#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/84/2238404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238404_Fobs loop_ _publ_author_name 'Anitha, R.' 'Athimoolam, S.' 'Gunasekaran, M.' 'Sridhar, B.' _publ_section_title ; 4-Sulfamoylanilinium perchlorate ; _journal_coeditor_code NG5332 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1236 _journal_volume 69 _journal_year 2013 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.716 _cell_angle_gamma 90.000 _cell_length_a 4.9158 _cell_length_b 10.5137 _cell_length_c 9.8140 _exptl_crystal_F_000 280.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file ng5332Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AS37 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 69.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -13 0 55.31 56.85 1.76 o 2 -13 0 56.04 62.42 2.56 o 0 -12 0 71.93 75.33 2.99 o 1 -12 0 14.24 13.81 0.67 o 2 -12 0 35.24 35.24 1.17 o 1 -11 0 2.57 1.93 0.29 o 2 -11 0 8.07 7.80 0.40 o 3 -11 0 153.40 162.71 4.39 o 0 -10 0 77.78 71.81 2.83 o 1 -10 0 37.49 38.04 1.11 o 2 -10 0 29.45 29.89 1.33 o 3 -10 0 6.67 6.09 0.49 o 4 -10 0 74.55 80.07 2.35 o 1 -9 0 106.95 102.67 2.63 o 2 -9 0 18.57 17.75 0.61 o 3 -9 0 219.02 226.67 6.09 o 4 -9 0 48.41 50.30 1.53 o 0 -8 0 1237.13 1196.57 43.54 o 1 -8 0 4.15 3.61 0.17 o 2 -8 0 65.95 70.03 1.62 o 3 -8 0 8.34 9.32 0.42 o 4 -8 0 50.15 49.51 1.54 o 5 -8 0 7.29 8.39 0.44 o 1 -7 0 789.85 835.19 17.25 o 2 -7 0 168.29 172.34 3.71 o 3 -7 0 115.47 111.79 3.10 o 4 -7 0 39.00 38.30 1.23 o 5 -7 0 14.98 16.97 0.90 o 0 -6 0 2435.36 2781.19 69.06 o 1 -6 0 326.00 320.53 8.17 o 2 -6 0 178.21 186.24 4.02 o 3 -6 0 106.21 102.85 2.85 o 4 -6 0 204.42 199.85 5.45 o 5 -6 0 36.45 36.49 1.92 o 1 -5 0 265.99 283.67 7.57 o 2 -5 0 98.84 101.90 2.14 o 3 -5 0 1063.89 1050.25 22.47 o 4 -5 0 199.46 205.46 5.46 o 5 -5 0 4.54 4.27 0.30 o 6 -5 0 5.05 6.19 0.52 o 0 -4 0 947.09 976.96 35.15 o 1 -4 0 852.43 897.24 18.84 o 2 -4 0 238.28 239.09 4.96 o 3 -4 0 220.33 214.94 4.69 o 4 -4 0 693.30 660.35 17.87 o 5 -4 0 63.62 65.93 1.96 o 6 -4 0 18.97 19.90 0.79 o 1 -3 0 497.46 521.99 10.87 o 2 -3 0 167.70 161.78 3.53 o 3 -3 0 1490.81 1444.17 33.13 o 4 -3 0 182.27 174.01 7.16 o 5 -3 0 1.92 2.46 0.34 o 6 -3 0 8.61 9.95 0.64 o 0 -2 0 2133.03 2313.01 85.46 o 1 -2 0 2115.82 1992.00 77.47 o 2 -2 0 184.01 167.24 3.13 o 3 -2 0 344.18 366.03 7.71 o 4 -2 0 265.01 267.65 6.84 o 5 -2 0 65.77 64.30 3.04 o 6 -2 0 24.85 29.44 1.02 o 2 -1 0 48.28 67.55 1.22 o 3 -1 0 268.23 274.67 5.02 o 4 -1 0 174.37 182.81 3.87 o 5 -1 0 12.24 13.15 0.54 o 6 -1 0 2.27 2.82 0.25 o 1 0 0 167.50 200.29 3.70 o 2 0 0 1216.47 1226.03 30.97 o 3 0 0 182.23 203.61 3.80 o 4 0 0 122.23 134.23 2.92 o 5 0 0 4.46 4.17 0.31 o 6 0 0 73.97 79.51 2.35 o 1 1 0 4325.60 4146.03 140.64 o 2 1 0 41.92 59.54 1.21 o 3 1 0 263.40 264.48 5.01 o 4 1 0 170.94 175.99 3.99 o 5 1 0 13.71 14.40 0.43 o 6 1 0 2.14 2.33 0.36 o 0 2 0 2182.07 2548.42 65.86 o 1 2 0 2098.98 2126.45 52.64 o 2 2 0 188.50 169.43 3.14 o 3 2 0 347.57 362.97 6.74 o 4 2 0 265.71 265.46 4.96 o 5 2 0 66.63 63.64 1.51 o 6 2 0 25.76 27.24 1.38 o 1 3 0 490.65 515.03 8.61 o 2 3 0 174.54 169.22 3.10 o 3 3 0 1483.12 1461.06 46.34 o 4 3 0 188.75 182.69 3.40 o 5 3 0 1.87 2.70 0.36 o 0 4 0 946.99 1022.90 22.32 o 1 4 0 830.36 895.84 18.73 o 2 4 0 223.07 228.26 4.33 o 3 4 0 218.44 208.16 4.14 o 4 4 0 691.80 685.59 12.53 o 5 4 0 64.86 66.59 1.56 o 1 5 0 274.30 302.28 4.55 o 2 5 0 90.75 94.52 1.85 o 3 5 0 1077.51 1094.52 22.69 o 4 5 0 195.91 197.83 4.65 o 5 5 0 4.14 4.27 0.25 o 6 5 0 4.98 5.24 0.46 o 0 6 0 2404.03 2688.79 113.01 o 1 6 0 318.20 320.38 4.90 o 2 6 0 184.76 190.84 4.49 o 3 6 0 104.06 102.45 2.78 o 4 6 0 205.41 201.42 5.67 o 5 6 0 37.06 38.57 0.98 o 1 7 0 795.79 842.51 15.94 o 2 7 0 167.65 172.47 3.77 o 3 7 0 113.00 111.70 2.51 o 4 7 0 40.45 38.60 0.97 o 5 7 0 13.69 14.62 0.66 o 0 8 0 1250.89 1277.77 33.63 o 1 8 0 4.98 4.06 0.21 o 2 8 0 68.94 74.52 1.68 o 3 8 0 8.37 9.10 0.34 o 4 8 0 51.07 49.80 1.68 o 5 8 0 6.74 6.63 0.39 o 1 9 0 105.31 98.18 2.31 o 2 9 0 16.37 15.95 0.74 o 3 9 0 222.18 225.63 6.48 o 4 9 0 47.65 47.04 1.79 o 0 10 0 79.53 75.45 2.16 o 1 10 0 37.42 36.50 0.96 o 2 10 0 29.88 28.83 2.28 o 3 10 0 6.87 6.29 0.39 o 4 10 0 73.06 78.76 2.69 o 1 11 0 2.64 2.57 0.22 o 2 11 0 8.01 7.62 0.54 o 3 11 0 152.01 159.75 7.20 o 0 12 0 72.67 77.43 3.19 o 1 12 0 13.78 13.63 0.58 o 2 12 0 36.32 35.15 1.19 o 3 12 0 16.46 16.12 0.95 o 1 13 0 56.90 58.90 1.81 o 2 13 0 53.64 56.84 1.82 o -1 -13 1 6.47 6.24 0.40 o 0 -13 1 4.35 4.81 0.49 o 1 -13 1 21.25 21.11 0.81 o 2 -13 1 29.59 30.92 1.48 o -2 -12 1 20.36 20.86 0.79 o -1 -12 1 75.31 74.83 2.17 o 0 -12 1 55.46 57.32 2.30 o 1 -12 1 16.34 17.01 0.92 o 2 -12 1 4.73 6.06 0.36 o -3 -11 1 64.32 67.33 2.02 o -2 -11 1 117.11 112.80 3.14 o -1 -11 1 48.65 44.33 1.39 o 0 -11 1 50.53 48.88 1.43 o 1 -11 1 17.89 18.09 0.66 o 2 -11 1 13.58 14.12 0.98 o 3 -11 1 15.42 16.55 0.95 o -4 -10 1 27.67 27.41 0.97 o -3 -10 1 26.08 25.35 0.95 o -2 -10 1 72.90 70.57 2.07 o -1 -10 1 253.90 256.31 6.93 o 0 -10 1 117.31 122.40 3.24 o 1 -10 1 178.73 173.29 4.39 o 2 -10 1 0.25 0.16 0.16 o 3 -10 1 49.61 47.45 1.47 o 4 -10 1 3.09 3.13 0.29 o -4 -9 1 35.14 35.62 1.18 o -3 -9 1 60.75 61.31 1.81 o -2 -9 1 294.75 294.39 7.72 o -1 -9 1 6.02 7.12 0.52 o 0 -9 1 194.11 196.49 5.00 o 1 -9 1 323.98 337.43 9.97 o 2 -9 1 93.02 88.69 2.05 o 3 -9 1 63.45 59.42 1.76 o 4 -9 1 57.89 57.62 1.74 o -5 -8 1 61.29 61.35 1.88 o -4 -8 1 45.54 44.58 1.40 o -3 -8 1 320.30 318.84 8.45 o -2 -8 1 109.03 101.90 2.90 o -1 -8 1 140.15 148.05 3.76 o 0 -8 1 274.01 280.64 7.18 o 1 -8 1 468.93 448.24 31.50 o 2 -8 1 28.93 26.17 1.28 o 3 -8 1 39.73 41.11 1.29 o 4 -8 1 71.40 72.46 2.10 o 5 -8 1 2.28 2.92 0.28 o -5 -7 1 43.39 45.49 1.44 o -4 -7 1 311.38 314.76 8.33 o -3 -7 1 413.09 404.22 10.77 o -2 -7 1 328.58 318.22 8.34 o -1 -7 1 54.03 53.62 2.17 o 0 -7 1 188.72 205.24 5.30 o 1 -7 1 109.22 111.79 2.90 o 2 -7 1 496.43 475.20 13.91 o 3 -7 1 185.31 184.35 5.02 o 4 -7 1 4.65 5.14 0.31 o 5 -7 1 4.15 4.38 0.32 o -5 -6 1 92.63 96.85 2.77 o -4 -6 1 23.47 22.86 0.79 o -3 -6 1 338.40 336.41 8.80 o -2 -6 1 271.20 248.79 5.30 o -1 -6 1 6.37 11.77 0.31 o 0 -6 1 8.86 5.60 0.28 o 1 -6 1 246.23 244.12 6.19 o 2 -6 1 131.33 141.11 3.03 o 3 -6 1 210.93 211.78 4.62 o 4 -6 1 284.34 283.43 7.69 o 5 -6 1 24.88 25.60 1.59 o -6 -5 1 88.23 94.05 3.94 o -5 -5 1 23.59 24.23 0.87 o -4 -5 1 114.00 109.88 3.17 o -3 -5 1 304.63 309.26 8.34 o -2 -5 1 443.36 419.13 8.95 o -1 -5 1 37.78 37.36 0.85 o 0 -5 1 96.01 117.54 3.17 o 1 -5 1 844.07 876.44 22.46 o 2 -5 1 387.50 384.70 8.25 o 3 -5 1 327.99 326.09 6.90 o 4 -5 1 122.76 123.27 5.60 o 5 -5 1 11.57 11.59 0.51 o -6 -4 1 43.33 46.97 2.07 o -5 -4 1 2.90 3.24 0.27 o -4 -4 1 161.30 157.69 4.32 o -3 -4 1 194.69 189.73 5.11 o -2 -4 1 265.41 275.21 5.78 o 0 -4 1 1205.15 1208.10 35.73 o 1 -4 1 1663.93 1729.59 98.41 o 2 -4 1 27.83 27.75 0.57 o 3 -4 1 136.46 136.44 3.36 o 4 -4 1 74.49 71.50 4.39 o 5 -4 1 287.84 289.80 7.87 o -6 -3 1 61.68 69.12 2.08 o -5 -3 1 1.16 2.69 0.98 o -4 -3 1 51.16 53.43 1.99 o -3 -3 1 215.19 191.39 4.07 o -2 -3 1 46.31 41.05 2.35 o -1 -3 1 122.17 136.67 2.91 o 0 -3 1 2958.28 3197.25 151.31 o 1 -3 1 2106.80 2180.24 81.36 o 2 -3 1 58.42 59.47 1.16 o 3 -3 1 66.18 75.93 2.01 o 4 -3 1 470.14 479.49 10.13 o 5 -3 1 8.89 8.86 0.84 o 6 -3 1 41.80 41.99 1.97 o -6 -2 1 20.68 22.26 0.92 o -5 -2 1 13.16 13.86 0.58 o -4 -2 1 49.12 42.84 1.31 o -3 -2 1 466.76 475.69 9.88 o -2 -2 1 82.34 67.11 1.44 o -1 -2 1 1780.80 1754.85 45.27 o 0 -2 1 3770.74 3787.13 172.40 o 1 -2 1 3862.28 3635.28 105.36 o 2 -2 1 80.34 89.69 1.70 o 3 -2 1 138.51 146.67 2.75 o 4 -2 1 239.12 246.05 5.23 o 5 -2 1 129.57 127.12 3.48 o 6 -2 1 37.43 39.32 1.84 o -6 -1 1 14.15 16.57 0.77 o -5 -1 1 22.64 21.35 0.79 o -4 -1 1 153.98 159.83 5.70 o -3 -1 1 691.40 746.59 13.84 o -2 -1 1 978.88 962.82 20.36 o -1 -1 1 2.89 3.28 0.20 o 1 -1 1 2914.20 2797.44 75.88 o 2 -1 1 1186.52 1136.51 28.93 o 3 -1 1 466.61 460.51 8.39 o 4 -1 1 25.51 24.20 0.87 o 5 -1 1 14.92 12.16 0.69 o 6 -1 1 14.73 17.10 0.98 o -6 0 1 18.71 18.31 1.08 o -5 0 1 8.57 8.25 0.61 o -4 0 1 2.88 1.90 0.14 o -3 0 1 1648.51 1700.88 39.66 o -2 0 1 4865.15 4783.27 166.08 o -1 0 1 375.73 413.16 7.60 o 0 0 1 865.01 865.21 22.40 o 1 0 1 3258.09 2967.09 103.10 o 2 0 1 168.98 177.40 3.30 o 3 0 1 40.46 34.62 0.71 o 4 0 1 319.31 307.69 6.53 o 5 0 1 2.97 2.81 0.17 o 6 0 1 13.79 14.55 0.88 o -6 1 1 14.38 15.49 0.66 o -5 1 1 24.67 24.55 0.80 o -4 1 1 152.69 157.19 2.99 o -3 1 1 709.53 757.93 13.86 o -2 1 1 962.40 980.74 20.51 o -1 1 1 2.77 3.56 0.28 o 0 1 1 103.59 113.95 1.91 o 1 1 1 2886.82 2977.75 99.11 o 2 1 1 1179.69 1140.93 21.03 o 3 1 1 460.51 446.14 8.38 o 4 1 1 23.72 21.34 0.50 o 5 1 1 14.74 13.18 0.46 o 6 1 1 14.25 15.96 0.92 o -6 2 1 20.85 22.50 0.98 o -5 2 1 13.41 15.11 0.58 o -4 2 1 49.21 41.37 0.86 o -3 2 1 460.78 460.91 8.62 o -2 2 1 80.06 64.77 1.26 o -1 2 1 1791.93 1707.38 43.68 o 0 2 1 3752.78 3707.43 98.47 o 1 2 1 3858.24 3345.03 131.33 o 2 2 1 82.64 90.42 1.71 o 3 2 1 141.26 145.96 2.76 o 4 2 1 243.17 243.11 4.57 o 5 2 1 123.76 122.84 2.75 o 6 2 1 38.08 38.70 1.77 o -6 3 1 62.01 66.97 2.04 o -5 3 1 1.07 2.08 0.18 o -4 3 1 52.27 53.09 1.08 o -3 3 1 214.04 189.30 3.56 o -2 3 1 48.79 43.24 0.84 o -1 3 1 122.90 138.59 2.32 o 0 3 1 2952.30 3164.10 89.80 o 1 3 1 2120.27 2209.12 50.00 o 2 3 1 61.35 61.42 1.17 o 3 3 1 67.48 71.15 1.61 o 4 3 1 468.91 476.74 8.85 o 5 3 1 8.92 8.55 0.38 o -6 4 1 44.00 46.65 2.07 o -5 4 1 2.64 3.32 0.17 o -4 4 1 162.51 158.32 3.02 o -3 4 1 194.91 189.96 3.57 o -2 4 1 259.21 271.87 5.08 o -1 4 1 53.48 48.25 0.93 o 0 4 1 1192.82 1173.65 17.89 o 1 4 1 1656.88 1787.23 29.45 o 2 4 1 27.95 27.67 0.64 o 3 4 1 138.27 135.49 4.90 o 4 4 1 71.51 66.69 1.58 o 5 4 1 291.05 293.13 7.70 o 6 4 1 53.43 67.86 2.69 o -5 5 1 25.06 24.08 0.67 o -4 5 1 115.33 115.38 2.21 o -3 5 1 307.37 315.10 5.84 o -2 5 1 441.58 430.56 7.89 o -1 5 1 37.56 38.37 0.77 o 0 5 1 105.75 131.50 2.22 o 1 5 1 845.53 896.30 14.87 o 2 5 1 387.00 395.46 7.24 o 3 5 1 325.23 322.22 6.96 o 4 5 1 127.72 131.42 3.21 o 5 5 1 11.03 10.52 0.47 o -5 6 1 90.55 93.46 2.20 o -4 6 1 23.67 22.26 0.62 o -3 6 1 329.24 324.85 7.09 o -2 6 1 268.91 249.87 4.66 o -1 6 1 5.20 10.75 0.33 o 0 6 1 8.04 5.11 0.21 o 1 6 1 241.67 241.21 4.09 o 2 6 1 128.52 139.77 3.75 o 3 6 1 218.67 220.89 4.78 o 4 6 1 286.26 288.59 6.23 o 5 6 1 25.13 26.27 0.89 o -5 7 1 42.97 43.66 1.13 o -4 7 1 311.34 306.46 6.73 o -3 7 1 419.90 407.21 8.76 o -2 7 1 326.53 309.06 8.54 o -1 7 1 53.79 54.16 1.76 o 0 7 1 192.20 214.72 3.72 o 1 7 1 103.62 109.90 1.91 o 2 7 1 488.34 469.98 13.77 o 3 7 1 183.46 186.16 5.71 o 4 7 1 4.84 5.77 0.26 o 5 7 1 3.75 4.34 0.31 o -5 8 1 62.63 59.97 1.49 o -4 8 1 45.41 44.29 1.21 o -3 8 1 318.62 315.09 6.88 o -2 8 1 115.92 108.39 4.10 o -1 8 1 136.10 146.16 4.10 o 0 8 1 274.80 290.43 4.92 o 1 8 1 467.92 474.85 7.87 o 2 8 1 29.78 28.36 0.75 o 3 8 1 41.96 42.74 2.32 o 4 8 1 69.31 69.31 2.05 o 5 8 1 1.73 1.74 0.23 o -4 9 1 35.69 35.25 1.21 o -3 9 1 60.75 61.37 2.58 o -2 9 1 291.62 296.17 8.10 o -1 9 1 6.20 7.04 0.35 o 0 9 1 189.98 196.61 3.83 o 1 9 1 326.91 336.52 7.43 o 2 9 1 96.12 95.14 2.11 o 3 9 1 61.76 59.77 2.23 o 4 9 1 57.12 54.82 1.85 o -4 10 1 28.17 27.65 1.15 o -3 10 1 25.84 26.13 1.34 o -2 10 1 73.73 74.12 2.16 o -1 10 1 259.98 272.05 7.27 o 0 10 1 120.52 124.85 2.47 o 1 10 1 178.86 166.69 3.98 o 2 10 1 0.23 0.33 0.12 o 3 10 1 50.01 48.18 1.20 o 4 10 1 3.35 3.80 0.30 o -3 11 1 64.50 69.36 2.09 o -2 11 1 115.56 113.96 3.27 o -1 11 1 47.72 46.81 1.44 o 0 11 1 50.78 50.39 1.25 o 1 11 1 18.88 19.21 0.57 o 2 11 1 13.35 14.53 0.58 o 3 11 1 14.34 15.12 0.97 o -3 12 1 10.35 13.30 0.85 o -2 12 1 20.60 21.58 0.81 o -1 12 1 75.24 75.29 2.24 o 0 12 1 54.59 54.26 1.69 o 1 12 1 15.83 17.02 0.55 o 2 12 1 4.62 5.48 0.36 o -2 13 1 40.89 40.96 1.37 o -1 13 1 6.35 6.99 0.56 o 0 13 1 4.73 5.71 0.57 o 1 13 1 21.35 21.16 0.80 o 2 13 1 29.01 29.78 1.29 o -1 -13 2 56.05 55.89 1.76 o 0 -13 2 35.43 37.58 1.64 o -2 -12 2 58.10 58.93 1.80 o -1 -12 2 76.34 77.19 2.26 o 0 -12 2 65.18 60.10 2.53 o 1 -12 2 6.56 5.31 0.35 o 2 -12 2 35.09 35.25 2.89 o -3 -11 2 16.58 15.64 0.65 o -2 -11 2 15.78 13.84 0.69 o -1 -11 2 209.01 205.40 5.43 o 0 -11 2 64.28 61.55 2.50 o 1 -11 2 119.81 115.20 3.01 o 2 -11 2 84.22 84.87 3.55 o 3 -11 2 2.17 1.87 0.33 o -4 -10 2 77.46 81.44 2.37 o -3 -10 2 84.78 83.84 2.40 o -2 -10 2 184.60 174.24 4.73 o -1 -10 2 47.55 41.51 1.90 o 0 -10 2 459.40 474.17 11.95 o 1 -10 2 38.70 35.40 1.10 o 2 -10 2 100.71 98.10 2.75 o 3 -10 2 121.75 127.19 3.55 o 4 -10 2 19.68 20.81 1.21 o -4 -9 2 126.10 127.76 2.87 o -3 -9 2 8.31 8.48 0.61 o -2 -9 2 126.93 120.37 3.31 o -1 -9 2 445.08 432.59 11.29 o 0 -9 2 35.58 35.82 1.06 o 1 -9 2 175.01 181.43 4.65 o 2 -9 2 88.52 88.85 1.98 o 3 -9 2 32.13 29.25 0.99 o 4 -9 2 54.63 62.03 1.87 o -5 -8 2 21.27 23.66 1.25 o -4 -8 2 42.41 42.26 1.32 o -3 -8 2 12.84 14.04 0.45 o -2 -8 2 473.88 478.08 12.25 o -1 -8 2 736.43 737.39 15.35 o 0 -8 2 33.50 35.92 1.03 o 1 -8 2 1.55 1.15 0.26 o 2 -8 2 148.64 145.63 3.16 o 3 -8 2 23.60 24.93 0.83 o 4 -8 2 23.80 23.38 1.23 o 5 -8 2 42.07 44.81 2.26 o -5 -7 2 27.23 26.72 0.96 o -4 -7 2 20.34 17.56 0.70 o -3 -7 2 363.77 370.65 9.80 o -2 -7 2 12.76 12.59 0.63 o -1 -7 2 232.76 226.38 4.31 o 0 -7 2 768.99 758.46 18.95 o 1 -7 2 41.42 44.63 1.23 o 2 -7 2 114.57 107.62 4.19 o 3 -7 2 405.69 386.85 8.26 o 4 -7 2 27.87 27.57 0.94 o 5 -7 2 31.26 33.45 1.85 o -5 -6 2 4.87 5.01 0.34 o -4 -6 2 169.85 171.44 4.71 o -3 -6 2 136.42 133.23 3.59 o -2 -6 2 136.47 140.47 3.73 o -1 -6 2 98.87 89.45 1.71 o 0 -6 2 18.48 14.56 0.72 o 1 -6 2 547.70 608.81 21.71 o 2 -6 2 173.73 171.61 4.45 o 3 -6 2 135.16 135.71 2.92 o 4 -6 2 166.57 162.66 4.47 o 5 -6 2 53.63 55.02 2.22 o -5 -5 2 170.71 172.66 4.77 o -4 -5 2 277.73 269.46 7.32 o -3 -5 2 126.28 123.61 3.41 o -2 -5 2 217.03 226.16 6.05 o -1 -5 2 400.53 392.78 7.05 o 0 -5 2 720.97 764.91 19.14 o 1 -5 2 453.52 455.40 15.78 o 2 -5 2 335.41 351.83 6.65 o 3 -5 2 419.52 422.31 8.94 o 4 -5 2 15.45 15.95 0.60 o 5 -5 2 2.08 2.20 0.23 o -6 -4 2 53.25 57.38 2.87 o -5 -4 2 21.48 19.60 0.90 o -4 -4 2 184.13 188.75 5.19 o -3 -4 2 47.88 47.62 1.36 o -2 -4 2 113.48 131.70 2.74 o -1 -4 2 329.98 333.72 5.95 o 0 -4 2 131.42 117.68 3.22 o 1 -4 2 659.55 738.94 38.29 o 2 -4 2 1006.55 995.18 18.62 o 3 -4 2 566.70 575.02 12.28 o 4 -4 2 220.03 217.60 4.68 o 5 -4 2 39.63 37.24 1.25 o -6 -3 2 27.82 27.69 1.02 o -5 -3 2 146.08 150.30 4.13 o -4 -3 2 70.76 72.32 3.06 o -3 -3 2 80.93 76.16 2.17 o -2 -3 2 123.13 137.53 3.72 o -1 -3 2 720.14 746.87 13.18 o 0 -3 2 384.83 402.94 14.53 o 1 -3 2 6.86 18.04 0.58 o 2 -3 2 1436.52 1405.97 31.09 o 3 -3 2 250.24 262.60 5.64 o 4 -3 2 335.58 345.43 7.30 o 5 -3 2 74.76 72.27 3.99 o 6 -3 2 8.28 9.63 0.69 o -6 -2 2 94.95 96.08 2.81 o -5 -2 2 9.71 9.28 0.59 o -4 -2 2 125.33 128.85 3.51 o -3 -2 2 370.17 388.47 8.15 o -2 -2 2 657.68 661.36 13.71 o -1 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