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Information card for entry 2238406
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| Coordinates | 2238406.cif |
|---|---|
| Structure factors | 2238406.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis{<i>N</i>-benzyl-<i>N</i>-[2-(thiophen-2-yl)ethyl]dithiocarbamato-κ^2^<i>S</i>,<i>S</i>'}lead(II) |
|---|---|
| Formula | C28 H28 N2 Pb S6 |
| Calculated formula | C28 H28 N2 Pb S6 |
| Title of publication | Bis{<i>N</i>-benzyl-<i>N</i>-[2-(thiophen-2-yl)ethyl]dithiocarbamato-κ^2^<i>S</i>,<i>S</i>'}lead(II) |
| Authors of publication | Sathiyaraj, E.; Thirumaran, S.; Sridhar, B.; Selvanayagam, S. |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2013 |
| Journal volume | 69 |
| Journal issue | 8 |
| Pages of publication | m457 |
| a | 27.459 ± 0.002 Å |
| b | 5.558 ± 0.0004 Å |
| c | 19.467 ± 0.0015 Å |
| α | 90° |
| β | 100.168 ± 0.002° |
| γ | 90° |
| Cell volume | 2924.3 ± 0.4 Å3 |
| Cell temperature | 292 ± 2 K |
| Ambient diffraction temperature | 292 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0304 |
| Residual factor for significantly intense reflections | 0.0255 |
| Weighted residual factors for significantly intense reflections | 0.0712 |
| Weighted residual factors for all reflections included in the refinement | 0.0743 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.007 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181306 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/84. |
2238406.cif 2238406.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2238406.cif 2238406.hkl |
| 89416 | 2013-10-25 | cif/ (saulius@koala.ibt.lt) Adding links pointing to FOBS data to the recently deposited structures from IUCr. |
2238406.cif 2238406.hkl |
| 89414 | 2013-10-24 | cod/ (saulius@koala.ibt.lt) Adding FOBS data for the recently deposited IUCr structures. |
2238406.cif 2238406.hkl |
| 88252 | 2013-09-04 | cif/ Adding structures of 2238406 via cif-deposit CGI script. |
2238406.cif |
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