#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:52:03 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181304 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/82/2238232.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238232_Fobs loop_ _publ_author_name 'Meng, Fan-Kun' 'Zhang, Xin' 'Yi, Hua' 'Zhang, De-Hui' 'Jia, Jun-Ying' _publ_section_title ; Bis(\m-6-methoxy-2-{[(3-oxidopropyl)imino]methyl}phenolato)nickel(II) methanol monosolvate ; _journal_coeditor_code QM2096 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m425 _journal_volume 69 _journal_year 2013 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.252 _cell_angle_gamma 90.000 _cell_length_a 23.6725 _cell_length_b 8.3124 _cell_length_c 25.5465 _exptl_crystal_F_000 2352.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file qm2096Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 565.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 52694.76 55668.34 1591.68 o 6 0 0 9812.86 10836.24 308.62 o 8 0 0 41836.16 43218.90 1325.07 o 10 0 0 34445.34 33897.23 996.09 o 12 0 0 10735.19 10375.13 520.57 o 14 0 0 3667.58 3520.36 201.49 o 16 0 0 949.30 978.46 183.17 o 18 0 0 1733.73 1569.32 222.38 o 20 0 0 6472.59 5876.30 309.90 o 22 0 0 731.67 814.30 309.57 o 24 0 0 68.11 68.14 107.61 o 26 0 0 102.79 121.32 237.62 o 28 0 0 345.65 756.21 257.23 o 3 1 0 939.66 1843.82 141.30 o 5 1 0 3605.83 3573.79 93.89 o 7 1 0 9888.01 9951.60 192.05 o 9 1 0 16219.40 15891.06 452.13 o 11 1 0 8350.48 8142.06 249.18 o 13 1 0 51.47 156.26 85.67 o 15 1 0 215.31 212.41 83.90 o 17 1 0 115.84 138.15 80.93 o 19 1 0 692.92 577.00 66.24 o 21 1 0 1276.24 1350.43 105.15 o 23 1 0 1025.70 1080.09 106.07 o 25 1 0 2182.89 2123.79 126.94 o 27 1 0 4063.78 4370.28 473.79 o 0 2 0 123887.02 123260.04 4070.83 o 2 2 0 93661.23 94842.52 1848.12 o 4 2 0 132492.34 127052.88 2675.60 o 6 2 0 9801.72 9962.92 202.75 o 8 2 0 4603.15 4868.72 168.15 o 10 2 0 10526.16 10398.42 270.92 o 12 2 0 11937.40 11723.33 302.25 o 14 2 0 1283.62 1216.46 106.20 o 16 2 0 2014.83 1943.05 125.06 o 18 2 0 6542.43 6218.92 231.29 o 20 2 0 10.25 8.40 49.48 o 22 2 0 197.49 256.38 68.39 o 24 2 0 809.05 803.25 88.95 o 26 2 0 42.70 13.98 148.08 o 1 3 0 19339.42 19750.27 397.61 o 3 3 0 8847.61 8822.65 237.83 o 5 3 0 533.09 494.45 59.61 o 7 3 0 1201.68 1068.15 88.23 o 9 3 0 2330.50 2102.59 75.52 o 11 3 0 902.59 1605.27 233.08 o 13 3 0 454.12 482.71 78.35 o 15 3 0 330.58 398.61 81.14 o 17 3 0 126.57 108.20 62.72 o 19 3 0 1022.59 1044.47 98.28 o 21 3 0 350.92 396.98 80.08 o 23 3 0 316.90 378.43 78.69 o 25 3 0 665.69 660.27 151.86 o 27 3 0 1300.74 1397.29 215.21 o 0 4 0 668.41 1810.34 548.28 o 2 4 0 5415.73 5297.95 232.57 o 4 4 0 10312.53 9903.91 259.70 o 6 4 0 2488.24 2487.62 103.51 o 8 4 0 155.83 971.83 435.73 o 10 4 0 12062.04 11503.93 412.98 o 12 4 0 8372.70 8332.43 300.90 o 14 4 0 3729.83 3880.84 156.91 o 16 4 0 555.31 557.09 92.56 o 18 4 0 17034.87 16898.27 385.42 o 20 4 0 7818.17 8017.58 242.09 o 22 4 0 3744.84 3904.34 150.84 o 24 4 0 103.50 90.03 100.50 o 26 4 0 147.39 185.45 134.19 o 1 5 0 4157.70 3977.79 305.23 o 3 5 0 6726.66 6771.65 275.83 o 5 5 0 4937.18 4687.81 197.38 o 7 5 0 2411.68 3123.34 368.30 o 9 5 0 23.83 48.55 71.98 o 11 5 0 651.66 592.59 77.63 o 13 5 0 31.66 -5.10 61.41 o 15 5 0 1295.47 906.61 129.46 o 17 5 0 0.59 -1.25 34.26 o 19 5 0 400.73 299.94 97.86 o 21 5 0 1414.52 1231.30 327.34 o 23 5 0 172.19 179.17 114.92 o 25 5 0 990.19 1271.54 451.26 o 0 6 0 16860.75 17392.33 647.96 o 2 6 0 22149.50 23227.25 499.10 o 4 6 0 7587.07 7466.26 269.99 o 6 6 0 6027.61 6125.84 201.69 o 8 6 0 15181.72 14752.71 389.04 o 10 6 0 18677.86 17926.83 457.00 o 12 6 0 7468.13 7997.42 589.98 o 14 6 0 10919.10 10535.93 374.92 o 16 6 0 2489.46 2413.63 180.04 o 18 6 0 307.90 284.96 170.20 o 20 6 0 617.85 696.97 170.57 o 22 6 0 1132.60 1254.79 177.08 o 1 7 0 568.31 803.29 112.40 o 3 7 0 348.47 654.46 283.39 o 5 7 0 8010.13 7717.63 348.76 o 7 7 0 9135.25 8767.27 247.42 o 9 7 0 1645.94 1546.51 162.06 o 11 7 0 13827.52 18606.85 2433.66 o 13 7 0 4433.62 5400.11 659.47 o 15 7 0 366.68 511.59 103.32 o 17 7 0 1089.96 1027.17 197.29 o 19 7 0 6.60 26.82 128.17 o 21 7 0 5.45 -0.44 88.53 o 0 8 0 6939.94 6976.04 343.35 o 2 8 0 11780.16 11974.00 393.92 o 4 8 0 6878.16 6726.34 239.17 o 6 8 0 7929.39 8025.79 271.01 o 8 8 0 1060.92 1313.44 125.98 o 10 8 0 1985.61 2775.50 370.79 o 12 8 0 311.15 711.99 167.48 o 14 8 0 2.14 1357.89 607.89 o 16 8 0 241.92 125.75 95.53 o 18 8 0 97.72 116.75 153.17 o 1 9 0 434.33 385.02 136.70 o 3 9 0 1694.95 1640.38 157.14 o 5 9 0 2310.14 2703.56 364.51 o 7 9 0 7235.48 7503.89 371.87 o 9 9 0 10914.33 11573.22 543.85 o 11 9 0 2744.99 2453.71 275.91 o 13 9 0 610.93 251.85 147.44 o 15 9 0 1686.14 1375.83 240.72 o 4 10 0 0.64 4468.98 1959.29 o 6 10 0 1.33 826.10 653.10 o 8 10 0 1415.18 1777.76 313.64 o 10 10 0 4724.78 5536.86 1150.47 o -27 1 1 395.61 418.65 170.14 o -25 1 1 114.98 147.33 59.88 o -23 1 1 1138.29 1206.81 103.46 o -21 1 1 698.07 801.47 88.45 o -19 1 1 1045.88 1009.05 95.93 o -17 1 1 209.61 186.59 115.66 o -15 1 1 8.96 10.42 66.31 o -13 1 1 102.41 114.72 61.34 o -11 1 1 18824.78 19589.89 440.15 o -9 1 1 8404.14 8508.14 250.64 o -7 1 1 1652.32 1609.20 69.30 o -5 1 1 23775.67 23358.54 399.65 o -3 1 1 3743.26 4161.83 79.93 o 3 1 1 99.78 284.22 75.25 o 5 1 1 4289.53 4144.76 91.60 o 7 1 1 21327.79 21477.33 428.79 o 9 1 1 3263.48 3697.96 176.52 o 11 1 1 2913.52 3453.41 159.76 o 13 1 1 17.77 82.45 56.72 o 15 1 1 2822.53 3299.84 165.29 o 17 1 1 1.41 41.17 74.31 o 19 1 1 1045.94 1002.41 81.30 o 21 1 1 123.37 114.60 63.12 o 23 1 1 9.06 21.66 48.29 o 25 1 1 453.56 657.95 195.10 o 27 1 1 73.85 86.04 111.07 o -28 2 1 8839.86 8943.96 546.78 o -26 2 1 3248.15 3018.74 274.37 o -24 2 1 1975.97 1936.07 115.52 o -22 2 1 1010.33 948.98 90.88 o -20 2 1 1329.27 1220.36 104.33 o -18 2 1 11966.72 11390.75 308.88 o -16 2 1 3961.91 3765.27 169.49 o -14 2 1 312.64 375.04 75.72 o -12 2 1 223.64 263.37 60.03 o -10 2 1 75.12 40.74 41.77 o -8 2 1 6641.23 6100.67 206.14 o -6 2 1 10285.08 10257.69 177.66 o -4 2 1 2579.56 2441.07 77.80 o -2 2 1 1260.33 879.30 136.81 o 0 2 1 150408.02 145982.00 3145.07 o 2 2 1 320079.72 299036.66 6978.56 o 4 2 1 118951.14 115079.61 2357.59 o 6 2 1 19309.52 20265.63 364.39 o 8 2 1 14804.31 14283.98 288.48 o 10 2 1 16566.81 15862.68 349.17 o 12 2 1 34907.52 34322.95 707.99 o 14 2 1 21284.89 21546.01 497.89 o 16 2 1 1594.14 1561.12 129.06 o 18 2 1 111.86 80.06 58.70 o 20 2 1 2844.14 2711.53 112.77 o 22 2 1 2708.90 2584.66 148.78 o 24 2 1 599.21 707.05 92.80 o 26 2 1 20.02 34.69 113.75 o -27 3 1 4274.16 5075.65 370.88 o -25 3 1 3513.92 3647.43 255.75 o -23 3 1 3028.32 2996.71 130.95 o -21 3 1 4311.64 4301.68 177.73 o -19 3 1 181.70 292.75 76.60 o -17 3 1 4.39 31.10 55.97 o -15 3 1 449.59 414.51 82.25 o -13 3 1 2963.39 2881.35 131.00 o -11 3 1 345.61 275.69 51.73 o -9 3 1 14737.25 13778.57 270.25 o -7 3 1 26461.05 26329.43 564.01 o -5 3 1 24429.61 24605.26 502.37 o -3 3 1 68949.92 68339.16 2737.45 o -1 3 1 77510.14 78887.02 1781.55 o 1 3 1 222104.94 223357.20 5449.63 o 3 3 1 75029.83 75900.00 1578.22 o 5 3 1 3756.97 4014.45 141.21 o 7 3 1 14344.71 13154.75 268.77 o 9 3 1 1319.16 1160.65 83.67 o 11 3 1 3003.08 2890.73 131.58 o 13 3 1 6113.54 6216.52 254.90 o 15 3 1 587.25 552.18 115.14 o 17 3 1 773.80 889.44 108.29 o 19 3 1 16.85 23.68 53.46 o 21 3 1 255.81 263.84 71.15 o 23 3 1 69.02 78.59 61.63 o 25 3 1 2.51 -40.97 127.47 o -26 4 1 6096.68 6298.67 414.13 o -24 4 1 358.59 356.28 167.77 o -22 4 1 1469.29 1317.63 111.06 o -20 4 1 601.27 503.68 71.83 o -18 4 1 622.43 550.89 77.40 o -16 4 1 161.08 127.10 59.76 o -14 4 1 26.15 0.56 42.93 o -12 4 1 2293.09 2097.20 95.72 o -10 4 1 549.08 467.74 104.68 o -8 4 1 895.66 779.57 79.65 o -6 4 1 1914.13 2173.60 113.64 o -4 4 1 7846.16 7990.88 194.90 o -2 4 1 5186.45 5341.66 163.13 o 0 4 1 2145.35 1987.68 122.94 o 2 4 1 9155.03 9631.03 274.80 o 4 4 1 79300.68 80315.84 1632.12 o 6 4 1 29987.90 30758.49 676.65 o 8 4 1 43926.01 42984.55 893.62 o 10 4 1 39337.62 40808.18 724.54 o 12 4 1 49349.50 50111.84 1009.60 o 14 4 1 35446.24 34224.27 711.64 o 16 4 1 1233.90 1071.08 105.59 o 18 4 1 118.45 119.52 59.85 o 20 4 1 5.11 -2.35 41.09 o 22 4 1 1.63 277.72 136.53 o 24 4 1 643.71 720.89 214.68 o -25 5 1 1884.54 2101.23 283.69 o -23 5 1 1648.62 1709.35 250.33 o -21 5 1 3516.39 3667.62 304.62 o -19 5 1 2047.56 2009.34 174.82 o -17 5 1 1811.15 1793.04 161.28 o -15 5 1 611.55 542.70 148.74 o -13 5 1 606.34 685.49 91.62 o -11 5 1 3453.62 3621.68 176.86 o -9 5 1 13361.03 13153.06 320.45 o -7 5 1 9088.48 9345.86 332.18 o -5 5 1 7399.89 6913.64 232.08 o -3 5 1 15909.90 16476.09 381.04 o -1 5 1 12558.19 12248.28 325.71 o 1 5 1 27449.77 27697.43 573.19 o 3 5 1 60395.36 69964.72 7232.09 o 5 5 1 25751.56 26340.03 588.89 o 7 5 1 2144.85 1788.50 239.95 o 9 5 1 15.82 15.29 74.04 o 11 5 1 169.36 208.99 74.60 o 13 5 1 7928.27 7336.91 216.10 o 15 5 1 1070.93 1090.11 130.99 o 17 5 1 455.37 547.98 99.20 o 19 5 1 2507.71 2414.99 151.63 o 21 5 1 747.91 677.81 113.66 o 23 5 1 408.96 423.19 199.61 o -22 6 1 509.65 550.55 230.76 o -20 6 1 416.93 461.47 206.87 o -18 6 1 2092.51 2172.94 242.19 o -16 6 1 2897.39 2955.98 180.59 o -14 6 1 1893.84 1746.37 163.02 o -12 6 1 3665.27 6735.55 1618.82 o -10 6 1 2902.50 2574.02 215.47 o -8 6 1 4178.15 4140.14 175.11 o -6 6 1 6191.69 5909.00 221.97 o -4 6 1 209.72 334.30 86.31 o -2 6 1 306.04 332.93 97.63 o 0 6 1 1974.24 1950.34 132.45 o 2 6 1 81.36 139.65 65.31 o 4 6 1 1242.16 1185.65 133.83 o 6 6 1 8918.54 8703.37 273.57 o 8 6 1 7370.94 8333.91 671.72 o 10 6 1 10979.35 10654.30 387.46 o 12 6 1 3446.12 3269.95 250.99 o 14 6 1 42.49 19.23 90.14 o 16 6 1 1083.31 1152.93 118.92 o 18 6 1 40.78 330.74 235.06 o 20 6 1 569.04 478.12 149.73 o 22 6 1 1333.62 1518.77 193.35 o -21 7 1 1257.70 1557.83 296.57 o -19 7 1 1306.86 1841.78 276.36 o -17 7 1 162.14 654.08 353.71 o -15 7 1 748.13 693.88 86.31 o -13 7 1 6.48 35.88 143.56 o -11 7 1 138.46 142.57 136.28 o -9 7 1 3.40 713.95 304.78 o -7 7 1 25.56 17.24 83.15 o -5 7 1 3200.50 3297.01 207.87 o -3 7 1 2040.92 2364.58 176.55 o -1 7 1 636.56 686.64 108.24 o 1 7 1 1.29 24.46 58.39 o 3 7 1 447.51 546.21 126.71 o 5 7 1 4288.94 4654.86 323.98 o 7 7 1 5.22 -23.50 65.02 o 9 7 1 7699.80 7555.94 374.40 o 11 7 1 12971.41 12721.14 513.91 o 13 7 1 3671.08 5329.76 773.16 o 15 7 1 1013.74 1173.01 92.36 o 17 7 1 1760.79 1852.59 176.92 o 19 7 1 5209.37 5308.46 333.66 o 21 7 1 4860.46 4941.44 327.05 o -18 8 1 1080.56 1082.04 255.01 o -16 8 1 258.85 246.12 95.48 o -14 8 1 6616.70 5248.69 824.12 o -12 8 1 4080.51 3682.50 201.67 o -10 8 1 4035.26 4118.22 230.84 o -8 8 1 13658.82 13240.33 376.59 o -6 8 1 5645.09 5493.37 221.12 o -4 8 1 2118.75 2258.28 187.81 o -2 8 1 4244.95 4303.67 233.48 o 0 8 1 877.83 1012.82 137.07 o 2 8 1 2368.27 2211.00 165.49 o 4 8 1 3673.22 3538.21 176.87 o 6 8 1 3227.59 3197.82 195.93 o 8 8 1 736.58 1308.44 270.21 o 10 8 1 1127.44 1829.75 236.21 o 12 8 1 5126.54 7353.73 1057.85 o 14 8 1 1744.74 1717.91 258.12 o 16 8 1 177.97 187.40 103.70 o 18 8 1 1255.73 1322.01 171.10 o -15 9 1 58.86 870.12 385.08 o -13 9 1 289.57 249.82 140.14 o -11 9 1 588.44 2050.10 870.70 o -9 9 1 1709.95 5168.59 1223.53 o -7 9 1 49.29 1037.46 532.15 o -5 9 1 138.27 728.10 443.18 o -3 9 1 2173.45 2105.51 218.41 o -1 9 1 2589.52 2448.34 189.91 o 1 9 1 865.77 809.10 134.89 o 3 9 1 1124.06 1145.06 167.92 o 5 9 1 904.25 949.12 169.65 o 7 9 1 2252.47 4030.76 602.73 o 9 9 1 3950.49 9198.34 3141.67 o 11 9 1 474.46 386.49 163.11 o 13 9 1 123.76 656.63 320.40 o 15 9 1 210.87 171.17 115.99 o -10 10 1 2.92 142.72 419.31 o -8 10 1 501.35 455.33 258.25 o -6 10 1 1013.03 2116.25 1021.10 o 2 10 1 3467.85 4672.94 403.00 o 4 10 1 3237.11 2924.33 581.06 o 6 10 1 5436.16 5066.34 384.62 o 8 10 1 6195.16 6537.05 448.83 o 10 10 1 2357.47 2935.29 403.46 o -28 0 2 20076.41 21772.20 876.46 o -26 0 2 15886.98 17340.13 1050.88 o -24 0 2 19407.26 19944.04 749.89 o -22 0 2 14036.93 13612.01 542.00 o -20 0 2 2536.21 2747.79 291.83 o -18 0 2 14361.49 14327.51 525.51 o -16 0 2 36226.76 37966.03 1161.71 o -14 0 2 25897.63 25243.44 841.88 o -12 0 2 422.27 457.76 106.90 o -10 0 2 44636.96 49137.73 1614.87 o -8 0 2 248.28 239.04 76.87 o -6 0 2 41.31 164.12 46.13 o -4 0 2 15306.71 16062.39 439.77 o 2 0 2 3910.54 3828.51 97.73 o 4 0 2 9377.80 8689.57 234.38 o 6 0 2 6427.97 6591.75 190.75 o 8 0 2 2135.38 2265.81 161.39 o 10 0 2 3789.38 3697.96 226.99 o 12 0 2 5470.33 5443.44 269.54 o 14 0 2 15284.46 15212.61 560.56 o 16 0 2 53992.63 54141.25 1715.68 o 18 0 2 27663.17 28442.55 1208.74 o 20 0 2 538.06 462.39 133.34 o 22 0 2 4032.75 4197.77 333.95 o 24 0 2 4045.88 4239.54 347.94 o 26 0 2 2158.70 2314.49 299.55 o -27 1 2 1767.11 1983.19 217.26 o -25 1 2 1472.18 1446.48 116.72 o -23 1 2 6.13 6.55 33.04 o -21 1 2 61.48 30.64 47.09 o -19 1 2 2277.69 2252.53 126.77 o -17 1 2 5564.05 5429.13 209.40 o -15 1 2 6.82 5.66 45.34 o -13 1 2 1097.05 990.08 133.87 o -11 1 2 24723.62 26112.35 602.27 o -9 1 2 7181.84 7358.38 205.13 o -7 1 2 2510.50 2256.74 76.99 o -5 1 2 67108.16 64691.67 1245.87 o -3 1 2 13974.19 14952.08 294.50 o 1 1 2 211943.50 199084.44 4141.87 o 3 1 2 45135.36 47072.48 813.32 o 5 1 2 67627.61 68826.55 1248.82 o 7 1 2 46259.26 48714.06 1010.52 o 9 1 2 11407.56 10855.17 293.96 o 11 1 2 36116.16 36843.06 839.37 o 13 1 2 13298.56 12495.61 368.69 o 15 1 2 27315.56 28087.06 645.57 o 17 1 2 1264.94 1324.90 148.25 o 19 1 2 195.71 170.02 57.49 o 21 1 2 2493.97 2572.83 129.53 o 23 1 2 57.57 105.08 73.94 o 25 1 2 182.57 236.90 111.13 o 27 1 2 647.37 648.64 207.17 o -28 2 2 6388.37 6902.00 425.17 o -26 2 2 6022.98 6028.91 443.63 o -24 2 2 3469.09 3969.39 149.76 o -22 2 2 683.77 843.40 86.29 o -20 2 2 10063.62 10295.14 281.50 o -18 2 2 1879.93 1771.68 105.52 o -16 2 2 7326.18 7087.28 220.82 o -14 2 2 291.69 377.27 60.10 o -12 2 2 3776.23 4065.14 124.19 o -10 2 2 3728.59 3633.67 125.52 o -8 2 2 9059.20 9101.45 193.19 o -6 2 2 8364.77 7922.45 218.01 o -4 2 2 3384.70 2789.30 80.31 o -2 2 2 50312.96 48448.28 831.43 o 0 2 2 80403.09 78241.04 1332.09 o 2 2 2 237534.97 225487.81 4950.26 o 4 2 2 3161.09 3020.84 91.89 o 6 2 2 2130.31 2418.39 126.43 o 8 2 2 84.00 89.67 49.76 o 10 2 2 9220.88 8864.24 191.32 o 12 2 2 27428.82 27754.13 608.90 o 14 2 2 41668.47 43175.98 941.50 o 16 2 2 9654.60 9436.78 270.22 o 18 2 2 2294.66 2242.08 165.72 o 20 2 2 9295.66 9091.05 310.28 o 22 2 2 1182.52 1430.02 122.08 o 24 2 2 896.83 1226.06 295.89 o 26 2 2 1011.58 1202.68 193.38 o -27 3 2 1293.33 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421.42 285.43 146.11 o -21 1 30 467.18 397.59 88.36 o -19 1 30 143.00 128.07 41.75 o -17 1 30 129.72 85.77 41.15 o -15 1 30 94.59 110.56 32.19 o -13 1 30 210.72 154.10 87.25 o -11 1 30 133.77 156.97 67.08 o -9 1 30 136.69 150.59 54.19 o -7 1 30 1204.19 1573.88 170.10 o -5 1 30 528.72 364.95 390.09 o -20 2 30 1442.12 1444.70 96.57 o -18 2 30 1574.54 1553.73 85.71 o -16 2 30 27.83 72.31 58.85 o -14 2 30 1708.87 1876.28 133.96 o -12 2 30 385.82 356.27 133.85 o -10 2 30 769.82 881.35 113.04 o -8 2 30 963.67 1233.80 183.06 o -6 2 30 1661.90 1799.79 152.05 o -4 2 30 5139.38 5304.05 309.04 o -2 2 30 1202.63 598.05 505.62 o -19 3 30 1330.69 3113.81 946.98 o -17 3 30 3230.51 3775.38 381.83 o -15 3 30 1585.95 1531.14 176.53 o -13 3 30 7.42 57.31 68.54 o -11 3 30 71.79 17.50 113.98 o -9 3 30 726.59 795.77 237.03 o -7 3 30 686.78 801.91 130.96 o -5 3 30 510.92 2515.36 1342.21 o -3 3 30 237.85 230.98 90.52 o -16 4 30 75.67 98.54 77.13 o -14 4 30 151.81 510.47 326.55 o -12 4 30 2.39 787.39 640.86 o -10 4 30 141.31 113.56 115.67 o -8 4 30 0.05 21.78 144.32 o -6 4 30 156.12 134.92 150.55 o -21 1 31 1964.89 1919.37 141.24 o -19 1 31 1914.63 1883.07 85.35 o -17 1 31 1771.81 1620.12 94.54 o -15 1 31 2026.60 1892.39 113.91 o -13 1 31 6.30 33.68 46.29 o -11 1 31 238.80 366.50 116.66 o -9 1 31 219.18 140.68 144.76 o -7 1 31 28.01 21.07 226.99 o -5 1 31 150.15 235.14 198.44 o -3 1 31 31.30 79.51 322.81 o -18 2 31 5.05 -13.74 62.20 o -16 2 31 8.90 -25.43 51.37 o -14 2 31 292.91 320.65 134.59 o -12 2 31 29.40 -3.77 53.94 o -10 2 31 226.70 190.46 77.50 o -8 2 31 47.66 18.36 37.93 o -6 2 31 980.52 1165.33 206.01 o -4 2 31 1592.98 1678.62 343.20 o -17 3 31 5779.55 5781.81 235.96 o -15 3 31 629.14 502.35 134.04 o -13 3 31 641.46 650.88 112.48 o -11 3 31 362.46 193.03 108.09 o -9 3 31 11.89 -24.32 78.59 o -7 3 31 27.59 34.32 101.40 o -18 0 32 3832.55 3889.60 224.15 o -16 0 32 3153.35 3023.22 134.81 o -14 0 32 578.60 416.60 137.96 o -12 0 32 509.15 317.37 144.08 o -10 0 32 48.66 64.56 118.93 o -8 0 32 681.65 92.43 269.80 o -17 1 32 9548.87 9091.80 252.56 o -15 1 32 8198.92 8074.64 231.35 o -13 1 32 4888.14 4903.87 167.09 o -11 1 32 2442.35 2338.51 281.36 o -9 1 32 1146.24 1039.11 235.82 o -7 1 32 624.45 138.64 311.94 o -16 2 32 619.75 908.96 247.97 o -14 2 32 63.82 2.94 55.22 o -12 2 32 6.73 -28.20 57.15 o -10 2 32 32.69 25.56 50.70 o -8 2 32 230.80 169.90 180.77 o