#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:51:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181303 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/81/2238198.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238198_Fobs loop_ _publ_author_name 'Tigyer, Benjamin R.' 'Zeller, Matthias' 'Zaleski, Curtis M.' _publ_section_title ; \m~3~-Acetato-\m~2~-acetato-(dimethylformamide)pentakis(\m-N,2-dioxidobenzene-1-carboximidato)pentakis(1-methyl-1H-imidazole)pentamanganese(III)manganese(II)--diethyl ether--dimethylformamide--methanol--water (1/1/1/1/0.49) ; _journal_coeditor_code JJ2164 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m393 _journal_page_last m394 _journal_volume 69 _journal_year 2013 _cell_angle_alpha 102.166 _cell_angle_beta 96.726 _cell_angle_gamma 107.496 _cell_length_a 12.4181 _cell_length_b 17.0108 _cell_length_c 20.6627 _exptl_crystal_F_000 1920.50 _reflns_d_resolution_high 0.8000 _cod_data_source_file jj2164Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 12mz401_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 356.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 79973.78 85764.23 8522.94 o 2 0 0 0.75 12.44 9.74 o 3 0 0 548.14 488.53 28.15 o 4 0 0 2047.26 2398.68 146.43 o 5 0 0 8794.65 9226.74 498.04 o 6 0 0 12161.05 12135.23 594.63 o 7 0 0 10752.12 10594.25 787.89 o 8 0 0 5236.58 7989.65 1479.23 o 8 0 0 5236.58 4647.90 652.55 o 9 0 0 77.13 92.22 43.84 o 10 0 0 2536.75 2571.84 183.75 o 11 0 0 335.53 374.81 82.79 o 12 0 0 690.39 633.78 96.79 o 13 0 0 797.60 725.03 109.28 o 14 0 0 1363.89 1448.44 156.37 o -14 1 0 43.27 95.25 106.69 o -13 1 0 183.49 136.32 117.31 o -12 1 0 852.87 749.08 103.50 o -11 1 0 1355.99 1521.93 148.24 o -10 1 0 9345.98 4936.29 879.70 o -9 1 0 9265.30 7726.04 912.81 o -9 1 0 9265.30 11618.22 1675.89 o -8 1 0 34.73 -0.21 37.64 o -7 1 0 76.61 77.05 99.69 o -6 1 0 822.47 976.65 63.08 o -5 1 0 5764.91 6021.48 316.69 o -4 1 0 5543.34 5284.76 252.14 o -3 1 0 5334.27 5045.45 255.42 o -2 1 0 1886.41 1391.79 72.47 o -1 1 0 2540.99 2550.73 156.99 o 0 1 0 246.76 293.08 31.19 o 1 1 0 13439.86 13628.01 1355.37 o 2 1 0 14162.76 12227.42 614.04 o 3 1 0 10.56 53.05 14.61 o 4 1 0 1821.34 1286.50 608.83 o 5 1 0 3651.84 3234.48 181.12 o 6 1 0 3019.92 3124.96 294.82 o 7 1 0 10.69 80.19 42.63 o 8 1 0 4933.84 4741.28 273.04 o 9 1 0 424.05 433.36 46.26 o 10 1 0 497.68 496.83 59.48 o 11 1 0 979.93 989.06 114.38 o 12 1 0 70.53 12.30 75.23 o 13 1 0 223.76 202.90 89.58 o 14 1 0 116.50 136.37 95.76 o -14 2 0 1039.42 901.44 404.31 o -13 2 0 385.06 167.81 194.29 o -12 2 0 226.74 260.96 120.56 o -11 2 0 630.92 1103.87 305.99 o -10 2 0 1257.42 1219.59 108.48 o -9 2 0 497.13 690.02 101.50 o -8 2 0 4774.16 5167.36 463.66 o -7 2 0 1408.41 1462.69 317.24 o -6 2 0 1279.29 1352.47 202.69 o -5 2 0 1202.41 1116.64 73.15 o -4 2 0 3552.57 3259.12 157.64 o -3 2 0 1770.07 1984.04 95.41 o -2 2 0 6276.50 6738.55 353.22 o -1 2 0 2767.22 3093.35 347.00 o 0 2 0 24368.99 23693.00 1958.32 o 1 2 0 31903.60 29818.19 5027.59 o 2 2 0 513.59 393.95 26.53 o 3 2 0 1109.23 1089.58 57.34 o 4 2 0 6443.23 4010.49 604.60 o 5 2 0 328.35 361.49 40.52 o 6 2 0 4940.44 4230.06 283.90 o 7 2 0 3589.86 3285.44 167.90 o 8 2 0 1356.45 1229.75 67.17 o 9 2 0 659.98 692.70 51.16 o 10 2 0 0.09 19.11 57.09 o 11 2 0 1755.86 1295.06 123.92 o 12 2 0 1737.44 1654.12 158.78 o 13 2 0 119.34 130.83 86.66 o -15 3 0 1908.94 2016.30 383.44 o -14 3 0 1705.21 1777.11 226.76 o -13 3 0 2994.24 2684.66 302.54 o -12 3 0 1728.39 1759.31 217.58 o -11 3 0 2.57 9.50 148.41 o -10 3 0 124.47 290.67 60.53 o -9 3 0 1693.43 1968.29 160.04 o -8 3 0 6108.38 7171.57 341.11 o -7 3 0 2866.23 2777.67 187.56 o -6 3 0 3812.14 4725.51 226.03 o -5 3 0 337.66 365.44 128.37 o -4 3 0 347.92 277.40 22.09 o -3 3 0 5765.54 6043.39 402.18 o -2 3 0 25075.80 26637.27 2972.02 o -1 3 0 7397.11 7669.37 857.56 o 0 3 0 1652.99 1190.89 207.63 o 0 3 0 1652.99 1530.42 235.33 o 1 3 0 17879.59 15501.35 721.43 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366.26 74.87 o 10 5 0 51.87 83.91 70.21 o 11 5 0 19.97 32.71 389.93 o 12 5 0 679.17 543.96 99.76 o -15 6 0 39.82 80.16 127.07 o -14 6 0 5.70 15.13 82.78 o -13 6 0 528.60 657.07 136.04 o -12 6 0 599.31 778.14 228.72 o -11 6 0 547.39 454.64 511.98 o -11 6 0 547.39 523.49 811.99 o -10 6 0 4358.63 3670.96 311.71 o -9 6 0 214.31 156.25 49.28 o -9 6 0 214.31 116.74 169.68 o -8 6 0 52.82 39.87 46.56 o -7 6 0 1637.47 1752.57 167.79 o -6 6 0 1958.37 2688.49 286.19 o -5 6 0 46.07 21.32 19.48 o -4 6 0 80.87 94.65 15.58 o -3 6 0 1583.90 1771.91 99.10 o -2 6 0 1471.39 1552.14 104.03 o -1 6 0 38053.64 36781.75 2177.08 o 0 6 0 1037.48 712.86 48.71 o 1 6 0 693.01 791.91 42.33 o 2 6 0 139.15 37.93 16.91 o 3 6 0 2401.52 2344.80 128.09 o 4 6 0 453.99 437.08 40.43 o 5 6 0 204.10 119.31 28.33 o 6 6 0 3693.60 3521.69 175.73 o 7 6 0 120.02 121.26 42.00 o 8 6 0 216.69 183.37 69.78 o 9 6 0 87.34 55.28 65.42 o 10 6 0 166.37 116.99 79.34 o 11 6 0 3.74 2.87 374.29 o 12 6 0 511.97 328.04 675.65 o -15 7 0 10.09 16.86 220.38 o -14 7 0 17.34 -92.91 165.96 o -13 7 0 26.91 346.88 275.23 o -12 7 0 2.37 3.21 200.68 o -11 7 0 361.81 389.38 861.86 o -10 7 0 2223.64 2514.26 292.00 o -9 7 0 523.15 522.19 192.81 o -8 7 0 2798.18 2890.47 259.09 o -7 7 0 2648.06 2682.60 403.87 o -6 7 0 15.79 -25.69 25.69 o -5 7 0 224.85 307.09 25.63 o -4 7 0 20534.60 23639.18 1203.10 o -3 7 0 192.51 210.34 30.45 o -2 7 0 38987.74 43526.50 2841.55 o -1 7 0 7056.28 7587.43 453.40 o 0 7 0 21.61 37.88 18.25 o 1 7 0 420.54 506.04 33.24 o 2 7 0 1473.26 1427.53 77.22 o 3 7 0 199.66 248.96 28.04 o 4 7 0 623.68 593.89 63.97 o 5 7 0 343.56 432.55 186.19 o 6 7 0 6016.01 6241.49 903.13 o 7 7 0 1814.17 1701.07 143.25 o 8 7 0 801.65 792.96 93.66 o 9 7 0 877.12 763.95 178.80 o 10 7 0 175.89 12.45 173.48 o 11 7 0 7.13 -36.05 176.16 o -15 8 0 165.67 111.88 125.65 o -14 8 0 146.95 120.58 122.03 o -13 8 0 552.55 754.35 224.70 o -13 8 0 552.55 264.69 209.78 o -12 8 0 9379.92 7914.15 2193.66 o -11 8 0 7016.75 5969.88 407.69 o -10 8 0 217.27 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