#------------------------------------------------------------------------------ #$Date: 2013-08-28 13:42:33 +0300 (Wed, 28 Aug 2013) $ #$Revision: 88054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/81/2238182.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238182_Fobs loop_ _publ_author_name 'Dawe, Louise Nicole' 'Adhikary, Bibhutosh' 'Collins, Julie L.' 'Lucas, C. Robert' _publ_section_title ; Bis{[2,2'-(5,8,11-trithia-2,14-diazapentadeca-1,14-diene-1,15-diyl)diphenolato]palladium(II)} acetonitrile monosolvate ; _journal_coeditor_code HG5318 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m360 _journal_page_last m361 _journal_volume 69 _journal_year 2013 _cell_angle_alpha 90.000 _cell_angle_beta 106.087 _cell_angle_gamma 90.000 _cell_length_a 14.7232 _cell_length_b 16.2151 _cell_length_c 20.9433 _exptl_crystal_F_000 2344.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file hg5318Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _BA-28' _shelx_refln_list_code 4 _shelx_f_calc_maximum 500.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 6058.46 7842.14 70.10 o 4 0 0 33960.57 29160.33 157.29 o 5 0 0 4550.77 4876.25 62.77 o 6 0 0 84249.09 87676.60 308.16 o 7 0 0 24164.89 23577.43 183.37 o 8 0 0 30331.20 31659.00 202.36 o 9 0 0 19107.81 19312.66 182.94 o 10 0 0 3224.28 3187.22 63.06 o 11 0 0 2982.31 2845.78 84.25 o 12 0 0 5908.57 5977.18 108.58 o 13 0 0 3211.14 3081.72 146.67 o 14 0 0 1730.31 1928.33 184.91 o 15 0 0 42.75 68.89 21.04 o 16 0 0 37.71 43.39 13.32 o 17 0 0 174.96 178.73 21.41 o 18 0 0 1063.40 1613.96 100.28 o 2 1 0 7348.78 5599.96 44.76 o 4 1 0 21592.66 23593.24 91.61 o 5 1 0 6926.33 7755.69 52.12 o 6 1 0 19746.46 18329.33 77.39 o 7 1 0 14205.17 13932.68 87.71 o 8 1 0 160.04 291.88 12.67 o 9 1 0 0.01 24.20 5.48 o 10 1 0 4475.69 4711.37 70.70 o 11 1 0 2949.17 2731.52 47.58 o 12 1 0 1380.00 1223.88 45.68 o 13 1 0 1474.36 1508.95 77.53 o 14 1 0 3.04 25.47 9.28 o 15 1 0 1497.77 1380.40 106.94 o 16 1 0 336.20 300.39 29.71 o 17 1 0 2392.76 2655.08 83.68 o 18 1 0 2.00 22.47 16.66 o 3 2 0 3641.74 2453.40 22.43 o 4 2 0 3718.37 2950.19 38.18 o 5 2 0 85.15 74.94 6.88 o 6 2 0 410.10 319.39 16.99 o 7 2 0 4186.38 3814.23 40.20 o 8 2 0 15592.78 15644.98 101.05 o 9 2 0 2744.46 2700.10 38.91 o 10 2 0 11399.30 11689.51 107.03 o 11 2 0 5906.11 5836.81 74.17 o 12 2 0 3459.45 3275.26 60.17 o 13 2 0 5585.46 5763.25 93.08 o 14 2 0 19693.06 19782.56 380.51 o 15 2 0 1907.13 1819.19 100.44 o 16 2 0 7158.90 7688.54 87.29 o 17 2 0 461.01 390.72 24.69 o 18 2 0 57.96 38.72 9.89 o 1 3 0 8252.21 7752.87 62.36 o 2 3 0 4401.19 4985.66 70.98 o 3 3 0 3186.22 2674.91 29.17 o 4 3 0 27.77 17.81 4.06 o 5 3 0 207.07 443.76 15.35 o 6 3 0 4340.47 4696.83 43.36 o 7 3 0 1168.33 1431.65 25.09 o 8 3 0 2777.65 2429.28 41.35 o 9 3 0 2791.07 2625.47 48.69 o 10 3 0 152.04 97.51 6.47 o 11 3 0 3412.76 3440.88 59.53 o 12 3 0 5565.62 5310.92 77.44 o 13 3 0 361.10 343.53 27.51 o 14 3 0 5200.22 4768.71 126.18 o 15 3 0 166.80 218.71 23.83 o 16 3 0 459.86 389.64 37.23 o 17 3 0 134.64 165.06 17.07 o 18 3 0 104.14 32.12 6.82 o 0 4 0 156700.25 153463.42 748.64 o 1 4 0 1014.13 495.63 7.70 o 2 4 0 6167.06 7149.67 48.39 o 3 4 0 199.03 143.49 16.37 o 4 4 0 1205.86 777.64 17.69 o 5 4 0 28932.87 28285.57 110.68 o 6 4 0 38944.53 42532.37 172.04 o 7 4 0 1521.26 1452.50 30.62 o 8 4 0 8205.01 8504.88 74.99 o 9 4 0 1238.16 1151.65 18.92 o 10 4 0 8063.12 8077.49 90.50 o 11 4 0 3431.89 3515.39 59.91 o 12 4 0 6676.67 7012.88 103.83 o 13 4 0 75.19 118.99 24.11 o 14 4 0 6091.71 6364.39 119.68 o 15 4 0 1433.33 1349.58 111.10 o 16 4 0 5599.41 5963.46 82.20 o 17 4 0 1009.60 732.10 50.98 o 18 4 0 1870.84 1567.04 87.65 o 1 5 0 63714.56 61256.65 173.18 o 2 5 0 6716.11 6413.67 44.13 o 3 5 0 13595.53 12208.31 66.03 o 4 5 0 43.02 25.72 3.54 o 5 5 0 30617.85 31385.22 138.49 o 6 5 0 11445.07 10559.60 74.11 o 7 5 0 6899.02 6414.15 83.46 o 8 5 0 14836.73 14856.45 138.74 o 9 5 0 95.00 119.40 11.77 o 10 5 0 2819.70 2645.39 43.53 o 11 5 0 2723.16 2654.65 51.42 o 12 5 0 2254.19 2364.47 81.06 o 13 5 0 11.93 29.51 5.77 o 14 5 0 1125.56 994.15 58.02 o 15 5 0 1256.00 1051.11 101.35 o 16 5 0 211.63 336.23 20.41 o 17 5 0 431.64 360.67 28.06 o 0 6 0 71467.44 70880.20 308.31 o 1 6 0 2370.41 2420.56 22.83 o 2 6 0 7829.82 6552.17 42.55 o 3 6 0 743.88 807.14 16.73 o 4 6 0 13135.55 13657.41 95.95 o 5 6 0 28544.80 28715.08 197.03 o 6 6 0 27017.25 27907.03 119.38 o 7 6 0 1493.41 1640.96 29.51 o 8 6 0 12125.81 11893.98 97.67 o 9 6 0 46.65 78.01 6.71 o 10 6 0 1024.59 850.70 30.01 o 11 6 0 1404.33 1408.34 49.82 o 12 6 0 97.89 90.43 8.94 o 13 6 0 2184.32 2175.16 73.97 o 14 6 0 202.70 177.81 21.66 o 15 6 0 0.55 20.11 5.51 o 16 6 0 38.71 31.83 8.74 o 17 6 0 48.98 42.36 14.93 o 1 7 0 1112.17 1142.11 17.93 o 2 7 0 5435.90 5121.70 42.72 o 3 7 0 3881.23 4466.44 38.74 o 4 7 0 3788.25 3744.71 36.07 o 5 7 0 169.68 148.08 8.95 o 6 7 0 14825.68 15620.36 96.40 o 7 7 0 1342.18 1157.12 26.30 o 8 7 0 6222.79 6439.09 67.68 o 9 7 0 9025.77 9001.54 91.21 o 10 7 0 443.64 423.68 20.32 o 11 7 0 5330.09 5695.84 82.77 o 12 7 0 5705.15 5624.17 106.96 o 13 7 0 2176.71 2119.36 71.63 o 14 7 0 1523.89 1563.40 113.70 o 15 7 0 4064.64 4218.69 50.93 o 16 7 0 1411.64 1229.18 68.78 o 17 7 0 2451.97 2074.58 122.84 o 0 8 0 259.35 251.50 17.28 o 1 8 0 1112.52 1073.94 19.96 o 2 8 0 107.85 114.29 9.30 o 3 8 0 289.17 269.00 8.98 o 4 8 0 4180.69 4016.20 64.67 o 5 8 0 362.72 391.04 10.68 o 6 8 0 16806.45 17634.36 124.90 o 7 8 0 19.40 30.46 6.94 o 8 8 0 1154.67 1100.69 22.18 o 9 8 0 7115.24 7175.80 77.00 o 10 8 0 44.37 44.74 5.11 o 11 8 0 5202.54 5253.23 77.47 o 12 8 0 1104.52 1093.89 44.26 o 13 8 0 872.02 751.40 50.76 o 14 8 0 1799.01 1785.47 64.26 o 15 8 0 173.54 192.04 16.51 o 16 8 0 1378.92 1447.04 143.09 o 17 8 0 711.18 545.73 73.85 o 1 9 0 579.28 672.33 19.75 o 2 9 0 697.58 646.52 14.38 o 3 9 0 4279.34 4238.44 44.86 o 4 9 0 1036.08 1001.99 8.84 o 5 9 0 10574.51 10810.74 94.05 o 6 9 0 2594.97 2648.07 40.49 o 7 9 0 1277.10 1174.75 21.36 o 8 9 0 43.30 44.05 4.51 o 9 9 0 1670.16 1632.93 40.29 o 10 9 0 331.20 376.83 20.74 o 11 9 0 5356.01 6076.84 108.51 o 12 9 0 863.00 839.75 45.42 o 13 9 0 1374.80 1330.70 52.77 o 14 9 0 576.43 542.69 34.62 o 15 9 0 1355.34 1157.31 120.31 o 16 9 0 360.95 285.25 31.45 o 0 10 0 11445.86 11513.23 113.05 o 1 10 0 4325.20 4338.42 44.83 o 2 10 0 449.53 453.90 11.25 o 3 10 0 550.58 478.95 19.02 o 4 10 0 490.56 422.30 11.19 o 5 10 0 562.44 501.48 5.97 o 6 10 0 1659.12 1539.80 63.12 o 7 10 0 6141.89 5857.42 137.10 o 8 10 0 61.76 38.09 4.38 o 9 10 0 7236.67 7445.17 109.87 o 10 10 0 2293.54 2235.46 64.22 o 11 10 0 1925.98 1948.75 58.31 o 12 10 0 1076.84 989.35 39.38 o 13 10 0 696.66 712.47 49.31 o 14 10 0 2928.86 3000.32 177.16 o 15 10 0 1147.45 1099.08 93.96 o 1 11 0 39871.38 41707.48 212.79 o 2 11 0 30.60 37.07 7.61 o 3 11 0 24245.70 24831.99 129.61 o 4 11 0 1834.34 1678.05 36.33 o 5 11 0 17904.47 19648.86 314.38 o 6 11 0 1993.00 1974.39 55.42 o 7 11 0 6067.93 6053.44 103.28 o 8 11 0 5621.69 6021.57 153.27 o 9 11 0 2998.10 3060.60 337.45 o 10 11 0 5767.96 5869.11 100.73 o 11 11 0 593.53 554.08 49.04 o 12 11 0 2934.46 3008.23 127.82 o 13 11 0 54.83 37.07 10.08 o 14 11 0 173.48 232.36 24.91 o 15 11 0 127.54 130.42 20.04 o 0 12 0 6594.12 7198.61 149.85 o 1 12 0 128.61 106.28 7.22 o 2 12 0 4038.07 4169.44 50.56 o 3 12 0 280.59 225.93 10.12 o 4 12 0 3860.27 3532.27 57.52 o 5 12 0 3700.45 3577.79 96.17 o 6 12 0 4857.12 4751.48 159.46 o 7 12 0 8553.75 9067.95 170.33 o 8 12 0 126.10 108.40 17.28 o 9 12 0 1152.33 1203.39 100.38 o 10 12 0 58.35 92.87 32.95 o 11 12 0 416.67 382.52 53.12 o 12 12 0 36.58 30.93 14.76 o 13 12 0 1664.42 1758.90 101.43 o 14 12 0 1094.61 1210.89 130.84 o 15 12 0 3.92 43.22 22.26 o 1 13 0 321.65 317.47 18.28 o 2 13 0 997.64 920.36 24.35 o 3 13 0 16.73 36.71 4.41 o 4 13 0 938.91 967.24 30.38 o 5 13 0 5152.66 5186.34 218.53 o 6 13 0 4075.30 4112.65 119.11 o 7 13 0 5149.88 5502.56 201.49 o 8 13 0 2463.47 2870.36 193.78 o 9 13 0 5358.51 5516.48 170.95 o 10 13 0 2445.68 2604.76 113.03 o 11 13 0 1460.52 1433.43 124.47 o 12 13 0 2201.95 2216.14 255.47 o 13 13 0 2457.29 2746.39 155.84 o 14 13 0 371.82 272.15 39.52 o 0 14 0 865.21 828.89 40.07 o 1 14 0 3144.65 2979.72 52.87 o 2 14 0 3121.04 3137.30 63.47 o 3 14 0 789.00 665.56 27.22 o 4 14 0 327.49 246.47 24.16 o 5 14 0 589.97 430.76 49.58 o 6 14 0 128.19 124.27 19.06 o 7 14 0 56.05 95.14 16.21 o 8 14 0 232.21 214.67 43.54 o 9 14 0 207.53 196.81 39.91 o 10 14 0 67.63 99.17 21.80 o 11 14 0 805.01 831.65 57.95 o 12 14 0 32.17 29.58 13.83 o 13 14 0 20.32 22.40 12.05 o 1 15 0 322.34 305.34 25.85 o 2 15 0 107.27 126.66 9.67 o 3 15 0 3204.50 3197.81 61.23 o 4 15 0 942.76 854.67 31.23 o 5 15 0 2553.58 2474.96 89.16 o 6 15 0 556.76 603.92 84.14 o 7 15 0 756.84 742.77 149.06 o 8 15 0 716.63 788.07 110.28 o 9 15 0 3860.23 4025.61 120.76 o 10 15 0 788.20 867.56 74.48 o 11 15 0 1502.41 1497.52 76.14 o 12 15 0 531.21 616.71 61.60 o 0 16 0 8081.48 8742.13 171.63 o 1 16 0 146.04 117.62 11.08 o 2 16 0 6192.44 6840.15 90.06 o 3 16 0 690.17 643.77 27.77 o 4 16 0 5255.36 5540.65 151.90 o 5 16 0 3606.33 3858.27 125.84 o 6 16 0 2140.56 2277.97 136.26 o 7 16 0 325.77 339.28 29.62 o 8 16 0 556.94 630.93 63.08 o 9 16 0 1300.12 1390.72 154.26 o 10 16 0 1.86 32.30 14.29 o 11 16 0 1270.40 1264.18 110.87 o 1 17 0 12916.53 13677.84 191.49 o 2 17 0 377.90 319.89 20.61 o 3 17 0 4536.32 4439.99 118.56 o 4 17 0 246.45 217.81 49.67 o 5 17 0 4997.14 5843.87 163.01 o 6 17 0 72.12 64.39 21.87 o 7 17 0 4484.96 5054.47 108.25 o 8 17 0 250.05 373.82 35.78 o 9 17 0 1982.15 2070.57 85.08 o 10 17 0 29.65 34.43 12.37 o 0 18 0 2436.91 2644.20 51.06 o 1 18 0 32.07 36.66 7.40 o 2 18 0 448.51 410.16 52.57 o 3 18 0 488.78 434.75 42.22 o 4 18 0 153.64 114.32 14.84 o 5 18 0 1336.60 1351.93 125.16 o 6 18 0 55.49 21.68 10.59 o 7 18 0 435.46 536.07 52.17 o 8 18 0 16.48 44.32 15.83 o 9 18 0 2271.20 2585.29 200.53 o 1 19 0 936.32 835.45 60.17 o 2 19 0 189.63 106.80 29.91 o 3 19 0 1805.24 1900.39 54.73 o 4 19 0 16.08 19.13 10.83 o 5 19 0 1436.96 1369.64 132.64 o 6 19 0 9.94 14.09 8.92 o 7 19 0 923.69 925.25 88.32 o 2 20 0 989.04 961.65 128.08 o 3 20 0 73.70 46.76 11.96 o 4 20 0 1295.47 1176.67 93.03 o 5 20 0 0.33 20.39 12.36 o -18 1 1 30.10 23.56 7.76 o -17 1 1 493.54 546.31 30.13 o -16 1 1 704.68 660.10 45.56 o -15 1 1 3272.68 3174.16 90.04 o -14 1 1 2.45 21.95 5.57 o -13 1 1 2927.42 2555.07 84.86 o -12 1 1 80.18 81.05 10.32 o -11 1 1 13019.21 13476.43 113.71 o -10 1 1 393.26 356.49 15.79 o -9 1 1 10917.03 11649.68 97.01 o -8 1 1 993.09 999.20 16.48 o -7 1 1 32987.61 35493.45 136.59 o -6 1 1 3462.42 3628.62 34.38 o -5 1 1 58869.09 58867.38 237.99 o -4 1 1 7333.21 7017.30 45.66 o -3 1 1 87641.16 85269.43 270.53 o 2 1 1 11750.05 12085.49 59.56 o 3 1 1 14778.16 14967.66 74.36 o 4 1 1 8352.63 7972.25 52.31 o 5 1 1 6648.82 6262.92 43.84 o 6 1 1 16.01 16.79 4.34 o 7 1 1 4026.30 3198.09 36.32 o 8 1 1 44.20 63.31 5.87 o 9 1 1 10408.07 10464.43 89.04 o 10 1 1 0.57 23.93 5.03 o 11 1 1 9897.79 10431.78 125.17 o 12 1 1 420.72 367.64 19.07 o 13 1 1 288.42 300.10 36.17 o 14 1 1 670.16 701.96 48.40 o 15 1 1 180.77 129.13 28.13 o 16 1 1 517.67 449.00 24.52 o 17 1 1 670.73 659.06 45.05 o 18 1 1 208.00 120.35 14.37 o -18 2 1 1131.18 849.68 61.66 o -17 2 1 736.89 627.67 35.39 o -16 2 1 514.27 421.72 28.17 o -15 2 1 4557.94 5029.80 83.77 o -14 2 1 237.35 228.13 20.57 o -13 2 1 10744.37 11699.60 110.13 o -12 2 1 4.62 13.61 3.63 o -11 2 1 1540.72 1470.94 44.77 o -10 2 1 1.39 23.12 4.86 o -9 2 1 9243.42 9667.15 88.57 o -8 2 1 5751.09 5733.08 121.00 o -7 2 1 19124.86 18702.69 118.10 o -6 2 1 8162.95 8174.25 108.24 o -5 2 1 5608.18 5824.02 44.76 o -4 2 1 14474.04 13649.66 68.66 o -3 2 1 4731.47 5025.56 42.20 o -2 2 1 3408.34 3927.24 42.00 o -1 2 1 4.63 17.62 4.44 o 1 2 1 17538.21 18637.72 74.59 o 2 2 1 13007.56 13497.62 103.89 o 3 2 1 11979.55 11645.49 95.32 o 4 2 1 2352.82 2261.35 23.75 o 5 2 1 8949.91 8739.15 66.31 o 6 2 1 7021.77 7604.64 74.65 o 7 2 1 9411.40 10032.42 71.95 o 8 2 1 14243.32 14234.29 118.34 o 9 2 1 12479.83 12840.29 107.72 o 10 2 1 2155.97 2093.68 61.34 o 11 2 1 3004.16 2833.36 60.83 o 12 2 1 2830.30 2651.94 96.85 o 13 2 1 2283.44 2025.42 50.95 o 14 2 1 5897.58 5988.52 129.37 o 15 2 1 57.36 65.31 24.45 o 16 2 1 2159.81 2244.60 94.64 o 17 2 1 192.85 144.48 13.57 o 18 2 1 1302.91 1227.13 68.82 o -18 3 1 950.10 800.75 41.96 o -17 3 1 4803.74 4944.41 89.09 o -16 3 1 3940.67 4569.00 111.91 o -15 3 1 7513.25 7805.50 167.65 o -14 3 1 6977.27 7060.14 120.42 o -13 3 1 5852.50 6151.98 96.25 o -12 3 1 1989.83 1828.04 58.58 o -11 3 1 5694.04 5998.97 70.30 o -10 3 1 4905.14 5106.80 72.47 o -9 3 1 3.24 27.65 5.62 o -8 3 1 15289.84 15128.17 103.44 o -7 3 1 505.52 424.29 18.87 o -6 3 1 15638.79 15586.11 87.12 o -5 3 1 11930.12 12114.85 63.18 o -4 3 1 958.33 994.12 23.07 o -3 3 1 305.08 445.95 7.71 o -2 3 1 7067.97 6015.57 56.00 o -1 3 1 459.02 666.50 11.81 o 0 3 1 8743.49 7856.41 48.17 o 1 3 1 17358.05 17763.13 67.47 o 2 3 1 35467.52 36752.42 153.49 o 3 3 1 23134.91 22664.69 87.49 o 4 3 1 5006.18 4915.53 43.24 o 5 3 1 11172.67 11979.21 84.31 o 6 3 1 5903.81 5880.93 60.03 o 7 3 1 19239.16 19120.41 118.04 o 8 3 1 21932.89 24182.26 109.39 o 9 3 1 25646.44 26512.38 145.35 o 10 3 1 3536.05 3338.55 46.26 o 11 3 1 15428.60 16951.06 144.61 o 12 3 1 824.37 823.33 49.92 o 13 3 1 17799.65 18502.70 263.20 o 14 3 1 1537.88 1407.28 57.75 o 15 3 1 12525.89 14352.26 280.59 o 16 3 1 341.44 450.28 34.23 o 17 3 1 3768.13 4160.31 108.93 o -18 4 1 179.11 91.92 13.78 o -17 4 1 291.39 270.74 20.13 o -16 4 1 484.30 511.17 29.56 o -15 4 1 869.69 761.90 74.97 o -14 4 1 160.49 214.82 21.48 o -13 4 1 1233.98 1141.20 47.48 o -12 4 1 87.23 58.67 10.88 o -11 4 1 3093.82 2924.49 54.43 o -10 4 1 4401.28 4414.07 72.82 o -9 4 1 4379.08 3976.92 53.20 o -8 4 1 19169.29 18815.56 117.23 o -7 4 1 2.07 25.01 5.68 o -6 4 1 16047.38 15831.33 120.19 o -5 4 1 9619.51 8911.16 57.39 o -4 4 1 40190.73 39766.91 249.73 o -3 4 1 2135.79 2316.57 25.05 o -2 4 1 84180.60 86535.62 389.02 o -1 4 1 4754.14 3766.33 31.86 o 0 4 1 88861.30 89589.45 250.04 o 1 4 1 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