#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:52:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181306 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/84/2238445.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238445_Fobs loop_ _publ_author_name 'Avila-Sorrosa, Alcives' 'Reyes-Arellano, Alicia' 'Germ\'an-Acacio, Juan Manuel' 'Reyes-Mart\'inez, Reyna' 'Morales-Morales, David' _publ_section_title ; trans-Bis(\m-benzenethiolato-\k^2^S:S)bis[chlorido(triphenylphosphane-\kP)palladium(II)] chloroform disolvate ; _journal_coeditor_code WM2753 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m472 _journal_volume 69 _journal_year 2013 _cell_angle_alpha 90.000 _cell_angle_beta 102.095 _cell_angle_gamma 90.000 _cell_length_a 10.8343 _cell_length_b 14.2291 _cell_length_c 17.3994 _exptl_crystal_F_000 1264.00 _reflns_d_resolution_high 0.8279 _cod_data_source_file wm2753Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ASA0030' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11088.17 12134.89 141.44 o 4 0 0 495.48 532.95 19.08 o 6 0 0 10737.92 10706.73 139.84 o -7 0 5 1.01 -49.94 27.11 o 8 0 0 1033.78 1055.11 66.08 o 10 0 0 592.94 649.87 65.99 o 12 0 0 176.88 198.70 30.50 o 1 1 0 13916.27 15535.75 158.48 o 2 1 0 18325.95 20264.44 455.01 o 3 1 0 1778.00 1728.70 24.08 o 4 1 0 11287.83 12111.16 208.69 o 5 1 0 4016.98 4268.33 124.50 o 6 1 0 2180.06 2076.78 28.81 o 7 1 0 4569.02 4556.48 86.06 o 8 1 0 1101.07 1110.31 47.98 o 9 1 0 784.33 737.89 19.71 o 10 1 0 1518.58 1588.69 93.11 o 11 1 0 136.47 108.18 17.30 o 12 1 0 146.50 129.05 18.73 o 0 2 0 2106.30 2404.43 37.10 o 1 2 0 422.47 493.89 9.01 o 2 2 0 429.49 513.15 9.81 o 3 2 0 410.94 389.99 11.86 o 4 2 0 2412.36 2464.18 75.18 o 5 2 0 9038.27 9218.82 168.38 o 6 2 0 1332.03 1310.62 21.58 o 7 2 0 510.48 516.18 23.54 o 8 2 0 1394.72 1401.05 71.52 o 9 2 0 1297.62 1190.49 27.56 o 10 2 0 573.75 508.60 34.60 o 11 2 0 2186.98 2093.99 116.03 o 12 2 0 7.81 42.27 19.98 o 1 3 0 478.03 454.02 7.85 o 2 3 0 11216.65 12388.25 111.66 o 3 3 0 772.92 772.94 15.16 o 4 3 0 4081.56 4001.50 110.05 o 5 3 0 244.27 223.31 8.56 o 6 3 0 1557.87 1548.46 25.68 o 7 3 0 1647.24 1478.46 77.32 o 8 3 0 553.14 570.59 20.96 o 9 3 0 816.08 711.67 24.17 o 10 3 0 3681.50 3607.50 88.83 o 11 3 0 346.05 612.59 67.60 o 12 3 0 946.11 868.19 39.24 o 0 4 0 48039.06 54695.68 703.20 o 1 4 0 21130.70 22503.44 506.55 o 2 4 0 2292.54 2224.37 24.79 o 3 4 0 512.46 516.54 12.84 o 4 4 0 4.65 19.00 4.73 o 5 4 0 461.37 440.65 13.02 o 6 4 0 4344.52 4090.59 51.01 o 7 4 0 1680.46 1769.99 55.56 o 8 4 0 3057.68 3328.27 111.30 o 9 4 0 570.79 547.93 22.12 o 10 4 0 286.56 267.90 30.32 o 11 4 0 1225.22 1356.46 96.49 o 12 4 0 933.60 947.20 35.76 o 1 5 0 19361.76 20670.75 196.65 o 2 5 0 1550.96 1598.67 21.76 o 3 5 0 3822.28 3861.75 47.53 o 4 5 0 145.62 116.29 8.47 o 5 5 0 1257.24 1132.16 21.94 o 6 5 0 1151.92 1143.31 23.72 o 7 5 0 4459.89 4675.18 139.57 o 8 5 0 1009.00 1091.76 58.59 o 9 5 0 1580.57 1606.61 37.46 o 10 5 0 825.87 793.90 41.83 o 11 5 0 6.96 38.35 11.59 o 12 5 0 109.20 125.92 16.14 o 0 6 0 36715.72 39429.71 449.21 o 1 6 0 10607.25 11359.36 99.71 o 2 6 0 8529.63 8875.29 80.89 o 3 6 0 2176.50 1948.71 25.06 o 4 6 0 1402.64 1284.40 23.10 o 5 6 0 5410.46 5459.00 63.32 o 6 6 0 4051.99 3960.12 52.08 o 7 6 0 17.86 21.49 7.76 o 8 6 0 825.61 816.01 25.51 o 9 6 0 377.16 387.05 19.89 o 10 6 0 70.11 103.36 25.60 o 11 6 0 372.81 407.03 22.74 o 1 7 0 61.85 85.26 6.51 o 2 7 0 11990.83 12195.00 108.53 o 3 7 0 277.15 232.32 8.83 o 4 7 0 10852.45 11097.17 110.94 o 5 7 0 54.15 71.61 8.92 o 6 7 0 3211.14 3119.76 45.13 o 7 7 0 303.75 303.84 14.54 o 8 7 0 325.84 323.02 18.28 o 9 7 0 228.27 229.82 17.30 o 10 7 0 537.14 581.20 39.15 o 11 7 0 1.72 11.24 11.86 o 0 8 0 2486.45 2175.15 40.67 o 1 8 0 17.75 10.52 4.64 o 2 8 0 222.02 211.18 9.45 o 3 8 0 4896.57 4923.46 56.36 o 4 8 0 940.39 902.97 20.69 o 5 8 0 316.74 299.38 13.64 o 6 8 0 1008.26 1042.71 24.61 o 7 8 0 95.81 108.00 11.59 o 8 8 0 1004.75 902.79 31.84 o 9 8 0 1002.89 965.22 34.60 o 10 8 0 253.41 304.73 33.80 o 11 8 0 317.69 394.36 27.29 o 1 9 0 1205.86 1143.85 20.51 o 2 9 0 36.25 59.22 6.96 o 3 9 0 762.45 836.17 17.48 o 4 9 0 5.62 0.62 6.15 o 5 9 0 290.54 321.50 17.21 o 6 9 0 95.49 110.32 12.84 o 7 9 0 3211.17 3075.17 61.62 o 8 9 0 205.90 257.65 22.65 o 9 9 0 1082.44 1016.94 36.30 o 10 9 0 395.79 398.02 35.94 o 0 10 0 1547.17 1681.52 38.08 o 1 10 0 2365.49 2341.11 81.87 o 2 10 0 1817.57 1842.50 28.63 o 3 10 0 616.35 623.56 18.19 o 4 10 0 635.38 629.45 24.08 o 5 10 0 121.66 149.83 14.98 o 6 10 0 830.35 848.48 26.49 o 7 10 0 480.91 380.63 59.31 o 8 10 0 1586.23 1505.84 43.79 o 9 10 0 40.37 58.06 14.89 o 10 10 0 166.61 188.89 32.11 o 1 11 0 693.15 738.51 20.24 o 2 11 0 1834.31 1884.06 33.89 o 3 11 0 1184.55 1081.42 28.81 o 4 11 0 1147.03 1156.87 30.23 o 5 11 0 24.53 24.97 11.15 o 6 11 0 807.45 788.64 29.43 o 7 11 0 1226.59 1235.53 92.84 o 8 11 0 532.74 537.05 27.56 o 9 11 0 269.33 290.29 22.56 o 0 12 0 33.56 31.66 13.11 o 1 12 0 294.84 282.80 15.43 o 2 12 0 573.51 609.83 20.07 o 3 12 0 5269.45 5455.25 77.77 o 4 12 0 26.17 71.52 12.40 o 5 12 0 2119.74 1995.00 43.43 o 6 12 0 87.20 81.07 15.34 o 7 12 0 12.96 50.48 45.04 o 8 12 0 38.20 33.44 13.02 o 9 12 0 551.75 567.02 34.16 o 1 13 0 1212.29 1154.46 31.12 o 2 13 0 2884.49 2648.79 55.65 o 3 13 0 617.72 639.17 24.44 o 4 13 0 1758.77 1744.66 40.76 o 5 13 0 34.58 75.09 12.75 o 6 13 0 443.74 521.80 26.67 o 7 13 0 635.05 681.53 75.63 o 8 13 0 180.19 125.57 60.47 o 0 14 0 1544.67 1450.90 51.55 o 1 14 0 13.91 37.55 11.68 o 2 14 0 1653.52 1562.38 42.90 o 3 14 0 169.65 197.00 17.66 o 4 14 0 133.76 169.36 16.05 o 5 14 0 232.92 231.07 19.26 o 6 14 0 235.71 212.79 19.44 o 7 14 0 43.30 18.73 51.90 o 1 15 0 129.16 128.24 16.32 o 2 15 0 175.69 201.11 19.44 o 3 15 0 131.82 152.59 16.50 o 4 15 0 200.14 192.90 52.26 o 5 15 0 160.54 156.25 21.49 o 6 15 0 354.08 396.77 29.79 o 0 16 0 5.34 -1.69 19.44 o 1 16 0 12.43 22.38 10.79 o 2 16 0 90.01 92.84 15.61 o 3 16 0 543.81 552.84 28.00 o 4 16 0 167.01 179.26 54.58 o 1 17 0 20.68 14.27 12.57 o -11 0 1 619.29 558.64 41.65 o -10 0 6 554.91 505.22 58.59 o -9 0 1 1441.74 1374.56 38.17 o -8 0 4 1396.51 1330.15 75.18 o -7 0 1 5080.36 5227.22 161.69 o -5 0 1 1271.76 1258.89 28.36 o -3 0 1 2329.08 2256.66 35.32 o -1 0 1 52628.89 58772.10 763.58 o 1 0 1 23131.88 25632.12 334.52 o 3 0 1 3605.27 3939.34 54.22 o 5 0 1 19755.39 21311.52 253.99 o 7 0 1 2129.88 2128.68 84.19 o -8 0 6 849.31 786.94 58.24 o 9 0 1 2283.97 2135.64 48.78 o 11 0 1 18.83 57.88 20.78 o -12 1 1 281.79 256.93 22.47 o -11 1 1 1048.67 959.95 83.30 o -10 1 1 223.64 221.08 34.69 o -9 1 1 746.31 680.90 19.00 o -8 1 1 1812.21 2001.87 65.99 o -7 1 1 2426.31 2513.86 50.83 o -6 1 1 8000.76 8035.73 90.79 o -5 1 1 4758.68 4987.67 102.74 o -4 1 1 1191.55 1118.16 34.60 o -3 1 1 1069.21 1089.98 15.16 o -2 1 1 10030.11 10681.67 249.62 o -1 1 1 3616.63 3974.57 40.04 o 0 1 1 17156.41 19398.30 219.21 o 1 1 1 73.91 78.48 3.48 o 2 1 1 1797.00 1947.73 39.60 o 3 1 1 6611.53 6897.68 61.71 o 4 1 1 3246.74 3205.37 91.59 o 5 1 1 11813.38 13872.60 331.31 o 6 1 1 12270.90 12721.44 114.87 o 7 1 1 207.24 223.40 21.58 o 8 1 1 3174.67 3134.30 81.60 o 9 1 1 524.84 500.85 16.68 o 10 1 1 22.78 38.88 13.38 o 11 1 1 475.20 482.47 28.27 o 12 1 1 315.50 275.30 24.53 o -12 2 1 1298.75 1305.00 53.42 o -11 2 1 137.01 224.56 51.73 o -10 2 1 2698.29 2718.98 62.43 o -9 2 1 131.67 140.10 12.22 o -8 2 1 216.57 320.16 42.36 o -7 2 1 2241.19 2099.97 45.57 o -6 2 1 7978.17 7944.85 89.98 o -5 2 1 5641.88 5684.01 156.78 o -4 2 1 9769.76 10057.93 247.21 o -3 2 1 2449.53 2650.13 30.41 o -2 2 1 43647.81 50050.64 422.72 o -1 2 1 18.13 42.45 3.03 o 0 2 1 324.29 308.48 5.98 o 1 2 1 136.38 132.79 4.28 o 2 2 1 7822.43 8954.75 82.14 o 3 2 1 18946.18 20863.65 183.89 o 4 2 1 10001.78 10748.11 186.66 o 5 2 1 1395.21 1278.24 39.78 o 6 2 1 3035.87 2953.17 36.48 o 7 2 1 2103.46 2105.05 45.04 o 8 2 1 519.19 492.19 46.82 o 9 2 1 253.40 289.22 17.03 o 10 2 1 4001.36 4317.47 118.52 o 11 2 1 94.42 102.29 15.34 o 12 2 1 79.60 76.87 18.10 o -12 3 1 405.58 392.22 21.76 o -11 3 1 2418.55 2255.94 118.34 o -10 3 1 369.60 405.78 32.19 o -9 3 1 1168.22 1125.12 29.97 o -8 3 1 490.40 559.88 48.34 o -7 3 1 340.59 375.90 27.56 o -6 3 1 2373.38 2240.96 34.60 o -5 3 1 6202.09 6114.67 65.19 o -4 3 1 3124.68 3308.74 95.69 o -3 3 1 19500.52 21183.46 186.66 o -2 3 1 2.85 3.48 2.85 o -1 3 1 27.97 40.76 3.92 o 0 3 1 14223.96 16132.46 131.54 o 1 3 1 875.45 810.93 34.07 o 2 3 1 532.95 580.84 11.24 o 3 3 1 1674.69 1790.95 24.17 o 4 3 1 3.75 10.70 2.94 o 5 3 1 306.02 360.65 21.05 o 6 3 1 3173.98 3191.19 42.00 o 7 3 1 428.90 391.06 31.39 o 8 3 1 459.75 475.43 19.62 o 9 3 1 2224.01 2152.23 43.07 o 10 3 1 78.99 120.93 28.18 o 11 3 1 1216.60 1168.91 37.99 o 12 3 1 359.27 371.00 28.27 o -12 4 1 378.61 427.45 22.92 o -11 4 1 3.39 13.11 10.17 o -10 4 1 1893.94 1946.04 62.52 o -9 4 1 1271.32 1187.37 27.91 o -8 4 1 2910.11 2873.26 103.90 o -7 4 1 4794.86 5052.78 150.00 o -6 4 1 2382.35 2205.38 31.21 o -5 4 1 1328.68 1153.92 52.26 o -4 4 1 3096.68 3220.71 39.51 o -3 4 1 720.10 708.37 14.00 o -2 4 1 288.29 334.16 7.49 o -1 4 1 4508.67 4558.80 46.82 o 0 4 1 66.19 54.40 4.19 o 1 4 1 4709.50 4930.42 126.28 o 2 4 1 237.58 237.58 6.51 o 3 4 1 791.15 899.84 16.41 o 4 4 1 5643.47 5962.61 63.68 o 5 4 1 9886.74 10136.86 101.22 o 6 4 1 3043.41 3030.04 36.83 o 7 4 1 2642.39 2642.28 58.68 o 8 4 1 0.22 9.54 8.65 o 9 4 1 635.23 646.48 24.08 o 10 4 1 1371.94 1296.08 52.44 o 11 4 1 622.11 791.58 75.18 o 12 4 1 408.11 458.31 26.40 o -12 5 1 329.81 348.70 21.05 o -11 5 1 80.20 82.05 13.91 o -10 5 1 1338.51 1340.05 52.53 o -9 5 1 371.70 348.88 18.10 o -8 5 1 2242.74 2469.89 95.51 o -7 5 1 3257.18 3333.44 112.10 o -6 5 1 6008.10 6042.87 74.38 o -5 5 1 65.11 53.33 7.13 o -4 5 1 76.14 87.67 7.49 o -3 5 1 751.69 690.09 12.40 o -2 5 1 15176.05 16019.11 135.11 o -1 5 1 23.41 20.51 4.01 o 0 5 1 43413.25 48311.51 385.00 o 1 5 1 4062.90 4150.79 41.56 o 2 5 1 675.18 690.00 14.09 o 3 5 1 2622.58 2719.07 34.60 o 4 5 1 2183.99 2207.61 31.48 o 5 5 1 312.13 267.19 11.15 o 6 5 1 5164.29 4928.81 59.66 o 7 5 1 2123.22 2112.99 100.24 o 8 5 1 1020.48 966.11 27.56 o 9 5 1 70.08 98.55 13.11 o 10 5 1 335.89 298.05 30.32 o 11 5 1 0.95 9.72 10.26 o 12 5 1 663.81 664.58 31.48 o -12 6 1 184.28 147.15 18.82 o -11 6 1 28.97 30.86 12.22 o -10 6 1 636.56 561.31 47.98 o -9 6 1 316.36 355.57 18.91 o -8 6 1 674.74 652.37 48.60 o -7 6 1 950.96 902.25 52.97 o -6 6 1 3731.29 3644.51 52.53 o -5 6 1 574.20 577.36 16.32 o -4 6 1 5309.09 5420.92 61.00 o -3 6 1 5441.34 5236.76 55.92 o -2 6 1 4385.34 4496.64 45.84 o -1 6 1 11343.99 11762.73 102.92 o 0 6 1 3032.31 2866.13 32.19 o 1 6 1 9780.51 10189.74 90.88 o 2 6 1 7774.40 8002.20 74.20 o 3 6 1 4593.45 4793.44 49.14 o 4 6 1 3485.12 3323.09 43.07 o 5 6 1 2532.01 2336.74 35.41 o 6 6 1 1126.42 1094.53 23.81 o 7 6 1 2022.24 1887.98 33.71 o 8 6 1 180.74 186.21 16.14 o 9 6 1 207.02 175.87 15.34 o 10 6 1 729.41 867.38 56.45 o 11 6 1 7.31 15.43 11.15 o -11 7 1 317.71 361.19 26.04 o -10 7 1 295.27 249.62 30.68 o -9 7 1 445.03 428.96 23.10 o -8 7 1 435.77 388.92 16.59 o -7 7 1 0.28 -6.15 6.15 o -6 7 1 582.36 642.20 18.82 o -5 7 1 6100.89 6127.69 75.18 o -4 7 1 111.44 149.47 9.99 o -3 7 1 11325.62 11756.58 120.75 o -2 7 1 359.77 312.14 9.45 o -1 7 1 3756.05 3804.41 41.38 o 0 7 1 86.34 103.90 6.42 o 1 7 1 4620.73 4543.46 56.27 o 2 7 1 361.65 348.26 10.43 o 3 7 1 10386.31 10404.58 95.51 o 4 7 1 1974.50 1914.02 30.95 o 5 7 1 5859.49 5757.67 67.69 o 6 7 1 528.40 552.93 17.66 o 7 7 1 954.13 967.44 50.66 o 8 7 1 6.72 30.68 9.54 o 9 7 1 819.39 803.08 27.74 o 10 7 1 283.46 349.95 34.42 o 11 7 1 94.02 85.17 15.34 o -11 8 1 44.43 42.36 13.56 o -10 8 1 1211.72 1101.22 51.64 o -9 8 1 981.50 1018.46 35.14 o -8 8 1 163.86 179.79 18.91 o -7 8 1 447.40 461.87 19.08 o -6 8 1 853.73 834.47 24.88 o -5 8 1 22.14 30.32 7.85 o -4 8 1 4198.78 4126.44 55.20 o -3 8 1 606.32 657.27 14.98 o -2 8 1 3490.21 3535.35 40.67 o -1 8 1 860.33 719.16 15.07 o 0 8 1 2.04 6.06 5.17 o 1 8 1 32.15 16.23 4.73 o 2 8 1 6734.53 6590.63 66.26 o 3 8 1 4964.99 5064.01 54.22 o 4 8 1 2032.96 2003.29 32.73 o 5 8 1 221.29 244.98 13.56 o 6 8 1 449.56 467.31 16.86 o 7 8 1 1055.74 939.17 75.09 o 8 8 1 634.27 609.38 26.84 o 9 8 1 873.45 837.42 32.91 o 10 8 1 900.69 822.61 45.57 o 11 8 1 118.50 142.60 19.08 o -11 9 1 84.02 28.00 48.25 o -10 9 1 535.98 650.76 55.47 o -9 9 1 677.69 598.50 29.16 o -8 9 1 2917.56 2918.21 61.71 o -7 9 1 452.93 442.52 19.80 o -6 9 1 832.88 827.61 27.74 o -5 9 1 248.54 252.30 16.23 o -4 9 1 199.58 185.94 14.45 o -3 9 1 899.19 911.44 20.96 o -2 9 1 946.78 918.39 18.10 o -1 9 1 4.91 17.93 5.44 o 0 9 1 1208.96 1185.41 20.78 o 1 9 1 184.01 199.59 9.72 o 2 9 1 1286.53 1219.03 21.67 o 3 9 1 995.24 954.16 20.24 o 4 9 1 523.89 522.78 16.77 o 5 9 1 293.32 321.95 14.72 o 6 9 1 2289.81 2277.79 43.34 o 7 9 1 40.76 53.24 41.47 o 8 9 1 1804.72 1750.10 46.73 o 9 9 1 465.15 469.45 25.77 o 10 9 1 2.03 33.98 26.84 o -10 10 1 459.85 533.13 39.69 o -9 10 1 1486.26 1580.30 52.35 o -8 10 1 184.39 188.35 19.98 o -7 10 1 1291.70 1273.78 33.35 o -6 10 1 27.60 41.56 11.86 o -5 10 1 502.15 507.44 20.33 o -4 10 1 1.23 10.61 8.03 o -3 10 1 1245.56 1129.58 24.88 o -2 10 1 1111.94 1068.76 23.63 o -1 10 1 1795.74 1766.25 64.84 o 0 10 1 1548.46 1577.09 25.95 o 1 10 1 1674.26 1787.20 72.15 o 2 10 1 873.20 906.00 19.62 o 3 10 1 424.49 458.75 17.39 o 4 10 1 342.88 342.28 17.21 o 5 10 1 2531.43 2424.32 45.39 o 6 10 1 534.07 522.52 24.97 o 7 10 1 1318.78 1247.48 89.72 o 8 10 1 179.55 201.55 20.60 o 9 10 1 220.51 238.12 20.96 o 10 10 1 331.23 330.86 34.60 o -9 11 1 600.11 607.77 33.71 o -8 11 1 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o -2 6 19 65.57 132.70 50.83 o -1 6 19 482.39 515.11 46.82 o 0 6 19 197.67 211.00 23.01 o -3 7 19 77.85 63.23 18.46 o -2 7 19 36.95 63.85 14.80 o -6 0 20 5.03 8.92 17.39 o 5 0 17 16.42 177.83 58.50 o -4 0 20 849.55 965.48 62.16 o -2 0 20 117.21 114.96 28.89 o 1 0 19 1.93 46.11 41.11 o 0 0 20 43.29 36.21 23.19 o -6 1 20 192.79 206.90 18.46 o -5 1 20 278.16 348.52 45.30 o -4 1 20 181.78 204.67 26.58 o -3 1 20 599.88 609.20 26.75 o -2 1 20 122.18 242.31 50.03 o -1 1 20 81.25 119.86 43.88 o 0 1 20 43.42 57.25 16.32 o 1 1 20 166.79 190.85 24.97 o -6 2 20 63.17 86.68 19.98 o -5 2 20 464.46 619.72 73.66 o -4 2 20 127.92 108.45 28.63 o -3 2 20 179.48 223.76 18.82 o -2 2 20 304.54 385.80 59.22 o -1 2 20 198.24 262.55 54.49 o 0 2 20 113.18 108.09 19.44 o -5 3 20 24.69 34.25 14.45 o -4 3 20 16.36 44.06 25.86 o -3 3 20 29.78 88.91 14.18 o -2 3 20 93.94 244.18 35.41 o -1 3 20 371.62 486.84 44.23 o 0 3 20 982.73 999.55 43.16 o -5 4 20 9.86 9.90 25.60 o -4 4 20 417.80 468.20 39.78 o -3 4 20 132.14 116.74 19.53 o -2 4 20 75.75 169.80 32.73 o -1 4 20 6.79 4.37 24.79 o -3 5 20 545.93 679.48 49.94 o -2 5 20 113.23 67.78 19.89 o