.48 56.55 o -7 3 1 545.30 581.15 19.14 o -6 3 1 233.26 289.68 19.72 o -5 3 1 741.49 746.33 19.44 o -4 3 1 73.54 79.27 8.81 o -3 3 1 16.61 22.44 7.40 o -2 3 1 596.94 574.75 18.23 o -1 3 1 96.36 111.17 9.76 o 0 3 1 10.78 4.32 7.29 o 1 3 1 9.39 7.53 5.78 o 2 3 1 241.78 210.71 10.47 o 3 3 1 891.70 807.02 19.50 o 4 3 1 3044.12 3074.66 49.18 o 5 3 1 983.47 965.37 22.53 o 6 3 1 38.19 20.35 8.36 o 7 3 1 1638.28 1774.87 37.32 o 8 3 1 81.94 55.01 10.18 o 9 3 1 1578.53 1479.33 32.21 o 10 3 1 2063.85 1909.51 38.97 o 11 3 1 1148.87 1077.35 28.69 o 12 3 1 3418.87 3464.51 66.43 o 13 3 1 349.14 364.29 23.01 o 14 3 1 12.47 30.73 14.09 o 15 3 1 0.02 12.75 15.85 o 16 3 1 29.33 12.41 17.12 o 17 3 1 231.85 251.85 25.22 o 18 3 1 63.53 87.48 36.79 o 19 3 1 150.32 147.54 29.68 o 20 3 1 44.95 76.52 25.81 o 21 3 1 3.82 22.52 22.88 o 22 3 1 80.82 95.63 38.83 o 23 3 1 21.08 87.18 30.80 o -23 4 1 13.98 65.24 26.94 o -22 4 1 0.30 49.77 30.91 o -21 4 1 17.45 68.94 26.36 o -20 4 1 14.60 25.05 24.09 o -19 4 1 0.94 8.99 19.55 o -18 4 1 21.61 22.27 20.84 o -17 4 1 32.92 38.21 18.40 o -16 4 1 196.79 214.10 23.73 o -15 4 1 70.83 54.40 17.98 o -14 4 1 301.31 277.66 25.13 o -13 4 1 141.94 110.24 16.88 o -12 4 1 1297.80 1148.72 31.47 o -11 4 1 112.36 118.65 14.61 o -10 4 1 120.95 155.38 14.92 o -9 4 1 1072.64 1059.13 27.95 o -8 4 1 84.50 98.74 12.38 o -7 4 1 3.17 -2.59 9.18 o -6 4 1 6.12 -6.99 8.53 o -5 4 1 572.89 630.54 20.18 o -4 4 1 84.56 60.60 9.05 o -3 4 1 156.94 171.97 16.98 o -2 4 1 201.98 236.10 14.25 o -1 4 1 6.94 53.10 13.38 o 0 4 1 65.16 199.13 20.27 o 1 4 1 17.86 0.43 7.86 o 2 4 1 85.02 159.01 16.07 o 3 4 1 116.21 150.64 15.21 o 4 4 1 2307.67 2468.92 56.57 o 5 4 1 732.46 767.51 23.17 o 6 4 1 385.80 465.79 20.34 o 7 4 1 203.93 245.71 15.86 o 8 4 1 1.03 -6.47 9.52 o 9 4 1 7.14 28.55 10.49 o 10 4 1 94.60 159.56 15.13 o 11 4 1 627.48 602.23 28.05 o 12 4 1 16.88 19.65 15.10 o 13 4 1 109.06 87.52 16.35 o 14 4 1 19.03 16.91 14.45 o 15 4 1 1.91 27.33 16.91 o 16 4 1 359.82 399.80 35.40 o 17 4 1 3.40 -2.85 16.07 o 18 4 1 51.89 94.92 20.09 o 19 4 1 105.44 102.84 26.36 o 20 4 1 39.61 84.02 34.86 o 21 4 1 109.03 116.47 28.07 o 22 4 1 15.25 69.97 27.98 o 23 4 1 43.19 125.59 30.96 o -22 5 1 9.73 68.48 32.13 o -21 5 1 7.02 51.50 26.58 o -20 5 1 106.25 134.59 30.23 o -19 5 1 187.60 218.63 32.96 o -18 5 1 22.23 43.41 23.66 o -17 5 1 7.81 17.30 18.90 o -16 5 1 15.56 58.03 22.96 o -15 5 1 951.49 962.18 46.08 o -14 5 1 888.71 891.79 48.36 o -13 5 1 1.54 17.14 23.03 o -12 5 1 34.32 27.77 14.71 o -11 5 1 162.26 144.85 17.80 o -10 5 1 38.95 18.62 13.50 o -9 5 1 31.16 24.51 13.09 o -8 5 1 18.39 31.98 12.83 o -7 5 1 49.30 48.02 13.34 o -6 5 1 338.20 345.17 20.79 o -5 5 1 0.23 -4.23 10.53 o -4 5 1 24.95 27.65 11.43 o -3 5 1 1022.52 900.89 27.94 o -2 5 1 47.22 28.63 10.63 o -1 5 1 1210.96 1094.65 28.94 o 0 5 1 339.88 350.64 18.18 o 1 5 1 201.71 254.33 16.43 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49.72 o -1 0 27 65.49 138.85 42.26 o -17 1 27 5.68 52.10 28.97 o -16 1 27 79.52 214.96 52.23 o -15 1 27 25.16 60.83 54.01 o -14 1 27 0.84 67.54 31.24 o -13 1 27 29.67 79.89 30.50 o -12 1 27 117.77 160.05 43.29 o -11 1 27 30.70 85.89 30.63 o -10 1 27 10.69 46.35 28.06 o -9 1 27 3.10 66.74 41.96 o -8 1 27 12.96 42.39 28.57 o -7 1 27 92.45 110.42 27.11 o -6 1 27 64.01 43.52 29.21 o -5 1 27 141.51 159.90 41.96 o -4 1 27 31.80 27.05 33.48 o -3 1 27 19.70 25.28 28.57 o -2 1 27 20.97 54.88 27.04 o -1 1 27 22.55 18.56 22.19 o 0 1 27 0.20 24.48 27.62 o -16 2 27 2.88 61.56 28.52 o -15 2 27 13.06 107.01 30.15 o -14 2 27 0.02 101.91 31.37 o -13 2 27 197.99 354.32 63.38 o -12 2 27 95.43 103.19 41.51 o -11 2 27 156.14 192.27 35.23 o -10 2 27 97.50 123.28 31.91 o -9 2 27 54.08 106.59 52.09 o -8 2 27 0.34 37.42 31.33 o -7 2 27 1.90 40.26 24.53 o -6 2 27 111.03 163.67 29.53 o -5 2 27 87.67 63.56 30.00 o -4 2 27 115.26 139.70 37.05 o -3 2 27 9.44 38.43 34.43 o -2 2 27 0.07 29.18 24.91 o -1 2 27 21.65 56.37 28.52 o -14 3 27 8.77 74.73 40.47 o -13 3 27 1.82 52.66 39.25 o -12 3 27 7.02 86.01 29.67 o -11 3 27 2.07 22.90 44.72 o -10 3 27 3.05 98.86 35.63 o -9 3 27 48.77 103.26 32.49 o -8 3 27 11.88 23.08 33.92 o -7 3 27 58.87 134.70 32.18 o -6 3 27 8.95 -6.23 24.13 o -5 3 27 48.35 97.35 28.18 o -4 3 27 0.61 -8.08 33.48 o -3 3 27 5.53 24.34 30.29 o -14 0 28 74.37 162.22 51.93 o -12 0 28 23.60 127.21 52.57 o -10 0 28 401.45 430.00 191.72 o -8 0 28 1.24 52.57 68.03 o -6 0 28 42.87 15.46 64.94 o -4 0 28 1.29 40.29 38.22 o -15 1 28 224.15 265.37 40.60 o -14 1 28 14.07 39.34 28.43 o -13 1 28 5.55 11.18 32.48 o -12 1 28 84.15 101.22 32.71 o -11 1 28 100.76 155.60 31.61 o -10 1 28 36.06 45.10 36.15 o -9 1 28 81.81 38.94 70.40 o -8 1 28 77.86 106.59 70.31 o -7 1 28 3.64 -17.17 27.23 o -6 1 28 0.03 -1.11 28.84 o -5 1 28 2.52 9.61 27.68 o -4 1 28 25.23 50.69 28.66 o -3 1 28 27.56 76.59 28.84 o -13 2 28 55.17 72.50 29.45 o -12 2 28 3.27 79.80 32.05 o -11 2 28 4.22 120.99 32.76 o -10 2 28 14.96 76.92 35.22 o -9 2 28 1.24 -5.13 36.10 o -8 2 28 93.85 86.66 32.09 o -7 2 28 0.01 51.87 29.90 o -6 2 28 6.30 42.26 29.32 o -5 2 28 20.66 34.04 27.51 o -9 0 29 205.38 259.75 95.86 o