#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/81/2238177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238177_Fobs loop_ _publ_author_name 'Arman, Hadi D.' 'Tiekink, Edward R. T.' _publ_section_title ; 4-Carboxypyridin-1-ium 2,4,5-tricarboxybenzoate monohydrate ; _journal_coeditor_code HB7093 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1122 _journal_page_last o1123 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.560 _cell_angle_beta 114.667 _cell_angle_gamma 110.283 _cell_length_a 9.7240 _cell_length_b 10.0070 _cell_length_c 10.7550 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7966 _[local]_cod_data_source_file hb7093Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 83.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 164.07 180.98 1.82 o 2 0 0 1657.78 1614.36 13.39 o 3 0 0 77.25 67.83 1.06 o 4 0 0 1560.49 1510.19 7.30 o 6 0 0 549.20 525.08 2.53 o 7 0 0 25.75 16.81 2.09 o 8 0 0 37.38 41.02 2.95 o 9 0 0 1.37 1.39 1.69 o -10 1 0 40.87 44.31 1.84 o -9 1 0 3.24 3.01 2.16 o -8 1 0 111.57 114.52 2.49 o -7 1 0 37.12 43.33 2.53 o -6 1 0 1.50 8.35 3.11 o -5 1 0 437.95 435.44 4.02 o -4 1 0 103.96 121.43 4.61 o -3 1 0 787.70 695.91 8.38 o -2 1 0 2221.72 2228.59 1.10 o -1 1 0 167.66 136.88 0.20 o 0 1 0 311.63 300.89 0.28 o 1 1 0 410.38 406.26 4.57 o 2 1 0 862.75 892.41 1.10 o 3 1 0 40.87 23.70 0.86 o 4 1 0 30.44 23.38 2.00 o 5 1 0 9.99 18.55 1.55 o 6 1 0 5.23 6.60 1.64 o 7 1 0 28.57 29.53 1.56 o 8 1 0 2.54 8.24 1.66 o 9 1 0 3.69 10.15 1.64 o -10 2 0 4.30 9.20 2.48 o -9 2 0 15.54 12.27 2.37 o -8 2 0 542.39 532.79 3.00 o -7 2 0 697.07 677.14 11.80 o -6 2 0 113.93 109.36 1.76 o -5 2 0 29.03 35.02 3.26 o -4 2 0 411.68 390.78 2.79 o -2 2 0 787.73 769.77 9.12 o -1 2 0 691.62 720.16 0.75 o 1 2 0 89.67 77.75 0.65 o 2 2 0 558.74 614.86 1.07 o 3 2 0 276.92 262.09 1.07 o 4 2 0 70.63 77.21 1.24 o 5 2 0 0.58 7.92 1.40 o 6 2 0 137.30 135.74 1.52 o 7 2 0 16.29 19.67 1.58 o 8 2 0 87.27 92.85 1.61 o -10 3 0 43.49 34.90 2.55 o -9 3 0 8.19 19.97 2.86 o -8 3 0 2928.37 2872.45 9.50 o -7 3 0 104.56 102.66 8.43 o -6 3 0 131.09 116.93 4.70 o -5 3 0 757.92 796.74 10.70 o -4 3 0 1362.21 1393.64 10.03 o -3 3 0 348.76 358.93 2.02 o -2 3 0 4775.23 4861.75 1.61 o 0 3 0 381.56 402.04 0.62 o 1 3 0 39.13 42.10 0.71 o 2 3 0 157.09 146.64 0.90 o 3 3 0 163.07 165.46 1.16 o 4 3 0 0.86 2.06 1.19 o 5 3 0 450.68 461.05 1.76 o 6 3 0 62.12 73.97 1.53 o 7 3 0 2.68 6.45 1.45 o 8 3 0 0.03 4.23 1.45 o -10 4 0 0.06 11.29 2.63 o -9 4 0 7.19 9.42 1.63 o -8 4 0 11.85 7.72 1.67 o -7 4 0 0.01 6.57 1.85 o -6 4 0 134.14 118.07 6.25 o -5 4 0 87.13 82.04 0.78 o -4 4 0 638.87 650.00 0.86 o -3 4 0 104.87 114.64 4.71 o -2 4 0 1133.72 1164.17 1.04 o -1 4 0 1114.21 1199.56 1.32 o 0 4 0 138.89 139.69 0.91 o 1 4 0 262.78 285.59 0.97 o 2 4 0 19.18 18.84 0.95 o 3 4 0 15.81 14.58 1.13 o 4 4 0 1.71 8.30 1.26 o 6 4 0 16.38 21.87 1.46 o 7 4 0 20.86 16.00 1.35 o -11 5 0 22.67 25.24 3.11 o -10 5 0 1.10 0.98 1.56 o -9 5 0 394.62 401.52 12.30 o -8 5 0 168.78 174.25 6.86 o -7 5 0 0.11 12.15 8.16 o -6 5 0 60.22 52.89 1.08 o -5 5 0 1189.73 1174.09 7.82 o -4 5 0 34.06 32.91 4.14 o -3 5 0 2.68 2.52 0.70 o -1 5 0 68.65 71.83 1.04 o 0 5 0 3.98 3.95 1.02 o 1 5 0 54.60 65.00 1.68 o 2 5 0 92.58 83.85 1.26 o 3 5 0 10.15 12.31 1.22 o 4 5 0 54.29 55.48 1.26 o 5 5 0 11.15 13.80 1.40 o 6 5 0 15.94 24.02 1.41 o -11 6 0 2.30 7.29 1.45 o -10 6 0 72.86 72.71 1.35 o -9 6 0 300.61 289.61 6.18 o -8 6 0 107.20 98.42 6.13 o -7 6 0 36.56 34.28 1.34 o -6 6 0 247.25 253.85 5.75 o -5 6 0 144.14 157.36 2.88 o -4 6 0 306.59 336.68 3.53 o -3 6 0 255.43 299.21 0.93 o -2 6 0 119.98 138.92 1.34 o -1 6 0 95.68 102.06 1.38 o 0 6 0 0.25 1.25 1.33 o 1 6 0 91.24 95.79 1.92 o 2 6 0 8.81 3.05 1.22 o 3 6 0 58.37 53.18 1.31 o 4 6 0 93.96 112.77 1.50 o 5 6 0 35.57 42.57 1.38 o 6 6 0 1.94 8.66 1.41 o -10 7 0 176.41 176.02 5.38 o -9 7 0 37.47 28.89 1.67 o -8 7 0 96.88 102.33 3.42 o -7 7 0 147.04 140.59 1.05 o -6 7 0 53.02 48.89 1.79 o -5 7 0 85.79 81.34 6.90 o -4 7 0 854.79 855.32 1.43 o -3 7 0 43.61 48.47 1.01 o -2 7 0 76.65 91.52 1.64 o -1 7 0 543.48 513.90 1.85 o 0 7 0 7.62 16.10 1.55 o 1 7 0 3.33 8.91 1.53 o 2 7 0 17.77 21.74 1.61 o 3 7 0 416.37 412.84 5.34 o 4 7 0 11.05 14.23 1.14 o 5 7 0 2.30 7.98 1.23 o -10 8 0 19.75 19.62 1.12 o -9 8 0 119.69 129.12 4.75 o -8 8 0 35.28 34.95 4.42 o -7 8 0 89.32 87.32 2.45 o -6 8 0 1.53 2.20 2.05 o -5 8 0 5.07 11.30 2.98 o -4 8 0 420.09 433.06 1.44 o -3 8 0 167.28 155.30 1.24 o -2 8 0 162.26 188.66 1.87 o -1 8 0 25.46 25.30 1.60 o 0 8 0 26.41 27.03 1.49 o 1 8 0 18.16 18.26 1.46 o 2 8 0 57.00 64.06 1.59 o 3 8 0 0.47 1.26 1.07 o 4 8 0 1.80 7.62 1.17 o -10 9 0 2.41 7.62 1.28 o -9 9 0 8.14 13.03 1.58 o -8 9 0 0.02 2.28 1.24 o -7 9 0 3.78 5.79 1.06 o -6 9 0 48.16 56.95 8.64 o -5 9 0 4.74 11.07 1.00 o -4 9 0 3.74 1.70 1.12 o -3 9 0 353.39 363.85 1.50 o -2 9 0 80.24 82.52 1.63 o -1 9 0 54.34 43.68 1.53 o 0 9 0 53.91 58.85 1.54 o 1 9 0 39.20 33.83 1.56 o 2 9 0 87.46 86.31 1.72 o 3 9 0 18.07 21.24 1.68 o -9 10 0 6.38 2.98 1.62 o -8 10 0 36.14 44.98 9.10 o -7 10 0 6.52 12.40 4.47 o -6 10 0 0.37 2.91 2.98 o -5 10 0 356.61 364.57 1.31 o -4 10 0 129.23 136.28 1.38 o -3 10 0 0.00 7.28 1.29 o -2 10 0 431.73 422.17 2.00 o -1 10 0 83.20 90.63 1.73 o 0 10 0 27.03 21.14 1.68 o 1 10 0 71.05 76.28 1.74 o -9 11 0 33.26 38.45 1.70 o -8 11 0 1.76 10.66 3.05 o -7 11 0 6.36 8.65 1.34 o -6 11 0 6.61 10.75 2.46 o -5 11 0 107.08 108.49 3.75 o -4 11 0 2.59 5.64 1.31 o -3 11 0 62.08 61.32 1.41 o -2 11 0 1.34 7.39 1.12 o -1 11 0 13.11 16.84 1.80 o -7 12 0 3.52 5.21 1.15 o -6 12 0 28.14 23.05 1.10 o -5 12 0 3.36 9.61 1.52 o -4 12 0 31.70 37.55 1.15 o -3 12 0 0.17 3.66 1.38 o 2 -12 1 1.12 6.47 2.86 o 3 -12 1 0.00 5.75 4.02 o 4 -12 1 17.02 23.52 2.22 o 5 -12 1 277.39 284.30 5.03 o 6 -12 1 62.95 63.58 4.59 o 7 -12 1 5.20 1.49 1.97 o 0 -11 1 36.31 44.34 1.94 o 1 -11 1 48.21 52.58 1.81 o 3 -11 1 2.56 4.77 4.66 o 4 -11 1 70.75 80.26 4.81 o 5 -11 1 113.35 104.42 4.14 o 6 -11 1 3.80 11.26 4.50 o 7 -11 1 56.81 56.53 6.66 o 8 -11 1 81.95 78.96 1.85 o -2 -10 1 144.93 152.07 1.74 o -1 -10 1 48.83 55.85 1.72 o 0 -10 1 34.02 37.60 1.74 o 1 -10 1 13.19 19.36 1.73 o 2 -10 1 4.30 12.04 1.65 o 3 -10 1 47.24 38.84 1.06 o 4 -10 1 6.41 9.45 1.46 o 5 -10 1 0.27 6.36 0.98 o 6 -10 1 16.94 28.64 0.93 o 7 -10 1 1.53 5.20 2.55 o 8 -10 1 9.53 14.39 1.61 o 9 -10 1 10.63 14.61 1.61 o -3 -9 1 111.21 107.03 1.80 o -2 -9 1 127.08 118.79 1.83 o -1 -9 1 5.44 2.95 1.60 o 0 -9 1 54.48 54.62 1.56 o 1 -9 1 31.80 25.10 1.60 o 2 -9 1 94.34 84.35 1.72 o 3 -9 1 15.84 10.18 2.24 o 4 -9 1 621.19 639.77 1.27 o 5 -9 1 469.94 463.24 6.65 o 6 -9 1 351.16 367.89 12.32 o 7 -9 1 110.00 115.48 1.28 o 8 -9 1 52.26 61.64 8.06 o 9 -9 1 26.45 35.02 1.34 o 10 -9 1 4.06 2.97 1.25 o -4 -8 1 8.64 16.44 2.06 o -3 -8 1 50.02 58.66 2.41 o -2 -8 1 22.68 26.12 1.55 o -1 -8 1 33.87 31.45 1.52 o 0 -8 1 432.16 408.09 1.92 o 1 -8 1 7.63 17.46 1.82 o 2 -8 1 1.53 13.80 1.83 o 3 -8 1 279.87 277.94 4.74 o 4 -8 1 337.43 350.17 1.11 o 5 -8 1 43.82 56.53 2.10 o 6 -8 1 355.34 393.40 1.07 o 7 -8 1 26.16 25.39 2.72 o 8 -8 1 48.25 47.79 1.45 o 9 -8 1 2.27 5.74 1.19 o 10 -8 1 109.34 109.57 1.19 o -5 -7 1 16.61 17.81 1.20 o -4 -7 1 1.99 9.86 1.26 o -3 -7 1 50.08 46.86 1.22 o -2 -7 1 32.48 39.26 5.95 o -1 -7 1 13.28 19.69 1.74 o 0 -7 1 342.46 330.28 1.71 o 1 -7 1 156.94 159.03 1.60 o 2 -7 1 517.56 527.32 1.80 o 3 -7 1 51.59 56.72 3.22 o 4 -7 1 62.60 62.39 1.70 o 5 -7 1 1496.52 1529.70 8.40 o 6 -7 1 58.04 65.05 2.40 o 7 -7 1 0.01 1.04 0.86 o 8 -7 1 45.49 44.34 0.86 o 9 -7 1 39.20 44.78 2.26 o 10 -7 1 38.36 50.06 0.99 o -6 -6 1 60.15 65.94 1.44 o -5 -6 1 93.92 94.62 1.41 o -4 -6 1 122.24 122.23 1.32 o -3 -6 1 79.69 72.04 1.07 o -2 -6 1 300.18 292.09 2.17 o -1 -6 1 160.27 168.72 1.61 o 0 -6 1 2.06 -0.04 1.26 o 1 -6 1 9.90 11.47 1.20 o 3 -6 1 657.55 682.38 4.84 o 4 -6 1 256.52 256.34 4.00 o 5 -6 1 1.79 9.09 3.74 o 6 -6 1 58.40 62.32 2.39 o 7 -6 1 2.47 7.53 2.60 o 8 -6 1 634.02 639.25 1.39 o 9 -6 1 64.62 62.74 0.85 o 10 -6 1 139.11 135.42 2.97 o -7 -5 1 11.70 9.30 1.39 o -6 -5 1 2.25 4.00 1.38 o -5 -5 1 0.57 -0.98 1.25 o -4 -5 1 208.94 196.79 1.30 o -3 -5 1 204.97 195.99 1.24 o -2 -5 1 3.82 4.31 0.82 o -1 -5 1 210.66 228.41 3.57 o 0 -5 1 113.89 102.93 1.07 o 1 -5 1 559.44 556.49 1.34 o 3 -5 1 39.60 35.25 1.87 o 4 -5 1 691.29 728.57 1.26 o 5 -5 1 1.45 21.75 3.77 o 6 -5 1 9.00 12.49 0.90 o 7 -5 1 1.34 4.79 1.63 o 8 -5 1 134.11 138.86 4.38 o 9 -5 1 0.76 6.17 2.80 o 10 -5 1 16.95 22.95 2.86 o -8 -4 1 42.44 42.69 1.46 o -7 -4 1 0.52 5.07 1.41 o -6 -4 1 18.38 15.12 1.31 o -5 -4 1 81.24 82.56 1.23 o -4 -4 1 0.97 5.12 1.10 o -3 -4 1 1007.61 1046.72 1.49 o -2 -4 1 15.83 6.68 0.76 o -1 -4 1 404.02 376.91 0.84 o 0 -4 1 583.28 620.74 1.16 o 1 -4 1 1042.09 1116.39 1.40 o 2 -4 1 1290.68 1300.78 1.82 o 3 -4 1 358.80 431.36 17.59 o 4 -4 1 27.96 19.34 1.63 o 5 -4 1 427.75 426.21 8.67 o 6 -4 1 183.18 187.89 2.58 o 7 -4 1 14.52 22.08 2.56 o 8 -4 1 202.41 187.20 1.42 o 9 -4 1 8.18 19.12 2.75 o 10 -4 1 3.00 11.84 2.60 o -8 -3 1 46.38 47.11 1.52 o -7 -3 1 68.95 63.17 1.48 o -6 -3 1 0.41 8.83 1.35 o -5 -3 1 123.73 140.65 1.46 o -4 -3 1 713.12 737.04 1.49 o -3 -3 1 105.62 115.18 0.89 o -2 -3 1 92.49 86.01 0.72 o -1 -3 1 38.97 24.55 0.54 o 0 -3 1 1608.12 1639.31 1.33 o 1 -3 1 38.93 40.70 0.81 o 3 -3 1 3553.61 3646.66 1.37 o 4 -3 1 2.83 6.78 1.04 o 5 -3 1 263.60 261.99 3.18 o 6 -3 1 360.06 367.53 6.65 o 7 -3 1 30.47 43.68 3.12 o 8 -3 1 208.19 212.54 3.14 o 9 -3 1 13.44 13.74 2.51 o 10 -3 1 70.97 68.19 2.63 o -9 -2 1 83.23 93.20 1.62 o -8 -2 1 44.35 48.54 1.55 o -7 -2 1 449.42 433.96 1.74 o -6 -2 1 35.33 43.33 1.56 o -5 -2 1 0.97 2.44 1.43 o -4 -2 1 262.85 285.46 1.19 o -3 -2 1 106.63 86.27 0.78 o -2 -2 1 0.28 10.05 0.59 o -1 -2 1 152.71 143.77 2.00 o 0 -2 1 432.04 413.89 0.79 o 2 -2 1 514.13 461.22 11.63 o 3 -2 1 436.64 485.86 0.76 o 4 -2 1 5.49 11.63 2.51 o 5 -2 1 80.41 92.16 1.88 o 6 -2 1 48.34 46.03 2.80 o 7 -2 1 258.27 252.31 2.82 o 8 -2 1 97.70 94.59 2.56 o 9 -2 1 480.03 472.18 2.81 o 10 -2 1 25.94 37.75 2.48 o -9 -1 1 37.90 35.74 1.51 o -8 -1 1 0.92 8.04 1.70 o -7 -1 1 2.03 3.57 1.50 o -6 -1 1 111.75 125.72 1.25 o -5 -1 1 346.85 390.18 14.62 o -4 -1 1 873.17 871.10 5.01 o -3 -1 1 928.26 883.54 7.06 o -2 -1 1 12.11 12.83 1.17 o -1 -1 1 532.39 555.62 13.48 o 0 -1 1 214.38 190.65 8.92 o 2 -1 1 6961.27 7143.37 2.91 o 3 -1 1 854.48 918.10 1.82 o 4 -1 1 2.25 3.50 1.88 o 5 -1 1 142.35 136.12 2.31 o 6 -1 1 4.18 5.02 2.55 o 7 -1 1 381.27 362.42 2.57 o 8 -1 1 632.17 614.05 2.81 o 9 -1 1 27.92 32.73 1.88 o -10 0 1 2.08 7.42 1.82 o -9 0 1 24.01 29.88 5.82 o -8 0 1 8.59 16.26 2.16 o -7 0 1 281.49 296.91 4.92 o -6 0 1 88.22 94.97 13.31 o -5 0 1 772.06 721.94 4.37 o -4 0 1 375.39 392.57 5.70 o -3 0 1 40.27 32.12 0.44 o -1 0 1 8.81 16.57 0.26 o 1 0 1 214.39 222.05 3.35 o 3 0 1 36.85 37.89 1.29 o 4 0 1 667.56 698.42 1.91 o 5 0 1 49.23 45.54 2.06 o 6 0 1 102.93 106.97 1.41 o 7 0 1 241.72 234.42 1.96 o 8 0 1 212.09 217.67 1.86 o 9 0 1 88.12 94.41 1.81 o -10 1 1 4.44 10.11 2.17 o -9 1 1 12.68 24.46 2.50 o -8 1 1 191.18 171.97 1.75 o -7 1 1 5.94 15.44 6.37 o -6 1 1 154.52 151.40 6.44 o -5 1 1 771.67 735.81 6.13 o -4 1 1 18.39 21.30 0.72 o -3 1 1 3380.42 3417.54 2.06 o -2 1 1 594.65 598.09 1.79 o -1 1 1 255.11 219.97 16.78 o 0 1 1 198.39 221.68 8.04 o 2 1 1 4513.79 4623.50 2.31 o 3 1 1 49.09 48.62 1.01 o 4 1 1 505.90 477.92 1.53 o 5 1 1 47.61 42.70 1.52 o 6 1 1 17.26 15.40 1.80 o 7 1 1 11.62 15.62 1.72 o 8 1 1 94.10 90.20 1.60 o -10 2 1 12.74 17.42 2.44 o -9 2 1 17.90 16.63 1.81 o -8 2 1 114.07 88.53 2.13 o -7 2 1 786.64 800.92 2.12 o -6 2 1 63.35 68.89 1.94 o -5 2 1 1628.15 1628.39 2.03 o -4 2 1 429.40 412.14 9.69 o -3 2 1 90.17 113.34 0.90 o -2 2 1 331.32 308.95 0.79 o -1 2 1 3660.25 3661.39 3.10 o 1 2 1 61.94 58.98 0.70 o 2 2 1 2014.89 2255.68 1.86 o 3 2 1 29.50 29.61 1.19 o 4 2 1 6.62 9.33 1.47 o 5 2 1 105.69 118.96 1.69 o 6 2 1 58.24 55.12 1.59 o 7 2 1 21.38 19.19 1.53 o 8 2 1 11.12 18.51 1.59 o -11 3 1 1.06 7.83 2.68 o -10 3 1 15.54 19.09 1.65 o -9 3 1 3.89 4.83 3.48 o -8 3 1 0.85 -3.21 2.14 o -7 3 1 0.00 1.24 3.37 o -6 3 1 1.06 3.41 1.73 o -5 3 1 203.45 222.55 1.66 o -4 3 1 344.42 398.70 3.30 o -3 3 1 1847.27 1791.25 1.34 o -2 3 1 850.14 860.18 0.97 o -1 3 1 2892.96 2862.70 1.48 o 2 3 1 2.40 9.08 1.06 o 3 3 1 475.62 451.51 1.51 o 4 3 1 9.92 12.00 1.39 o 5 3 1 307.95 287.81 1.65 o 6 3 1 268.54 253.53 1.68 o 7 3 1 5.77 8.32 1.42 o -11 4 1 6.59 15.82 1.95 o -10 4 1 0.00 7.17 1.66 o -9 4 1 31.89 31.90 2.06 o -8 4 1 1553.53 1525.91 22.47 o -7 4 1 4731.05 4794.81 3.78 o -6 4 1 0.50 7.45 2.95 o -5 4 1 46.22 50.41 2.12 o -4 4 1 768.75 795.43 1.20 o -3 4 1 82.93 87.86 0.76 o -2 4 1 80.84 78.28 0.77 o -1 4 1 404.40 359.96 0.90 o 0 4 1 341.15 395.52 4.33 o 1 4 1 471.31 499.26 1.28 o 2 4 1 38.53 41.38 1.20 o 3 4 1 2.27 2.38 1.30 o 4 4 1 6.84 9.96 1.42 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105.73 108.51 2.45 o 1 2 9 19.70 19.23 1.96 o 2 2 9 46.63 48.12 1.10 o -11 3 9 33.58 38.23 2.81 o -10 3 9 8.03 19.46 2.61 o -9 3 9 182.73 190.03 2.74 o -8 3 9 229.75 218.52 2.56 o -7 3 9 167.58 159.59 2.31 o -6 3 9 14.88 14.55 2.01 o -5 3 9 982.50 938.98 2.51 o -4 3 9 0.07 2.86 1.72 o -3 3 9 371.62 365.44 1.85 o -2 3 9 28.35 27.96 4.33 o -1 3 9 4.59 3.19 3.37 o 0 3 9 28.21 21.20 1.04 o 1 3 9 19.30 21.09 3.06 o -11 4 9 1.73 4.39 2.63 o -10 4 9 19.48 15.50 2.59 o -9 4 9 133.55 127.03 2.63 o -8 4 9 8.92 12.31 2.34 o -7 4 9 80.72 79.88 2.33 o -6 4 9 2.26 19.29 2.01 o -5 4 9 198.75 206.00 2.29 o -4 4 9 102.44 98.27 2.00 o -3 4 9 204.31 219.95 2.13 o -2 4 9 143.92 139.91 1.90 o -1 4 9 30.36 28.95 1.14 o 0 4 9 58.64 54.88 1.24 o -11 5 9 51.55 54.12 2.85 o -10 5 9 78.50 79.50 2.49 o -9 5 9 0.73 0.99 2.39 o -8 5 9 46.70 45.93 2.26 o -7 5 9 21.43 19.17 2.19 o -6 5 9 75.36 73.99 2.00 o -5 5 9 302.87 286.13 2.17 o -4 5 9 47.93 48.84 1.87 o -3 5 9 15.66 21.64 1.79 o -2 5 9 1.53 11.79 1.75 o -1 5 9 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