#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:51:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181303 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/81/2238189.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238189_Fobs loop_ _publ_author_name 'Pan, Gang-Hong' 'Tang, Jin-Niu' 'Huang, Zhong-Jing' 'Liao, Yi-Fan' 'Mo, Bo-Fa' _publ_section_title ; catena-Poly[(diaquacadmium)-\m-iminodiacetato-\k^4^O,N,O':O''] ; _journal_coeditor_code HY2628 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m416 _journal_volume 69 _journal_year 2013 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2ac' _symmetry_space_group_name_H-M 'P c a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.6600 _cell_length_b 5.4905 _cell_length_c 9.7928 _exptl_crystal_F_000 544.00 _reflns_d_resolution_high 0.8412 _cod_data_source_file hy2628Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sdc in Pca2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 2 -9 162.37 157.76 33.57 o 6 2 -9 18.24 0.81 25.89 o 7 2 -9 1345.74 1304.92 86.56 o 8 2 -9 37.67 45.71 32.36 o 9 2 -9 1600.46 1656.83 109.62 o 1 3 -9 793.85 951.17 54.86 o 2 3 -9 653.90 762.64 49.46 o 3 3 -9 202.27 233.40 40.45 o 4 3 -9 1424.77 1394.31 90.61 o 5 3 -9 22.30 21.84 25.08 o 6 3 -9 626.24 753.58 67.55 o 7 3 -9 329.39 329.26 48.94 o 1 4 -9 57.77 8.48 23.94 o 2 4 -9 640.45 591.60 53.19 o 4 1 -8 277.74 326.84 37.21 o 6 1 -8 376.19 304.59 40.45 o 7 1 -8 950.51 1040.78 77.66 o 8 1 -8 772.28 745.49 66.34 o 9 1 -8 38.26 55.01 32.36 o 10 1 -8 887.43 840.15 80.09 o 11 1 -8 416.90 420.68 62.29 o 12 1 -8 216.29 171.51 50.97 o 0 2 -8 250.82 220.45 34.38 o 1 2 -8 447.24 537.18 49.35 o 2 2 -8 15.03 21.26 14.56 o 3 2 -8 1456.69 1352.65 79.69 o 4 2 -8 28.75 37.62 21.44 o 5 2 -8 1883.37 1868.79 101.13 o 6 2 -8 6.20 19.01 22.25 o 7 2 -8 761.67 713.54 63.10 o 8 2 -8 104.59 115.69 32.36 o 9 2 -8 0.39 2.83 26.29 o 10 2 -8 1.97 -26.70 25.48 o 11 2 -8 580.52 580.46 67.55 o 0 3 -8 859.91 1074.76 79.28 o 1 3 -8 114.13 135.38 25.74 o 2 3 -8 799.30 889.68 51.19 o 3 3 -8 436.80 527.37 38.25 o 4 3 -8 18.50 44.50 25.48 o 5 3 -8 1009.27 995.07 74.83 o 6 3 -8 270.75 277.49 41.26 o 7 3 -8 173.89 216.00 40.05 o 8 3 -8 949.91 964.73 76.86 o 9 3 -8 35.49 25.08 29.53 o 0 4 -8 711.16 857.95 78.88 o 1 4 -8 28.84 -10.61 22.17 o 2 4 -8 1022.07 1055.28 61.49 o 3 4 -8 121.68 135.93 26.95 o 4 4 -8 66.18 96.98 24.23 o 5 4 -8 122.42 107.60 34.79 o 6 4 -8 336.86 315.11 47.33 o 4 0 -7 7329.14 6968.73 307.82 o 6 0 -7 4106.88 4022.35 192.54 o 8 0 -7 576.69 569.54 60.68 o 10 0 -7 437.97 449.40 60.27 o 12 0 -7 1587.10 1748.66 120.14 o 1 1 -7 4649.38 4698.66 150.45 o 2 1 -7 624.76 852.44 130.86 o 3 1 -7 234.22 259.28 29.93 o 5 1 -7 59.17 62.70 22.65 o 6 1 -7 1504.18 1546.81 87.78 o 7 1 -7 1322.27 1244.24 80.09 o 8 1 -7 232.11 242.70 38.02 o 9 1 -7 2153.86 2081.56 120.95 o 10 1 -7 304.75 300.95 49.35 o 11 1 -7 574.07 559.02 66.34 o 12 1 -7 848.78 1009.55 94.05 o 13 1 -7 25.55 11.49 29.53 o 1 2 -7 6302.72 6185.38 203.79 o 2 2 -7 84.35 163.42 34.38 o 3 2 -7 1836.43 1666.95 92.63 o 4 2 -7 62.21 46.52 19.42 o 5 2 -7 149.06 116.90 26.29 o 6 2 -7 26.00 15.78 20.63 o 7 2 -7 2687.95 2516.80 127.01 o 8 2 -7 72.59 93.04 28.32 o 9 2 -7 3899.32 3911.11 198.21 o 10 2 -7 52.66 31.15 28.72 o 11 2 -7 1317.98 1483.71 104.36 o 12 2 -7 9.52 10.92 32.76 o 1 3 -7 1375.22 1415.02 65.07 o 2 3 -7 1117.92 1238.11 60.56 o 3 3 -7 468.12 597.85 55.42 o 4 3 -7 2801.35 2496.58 132.68 o 5 3 -7 265.89 257.26 38.02 o 6 3 -7 2334.96 2038.28 117.31 o 7 3 -7 762.20 803.34 66.34 o 8 3 -7 245.33 230.16 40.45 o 9 3 -7 559.44 524.23 57.03 o 10 3 -7 203.59 184.05 40.45 o 11 3 -7 312.22 297.71 50.16 o 1 4 -7 36.54 46.64 34.38 o 2 4 -7 1071.89 1294.20 65.21 o 3 4 -7 21.55 82.19 31.15 o 4 4 -7 3529.74 3172.50 168.27 o 5 4 -7 9.03 40.45 27.10 o 6 4 -7 1594.21 1421.01 96.68 o 7 4 -7 143.59 116.90 33.98 o 8 4 -7 147.03 146.02 38.02 o 1 5 -7 1169.62 1399.29 76.65 o 2 5 -7 218.73 243.07 37.60 o 3 5 -7 443.04 515.84 45.28 o 0 0 -6 9034.94 8441.52 354.75 o 2 0 -6 2478.49 2225.54 120.34 o 4 0 -6 337.17 331.29 35.60 o 8 0 -6 4057.62 3793.40 187.28 o 10 0 -6 1831.52 1673.01 107.60 o 12 0 -6 426.51 444.95 61.08 o 14 0 -6 162.38 172.72 48.14 o 0 1 -6 4393.66 4192.65 181.62 o 1 1 -6 1221.36 1632.72 111.24 o 4 1 -6 168.71 176.33 34.58 o 5 1 -6 4400.34 3959.13 134.50 o 6 1 -6 1009.30 912.06 46.24 o 7 1 -6 1270.36 1202.81 65.93 o 8 1 -6 2299.26 2053.65 116.50 o 9 1 -6 64.80 87.92 22.24 o 10 1 -6 1775.53 1784.08 245.73 o 11 1 -6 626.93 721.54 51.87 o 12 1 -6 178.59 197.49 46.52 o 13 1 -6 799.21 890.47 61.29 o 14 1 -6 77.94 86.51 29.64 o 0 2 -6 640.17 749.54 56.63 o 1 2 -6 834.26 897.22 42.74 o 2 2 -6 289.11 389.53 40.05 o 3 2 -6 3943.09 3552.32 167.06 o 4 2 -6 350.68 343.42 36.41 o 5 2 -6 5239.48 4965.24 216.81 o 6 2 -6 306.26 285.98 35.60 o 7 2 -6 1891.78 1626.09 95.46 o 8 2 -6 261.42 242.30 37.21 o 9 2 -6 56.40 70.79 29.53 o 10 2 -6 49.59 10.11 28.32 o 11 2 -6 1498.31 1425.21 71.42 o 12 2 -6 77.28 61.15 26.27 o 13 2 -6 1671.34 1737.68 82.15 o 0 3 -6 3807.62 4285.28 197.80 o 1 3 -6 668.41 1211.00 110.23 o 2 3 -6 2284.43 2219.09 122.56 o 3 3 -6 2684.67 2435.09 129.44 o 4 3 -6 58.56 67.55 25.08 o 5 3 -6 2171.70 2041.92 107.19 o 6 3 -6 514.83 505.63 50.56 o 7 3 -6 425.86 524.23 52.18 o 8 3 -6 1915.99 1817.82 102.74 o 9 3 -6 10.10 -0.40 23.87 o 10 3 -6 1270.97 1353.46 95.06 o 11 3 -6 336.61 356.77 52.18 o 12 3 -6 202.16 211.55 44.50 o 0 4 -6 4095.63 4292.56 210.34 o 1 4 -6 141.41 398.83 43.69 o 2 4 -6 2892.18 2609.44 102.54 o 3 4 -6 213.97 290.03 45.30 o 4 4 -6 20.90 33.57 24.67 o 5 4 -6 94.71 68.77 28.32 o 6 4 -6 828.02 853.50 70.38 o 7 4 -6 60.29 48.54 28.72 o 8 4 -6 1725.25 1334.45 93.04 o 9 4 -6 12.37 -10.52 23.87 o 10 4 -6 1203.36 1127.75 88.59 o 0 5 -6 473.52 596.23 70.79 o 1 5 -6 126.22 139.43 31.17 o 2 5 -6 656.72 761.06 54.47 o 3 5 -6 898.89 1114.75 65.15 o 4 5 -6 99.53 120.95 37.21 o 5 5 -6 848.42 917.41 78.07 o 6 5 -6 192.16 180.41 40.05 o 2 0 -5 5222.85 4657.42 208.72 o 4 0 -5 16803.28 15732.23 678.35 o 6 0 -5 7906.10 7651.13 331.69 o 8 0 -5 1508.11 1330.00 86.16 o 10 0 -5 476.54 518.97 58.65 o 12 0 -5 2262.31 2253.47 134.70 o 14 0 -5 2184.22 2476.35 140.77 o 1 1 -5 4518.57 4227.03 196.59 o 2 1 -5 1954.23 2069.82 114.27 o 3 1 -5 2107.68 1993.30 181.42 o 4 1 -5 3427.28 2998.00 214.99 o 5 1 -5 239.68 264.84 23.31 o 6 1 -5 4035.29 3782.68 133.50 o 7 1 -5 2691.90 2537.43 128.63 o 8 1 -5 403.35 463.67 47.12 o 9 1 -5 2049.88 1980.52 155.93 o 10 1 -5 260.13 308.21 56.83 o 11 1 -5 1189.92 1448.77 186.27 o 12 1 -5 1133.15 1259.87 158.16 o 13 1 -5 87.66 89.11 27.93 o 14 1 -5 851.71 856.04 59.44 o 15 1 -5 267.46 293.62 38.98 o 1 2 -5 8581.56 8974.65 372.54 o 3 2 -5 3011.68 3034.56 140.36 o 4 2 -5 49.43 27.86 9.82 o 5 2 -5 176.64 187.56 17.71 o 6 2 -5 49.88 54.45 13.57 o 7 2 -5 2919.95 2679.26 114.07 o 8 2 -5 43.40 15.36 16.58 o 9 2 -5 5374.92 4730.65 467.40 o 10 2 -5 38.04 18.75 18.61 o 11 2 -5 1923.24 1729.75 139.75 o 12 2 -5 116.79 164.18 32.36 o 13 2 -5 141.34 138.34 31.73 o 14 2 -5 2.98 11.19 24.76 o 1 3 -5 1939.68 2045.96 116.90 o 2 3 -5 2215.68 2161.65 114.88 o 3 3 -5 107.37 150.88 28.72 o 4 3 -5 2784.94 2465.43 126.20 o 5 3 -5 38.12 49.75 20.63 o 6 3 -5 2629.13 2348.13 124.99 o 7 3 -5 620.36 660.55 57.03 o 8 3 -5 567.43 511.29 50.56 o 9 3 -5 1059.40 1112.38 78.47 o 10 3 -5 157.26 130.78 43.69 o 11 3 -5 391.21 404.13 37.70 o 12 3 -5 1279.77 1175.04 209.53 o 13 3 -5 44.70 45.03 24.84 o 1 4 -5 124.05 211.84 27.60 o 2 4 -5 1769.89 1677.06 103.96 o 3 4 -5 64.02 120.14 31.96 o 4 4 -5 2969.56 2646.65 144.00 o 5 4 -5 112.48 99.91 29.53 o 6 4 -5 1957.41 1661.28 102.74 o 7 4 -5 26.33 24.27 23.87 o 8 4 -5 347.69 307.82 44.50 o 9 4 -5 100.90 91.01 31.15 o 10 4 -5 238.18 199.82 40.45 o 11 4 -5 10.34 13.35 28.72 o 1 5 -5 2184.32 2091.34 92.38 o 2 5 -5 83.77 305.19 37.17 o 3 5 -5 503.97 581.27 66.34 o 4 5 -5 587.42 509.67 59.06 o 5 5 -5 54.42 41.66 29.12 o 6 5 -5 377.68 373.35 51.78 o 7 5 -5 815.70 721.63 70.79 o 8 5 -5 110.33 65.12 32.36 o 0 0 -4 22271.61 20791.73 912.15 o 2 0 -4 11841.58 11012.93 486.21 o 6 0 -4 2630.98 2785.79 140.77 o 8 0 -4 7244.61 6955.79 319.15 o 10 0 -4 6827.24 6884.60 317.13 o 12 0 -4 1520.28 1682.72 106.38 o 14 0 -4 573.86 703.83 74.83 o 16 0 -4 432.29 525.85 68.36 o 0 1 -4 14916.38 15278.38 641.13 o 2 1 -4 10129.96 9875.23 295.60 o 3 1 -4 9562.68 8333.71 270.29 o 4 1 -4 89.04 83.88 13.30 o 5 1 -4 7166.68 6338.42 343.62 o 6 1 -4 979.71 928.45 45.02 o 7 1 -4 1771.13 1643.69 66.58 o 8 1 -4 3875.76 3647.97 182.83 o 9 1 -4 55.05 49.83 18.24 o 10 1 -4 2403.54 2531.22 96.49 o 11 1 -4 1316.46 1459.42 115.48 o 12 1 -4 817.00 1049.50 102.95 o 13 1 -4 1929.77 2063.71 121.96 o 14 1 -4 46.57 59.23 26.74 o 15 1 -4 676.99 715.64 54.11 o 16 1 -4 250.41 288.76 39.61 o 0 2 -4 434.97 468.82 40.45 o 1 2 -4 1062.00 1047.66 61.89 o 2 2 -4 296.19 447.27 71.60 o 3 2 -4 8796.49 8645.51 256.52 o 4 2 -4 97.22 88.51 12.50 o 5 2 -4 9347.02 8566.90 269.80 o 6 2 -4 263.55 287.08 33.98 o 7 2 -4 2043.94 1831.83 162.61 o 8 2 -4 128.03 167.02 35.19 o 9 2 -4 129.17 111.99 21.38 o 10 2 -4 190.16 297.67 32.26 o 11 2 -4 1109.67 1045.35 63.71 o 12 2 -4 0.40 17.73 21.77 o 13 2 -4 2676.29 2472.41 105.22 o 14 2 -4 44.90 -6.25 25.48 o 15 2 -4 1112.66 1211.86 72.41 o 0 3 -4 4451.92 4600.38 220.05 o 1 3 -4 370.50 787.56 60.27 o 2 3 -4 2042.40 2096.88 160.59 o 3 3 -4 1813.09 1893.20 159.78 o 4 3 -4 222.11 197.35 19.00 o 5 3 -4 2284.09 2050.47 79.69 o 6 3 -4 1694.65 1524.78 61.31 o 7 3 -4 1710.37 1509.60 86.97 o 8 3 -4 1950.50 1774.68 70.93 o 9 3 -4 113.02 98.54 20.62 o 10 3 -4 2117.06 2037.99 82.51 o 11 3 -4 478.03 456.43 54.61 o 12 3 -4 116.71 133.02 27.88 o 13 3 -4 700.05 648.29 98.09 o 14 3 -4 37.29 10.34 24.67 o 0 4 -4 5296.18 6125.35 281.94 o 2 4 -4 1721.59 1621.24 99.10 o 3 4 -4 71.26 127.82 31.96 o 4 4 -4 258.15 293.26 40.05 o 5 4 -4 936.35 800.51 64.32 o 6 4 -4 1111.54 1112.38 80.90 o 7 4 -4 114.34 114.07 30.34 o 8 4 -4 3083.76 2541.48 140.77 o 9 4 -4 27.66 8.49 24.67 o 10 4 -4 1949.68 1802.48 121.75 o 11 4 -4 3.14 14.53 20.27 o 12 4 -4 227.54 229.98 33.82 o 0 5 -4 1371.47 1450.13 106.79 o 1 5 -4 336.22 456.41 42.05 o 2 5 -4 330.03 526.26 63.91 o 3 5 -4 1550.63 1658.86 106.79 o 4 5 -4 13.53 54.20 31.15 o 5 5 -4 1988.52 1623.66 106.79 o 6 5 -4 246.75 219.64 41.26 o 7 5 -4 684.29 655.70 65.53 o 8 5 -4 473.32 417.44 55.01 o 9 5 -4 2.81 5.26 27.10 o 0 6 -4 596.62 639.52 79.28 o 1 6 -4 696.53 787.27 60.20 o 2 6 -4 125.64 166.43 68.16 o 3 6 -4 1227.21 1250.14 74.22 o 2 0 -3 7878.25 7235.70 313.08 o 4 0 -3 16214.72 15633.94 653.27 o 6 0 -3 7519.83 7332.38 322.79 o 8 0 -3 2541.59 2581.93 129.04 o 10 0 -3 1690.34 1665.33 101.53 o 12 0 -3 5033.39 5455.90 257.26 o 14 0 -3 1891.43 2047.99 124.99 o 16 0 -3 413.44 375.38 61.08 o 1 1 -3 7753.55 8039.41 247.95 o 2 1 -3 8170.62 8717.92 278.30 o 3 1 -3 4470.61 4260.80 137.72 o 4 1 -3 7191.10 6352.62 426.34 o 5 1 -3 606.81 653.14 32.36 o 6 1 -3 3593.89 3232.93 117.64 o 7 1 -3 4924.48 4447.07 201.24 o 8 1 -3 67.89 95.33 19.73 o 9 1 -3 3511.03 3645.67 132.20 o 10 1 -3 391.24 415.36 35.94 o 11 1 -3 1929.18 1872.06 79.77 o 12 1 -3 1609.61 1628.44 83.33 o 13 1 -3 54.81 43.70 23.25 o 14 1 -3 938.69 969.10 61.71 o 15 1 -3 587.65 590.96 50.28 o 16 1 -3 242.77 280.40 39.23 o 1 2 -3 14687.50 15905.69 521.40 o 3 2 -3 5240.99 5349.49 265.96 o 4 2 -3 797.02 796.06 42.47 o 5 2 -3 2507.61 2546.73 120.95 o 6 2 -3 626.51 740.43 37.21 o 7 2 -3 5145.07 4706.04 150.59 o 8 2 -3 95.46 155.01 20.85 o 9 2 -3 6023.88 5416.77 305.20 o 10 2 -3 69.01 39.11 18.15 o 11 2 -3 1497.59 1277.48 73.82 o 12 2 -3 190.73 147.13 28.68 o 13 2 -3 140.09 148.33 30.91 o 14 2 -3 8.82 4.17 23.51 o 15 2 -3 655.44 668.37 54.32 o 1 3 -3 3573.48 4037.06 324.00 o 2 3 -3 4014.66 4399.88 297.51 o 3 3 -3 876.66 962.66 42.64 o 4 3 -3 4314.88 3857.74 309.85 o 5 3 -3 10.17 7.14 8.44 o 6 3 -3 4243.03 3875.35 130.99 o 7 3 -3 1890.80 1733.38 68.79 o 8 3 -3 138.75 155.20 21.69 o 9 3 -3 2394.38 2250.05 87.94 o 10 3 -3 230.27 258.39 29.42 o 11 3 -3 753.21 779.70 61.48 o 12 3 -3 1825.69 1621.37 272.84 o 13 3 -3 3.67 -21.75 21.25 o 14 3 -3 693.36 612.71 114.68 o 1 4 -3 83.61 128.92 42.27 o 2 4 -3 2468.44 2543.88 142.38 o 3 4 -3 528.46 566.37 68.36 o 4 4 -3 5014.81 4567.46 289.82 o 5 4 -3 36.36 17.38 16.58 o 6 4 -3 3875.79 3176.19 198.00 o 7 4 -3 118.97 128.99 28.72 o 8 4 -3 541.65 549.31 39.19 o 9 4 -3 240.75 288.24 31.31 o 10 4 -3 756.36 731.45 48.74 o 11 4 -3 23.40 31.52 21.30 o 12 4 -3 1298.67 1366.75 195.17 o 13 4 -3 29.42 6.67 24.42 o 1 5 -3 2326.31 2448.48 97.82 o 2 5 -3 883.07 1027.43 86.56 o 3 5 -3 530.73 639.92 67.15 o 4 5 -3 1400.28 1340.11 96.68 o 5 5 -3 51.84 86.16 32.36 o 6 5 -3 469.05 444.55 54.20 o 7 5 -3 1368.51 1214.71 92.23 o 8 5 -3 59.15 30.34 28.72 o 9 5 -3 1180.84 1028.24 84.14 o 10 5 -3 144.31 118.11 37.62 o 1 6 -3 2126.17 2031.72 94.10 o 2 6 -3 175.21 294.25 90.00 o 3 6 -3 234.51 334.93 59.87 o 4 6 -3 72.72 62.70 37.62 o 5 6 -3 63.73 66.34 36.41 o 0 0 -2 37848.24 37964.39 1643.08 o 4 0 -2 7601.19 7905.56 341.40 o 6 0 -2 4851.95 4932.48 224.09 o 8 0 -2 13312.09 13643.39 571.56 o 10 0 -2 7766.57 8083.54 364.45 o 12 0 -2 1484.65 1605.87 103.96 o 14 0 -2 434.67 396.01 57.44 o 16 0 -2 905.24 1107.93 93.84 o 1 1 -2 761.14 1077.41 35.59 o 2 1 -2 5003.13 5076.01 162.00 o 3 1 -2 13179.75 12561.76 540.01 o 4 1 -2 542.15 555.74 29.53 o 5 1 -2 14353.61 13996.17 410.72 o 6 1 -2 1557.00 1489.21 58.82 o 7 1 -2 3394.61 3235.57 148.86 o 8 1 -2 4459.49 4204.93 146.63 o 9 1 -2 43.76 28.20 16.81 o 10 1 -2 2802.29 2708.95 102.61 o 11 1 -2 1170.64 1214.94 63.56 o 12 1 -2 239.36 199.57 30.38 o 13 1 -2 1969.37 1978.13 85.27 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15.53 o 2 4 3 2479.39 2404.15 52.81 o 3 4 3 522.91 528.87 25.26 o 4 4 3 5189.94 4546.27 95.51 o 5 4 3 36.68 39.73 13.43 o 6 4 3 3928.31 3184.86 93.17 o 7 4 3 104.71 103.19 19.36 o 8 4 3 571.33 608.38 38.33 o 9 4 3 261.72 326.53 35.20 o 10 4 3 738.85 699.24 40.42 o 11 4 3 23.24 33.51 20.34 o 12 4 3 1313.30 1388.20 62.46 o 13 4 3 29.44 29.76 22.25 o 1 5 3 2285.40 2301.76 67.65 o 2 5 3 880.57 917.38 40.80 o 3 5 3 497.64 598.23 34.51 o 4 5 3 1463.22 1319.42 47.72 o 5 5 3 55.22 57.06 18.22 o 6 5 3 500.90 508.84 34.28 o 7 5 3 1353.55 1331.31 56.12 o 8 5 3 66.52 45.70 20.82 o 9 5 3 1170.61 1067.12 136.11 o 10 5 3 142.06 88.34 28.30 o 1 6 3 2122.14 2018.18 98.03 o 2 6 3 172.81 239.06 58.25 o 3 6 3 268.60 345.37 38.78 o 4 6 3 84.21 107.07 31.10 o 5 6 3 65.47 96.77 30.70 o 0 0 4 22815.29 22647.98 879.79 o 2 0 4 11778.33 11561.91 235.05 o 4 0 4 776.78 731.67 34.95 o 6 0 4 2814.90 2864.36 80.16 o 8 0 4 7132.72 6996.23 189.63 o 10 0 4 6682.43 6728.45 175.98 o 12 0 4 1554.80 1566.89 86.36 o 14 0 4 590.51 616.84 50.43 o 16 0 4 402.14 456.13 47.30 o 0 1 4 14259.26 14989.52 350.87 o 1 1 4 9.20 1810.95 90.20 o 2 1 4 9992.36 9734.17 141.53 o 3 1 4 9725.38 9060.04 151.11 o 4 1 4 81.62 68.81 5.72 o 5 1 4 6815.12 6525.27 98.08 o 6 1 4 981.07 993.84 21.05 o 7 1 4 1746.77 1636.98 33.72 o 8 1 4 3837.11 3681.98 65.58 o 9 1 4 53.59 54.95 10.75 o 10 1 4 2318.17 2362.61 57.90 o 11 1 4 1358.16 1411.02 38.97 o 12 1 4 781.82 1001.34 36.93 o 13 1 4 1884.46 1990.53 55.46 o 14 1 4 55.53 63.07 22.00 o 15 1 4 655.77 639.12 42.97 o 16 1 4 262.56 269.45 43.00 o 0 2 4 428.91 484.59 28.74 o 1 2 4 1088.31 1022.10 28.51 o 2 2 4 281.46 306.95 15.06 o 3 2 4 8731.12 8229.91 144.35 o 4 2 4 99.62 83.81 7.54 o 5 2 4 9344.70 8228.91 133.58 o 6 2 4 267.07 307.15 14.63 o 7 2 4 2126.78 2005.33 42.38 o 8 2 4 119.30 134.60 13.66 o 9 2 4 132.18 126.97 13.96 o 10 2 4 191.48 298.52 49.00 o 11 2 4 1140.44 1152.90 49.78 o 12 2 4 0.62 -16.29 18.73 o 13 2 4 2665.83 2623.04 95.57 o 14 2 4 45.29 41.31 22.74 o 15 2 4 1072.34 1004.49 71.93 o 0 3 4 4334.97 4749.14 151.88 o 1 3 4 376.94 793.36 92.16 o 2 3 4 2110.20 2045.17 49.03 o 3 3 4 1813.06 1809.17 40.08 o 4 3 4 242.01 217.07 13.56 o 5 3 4 2221.93 1924.37 47.54 o 6 3 4 1755.72 1563.12 40.90 o 7 3 4 1647.72 1464.65 39.73 o 8 3 4 1920.20 1756.32 59.67 o 9 3 4 115.84 96.03 19.22 o 10 3 4 2109.93 1945.62 66.92 o 11 3 4 474.07 431.06 33.07 o 12 3 4 115.82 115.40 23.90 o 13 3 4 672.79 710.85 43.68 o 14 3 4 33.44 19.43 22.44 o 0 4 4 5398.42 5862.14 192.64 o 1 4 4 2.37 494.51 151.28 o 2 4 4 1684.34 1565.34 43.58 o 3 4 4 67.49 95.76 12.82 o 4 4 4 260.24 244.98 18.82 o 5 4 4 914.01 774.06 30.33 o 6 4 4 1157.81 1155.46 53.09 o 7 4 4 107.84 85.71 16.67 o 8 4 4 3058.54 2677.60 82.95 o 9 4 4 27.06 17.30 18.43 o 10 4 4 1889.70 1764.21 64.39 o 11 4 4 2.33 1.11 19.64 o 12 4 4 227.62 270.88 31.14 o 0 5 4 1370.00 1374.05 72.79 o 1 5 4 333.55 416.80 29.36 o 2 5 4 320.72 503.43 31.62 o 3 5 4 1584.06 1620.22 47.43 o 4 5 4 11.38 11.79 15.36 o 5 5 4 1956.80 1789.46 55.79 o 6 5 4 231.78 166.77 25.32 o 7 5 4 707.27 705.02 55.58 o 8 5 4 485.27 512.93 37.03 o 9 5 4 2.66 24.60 20.20 o 0 6 4 581.23 678.35 81.30 o 1 6 4 706.87 626.57 79.69 o 2 6 4 113.86 191.04 36.94 o 3 6 4 1190.94 1146.35 83.61 o 2 0 5 5256.99 4785.65 102.63 o 4 0 5 17304.93 15932.46 326.51 o 6 0 5 7778.66 7320.32 157.85 o 8 0 5 1506.34 1371.81 47.86 o 10 0 5 415.84 457.85 38.51 o 12 0 5 2277.75 2320.48 160.33 o 14 0 5 2213.37 2090.21 121.55 o 1 1 5 4742.65 4436.35 71.50 o 2 1 5 1935.63 2154.92 55.45 o 3 1 5 2066.76 1975.10 36.75 o 4 1 5 3605.92 3136.10 54.14 o 5 1 5 255.48 267.87 11.59 o 6 1 5 4313.41 4039.23 64.21 o 7 1 5 2637.93 2541.75 48.28 o 8 1 5 426.43 472.19 18.11 o 9 1 5 2082.12 1974.63 45.26 o 10 1 5 231.56 251.19 20.57 o 11 1 5 1247.72 1403.94 50.19 o 12 1 5 1153.00 1280.52 49.23 o 13 1 5 84.25 89.57 20.95 o 14 1 5 875.37 913.45 43.85 o 15 1 5 267.53 285.62 34.99 o 1 2 5 8452.24 8295.45 145.48 o 3 2 5 3063.36 2834.81 51.49 o 4 2 5 55.77 36.48 7.88 o 5 2 5 173.39 176.85 13.54 o 6 2 5 43.83 31.47 9.46 o 7 2 5 2824.71 2652.26 55.52 o 8 2 5 41.63 30.27 10.81 o 9 2 5 5573.48 5274.42 97.21 o 10 2 5 36.62 42.25 14.51 o 11 2 5 1893.06 1775.70 64.01 o 12 2 5 123.93 191.76 27.19 o 13 2 5 139.82 155.38 26.82 o 14 2 5 2.02 8.54 22.73 o 1 3 5 2044.41 2205.95 65.22 o 2 3 5 2134.51 2062.67 49.93 o 3 3 5 94.54 131.09 13.57 o 4 3 5 2773.74 2399.61 50.72 o 5 3 5 37.01 31.09 11.08 o 6 3 5 2699.33 2381.75 56.70 o 7 3 5 665.15 690.21 28.28 o 8 3 5 513.32 475.43 24.33 o 9 3 5 1053.58 993.48 40.04 o 10 3 5 137.57 133.34 22.87 o 11 3 5 385.95 402.73 33.22 o 12 3 5 1313.03 1274.57 57.32 o 13 3 5 48.34 58.52 23.80 o 1 4 5 140.66 224.17 20.95 o 2 4 5 1790.62 1699.86 46.14 o 3 4 5 71.37 123.38 15.61 o 4 4 5 2977.63 2707.69 64.50 o 5 4 5 114.66 97.49 15.87 o 6 4 5 1949.24 1765.44 47.89 o 7 4 5 21.67 7.67 13.13 o 8 4 5 338.61 336.91 29.61 o 9 4 5 111.08 126.95 23.33 o 10 4 5 247.23 249.68 28.49 o 11 4 5 8.62 26.97 21.48 o 1 5 5 2211.13 2124.22 64.05 o 2 5 5 95.01 256.38 33.26 o 3 5 5 482.10 491.01 27.51 o 4 5 5 557.35 456.81 26.89 o 5 5 5 45.33 27.37 15.69 o 6 5 5 378.26 371.45 28.40 o 7 5 5 811.18 770.41 44.37 o 8 5 5 121.62 77.94 23.49 o 0 0 6 8784.89 8018.82 350.30 o 2 0 6 2506.66 2389.46 64.89 o 4 0 6 378.79 368.78 17.77 o 6 0 6 3255.65 2960.78 72.57 o 8 0 6 3943.62 3673.62 103.94 o 10 0 6 1709.73 1711.96 82.35 o 12 0 6 494.60 538.00 54.00 o 14 0 6 168.18 199.01 59.46 o 0 1 6 4164.89 3808.55 99.98 o 1 1 6 1137.26 1635.49 54.80 o 2 1 6 2180.02 2018.11 38.30 o 3 1 6 4856.72 4323.61 73.34 o 4 1 6 167.71 162.03 13.71 o 5 1 6 4254.29 3948.56 68.76 o 6 1 6 970.97 920.53 27.62 o 7 1 6 1250.37 1189.01 45.95 o 8 1 6 2271.81 2201.32 48.81 o 9 1 6 65.66 71.54 14.70 o 10 1 6 1749.98 1817.80 50.20 o 11 1 6 627.32 691.93 32.49 o 12 1 6 193.02 226.85 22.69 o 13 1 6 768.44 910.62 44.28 o 14 1 6 78.31 76.73 22.57 o 0 2 6 628.44 695.33 39.61 o 1 2 6 836.94 951.21 33.21 o 2 2 6 282.65 316.65 15.95 o 3 2 6 3834.36 3463.16 67.20 o 4 2 6 354.23 336.04 15.26 o 5 2 6 5025.99 4541.21 87.05 o 6 2 6 314.76 255.37 29.59 o 7 2 6 1910.33 1723.25 41.14 o 8 2 6 254.02 259.44 17.51 o 9 2 6 56.86 54.01 13.73 o 10 2 6 48.17 46.36 16.07 o 11 2 6 1482.60 1570.53 61.22 o 12 2 6 76.94 59.05 22.76 o 13 2 6 1676.46 1732.23 69.40 o 0 3 6 3688.38 3846.75 134.29 o 1 3 6 669.94 1048.02 38.90 o 2 3 6 2235.96 2221.46 48.50 o 3 3 6 2649.31 2425.29 52.01 o 4 3 6 64.65 88.49 14.07 o 5 3 6 2070.91 1822.46 48.01 o 6 3 6 546.85 563.23 26.24 o 7 3 6 432.46 459.21 24.57 o 8 3 6 1826.06 1680.20 48.32 o 9 3 6 9.94 -7.75 13.44 o 10 3 6 1278.31 1280.32 56.47 o 11 3 6 324.25 370.72 33.38 o 12 3 6 192.64 194.74 28.80 o 0 4 6 4120.30 4028.68 162.00 o 1 4 6 146.41 495.90 28.91 o 2 4 6 2770.73 2403.46 67.74 o 3 4 6 222.29 228.77 24.17 o 4 4 6 23.97 25.51 14.56 o 5 4 6 88.67 61.66 15.73 o 6 4 6 816.71 774.90 33.15 o 7 4 6 60.75 65.28 16.63 o 8 4 6 1684.03 1521.24 60.50 o 9 4 6 12.57 10.00 20.15 o 10 4 6 1175.29 1144.63 55.04 o 0 5 6 437.58 473.33 45.74 o 1 5 6 135.49 188.59 28.22 o 2 5 6 631.62 648.81 35.53 o 3 5 6 899.44 1004.79 51.21 o 4 5 6 99.13 89.59 18.44 o 5 5 6 810.69 763.80 35.09 o 6 5 6 178.17 147.08 20.68 o 2 0 7 5943.08 5607.13 142.23 o 4 0 7 7546.01 6877.49 172.80 o 6 0 7 4173.44 3932.88 107.53 o 8 0 7 546.63 619.03 46.41 o 10 0 7 463.91 514.51 54.20 o 12 0 7 1622.86 1979.61 95.65 o 1 1 7 4696.31 4605.12 84.76 o 2 1 7 668.60 1052.01 53.18 o 3 1 7 242.78 255.47 13.58 o 4 1 7 1861.67 1666.98 40.19 o 5 1 7 56.36 49.62 9.88 o 6 1 7 1498.32 1514.07 46.04 o 7 1 7 1363.83 1342.17 57.71 o 8 1 7 200.67 200.79 19.18 o 9 1 7 2201.69 2139.53 63.81 o 10 1 7 309.29 332.57 29.05 o 11 1 7 571.53 647.16 37.48 o 12 1 7 875.73 1043.88 48.45 o 13 1 7 23.00 15.52 24.85 o 1 2 7 6519.10 6372.78 124.67 o 2 2 7 81.03 358.80 102.74 o 3 2 7 1843.31 1667.24 38.88 o 4 2 7 69.34 34.03 11.03 o 5 2 7 174.76 150.40 15.86 o 6 2 7 29.22 22.91 11.57 o 7 2 7 2656.85 2303.48 62.74 o 8 2 7 71.51 48.74 14.04 o 9 2 7 4017.29 3994.86 88.16 o 10 2 7 51.57 31.55 16.42 o 11 2 7 1305.52 1440.93 49.12 o 12 2 7 8.07 -2.39 19.17 o 1 3 7 1403.76 1473.98 45.89 o 2 3 7 1161.43 1274.05 38.30 o 3 3 7 468.51 497.36 22.27 o 4 3 7 2853.51 2478.41 60.46 o 5 3 7 264.35 214.99 19.37 o 6 3 7 2413.74 2144.65 55.32 o 7 3 7 790.81 723.07 31.92 o 8 3 7 230.86 206.01 20.64 o 9 3 7 587.14 506.17 28.75 o 10 3 7 183.75 185.99 21.64 o 11 3 7 315.77 313.78 32.52 o 1 4 7 28.62 60.52 17.88 o 2 4 7 1098.81 1018.62 42.58 o 3 4 7 17.68 59.39 17.57 o 4 4 7 3600.49 3208.08 76.08 o 5 4 7 9.66 5.94 14.52 o 6 4 7 1637.50 1584.96 56.98 o 7 4 7 132.25 124.84 19.49 o 8 4 7 156.35 142.77 20.50 o 1 5 7 1200.85 1156.74 58.70 o 2 5 7 237.25 247.45 26.00 o 3 5 7 433.05 423.75 31.45 o 0 0 8 4368.84 4013.64 132.88 o 2 0 8 1917.33 1964.41 52.01 o 4 0 8 283.19 283.36 24.46 o 6 0 8 533.77 548.12 32.87 o 8 0 8 1710.42 1769.01 85.44 o 10 0 8 1506.91 1563.89 83.87 o 12 0 8 258.40 314.98 46.05 o 0 1 8 2455.72 2301.49 69.43 o 1 1 8 616.28 910.35 34.93 o 2 1 8 1109.38 1272.92 37.40 o 3 1 8 1228.61 1203.30 36.69 o 4 1 8 274.89 289.66 17.43 o 5 1 8 1270.80 1273.82 45.04 o 6 1 8 393.67 405.57 23.90 o 7 1 8 999.99 1042.74 38.18 o 8 1 8 744.93 714.49 38.27 o 9 1 8 37.17 47.85 20.41 o 10 1 8 872.72 969.66 45.88 o 11 1 8 436.92 532.48 36.81 o 12 1 8 214.65 259.14 30.27 o 0 2 8 265.59 289.24 30.85 o 1 2 8 467.56 510.08 24.47 o 2 2 8 16.51 41.73 13.01 o 3 2 8 1442.78 1279.84 39.02 o 4 2 8 29.24 1.37 14.51 o 5 2 8 1820.22 1689.11 47.11 o 6 2 8 5.58 0.60 13.31 o 7 2 8 740.90 780.08 37.89 o 8 2 8 106.95 96.88 20.71 o 9 2 8 0.65 -8.15 20.73 o 10 2 8 2.10 -28.52 19.01 o 11 2 8 557.54 710.91 71.46 o 0 3 8 807.58 829.59 52.59 o 1 3 8 99.79 162.47 17.60 o 2 3 8 813.33 812.36 32.12 o 3 3 8 418.47 449.84 28.72 o 4 3 8 22.90 12.91 14.40 o 5 3 8 1058.40 915.04 35.93 o 6 3 8 275.18 250.26 22.04 o 7 3 8 186.58 175.58 21.08 o 8 3 8 942.06 848.69 36.66 o 9 3 8 33.89 25.45 17.35 o 0 4 8 655.09 756.38 54.77 o 1 4 8 28.05 98.01 19.43 o 2 4 8 1029.33 972.44 54.06 o 3 4 8 120.77 111.53 21.31 o 4 4 8 74.64 81.18 20.48 o 5 4 8 122.51 63.49 18.05 o 6 4 8 329.54 334.53 25.82 o 2 0 9 1226.46 1184.71 61.78 o 4 0 9 4459.25 4260.64 117.96 o 6 0 9 3551.61 3491.94 128.33 o 8 0 9 351.11 368.05 44.65 o 10 0 9 275.48 321.80 45.54 o 1 1 9 1640.00 1750.36 41.93 o 2 1 9 1029.58 1267.06 40.45 o 3 1 9 581.01 602.51 27.83 o 4 1 9 2049.81 1938.01 50.75 o 5 1 9 55.64 26.93 17.69 o 6 1 9 834.72 872.48 39.90 o 7 1 9 1020.51 1159.27 48.59 o 8 1 9 109.66 130.08 24.50 o 9 1 9 1222.34 1368.37 55.74 o 10 1 9 101.40 89.43 25.43 o 1 2 9 3825.42 3752.65 105.62 o 2 2 9 1.88 295.29 102.97 o 3 2 9 419.75 472.75 25.42 o 4 2 9 52.72 38.63 18.24 o 5 2 9 166.68 157.53 22.44 o 6 2 9 15.61 23.60 18.51 o 7 2 9 1314.33 1284.10 69.07 o 8 2 9 36.22 28.04 24.26 o 9 2 9 1629.66 1825.95 97.43 o 1 3 9 735.23 798.47 33.51 o 2 3 9 651.62 741.82 39.06 o 3 3 9 205.41 190.78 23.36 o 4 3 9 1401.07 1380.60 52.22 o 5 3 9 22.49 21.68 18.85 o 6 3 9 655.64 648.14 38.01 o 7 3 9 322.99 310.72 29.54 o 1 4 9 55.49 66.71 20.38 o 2 4 9 609.38 597.03 35.47 o 0 0 10 1020.20 1056.96 86.16 o 2 0 10 1436.60 1318.24 68.90 o 4 0 10 127.66 94.41 29.45 o 6 0 10 483.03 449.78 45.55 o 8 0 10 1224.74 1378.55 85.35 o 0 1 10 966.70 943.29 58.92 o 1 1 10 119.04 228.08 18.72 o 2 1 10 550.86 626.46 29.71 o 3 1 10 603.32 695.07 31.61 o 4 1 10 51.95 63.22 19.56 o 5 1 10 912.24 885.90 41.84 o 6 1 10 275.48 292.53 27.91 o 7 1 10 302.74 345.38 36.92 o 8 1 10 473.22 436.71 41.21 o 0 2 10 10.45 24.20 19.65 o 1 2 10 340.19 395.54 22.91 o 2 2 10 36.38 67.57 17.22 o 3 2 10 1479.77 1413.27 57.10 o 4 2 10 14.37 23.80 18.79 o 5 2 10 1151.26 1123.69 76.02 o 6 2 10 26.04 23.41 20.53 o 7 2 10 370.33 382.54 32.51 o 0 3 10 833.06 919.97 47.68 o 1 3 10 89.81 141.49 19.36 o 2 3 10 546.92 646.75 36.53 o 3 3 10 277.10 315.87 28.66 o 2 0 11 421.93 389.22 43.41 o 4 0 11 1247.75 1250.01 72.03 o 1 1 11 816.23 798.32 39.88 o 2 1 11 188.59 324.33 44.12 o 3 1 11 183.81 236.08 26.33 o 4 1 11 706.32 750.12 57.86 o 5 1 11 34.33 20.41 21.12 o 1 2 11 1017.14 1132.69 38.13 o 2 2 11 17.92 81.01 18.98 o