#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/80/2238051.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238051_Fobs loop_ _publ_author_name 'Bozkurt, Nihat' 'Dilek, Nefise' '\,Caylak Deliba\,s, Nagihan' 'Necefo\(glu, Hacali' 'H\"okelek, Tuncer' _publ_section_title ; Diaquabis(3-chlorobenzoato-\kO)bis(nicotinamide-\kN^1^)cobalt(II) ; _journal_coeditor_code SU2606 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m349 _journal_page_last m350 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.546 _cell_angle_gamma 90.000 _cell_length_a 11.5181 _cell_length_b 8.8191 _cell_length_c 13.5089 _exptl_crystal_F_000 666.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file su2606Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bn2_15mayis_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 170.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17154.04 8177.44 490.96 o 4 0 0 342.54 346.57 3.96 o 6 0 0 3601.17 3797.32 79.90 o 8 0 0 76.91 60.93 3.82 o 10 0 0 29.75 33.00 3.09 o 12 0 0 766.60 767.56 12.03 o 14 0 0 246.59 265.46 6.45 o 1 1 0 902.77 976.86 15.16 o 2 1 0 172.66 193.12 1.81 o 3 1 0 5396.43 5259.97 78.93 o 4 1 0 2326.44 2427.86 26.87 o 5 1 0 6236.00 6396.97 131.93 o 6 1 0 2224.00 2449.74 35.72 o 7 1 0 1011.17 1003.69 9.15 o 8 1 0 936.89 920.63 8.65 o 9 1 0 671.77 675.08 6.72 o 10 1 0 1122.70 1103.64 11.53 o 11 1 0 682.58 694.66 7.93 o 12 1 0 507.22 466.14 5.55 o 13 1 0 15.45 16.44 0.77 o 14 1 0 8.40 8.86 0.87 o 0 2 0 538.76 565.83 8.66 o 1 2 0 5334.00 5781.78 49.25 o 2 2 0 1290.03 1388.37 12.07 o 3 2 0 751.37 781.28 6.43 o 4 2 0 3442.38 3310.22 28.80 o 5 2 0 8418.06 9112.97 161.82 o 6 2 0 2563.28 2450.66 19.86 o 7 2 0 245.56 196.46 1.85 o 8 2 0 312.79 297.01 2.75 o 9 2 0 0.42 0.30 0.35 o 10 2 0 4.37 7.40 0.44 o 11 2 0 7.62 3.64 0.58 o 12 2 0 34.38 33.20 1.13 o 13 2 0 52.17 54.34 1.48 o 14 2 0 9.28 10.21 0.85 o 1 3 0 1271.40 1314.36 12.46 o 2 3 0 72.39 89.08 1.16 o 3 3 0 47.31 69.68 0.79 o 4 3 0 3427.23 3588.61 46.99 o 5 3 0 38.62 22.48 0.40 o 6 3 0 0.60 1.74 0.23 o 7 3 0 433.98 414.80 4.02 o 8 3 0 6.73 3.62 0.36 o 9 3 0 316.54 297.70 3.31 o 10 3 0 313.02 279.78 3.34 o 11 3 0 1316.79 1236.75 12.76 o 12 3 0 212.40 188.96 3.13 o 13 3 0 298.42 298.61 4.97 o 0 4 0 3809.09 3931.24 49.84 o 1 4 0 25.37 35.95 0.68 o 2 4 0 5958.68 6115.50 53.85 o 3 4 0 20.00 13.66 0.45 o 4 4 0 619.75 607.07 5.59 o 5 4 0 239.96 224.43 2.14 o 6 4 0 213.48 219.99 2.23 o 7 4 0 3.64 4.25 0.45 o 8 4 0 454.49 465.89 5.16 o 9 4 0 157.49 170.24 2.37 o 10 4 0 201.16 212.10 2.83 o 11 4 0 9.75 7.49 0.67 o 12 4 0 275.91 286.43 4.07 o 13 4 0 22.42 29.86 2.27 o 1 5 0 128.43 147.71 1.83 o 2 5 0 371.26 393.78 4.05 o 3 5 0 2433.88 2505.31 21.72 o 4 5 0 2.97 3.14 0.26 o 5 5 0 1110.20 1145.49 11.12 o 6 5 0 113.17 107.74 1.23 o 7 5 0 1348.53 1352.24 12.99 o 8 5 0 37.30 42.40 0.87 o 9 5 0 1051.37 1033.47 12.21 o 10 5 0 448.41 406.79 4.81 o 11 5 0 177.10 165.02 2.58 o 12 5 0 3.25 3.24 0.70 o 0 6 0 237.90 276.29 6.11 o 1 6 0 151.64 168.00 4.15 o 2 6 0 332.62 317.85 3.82 o 3 6 0 219.54 200.55 2.35 o 4 6 0 41.53 40.00 0.72 o 5 6 0 1441.36 1429.75 13.12 o 6 6 0 1090.89 1080.72 11.86 o 7 6 0 2.88 1.94 0.62 o 8 6 0 257.81 252.80 3.58 o 9 6 0 72.44 78.66 1.94 o 10 6 0 255.12 263.85 4.76 o 11 6 0 0.86 0.80 0.75 o 12 6 0 270.90 278.00 5.15 o 1 7 0 618.04 600.32 10.15 o 2 7 0 110.38 109.03 1.95 o 3 7 0 666.69 650.45 9.16 o 4 7 0 347.56 334.82 4.81 o 5 7 0 101.41 92.01 1.74 o 6 7 0 116.35 118.99 2.22 o 7 7 0 64.32 65.06 1.36 o 8 7 0 5.63 6.79 0.87 o 9 7 0 416.74 420.56 5.75 o 10 7 0 0.64 0.93 0.91 o 11 7 0 71.58 87.03 2.36 o 0 8 0 11.39 11.77 2.21 o 1 8 0 348.95 346.56 5.60 o 2 8 0 501.09 511.87 8.22 o 3 8 0 291.56 289.59 4.23 o 4 8 0 700.29 689.22 12.31 o 5 8 0 5.26 1.35 0.58 o 6 8 0 393.16 402.95 8.94 o 7 8 0 116.51 108.28 2.55 o 8 8 0 295.50 304.43 4.90 o 9 8 0 0.60 1.40 0.90 o 1 9 0 306.26 298.02 5.03 o 2 9 0 1.35 1.39 0.62 o 3 9 0 49.20 53.46 1.96 o 4 9 0 1.12 0.55 0.86 o 5 9 0 380.33 394.80 6.43 o 6 9 0 0.60 0.25 1.16 o 7 9 0 233.39 246.37 6.75 o 8 9 0 25.85 30.41 3.82 o 0 10 0 133.38 124.96 4.04 o 1 10 0 0.27 0.24 0.78 o 2 10 0 292.54 300.79 6.21 o 3 10 0 112.39 108.50 3.03 o 4 10 0 132.16 129.06 3.31 o 5 10 0 5.82 4.64 0.81 o 6 10 0 15.24 13.96 1.19 o -13 0 1 76.02 67.95 3.40 o -11 0 1 13.81 18.21 1.24 o -9 0 1 92.41 88.54 1.62 o -7 0 1 1061.99 991.57 12.97 o -5 0 1 4433.62 4122.39 136.19 o -3 0 1 913.91 812.75 21.59 o -1 0 1 6666.31 5061.30 335.57 o 3 0 1 2599.55 2654.55 51.06 o 5 0 1 9411.44 9783.47 196.79 o 7 0 1 1864.23 1814.41 21.64 o 9 0 1 169.91 168.04 2.84 o 11 0 1 23.34 21.76 1.21 o 13 0 1 13.36 12.63 1.57 o -14 1 1 165.73 164.20 2.89 o -13 1 1 8.72 8.17 0.57 o -12 1 1 573.66 561.87 6.46 o -11 1 1 64.21 63.23 1.54 o -10 1 1 781.79 779.93 9.70 o -9 1 1 257.48 247.11 2.60 o -8 1 1 359.99 330.25 3.23 o -7 1 1 252.43 232.17 2.45 o -6 1 1 2043.26 2137.99 38.08 o -5 1 1 1001.77 1104.97 10.24 o -4 1 1 209.29 249.49 2.55 o -3 1 1 461.55 440.70 4.13 o -2 1 1 1644.96 1656.45 17.76 o -1 1 1 106.02 98.21 1.09 o 0 1 1 3842.30 4244.45 34.40 o 1 1 1 116.51 134.77 1.44 o 2 1 1 83.47 120.00 1.17 o 3 1 1 3598.91 3665.76 29.50 o 4 1 1 9081.61 9113.08 156.66 o 5 1 1 1134.81 1189.76 9.50 o 6 1 1 1605.35 1677.82 14.45 o 7 1 1 954.21 1034.39 8.87 o 8 1 1 231.88 214.14 2.30 o 9 1 1 543.52 554.07 5.77 o 10 1 1 1237.78 1216.22 13.04 o 11 1 1 142.56 149.55 2.06 o 12 1 1 485.37 441.63 5.64 o 13 1 1 161.40 149.48 2.86 o 14 1 1 2.63 5.24 0.79 o -14 2 1 35.93 44.28 1.46 o -13 2 1 467.66 461.70 6.46 o -12 2 1 22.28 27.10 0.98 o -11 2 1 822.97 801.35 8.81 o -10 2 1 34.44 29.95 0.77 o -9 2 1 28.60 29.02 0.67 o -8 2 1 6.68 5.90 0.48 o -7 2 1 503.28 484.80 4.16 o -6 2 1 17.50 16.73 0.46 o -5 2 1 409.73 438.62 3.94 o -4 2 1 4850.09 4919.94 57.28 o -3 2 1 2.75 0.21 0.19 o -2 2 1 1960.88 2060.83 28.19 o -1 2 1 7283.27 7724.57 76.23 o 0 2 1 1360.56 1418.02 12.76 o 1 2 1 29213.84 29122.80 261.31 o 2 2 1 613.14 594.66 5.48 o 3 2 1 3587.01 3619.74 31.14 o 4 2 1 1956.49 2220.96 19.77 o 5 2 1 2556.46 2630.78 22.76 o 6 2 1 353.54 414.60 3.78 o 7 2 1 150.31 152.75 1.55 o 8 2 1 122.54 118.51 1.38 o 9 2 1 44.35 46.58 0.90 o 10 2 1 185.59 177.70 2.22 o 11 2 1 368.24 344.89 4.08 o 12 2 1 51.19 48.60 1.51 o 13 2 1 496.69 502.93 6.90 o 14 2 1 24.59 28.06 1.37 o -13 3 1 161.40 171.10 3.16 o -12 3 1 30.90 27.95 1.04 o -11 3 1 2.52 4.23 0.89 o -10 3 1 144.47 140.05 1.92 o -9 3 1 55.13 50.45 0.95 o -8 3 1 214.75 228.05 2.52 o -7 3 1 41.21 37.87 0.70 o -6 3 1 1012.65 952.52 8.41 o -5 3 1 0.19 0.79 0.20 o -4 3 1 3040.17 3050.50 25.51 o -3 3 1 730.11 759.68 7.02 o -2 3 1 881.61 809.57 7.55 o -1 3 1 169.29 174.40 2.04 o 0 3 1 418.88 385.52 3.57 o 1 3 1 2220.84 2368.03 19.85 o 2 3 1 2549.93 2699.22 26.04 o 3 3 1 204.83 211.22 2.11 o 4 3 1 738.38 730.45 7.27 o 5 3 1 925.18 994.59 8.84 o 6 3 1 2564.24 2652.67 24.40 o 7 3 1 624.88 668.61 6.14 o 8 3 1 1052.32 1018.03 8.76 o 9 3 1 169.41 181.22 2.32 o 10 3 1 343.09 323.46 3.84 o 11 3 1 7.16 7.09 0.60 o 12 3 1 146.42 145.00 2.12 o 13 3 1 38.15 39.06 2.05 o -13 4 1 1.21 1.39 0.68 o -12 4 1 5.99 6.30 0.70 o -11 4 1 103.86 101.11 1.77 o -10 4 1 0.03 0.19 0.51 o -9 4 1 315.14 327.14 3.73 o -8 4 1 258.82 262.60 3.10 o -7 4 1 1265.34 1243.40 11.96 o -6 4 1 59.15 68.15 0.81 o -5 4 1 2350.59 2445.34 19.98 o -4 4 1 1632.16 1782.42 15.41 o -3 4 1 4592.77 4636.71 41.71 o -2 4 1 69.63 73.99 0.86 o -1 4 1 2239.24 2287.58 22.36 o 0 4 1 4876.44 5241.85 46.96 o 1 4 1 1335.30 1363.08 12.42 o 2 4 1 545.40 588.34 5.49 o 3 4 1 72.31 67.90 0.86 o 4 4 1 210.41 213.53 2.15 o 5 4 1 83.62 76.20 0.94 o 6 4 1 15.35 11.10 0.45 o 7 4 1 1346.61 1334.67 12.68 o 8 4 1 39.00 46.67 0.96 o 9 4 1 373.42 384.46 4.17 o 10 4 1 60.61 46.72 1.08 o 11 4 1 156.44 162.89 2.39 o 12 4 1 5.64 7.24 0.73 o 13 4 1 37.67 48.48 2.89 o -12 5 1 710.73 733.88 9.42 o -11 5 1 34.39 33.57 1.41 o -10 5 1 865.80 863.05 10.61 o -9 5 1 0.01 0.53 0.50 o -8 5 1 1317.88 1324.91 14.54 o -7 5 1 165.95 164.74 2.46 o -6 5 1 426.97 416.68 4.26 o -5 5 1 8.49 10.89 0.39 o -4 5 1 967.49 931.53 8.66 o -3 5 1 1637.70 1730.73 15.08 o -2 5 1 1064.60 1002.44 9.66 o -1 5 1 12.81 8.69 0.35 o 0 5 1 508.09 479.31 5.01 o 1 5 1 2.55 7.67 0.58 o 2 5 1 1829.70 1794.69 16.51 o 3 5 1 247.18 243.00 2.54 o 4 5 1 707.82 657.20 5.95 o 5 5 1 101.81 107.86 1.44 o 6 5 1 1287.96 1296.62 12.28 o 7 5 1 8.11 7.81 0.38 o 8 5 1 141.26 135.33 1.61 o 9 5 1 64.33 60.42 1.13 o 10 5 1 347.60 343.73 4.15 o 11 5 1 2.53 2.90 0.64 o 12 5 1 498.53 521.54 8.22 o -12 6 1 16.18 17.50 1.01 o -11 6 1 407.68 425.25 5.86 o -10 6 1 2.76 3.24 0.58 o -9 6 1 464.98 476.53 6.71 o -8 6 1 24.68 30.50 0.97 o -7 6 1 303.68 310.49 4.30 o -6 6 1 488.67 502.68 5.50 o -5 6 1 1913.16 1957.47 18.36 o -4 6 1 168.61 172.21 2.04 o -3 6 1 754.81 749.91 7.98 o -2 6 1 169.89 156.68 1.91 o -1 6 1 26.97 17.21 0.56 o 0 6 1 0.82 0.41 0.29 o 1 6 1 536.15 531.16 5.77 o 2 6 1 61.50 59.09 1.24 o 3 6 1 956.83 961.86 9.89 o 4 6 1 19.13 14.90 0.63 o 5 6 1 6.42 8.82 0.47 o 6 6 1 396.75 402.85 4.06 o 7 6 1 387.02 371.82 4.04 o 8 6 1 9.85 13.05 0.76 o 9 6 1 187.22 194.99 2.76 o 10 6 1 68.83 67.17 1.81 o 11 6 1 201.05 226.31 4.89 o 12 6 1 1.13 2.33 0.95 o -11 7 1 53.55 54.35 1.52 o -10 7 1 51.22 40.84 1.53 o -9 7 1 13.91 12.43 0.78 o -8 7 1 1038.86 1030.88 14.16 o -7 7 1 1.88 1.68 0.48 o -6 7 1 3.28 3.24 0.67 o -5 7 1 24.97 22.09 1.01 o -4 7 1 15.74 15.77 0.70 o -3 7 1 222.27 213.27 3.47 o -2 7 1 536.31 550.82 7.61 o -1 7 1 79.82 87.43 1.80 o 0 7 1 104.31 98.18 1.95 o 1 7 1 8.68 10.94 0.53 o 2 7 1 1.78 2.64 0.62 o 3 7 1 8.65 7.53 0.72 o 4 7 1 250.12 252.08 3.68 o 5 7 1 2.67 3.93 0.63 o 6 7 1 202.08 216.44 3.47 o 7 7 1 221.58 212.42 3.66 o 8 7 1 248.62 246.18 4.31 o 9 7 1 6.22 9.48 1.12 o 10 7 1 331.75 318.93 6.41 o 11 7 1 0.84 2.08 0.84 o -9 8 1 227.66 237.26 4.21 o -8 8 1 42.85 41.21 1.50 o -7 8 1 221.20 232.54 4.38 o -6 8 1 247.33 262.96 5.82 o -5 8 1 1755.36 1773.85 27.81 o -4 8 1 10.55 9.28 0.64 o -3 8 1 408.77 395.60 7.23 o -2 8 1 43.01 36.56 1.23 o -1 8 1 371.56 373.53 5.98 o 0 8 1 241.75 213.57 3.91 o 1 8 1 27.85 34.86 1.20 o 2 8 1 0.01 1.66 0.74 o 3 8 1 135.74 134.21 2.75 o 4 8 1 34.44 39.96 1.20 o 5 8 1 26.09 27.31 1.18 o 6 8 1 0.01 0.79 0.53 o 7 8 1 57.22 57.23 2.16 o 8 8 1 203.57 217.63 4.03 o 9 8 1 254.40 261.59 4.28 o -8 9 1 212.42 237.56 5.53 o -7 9 1 8.09 7.04 1.31 o -6 9 1 115.50 126.53 3.01 o -5 9 1 0.28 0.66 1.11 o -4 9 1 623.20 628.34 10.54 o -3 9 1 197.17 208.08 3.85 o -2 9 1 453.60 452.21 7.99 o -1 9 1 41.33 32.21 1.28 o 0 9 1 407.87 395.16 6.41 o 1 9 1 39.15 34.39 1.20 o 2 9 1 561.15 546.70 9.44 o 3 9 1 60.82 65.39 1.55 o 4 9 1 1024.44 1019.36 16.92 o 5 9 1 13.48 14.09 1.21 o 6 9 1 388.91 387.21 8.05 o 7 9 1 0.09 0.10 1.16 o 8 9 1 127.16 120.22 3.42 o -6 10 1 3.94 4.95 0.96 o -5 10 1 134.51 140.48 5.17 o -4 10 1 1.84 1.87 0.73 o -3 10 1 446.07 464.28 8.20 o -2 10 1 124.00 123.44 3.00 o -1 10 1 677.69 672.54 11.85 o 0 10 1 228.47 224.16 4.18 o 1 10 1 164.40 169.13 3.54 o 2 10 1 13.44 11.92 0.85 o 3 10 1 582.51 600.93 11.43 o 4 10 1 0.02 1.42 0.77 o 5 10 1 94.48 85.33 2.33 o 0 11 1 104.29 115.14 3.99 o -14 0 2 103.55 112.43 4.15 o -12 0 2 689.03 692.71 11.10 o -10 0 2 4599.99 4636.03 79.68 o -8 0 2 2005.38 1955.23 24.91 o -6 0 2 996.99 1011.93 13.03 o -4 0 2 1672.70 1817.69 78.91 o -2 0 2 1566.63 1398.97 68.06 o 0 0 2 6251.63 4734.09 86.89 o 2 0 2 25172.62 23668.18 1036.89 o 4 0 2 10380.83 10664.00 253.26 o 6 0 2 2828.71 3095.36 49.23 o 8 0 2 931.43 997.93 12.80 o 10 0 2 6.07 7.17 0.74 o 12 0 2 14.49 12.80 1.78 o 14 0 2 130.93 150.65 5.40 o -14 1 2 172.88 176.03 3.30 o -13 1 2 648.85 654.40 8.43 o -12 1 2 0.19 1.20 0.56 o -11 1 2 37.79 43.68 1.68 o -10 1 2 78.49 80.74 1.77 o -9 1 2 6.07 7.74 0.57 o -8 1 2 36.22 32.96 0.71 o -7 1 2 1088.32 1093.94 10.44 o -6 1 2 2077.25 2150.04 31.13 o -5 1 2 1909.21 2010.48 30.94 o -4 1 2 94.52 73.26 1.02 o -3 1 2 5.62 7.66 0.72 o -2 1 2 2073.32 2171.69 24.37 o -1 1 2 10216.85 9915.57 109.36 o 0 1 2 2.51 0.00 0.12 o 1 1 2 344.10 342.80 2.56 o 2 1 2 4805.85 5241.40 54.39 o 3 1 2 1857.68 1915.40 19.66 o 4 1 2 59.27 38.03 0.73 o 5 1 2 5435.13 5470.12 50.99 o 6 1 2 3327.88 3417.40 45.20 o 7 1 2 254.15 225.77 2.31 o 8 1 2 164.82 160.00 1.62 o 9 1 2 698.93 694.63 6.46 o 10 1 2 51.51 44.54 1.16 o 11 1 2 599.67 579.86 6.96 o 12 1 2 107.93 104.64 2.04 o 13 1 2 97.35 99.60 1.77 o 14 1 2 246.80 249.57 3.88 o -14 2 2 108.22 112.08 2.53 o -13 2 2 22.83 29.78 1.25 o -12 2 2 40.88 36.39 1.51 o -11 2 2 187.39 179.88 2.70 o -10 2 2 12.98 9.08 0.62 o -9 2 2 57.38 60.47 1.08 o -8 2 2 5.15 5.25 0.37 o -7 2 2 27.58 27.12 0.51 o -6 2 2 1418.09 1312.98 11.33 o -5 2 2 439.21 447.64 4.02 o -4 2 2 911.87 805.13 7.24 o -3 2 2 11.64 13.69 0.81 o -2 2 2 4877.02 4734.53 65.78 o -1 2 2 2776.92 2833.86 24.84 o 0 2 2 375.69 384.77 3.51 o 1 2 2 16108.65 17916.63 176.68 o 2 2 2 2919.60 3222.29 26.24 o 3 2 2 712.55 787.39 7.36 o 4 2 2 5.14 2.66 0.16 o 5 2 2 205.95 189.47 1.89 o 6 2 2 1221.45 1184.35 10.15 o 7 2 2 904.39 939.85 8.37 o 8 2 2 774.47 744.47 6.74 o 9 2 2 3.48 4.06 0.35 o 10 2 2 1742.62 1745.97 17.96 o 11 2 2 27.50 29.21 0.93 o 12 2 2 697.76 653.10 7.72 o 13 2 2 2.17 3.37 0.93 o 14 2 2 47.49 45.67 1.56 o -13 3 2 197.99 187.51 3.19 o -12 3 2 3.29 3.92 0.55 o -11 3 2 1314.89 1313.25 16.12 o -10 3 2 1.10 1.45 0.45 o -9 3 2 1173.16 1162.01 11.37 o -8 3 2 1481.69 1481.57 13.84 o -7 3 2 251.78 225.88 2.34 o -6 3 2 129.19 110.95 1.42 o -5 3 2 61.93 28.55 0.44 o -4 3 2 647.21 722.74 6.18 o -3 3 2 131.10 162.48 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