#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/80/2238059.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238059_Fobs loop_ _publ_author_name 'Ourhriss, Naja' 'Benharref, Ahmed' 'Oukhrib, Abdelouahd' 'Daran, Jean-Claude' 'Berraho, Moha' _publ_section_title ; (1S,3R,8R)-2,2-Dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3^]dodec-9-en-11-one ; _journal_coeditor_code TK5222 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o830 _journal_volume 69 _journal_year 2013 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.805 _cell_angle_gamma 90.000 _cell_length_a 8.8780 _cell_length_b 10.3340 _cell_length_c 8.9230 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8854 _[local]_cod_data_source_file tk5222Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' EnCl in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -11 0 61.63 69.00 6.60 o 2 -11 0 24.57 28.43 3.99 o 2 -10 0 111.38 120.26 9.28 o 3 -10 0 11.92 11.20 2.57 o 2 -9 0 89.00 86.36 8.03 o 3 -9 0 23.55 28.57 4.46 o 3 -8 0 250.22 256.59 13.17 o 4 -8 0 136.91 133.13 6.58 o 5 -8 0 239.27 209.06 11.61 o 6 -8 0 18.19 18.07 3.14 o 2 -7 0 370.04 370.63 14.05 o 3 -7 0 214.57 212.05 7.87 o 4 -7 0 205.11 196.02 7.93 o 5 -7 0 202.69 177.43 11.20 o 6 -7 0 88.75 81.57 7.51 o 7 -7 0 86.98 86.15 7.09 o 1 -6 0 527.31 550.49 28.63 o 2 -6 0 589.26 599.18 14.35 o 3 -6 0 114.80 113.76 5.11 o 4 -6 0 676.65 664.46 13.29 o 5 -6 0 226.73 231.90 14.39 o 6 -6 0 22.51 17.76 3.71 o 7 -6 0 130.67 115.94 9.02 o 8 -6 0 16.28 20.27 3.28 o 1 -5 0 241.03 256.62 17.70 o 2 -5 0 243.33 282.69 21.21 o 3 -5 0 460.50 486.46 10.38 o 4 -5 0 123.35 121.92 5.35 o 5 -5 0 217.70 208.65 8.21 o 6 -5 0 334.45 303.84 15.52 o 7 -5 0 99.85 99.84 8.90 o 8 -5 0 24.06 27.06 4.16 o 0 -4 0 3117.19 3122.64 47.02 o 1 -4 0 1166.81 1158.28 33.82 o 2 -4 0 242.02 233.47 17.26 o 3 -4 0 331.69 295.33 21.80 o 4 -4 0 458.19 449.81 17.67 o 5 -4 0 450.00 468.54 13.05 o 7 -4 0 5.78 4.81 2.39 o 8 -4 0 50.94 59.72 6.55 o 1 -3 0 262.58 258.47 6.77 o 2 -3 0 210.42 199.69 7.74 o 3 -3 0 244.58 250.14 11.03 o 4 -3 0 509.37 500.43 31.77 o 5 -3 0 205.02 210.81 11.11 o 6 -3 0 12.00 13.88 3.26 o 7 -3 0 67.06 57.43 6.75 o 9 -3 0 116.51 124.00 8.32 o 0 -2 0 8596.54 7752.26 50.32 o 1 -2 0 164.47 177.05 5.29 o 2 -2 0 1493.10 1455.40 21.62 o 3 -2 0 354.64 342.46 12.98 o 4 -2 0 664.61 665.97 25.42 o 5 -2 0 246.75 231.78 6.28 o 6 -2 0 14.37 14.01 2.66 o 7 -2 0 3.15 2.52 1.26 o 8 -2 0 109.94 122.53 9.68 o 9 -2 0 21.13 25.32 3.95 o 1 -1 0 2204.04 2191.23 18.10 o 2 -1 0 2141.68 2023.53 35.99 o 3 -1 0 396.45 394.64 14.17 o 4 -1 0 322.99 349.01 21.54 o 5 -1 0 300.16 301.09 8.88 o 6 -1 0 372.26 394.08 12.71 o 7 -1 0 262.37 280.98 14.79 o 8 -1 0 125.85 125.25 9.80 o 1 0 0 2949.19 2743.70 105.96 o 2 0 0 179.27 163.38 6.59 o 3 0 0 77.70 73.33 5.48 o 4 0 0 27.08 32.79 4.41 o 5 0 0 64.25 65.69 5.01 o 6 0 0 148.59 164.34 8.11 o 7 0 0 153.79 145.82 10.37 o 8 0 0 42.90 42.23 5.61 o 9 0 0 78.18 92.91 7.34 o 1 1 0 2035.84 2128.44 36.81 o 2 1 0 2185.36 2071.26 34.75 o 3 1 0 346.27 334.66 10.39 o 4 1 0 354.59 396.98 24.31 o 5 1 0 295.23 301.37 11.68 o 6 1 0 360.96 381.30 10.39 o 7 1 0 312.19 339.72 15.51 o 8 1 0 154.44 169.23 10.93 o 9 1 0 50.74 59.64 5.71 o 0 2 0 8354.91 7586.23 39.88 o 1 2 0 173.67 157.09 10.28 o 2 2 0 1551.50 1475.05 34.47 o 3 2 0 323.54 292.09 18.44 o 4 2 0 580.25 616.37 30.84 o 5 2 0 290.83 300.60 10.71 o 6 2 0 18.33 21.51 3.30 o 7 2 0 1.59 3.59 1.76 o 8 2 0 115.34 132.83 9.35 o 1 3 0 291.50 282.70 6.47 o 2 3 0 240.84 216.07 14.58 o 4 3 0 508.46 469.53 13.29 o 5 3 0 199.93 216.43 9.23 o 6 3 0 11.40 11.49 2.63 o 7 3 0 78.52 78.67 7.09 o 8 3 0 61.53 58.92 6.52 o 4 4 0 445.50 422.68 15.43 o 5 4 0 417.87 438.09 30.69 o 7 4 0 5.92 5.51 2.12 o 8 4 0 47.88 46.73 5.65 o 3 5 0 470.16 499.26 11.24 o 4 5 0 130.45 123.42 6.29 o 6 5 0 344.46 318.37 16.42 o 7 5 0 95.95 93.11 8.70 o 8 5 0 35.64 37.12 4.86 o 0 6 0 1088.56 1144.48 25.08 o 1 6 0 481.20 500.10 7.65 o 2 6 0 628.11 650.86 12.96 o 3 6 0 123.91 125.73 6.16 o 4 6 0 669.45 642.92 15.32 o 5 6 0 235.94 223.76 13.81 o 6 6 0 25.10 25.54 4.73 o 7 6 0 126.65 120.15 9.63 o 8 6 0 25.12 28.49 3.98 o 1 7 0 68.52 65.17 3.59 o 2 7 0 371.38 380.02 10.97 o 3 7 0 183.85 183.91 8.13 o 4 7 0 201.35 178.43 8.54 o 5 7 0 224.47 187.97 12.90 o 6 7 0 92.20 83.30 8.38 o 7 7 0 93.55 93.57 8.01 o 0 8 0 116.63 120.06 8.91 o 1 8 0 59.92 62.20 4.69 o 2 8 0 129.16 133.19 7.09 o 3 8 0 250.07 253.75 10.15 o 4 8 0 127.97 128.15 7.52 o 5 8 0 227.83 194.34 13.03 o 6 8 0 19.20 15.04 3.37 o 1 9 0 29.26 29.15 3.76 o 2 9 0 91.78 98.22 6.32 o 3 9 0 36.83 44.57 4.34 o 4 9 0 7.98 5.00 1.58 o 5 9 0 31.73 29.23 4.79 o 6 9 0 47.36 56.32 5.90 o 0 10 0 327.28 334.03 15.35 o 1 10 0 151.98 153.94 7.36 o 2 10 0 125.13 131.73 8.80 o 3 10 0 10.82 8.29 2.39 o 4 10 0 40.20 30.44 4.69 o 1 11 0 55.41 57.27 3.99 o 2 11 0 22.98 19.11 2.26 o -2 -11 1 143.01 149.81 8.75 o -1 -11 1 203.78 207.30 11.04 o 0 -11 1 131.66 135.09 9.59 o 1 -11 1 95.81 100.82 8.06 o 2 -11 1 27.09 29.62 4.17 o -2 -10 1 20.20 19.79 3.57 o 1 -10 1 275.32 294.26 15.10 o 2 -10 1 259.84 268.79 14.03 o 3 -10 1 12.66 13.00 2.89 o 4 -10 1 26.51 20.36 3.21 o -6 -9 1 82.47 71.01 5.82 o -5 -9 1 73.86 66.74 6.29 o -4 -9 1 80.96 88.71 7.51 o -3 -9 1 74.49 83.45 5.15 o 2 -9 1 12.64 14.72 3.55 o 3 -9 1 94.61 96.52 8.54 o 5 -9 1 59.66 51.89 5.22 o -7 -8 1 29.77 37.61 4.43 o -6 -8 1 18.67 15.11 3.09 o -5 -8 1 64.63 57.35 6.41 o -3 -8 1 449.45 462.28 12.09 o -2 -8 1 500.93 518.91 17.79 o -1 -8 1 216.05 234.67 11.70 o 2 -8 1 54.16 50.32 6.06 o 3 -8 1 36.52 38.72 5.37 o 4 -8 1 33.41 39.58 5.39 o 5 -8 1 67.02 60.67 6.24 o -7 -7 1 25.45 25.00 4.12 o -6 -7 1 166.87 148.03 10.65 o -5 -7 1 121.97 107.12 9.06 o -4 -7 1 142.04 139.40 9.90 o -3 -7 1 60.13 54.93 3.73 o -2 -7 1 192.23 195.94 9.17 o -1 -7 1 299.69 296.20 12.11 o 2 -7 1 613.52 625.84 17.42 o 3 -7 1 325.87 304.46 14.16 o 4 -7 1 113.57 111.13 8.85 o 5 -7 1 159.43 139.93 6.84 o 6 -7 1 41.93 37.72 4.68 o -8 -6 1 79.89 85.87 7.22 o -7 -6 1 40.16 40.90 5.64 o -6 -6 1 20.40 18.74 3.92 o -5 -6 1 17.18 12.68 2.97 o -4 -6 1 104.78 106.49 12.46 o -3 -6 1 388.68 395.86 9.49 o -2 -6 1 142.61 145.70 7.31 o -1 -6 1 234.85 246.33 8.85 o 1 -6 1 455.67 438.68 26.64 o 2 -6 1 47.89 48.01 4.35 o 3 -6 1 236.51 219.80 7.27 o 4 -6 1 66.54 63.44 4.45 o 5 -6 1 88.92 73.47 5.10 o 6 -6 1 215.43 210.72 8.37 o 7 -6 1 36.48 38.98 4.82 o -8 -5 1 69.39 74.48 7.20 o -7 -5 1 99.85 84.35 8.34 o -6 -5 1 673.20 628.45 22.30 o -5 -5 1 363.29 369.15 14.21 o -4 -5 1 396.11 392.29 17.09 o -3 -5 1 245.83 262.54 11.03 o -2 -5 1 74.78 81.28 11.20 o -1 -5 1 659.62 700.98 28.99 o 0 -5 1 662.72 661.82 25.66 o 1 -5 1 90.21 96.75 11.61 o 2 -5 1 154.12 166.42 7.42 o 3 -5 1 48.35 52.76 3.36 o 4 -5 1 26.59 28.85 2.68 o 5 -5 1 209.41 185.45 7.97 o 6 -5 1 140.45 142.33 7.12 o 7 -5 1 224.88 225.56 12.68 o 8 -5 1 151.55 161.39 9.21 o -9 -4 1 30.35 32.29 4.26 o -8 -4 1 138.63 140.94 10.45 o -7 -4 1 384.64 370.74 17.64 o -6 -4 1 115.63 105.42 8.96 o -5 -4 1 45.29 47.91 4.43 o -4 -4 1 11.25 16.48 2.41 o -3 -4 1 131.45 136.62 14.80 o -2 -4 1 1210.73 1163.13 38.39 o -1 -4 1 690.43 726.69 15.37 o 0 -4 1 390.08 399.45 18.27 o 1 -4 1 2030.43 2046.71 28.82 o 2 -4 1 1231.02 1166.77 42.08 o 3 -4 1 391.70 393.43 14.35 o 4 -4 1 48.51 47.53 3.31 o 5 -4 1 326.96 317.45 9.00 o 6 -4 1 83.45 84.31 5.45 o 8 -4 1 50.34 51.01 5.73 o -9 -3 1 181.03 197.10 11.00 o -8 -3 1 167.56 167.78 11.56 o -6 -3 1 28.60 26.81 6.67 o -5 -3 1 89.17 86.21 5.64 o -4 -3 1 70.81 70.02 10.63 o -3 -3 1 483.62 475.43 24.77 o -2 -3 1 1902.39 1884.32 43.16 o -1 -3 1 1240.00 1224.53 45.65 o 0 -3 1 582.91 546.17 12.81 o 1 -3 1 118.35 112.50 6.43 o 2 -3 1 376.27 366.74 13.49 o 3 -3 1 688.03 639.92 20.59 o 4 -3 1 629.31 618.37 10.74 o 5 -3 1 215.73 210.75 7.05 o 6 -3 1 340.88 357.06 11.05 o 7 -3 1 217.94 218.29 13.18 o -9 -2 1 59.64 65.10 6.45 o -7 -2 1 94.55 94.02 8.54 o -6 -2 1 44.30 38.70 4.43 o -5 -2 1 77.15 82.83 5.18 o -4 -2 1 1899.17 1932.31 38.03 o -3 -2 1 1850.09 1757.23 42.53 o -2 -2 1 392.93 362.25 16.79 o -1 -2 1 798.70 813.18 43.59 o 0 -2 1 1230.41 1220.08 22.52 o 1 -2 1 1470.11 1448.58 53.06 o 2 -2 1 73.95 71.07 5.67 o 3 -2 1 97.50 107.46 8.36 o 4 -2 1 410.56 417.38 10.15 o 5 -2 1 213.78 209.41 6.41 o 6 -2 1 172.15 176.43 7.63 o 7 -2 1 95.26 96.43 5.77 o 8 -2 1 4.63 3.89 1.45 o -8 -1 1 145.02 161.46 11.12 o -7 -1 1 482.57 489.36 18.83 o -6 -1 1 556.43 573.02 18.64 o -5 -1 1 744.22 732.33 14.54 o -4 -1 1 779.15 763.68 21.80 o -3 -1 1 1161.56 1163.03 29.98 o -2 -1 1 1025.58 996.13 23.59 o -1 -1 1 678.85 626.57 15.52 o 0 -1 1 3310.91 3250.96 24.62 o 1 -1 1 187.16 187.92 7.00 o 2 -1 1 321.87 299.93 11.41 o 3 -1 1 420.26 444.10 14.11 o 4 -1 1 184.28 182.32 10.18 o 5 -1 1 117.57 110.40 4.53 o 6 -1 1 641.58 692.30 15.08 o 7 -1 1 841.14 872.24 17.74 o 8 -1 1 48.88 56.51 6.56 o -8 0 1 22.93 21.41 3.88 o -7 0 1 470.11 487.14 18.26 o -6 0 1 389.03 390.43 13.61 o -5 0 1 23.25 27.35 7.27 o -4 0 1 14.48 25.77 3.71 o -3 0 1 308.97 317.16 14.97 o -2 0 1 147.80 138.45 5.79 o -1 0 1 1330.92 1191.82 19.92 o 0 0 1 266.13 263.67 8.54 o 1 0 1 3559.29 3602.64 27.05 o 2 0 1 3920.65 3829.45 108.54 o 3 0 1 637.32 611.85 17.09 o 4 0 1 91.22 81.78 6.12 o 5 0 1 111.57 112.43 4.82 o 6 0 1 1.50 1.02 0.75 o 7 0 1 226.77 233.77 9.14 o 8 0 1 80.04 70.58 7.21 o 9 0 1 0.39 0.07 0.43 o -8 1 1 141.84 153.41 10.14 o -7 1 1 464.14 496.48 17.79 o -6 1 1 537.23 580.03 17.48 o -4 1 1 780.00 825.22 35.78 o -3 1 1 1139.67 1147.55 19.61 o -2 1 1 934.50 943.12 26.78 o -1 1 1 579.34 598.24 16.26 o 0 1 1 3083.91 3188.13 29.12 o 1 1 1 208.01 227.41 8.57 o 2 1 1 314.07 298.52 11.22 o 3 1 1 382.94 407.64 13.45 o 4 1 1 147.15 169.10 15.25 o 5 1 1 122.93 122.22 5.47 o 6 1 1 617.68 671.79 15.80 o 7 1 1 777.86 827.06 24.89 o 8 1 1 50.77 66.91 6.79 o 9 1 1 49.03 51.28 4.96 o -7 2 1 71.53 71.44 6.61 o -6 2 1 51.83 53.71 4.71 o -5 2 1 74.32 83.57 13.25 o -4 2 1 1868.09 1807.23 54.97 o -3 2 1 1872.36 1808.04 47.69 o -2 2 1 292.80 282.57 15.77 o 0 2 1 1254.82 1201.76 14.55 o 1 2 1 1406.19 1430.20 34.59 o 2 2 1 76.75 72.63 6.57 o 3 2 1 90.20 96.99 10.11 o 4 2 1 373.46 394.88 23.61 o 5 2 1 190.61 191.51 7.37 o 6 2 1 143.45 145.19 9.85 o 7 2 1 91.24 96.88 8.47 o 8 2 1 2.30 5.26 1.93 o -7 3 1 135.80 131.50 9.83 o -6 3 1 37.24 37.43 9.89 o -5 3 1 97.58 102.40 14.93 o -4 3 1 83.48 83.17 12.18 o -3 3 1 461.45 454.78 25.36 o -2 3 1 1924.26 1863.44 45.47 o -1 3 1 1208.19 1172.16 24.71 o 0 3 1 564.53 554.06 18.34 o 1 3 1 130.10 121.93 11.29 o 2 3 1 417.14 411.03 25.30 o 3 3 1 683.12 637.13 27.05 o 4 3 1 717.99 729.95 21.92 o 5 3 1 235.15 248.64 12.09 o 6 3 1 337.12 363.35 15.65 o 7 3 1 225.84 236.79 12.80 o 8 3 1 4.42 3.68 1.26 o -8 4 1 141.27 146.68 9.80 o -7 4 1 390.53 359.78 16.52 o -6 4 1 124.89 108.99 8.83 o -5 4 1 32.02 29.98 3.89 o -4 4 1 15.19 17.63 1.97 o 0 4 1 338.23 363.48 16.72 o 1 4 1 2001.37 1934.78 48.29 o 2 4 1 1268.22 1231.22 46.55 o 4 4 1 59.82 53.89 4.25 o 5 4 1 352.81 365.23 14.91 o 6 4 1 82.68 87.50 7.72 o 7 4 1 14.95 17.15 2.54 o 8 4 1 54.30 56.81 6.11 o -8 5 1 67.82 75.07 6.82 o -7 5 1 92.66 81.42 7.96 o -6 5 1 727.53 654.03 22.66 o -5 5 1 388.36 351.60 15.84 o -4 5 1 404.62 401.97 10.81 o -3 5 1 224.50 242.69 7.43 o 2 5 1 140.49 166.11 6.11 o 3 5 1 60.31 64.65 4.29 o 4 5 1 25.42 25.77 2.36 o 5 5 1 216.37 206.77 16.65 o 6 5 1 132.20 136.07 7.08 o 7 5 1 210.15 213.25 13.03 o 8 5 1 153.01 169.16 9.82 o -8 6 1 81.41 85.40 6.88 o -7 6 1 51.51 49.31 6.10 o -6 6 1 22.26 18.62 4.07 o -5 6 1 20.74 13.06 3.23 o -4 6 1 120.67 112.97 6.17 o -3 6 1 377.95 400.57 10.59 o -2 6 1 133.97 137.05 4.76 o -1 6 1 262.86 284.70 8.57 o 0 6 1 913.86 956.46 12.45 o 1 6 1 473.22 465.71 8.76 o 2 6 1 39.83 41.74 2.66 o 3 6 1 229.18 222.42 8.56 o 4 6 1 50.42 47.88 4.34 o 6 6 1 221.13 216.99 13.64 o 7 6 1 38.65 37.21 5.19 o -7 7 1 26.07 28.13 4.54 o -6 7 1 151.10 129.40 10.44 o -5 7 1 116.29 100.20 9.39 o -4 7 1 140.85 130.28 7.09 o -3 7 1 54.71 51.88 4.17 o -2 7 1 207.01 213.98 6.66 o -1 7 1 331.61 325.15 8.01 o 0 7 1 150.05 147.99 5.45 o 1 7 1 29.08 27.62 2.41 o 2 7 1 605.01 614.05 24.28 o 3 7 1 304.66 276.46 10.27 o 4 7 1 124.03 108.32 7.40 o 5 7 1 155.01 141.63 11.19 o 6 7 1 36.04 35.01 5.28 o 7 7 1 7.22 9.42 2.41 o -7 8 1 25.23 22.86 3.60 o -6 8 1 14.23 9.59 2.52 o -5 8 1 76.72 66.00 7.72 o -4 8 1 226.40 228.71 9.69 o -3 8 1 385.10 386.23 12.22 o -2 8 1 540.50 560.23 15.54 o -1 8 1 232.35 244.14 7.62 o 0 8 1 12.53 12.43 1.45 o 1 8 1 23.05 18.75 2.49 o 2 8 1 47.95 45.83 3.34 o 3 8 1 32.57 34.31 3.78 o 4 8 1 37.21 39.60 4.22 o 5 8 1 53.50 50.39 6.45 o 6 8 1 4.44 5.44 2.00 o -6 9 1 73.85 61.95 6.38 o -5 9 1 79.57 65.84 7.35 o -4 9 1 94.06 94.03 9.28 o -3 9 1 65.69 80.08 8.88 o -2 9 1 83.04 83.75 8.88 o -1 9 1 130.01 137.67 6.94 o 0 9 1 6.58 6.29 1.57 o 1 9 1 66.23 64.82 3.48 o 2 9 1 12.86 11.83 2.30 o 3 9 1 80.10 79.47 5.82 o 4 9 1 203.88 183.19 8.68 o 5 9 1 57.60 53.22 6.08 o -5 10 1 38.24 34.39 4.67 o -4 10 1 80.46 81.63 8.14 o -2 10 1 19.44 20.51 3.95 o -1 10 1 75.37 73.63 7.53 o 0 10 1 73.55 81.60 7.84 o 1 10 1 282.48 294.47 15.13 o 2 10 1 261.35 267.07 10.19 o 3 10 1 14.21 11.70 2.17 o 4 10 1 25.09 22.85 3.82 o -3 11 1 0.01 0.33 0.79 o -2 11 1 144.14 136.34 9.07 o -1 11 1 226.42 230.91 12.02 o 0 11 1 127.26 136.12 9.31 o 1 11 1 89.97 91.40 7.57 o 2 11 1 29.86 33.28 4.55 o -2 -11 2 26.30 22.00 3.57 o -1 -11 2 8.30 7.33 1.41 o 0 -11 2 144.06 139.74 9.51 o 1 -11 2 77.89 81.84 7.08 o -4 -10 2 47.01 43.03 4.88 o 0 -10 2 63.89 72.34 7.45 o 1 -10 2 45.30 50.18 6.16 o 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176.62 153.68 11.03 o -6 -6 2 358.73 330.24 16.45 o -5 -6 2 315.11 306.83 15.28 o -4 -6 2 11.83 11.22 2.48 o -3 -6 2 404.63 412.40 17.58 o -2 -6 2 261.15 273.81 11.85 o -1 -6 2 163.49 163.12 8.78 o 1 -6 2 300.59 301.28 23.63 o 2 -6 2 692.40 709.19 20.29 o 3 -6 2 537.17 550.72 17.12 o 4 -6 2 79.02 75.42 7.53 o 5 -6 2 8.99 8.42 2.56 o 6 -6 2 55.98 55.85 4.15 o -8 -5 2 29.25 29.31 4.62 o -7 -5 2 20.98 15.31 3.64 o -6 -5 2 125.39 111.21 9.38 o -5 -5 2 369.74 380.10 13.22 o -4 -5 2 931.79 953.07 20.75 o -3 -5 2 27.31 25.89 3.10 o -2 -5 2 95.66 108.95 6.60 o 0 -5 2 334.42 361.15 21.47 o 1 -5 2 100.95 87.15 12.12 o 2 -5 2 156.94 143.30 10.31 o 3 -5 2 18.90 19.40 3.07 o 4 -5 2 58.91 59.29 6.37 o 5 -5 2 199.83 195.15 12.10 o 6 -5 2 123.75 121.18 6.48 o 7 -5 2 154.40 163.42 6.72 o -9 -4 2 22.06 19.59 3.36 o -8 -4 2 177.71 171.63 11.53 o -7 -4 2 79.28 69.11 7.49 o -6 -4 2 150.29 156.90 10.70 o -5 -4 2 394.81 402.98 12.83 o -4 -4 2 81.04 72.51 5.26 o -3 -4 2 368.61 359.90 23.72 o -2 -4 2 987.58 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