#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/84/2238458.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238458_Fobs loop_ _publ_author_name 'Ishikawa, Yoshinobu' 'Matsuo, Soichiro' _publ_section_title ; 2-(Benzyloxy)isoquinoline-1,3(2H,4H)-dione ; _journal_coeditor_code ZL2556 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1311 _journal_volume 69 _journal_year 2013 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6768 _cell_length_b 12.0027 _cell_length_c 13.8854 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7688 _[local]_cod_data_source_file zl2556Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2-(benzyloxy)isoquinoline-1,3(4H)-dione' _shelx_refln_list_code 4 _shelx_f_calc_maximum 130.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' '-x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -17 31.71 -5.39 30.81 o 0 1 -17 34.35 80.88 21.70 o 1 1 -17 93.94 191.86 22.10 o 2 1 -17 29.24 35.02 21.66 o 3 1 -17 7.30 27.01 23.04 o 1 2 -17 1.44 -0.20 29.88 o 2 2 -17 66.06 142.84 22.67 o 3 2 -17 26.16 16.12 25.39 o 0 3 -17 20.27 39.83 21.09 o 1 3 -17 2.91 -29.84 29.84 o 2 3 -17 19.06 19.03 30.57 o 1 4 -17 5.40 -31.54 31.54 o 2 4 -17 11.34 -14.50 31.26 o 0 5 -17 38.97 55.34 22.79 o 1 5 -17 1.96 -4.70 31.46 o 0 0 -16 103.75 149.71 21.47 o 2 0 -16 12.67 5.74 27.46 o 4 0 -16 40.32 52.21 16.04 o 1 1 -16 19.22 -2.10 27.94 o 2 1 -16 3.21 -11.65 28.71 o 3 1 -16 54.58 52.48 15.59 o 4 1 -16 4.71 20.25 21.99 o 0 2 -16 14.68 47.75 19.12 o 1 2 -16 2.16 -20.42 28.51 o 2 2 -16 16.62 33.85 29.19 o 3 2 -16 19.12 38.23 14.90 o 4 2 -16 1.82 8.30 22.48 o 1 3 -16 31.89 33.73 28.55 o 2 3 -16 6.69 33.12 28.30 o 3 3 -16 12.45 -1.26 22.11 o 4 3 -16 14.55 -13.16 23.73 o 0 4 -16 6.14 38.50 29.51 o 1 4 -16 17.48 24.21 28.10 o 2 4 -16 98.84 142.32 22.39 o 3 4 -16 32.47 66.94 16.81 o 1 5 -16 10.26 61.74 20.16 o 2 5 -16 7.44 -7.73 22.06 o 3 5 -16 12.35 10.69 24.50 o 0 6 -16 19.85 22.71 29.63 o 1 6 -16 43.39 64.74 22.31 o 2 6 -16 23.78 32.47 22.11 o 1 7 -16 30.91 59.96 22.39 o 2 0 -15 79.53 67.37 20.22 o 4 0 -15 78.18 47.87 15.35 o 0 1 -15 39.09 51.99 19.49 o 1 1 -15 20.90 35.46 26.20 o 2 1 -15 25.76 42.83 18.81 o 3 1 -15 14.47 -15.33 28.92 o 4 1 -15 3.44 -3.44 22.07 o 5 1 -15 14.97 -11.75 22.36 o 1 2 -15 22.74 -17.02 27.98 o 2 2 -15 5.06 -27.54 27.54 o 3 2 -15 22.33 6.31 28.51 o 4 2 -15 13.83 13.16 21.55 o 5 2 -15 8.88 13.16 21.91 o 0 3 -15 26.47 29.76 27.78 o 1 3 -15 14.90 26.85 24.79 o 2 3 -15 4.04 -1.45 27.99 o 3 3 -15 13.68 23.14 27.30 o 4 3 -15 5.47 21.67 14.70 o 5 3 -15 0.01 18.07 19.89 o 1 4 -15 7.40 35.34 27.29 o 2 4 -15 4.85 -29.40 29.40 o 3 4 -15 3.59 -12.07 22.48 o 4 4 -15 20.75 23.09 21.34 o 0 5 -15 74.37 125.99 20.18 o 1 5 -15 11.90 36.72 27.82 o 2 5 -15 3.35 12.09 27.54 o 3 5 -15 0.91 29.48 14.01 o 4 5 -15 20.50 60.27 15.11 o 1 6 -15 16.15 8.78 27.73 o 2 6 -15 5.41 6.03 28.87 o 3 6 -15 18.70 31.26 15.79 o 4 6 -15 20.75 38.96 16.16 o 0 7 -15 14.93 16.11 29.35 o 1 7 -15 46.84 112.31 21.94 o 2 7 -15 37.08 56.16 21.79 o 3 7 -15 0.34 2.67 22.60 o 1 8 -15 10.67 -31.13 31.13 o 2 8 -15 9.08 -10.81 33.29 o 0 0 -14 182.24 225.91 18.94 o 2 0 -14 0.10 25.29 23.60 o 4 0 -14 30.76 -0.40 27.55 o 6 0 -14 8.20 3.48 21.35 o 1 1 -14 22.78 6.63 24.60 o 2 1 -14 32.28 36.72 17.49 o 3 1 -14 47.77 -9.55 28.80 o 4 1 -14 40.44 20.02 27.47 o 5 1 -14 26.18 27.54 15.48 o 6 1 -14 1.25 -13.41 23.30 o 0 2 -14 144.19 168.92 18.90 o 1 2 -14 70.24 106.53 17.41 o 2 2 -14 51.25 54.94 17.90 o 3 2 -14 10.48 38.50 17.51 o 4 2 -14 1.38 -28.24 28.24 o 5 2 -14 1.77 19.89 14.99 o 6 2 -14 17.49 4.66 21.88 o 1 3 -14 6.21 -14.54 24.03 o 2 3 -14 6.95 1.13 24.20 o 3 3 -14 16.45 19.90 19.01 o 4 3 -14 29.79 -24.19 30.50 o 5 3 -14 37.99 24.51 15.19 o 6 3 -14 3.26 -13.49 21.63 o 0 4 -14 78.22 94.19 18.46 o 1 4 -14 10.45 2.99 25.69 o 2 4 -14 7.84 21.07 24.47 o 3 4 -14 32.70 23.10 26.81 o 4 4 -14 18.19 15.50 27.71 o 5 4 -14 9.77 23.17 19.36 o 1 5 -14 9.92 50.22 17.19 o 2 5 -14 14.32 22.00 26.69 o 3 5 -14 24.91 25.65 19.70 o 4 5 -14 18.87 14.34 22.03 o 5 5 -14 33.83 28.68 23.78 o 0 6 -14 3.02 -5.01 27.86 o 1 6 -14 3.24 15.00 27.74 o 2 6 -14 4.29 -28.55 28.55 o 3 6 -14 16.27 7.81 28.60 o 4 6 -14 2.83 9.11 21.22 o 5 6 -14 46.93 60.64 16.93 o 1 7 -14 5.32 -15.08 26.28 o 2 7 -14 19.30 5.47 29.07 o 3 7 -14 48.94 76.94 15.87 o 4 7 -14 5.47 -7.33 23.37 o 0 8 -14 41.82 46.51 20.44 o 1 8 -14 1.16 -28.82 28.82 o 2 8 -14 10.31 40.21 29.88 o 3 8 -14 41.27 14.34 24.98 o 1 9 -14 27.84 60.00 21.21 o 2 9 -14 4.77 -30.69 30.69 o 2 0 -13 62.27 86.33 15.48 o 4 0 -13 82.72 24.61 26.35 o 6 0 -13 2.53 22.65 19.77 o 0 1 -13 7.79 -6.04 18.81 o 1 1 -13 20.44 12.90 20.72 o 2 1 -13 54.89 57.37 15.76 o 3 1 -13 50.52 16.28 23.92 o 4 1 -13 79.83 27.52 25.98 o 5 1 -13 18.55 7.60 27.11 o 6 1 -13 33.21 -7.78 21.96 o 1 2 -13 95.98 111.60 15.27 o 2 2 -13 47.72 10.46 24.12 o 3 2 -13 84.91 17.94 25.01 o 4 2 -13 87.39 49.68 18.53 o 5 2 -13 11.38 20.47 19.06 o 6 2 -13 28.82 26.25 22.89 o 0 3 -13 46.02 64.67 15.95 o 1 3 -13 114.74 117.96 17.90 o 2 3 -13 59.06 66.17 16.28 o 3 3 -13 7.69 -20.85 24.65 o 4 3 -13 5.98 19.13 25.08 o 5 3 -13 14.24 27.83 19.70 o 6 3 -13 35.22 13.82 23.78 o 1 4 -13 1.32 27.47 22.38 o 2 4 -13 18.70 30.34 24.16 o 3 4 -13 46.59 20.77 26.26 o 4 4 -13 39.21 36.04 19.30 o 5 4 -13 1.87 34.87 26.05 o 6 4 -13 28.98 -10.53 23.34 o 0 5 -13 50.80 21.57 24.07 o 1 5 -13 82.85 87.26 17.25 o 2 5 -13 81.00 90.17 18.22 o 3 5 -13 8.81 -16.70 27.14 o 4 5 -13 13.67 -10.15 26.74 o 5 5 -13 61.35 32.21 16.81 o 6 5 -13 14.77 -16.81 24.39 o 1 6 -13 53.22 75.02 17.69 o 2 6 -13 79.10 79.91 19.49 o 3 6 -13 34.69 66.62 19.41 o 4 6 -13 129.86 136.12 21.72 o 5 6 -13 75.71 73.61 17.13 o 0 7 -13 58.37 33.68 28.46 o 1 7 -13 23.45 26.85 27.17 o 2 7 -13 0.37 27.22 26.17 o 3 7 -13 87.81 121.91 20.18 o 4 7 -13 0.99 20.49 20.25 o 5 7 -13 21.57 26.45 24.55 o 1 8 -13 9.95 36.55 27.17 o 2 8 -13 11.38 -27.26 29.24 o 3 8 -13 14.68 10.98 20.65 o 4 8 -13 18.22 7.21 22.64 o 0 9 -13 88.95 86.91 21.82 o 1 9 -13 5.74 26.43 27.04 o 2 9 -13 53.66 58.19 21.38 o 3 9 -13 4.87 15.47 21.10 o 1 10 -13 68.22 57.45 22.27 o 2 10 -13 40.99 62.60 21.83 o 0 0 -12 124.75 103.64 14.06 o 2 0 -12 803.00 573.25 28.02 o 4 0 -12 526.72 318.50 29.25 o 6 0 -12 81.06 6.15 27.51 o 1 1 -12 168.76 171.59 15.31 o 2 1 -12 135.99 120.35 15.52 o 3 1 -12 410.41 252.00 18.07 o 4 1 -12 158.14 125.55 17.22 o 5 1 -12 110.66 79.86 19.14 o 6 1 -12 266.48 158.16 22.01 o 7 1 -12 2.57 9.52 21.11 o 0 2 -12 804.81 1089.61 33.48 o 1 2 -12 264.45 326.25 23.58 o 2 2 -12 277.90 262.67 24.28 o 3 2 -12 130.04 122.71 16.06 o 4 2 -12 58.43 26.83 25.05 o 5 2 -12 57.16 -7.97 27.43 o 6 2 -12 97.32 89.54 20.59 o 7 2 -12 9.17 -4.78 23.22 o 1 3 -12 28.87 43.86 13.62 o 2 3 -12 78.37 67.95 13.91 o 3 3 -12 168.57 143.51 17.49 o 4 3 -12 21.49 35.60 16.12 o 5 3 -12 70.01 55.51 20.11 o 6 3 -12 57.25 63.36 15.60 o 7 3 -12 96.22 33.71 25.61 o 0 4 -12 94.29 102.17 13.30 o 1 4 -12 415.58 543.98 28.30 o 2 4 -12 15.17 40.17 13.19 o 3 4 -12 19.68 44.36 16.24 o 4 4 -12 23.36 50.91 16.57 o 5 4 -12 40.82 16.02 28.32 o 6 4 -12 51.50 24.35 22.69 o 7 4 -12 53.42 52.59 16.65 o 1 5 -12 8.63 3.11 20.84 o 2 5 -12 13.23 2.71 21.94 o 3 5 -12 51.95 35.15 17.66 o 4 5 -12 3.73 -12.74 25.77 o 5 5 -12 5.04 18.85 26.94 o 6 5 -12 8.28 -22.97 22.97 o 0 6 -12 20.83 21.33 16.32 o 1 6 -12 34.87 -5.17 23.91 o 2 6 -12 19.94 42.54 16.56 o 3 6 -12 5.11 -13.90 24.93 o 4 6 -12 36.07 79.00 18.53 o 5 6 -12 5.98 15.39 20.90 o 6 6 -12 13.54 19.08 15.60 o 1 7 -12 21.09 14.46 23.47 o 2 7 -12 94.88 109.97 18.50 o 3 7 -12 42.84 26.94 19.17 o 4 7 -12 7.94 14.56 28.28 o 5 7 -12 13.58 14.95 21.84 o 0 8 -12 92.15 72.05 19.00 o 1 8 -12 46.77 99.84 19.25 o 2 8 -12 10.11 32.03 26.57 o 3 8 -12 118.66 142.46 21.15 o 4 8 -12 28.64 52.25 15.43 o 5 8 -12 5.91 9.56 22.16 o 1 9 -12 8.58 -5.01 26.41 o 2 9 -12 8.76 24.31 27.50 o 3 9 -12 9.59 -20.86 20.86 o 4 9 -12 19.49 58.94 15.11 o 0 10 -12 27.47 39.63 27.53 o 1 10 -12 11.39 -2.43 28.10 o 2 10 -12 9.42 -15.71 29.84 o 3 10 -12 1.02 -23.77 23.77 o 1 11 -12 34.99 35.67 31.62 o 2 11 -12 26.98 -32.60 32.60 o 2 0 -11 869.81 703.53 27.66 o 4 0 -11 465.89 254.32 24.78 o 6 0 -11 26.81 12.10 26.99 o 0 1 -11 1060.03 1322.89 33.48 o 1 1 -11 580.67 684.32 26.39 o 2 1 -11 407.40 329.29 23.79 o 3 1 -11 81.00 50.71 14.44 o 4 1 -11 102.45 51.41 15.45 o 5 1 -11 126.90 77.51 17.66 o 6 1 -11 66.93 30.83 19.78 o 7 1 -11 73.70 47.20 15.56 o 1 2 -11 39.98 62.71 13.46 o 2 2 -11 279.24 319.32 23.47 o 3 2 -11 55.80 65.31 13.84 o 4 2 -11 213.03 130.08 15.98 o 5 2 -11 34.14 25.66 16.69 o 6 2 -11 77.34 65.34 20.72 o 7 2 -11 81.67 63.33 15.48 o 0 3 -11 603.19 807.87 28.96 o 1 3 -11 663.85 823.83 30.23 o 2 3 -11 458.78 535.41 26.21 o 3 3 -11 543.77 472.18 27.11 o 4 3 -11 170.25 136.82 17.50 o 5 3 -11 44.23 31.56 17.74 o 6 3 -11 31.06 27.03 27.84 o 7 3 -11 23.60 29.78 19.89 o 1 4 -11 188.29 222.70 15.32 o 2 4 -11 250.23 295.11 24.72 o 3 4 -11 370.82 321.13 26.14 o 4 4 -11 153.09 158.04 17.58 o 5 4 -11 205.28 203.66 19.48 o 6 4 -11 1.60 3.16 28.16 o 7 4 -11 50.58 79.29 16.45 o 0 5 -11 177.61 221.40 21.88 o 1 5 -11 10.71 20.36 18.02 o 2 5 -11 287.45 393.99 26.94 o 3 5 -11 201.46 232.65 18.83 o 4 5 -11 143.16 132.42 18.99 o 5 5 -11 38.72 2.18 26.82 o 6 5 -11 110.89 83.76 20.51 o 7 5 -11 17.97 30.03 21.92 o 1 6 -11 417.21 481.68 27.21 o 2 6 -11 50.83 50.94 16.48 o 3 6 -11 102.66 124.16 17.49 o 4 6 -11 66.71 79.08 18.31 o 5 6 -11 17.18 9.63 27.31 o 6 6 -11 79.39 57.77 16.89 o 0 7 -11 295.39 333.48 29.08 o 1 7 -11 47.01 56.47 16.64 o 2 7 -11 10.25 -2.10 23.27 o 3 7 -11 59.88 74.42 18.14 o 4 7 -11 3.17 20.95 25.61 o 5 7 -11 75.64 86.29 20.55 o 6 7 -11 40.47 56.07 15.76 o 1 8 -11 28.37 38.50 16.93 o 2 8 -11 2.83 -5.41 25.45 o 3 8 -11 9.30 -13.35 25.85 o 4 8 -11 4.26 -2.10 29.21 o 5 8 -11 55.42 74.25 16.73 o 6 8 -11 46.16 52.47 17.46 o 0 9 -11 50.13 56.56 19.89 o 1 9 -11 34.62 57.01 18.08 o 2 9 -11 67.53 104.02 19.58 o 3 9 -11 140.93 128.79 22.25 o 4 9 -11 89.50 110.62 16.93 o 5 9 -11 50.92 60.93 15.84 o 1 10 -11 23.26 27.17 26.65 o 2 10 -11 85.67 98.48 20.14 o 3 10 -11 6.50 -0.20 21.10 o 4 10 -11 0.65 11.95 20.82 o 0 11 -11 41.48 20.81 28.34 o 1 11 -11 16.06 0.41 29.40 o 2 11 -11 2.13 -19.80 29.76 o 3 11 -11 5.58 -22.68 22.68 o 1 12 -11 16.41 21.58 29.52 o 0 0 -10 91.22 98.80 11.76 o 2 0 -10 1.28 -8.87 17.50 o 4 0 -10 349.56 186.16 16.06 o 6 0 -10 149.86 130.83 18.96 o 8 0 -10 32.14 65.49 14.10 o 1 1 -10 22.33 32.69 11.77 o 2 1 -10 114.34 99.75 13.30 o 3 1 -10 89.62 62.44 13.47 o 4 1 -10 234.84 138.38 15.29 o 5 1 -10 128.24 73.03 17.09 o 6 1 -10 166.68 146.26 18.55 o 7 1 -10 46.94 42.00 19.91 o 8 1 -10 65.70 50.13 16.74 o 0 2 -10 535.34 632.80 24.74 o 1 2 -10 604.79 691.64 27.04 o 2 2 -10 122.89 150.49 13.83 o 3 2 -10 24.31 16.98 18.84 o 4 2 -10 86.36 47.75 14.65 o 5 2 -10 140.55 111.05 16.85 o 6 2 -10 3.59 -21.50 25.54 o 7 2 -10 160.82 109.95 22.18 o 8 2 -10 34.15 55.93 16.13 o 1 3 -10 147.63 193.76 13.78 o 2 3 -10 233.94 294.72 22.70 o 3 3 -10 345.53 290.03 22.91 o 4 3 -10 9.29 -13.84 20.74 o 5 3 -10 30.37 18.02 22.79 o 6 3 -10 33.54 59.15 18.04 o 7 3 -10 21.41 36.02 29.18 o 8 3 -10 90.47 72.42 17.10 o 0 4 -10 1418.41 1732.94 37.79 o 1 4 -10 109.18 127.89 13.98 o 2 4 -10 542.49 751.78 28.80 o 3 4 -10 49.74 66.52 14.36 o 4 4 -10 119.86 95.13 15.74 o 5 4 -10 144.84 139.92 17.98 o 6 4 -10 24.61 15.05 26.10 o 7 4 -10 24.18 16.57 21.56 o 1 5 -10 147.78 215.54 20.80 o 2 5 -10 431.03 492.07 25.73 o 3 5 -10 454.53 548.77 27.48 o 4 5 -10 554.29 530.52 31.03 o 5 5 -10 21.12 18.27 17.09 o 6 5 -10 162.26 150.15 21.28 o 7 5 -10 16.75 -10.33 21.84 o 0 6 -10 95.68 97.50 13.13 o 1 6 -10 80.59 113.76 13.63 o 2 6 -10 93.16 96.55 14.48 o 3 6 -10 168.01 224.21 17.07 o 4 6 -10 121.11 92.25 18.55 o 5 6 -10 377.24 368.32 32.73 o 6 6 -10 68.74 109.05 20.19 o 7 6 -10 62.97 65.44 16.33 o 1 7 -10 539.50 665.69 28.94 o 2 7 -10 147.53 147.41 16.49 o 3 7 -10 138.79 196.97 18.30 o 4 7 -10 130.71 136.42 18.63 o 5 7 -10 131.66 152.00 20.92 o 6 7 -10 24.19 4.25 20.99 o 7 7 -10 78.69 81.04 16.98 o 0 8 -10 20.22 2.02 22.66 o 1 8 -10 408.88 386.67 29.53 o 2 8 -10 285.06 337.62 28.00 o 3 8 -10 88.70 97.86 19.31 o 4 8 -10 35.37 -2.75 27.63 o 5 8 -10 10.08 -17.60 29.17 o 6 8 -10 61.26 33.14 24.63 o 1 9 -10 56.93 87.70 17.94 o 2 9 -10 20.05 46.18 17.29 o 3 9 -10 46.23 45.14 19.70 o 4 9 -10 4.61 41.58 19.01 o 5 9 -10 0.34 13.73 21.03 o 6 9 -10 13.01 17.30 23.34 o 0 10 -10 50.47 65.70 18.92 o 1 10 -10 5.81 -5.70 26.97 o 2 10 -10 88.29 88.41 20.59 o 3 10 -10 75.65 61.24 20.47 o 4 10 -10 2.26 20.45 19.85 o 5 10 -10 47.35 60.24 15.92 o 1 11 -10 18.82 -2.34 28.43 o 2 11 -10 47.82 56.89 20.94 o 3 11 -10 43.55 65.53 16.28 o 4 11 -10 2.51 -4.90 21.35 o 0 12 -10 27.09 13.72 29.75 o 1 12 -10 2.81 -17.49 30.49 o 2 12 -10 7.36 34.38 28.99 o 3 12 -10 42.07 -15.79 24.86 o 2 0 -9 98.02 69.15 12.26 o 4 0 -9 40.67 27.00 19.33 o 6 0 -9 605.78 403.27 30.92 o 8 0 -9 192.30 99.65 17.95 o 0 1 -9 165.29 194.57 16.39 o 1 1 -9 11.40 10.76 14.71 o 2 1 -9 195.91 166.68 13.14 o 3 1 -9 81.76 79.39 13.03 o 4 1 -9 251.12 151.74 15.17 o 5 1 -9 127.84 115.42 15.95 o 6 1 -9 45.90 20.74 23.16 o 7 1 -9 70.66 44.06 19.18 o 8 1 -9 11.12 13.70 20.75 o 1 2 -9 126.53 142.43 12.01 o 2 2 -9 109.81 84.96 12.91 o 3 2 -9 31.23 33.56 12.95 o 4 2 -9 258.62 150.58 15.94 o 5 2 -9 163.10 129.83 16.07 o 6 2 -9 51.45 45.51 17.14 o 7 2 -9 29.95 20.07 27.12 o 8 2 -9 42.63 66.75 16.53 o 0 3 -9 611.66 775.28 25.34 o 1 3 -9 539.09 735.48 25.43 o 2 3 -9 44.38 27.01 18.27 o 3 3 -9 149.59 128.86 14.28 o 4 3 -9 183.06 104.13 15.18 o 5 3 -9 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111.74 90.75 18.11 o 0 14 0 11.47 7.20 27.05 o 1 14 0 0.60 -3.56 26.45 o 2 14 0 87.17 78.84 15.63 o 3 14 0 56.59 49.05 15.39 o 4 14 0 58.02 28.80 23.98 o 1 15 0 0.01 28.38 29.07 o 2 15 0 75.26 32.36 24.22 o 2 0 1 2087.50 2101.13 18.16 o 4 0 1 33.47 37.74 8.43 o 2 1 1 14087.41 13792.19 436.54 o 3 1 1 1367.42 1395.64 46.42 o 4 1 1 40.82 43.72 4.31 o 5 1 1 153.79 191.24 8.27 o 2 2 1 17030.08 16915.87 674.32 o 3 2 1 515.39 471.43 20.05 o 4 2 1 539.14 567.39 32.86 o 5 2 1 721.38 762.05 12.59 o 0 3 1 613.03 638.43 9.86 o 1 3 1 231.34 227.39 10.39 o 2 3 1 12.49 8.28 4.99 o 3 3 1 729.00 761.42 51.10 o 4 3 1 762.70 802.27 69.87 o 5 3 1 1351.26 1459.30 43.02 o 1 4 1 187.82 190.87 7.41 o 2 4 1 1658.10 1550.98 79.85 o 3 4 1 968.00 956.03 69.49 o 4 4 1 797.21 747.78 47.67 o 0 5 1 3689.75 3673.66 39.77 o 1 5 1 305.53 308.33 7.12 o 2 5 1 806.23 772.01 28.37 o 3 5 1 55.86 57.40 6.41 o 4 5 1 158.08 189.66 8.80 o 1 6 1 542.81 582.12 12.96 o 2 6 1 63.51 65.99 4.48 o 3 6 1 294.88 277.56 17.11 o 4 6 1 66.93 66.42 9.45 o 0 7 1 246.51 263.75 11.27 o 1 7 1 1012.79 1015.71 12.35 o 2 7 1 244.29 225.26 8.56 o 3 7 1 13.42 23.67 9.49 o 1 8 1 97.69 95.22 9.32 o 2 8 1 115.77 122.18 8.02 o 2 0 2 2501.36 2147.03 24.00 o 4 0 2 595.50 719.49 64.35 o 2 1 2 929.05 838.61 68.47 o 3 1 2 185.65 191.53 13.84 o 4 1 2 122.89 138.82 14.04 o 5 1 2 82.30 86.18 5.59 o 1 2 2 477.11 439.52 42.60 o 2 2 2 160.61 149.06 15.28 o 3 2 2 456.58 455.47 41.06 o 4 2 2 357.30 403.03 45.03 o 5 2 2 326.74 346.40 18.83 o 1 3 2 156.20 139.70 10.17 o 2 3 2 165.13 126.95 15.38 o 3 3 2 939.63 831.03 89.97 o 4 3 2 983.15 937.80 107.86 o 5 3 2 138.10 169.76 14.97 o 0 4 2 3524.97 3578.25 45.80 o 1 4 2 1531.95 1595.29 27.23 o 2 4 2 200.66 191.22 15.58 o 3 4 2 468.47 467.22 39.81 o 4 4 2 227.28 224.15 16.68 o 1 5 2 723.12 733.71 11.11 o 2 5 2 12.13 10.66 5.15 o 3 5 2 707.22 666.53 57.51 o 4 5 2 76.48 76.02 8.08 o 0 6 2 1758.28 1833.23 65.10 o 1 6 2 1470.80 1472.47 13.39 o 2 6 2 340.52 343.96 8.55 o 3 6 2 39.70 36.98 4.97 o 1 7 2 314.36 349.66 8.85 o 2 7 2 139.01 136.60 7.74 o 3 7 2 75.60 86.35 7.04 o 0 8 2 363.50 424.73 14.37 o 1 8 2 92.11 98.63 5.64 o 2 0 3 145.01 137.40 11.72 o 4 0 3 46.20 49.80 13.83 o 1 1 3 2190.82 1700.38 158.80 o 2 1 3 455.07 363.98 31.75 o 3 1 3 43.20 42.62 5.03 o 4 1 3 198.59 217.13 30.01 o 5 1 3 136.46 149.85 12.15 o 1 2 3 1029.05 900.10 101.52 o 2 2 3 53.96 43.69 4.15 o 3 2 3 122.98 107.85 15.30 o 4 2 3 1113.50 1036.03 132.59 o 5 2 3 253.46 292.94 21.43 o 0 3 3 610.04 628.66 27.80 o 1 3 3 735.24 717.82 59.97 o 2 3 3 480.90 469.46 54.28 o 3 3 3 653.60 612.50 74.47 o 4 3 3 73.75 66.29 11.46 o 1 4 3 192.33 193.41 8.65 o 2 4 3 231.88 200.03 26.09 o 3 4 3 352.27 332.24 38.41 o 4 4 3 139.16 144.00 18.06 o 0 5 3 1368.82 1476.02 23.47 o 1 5 3 148.96 158.35 6.37 o 2 5 3 299.77 305.72 19.62 o 3 5 3 0.68 3.86 5.11 o 4 5 3 43.73 52.55 6.83 o 1 6 3 700.64 793.82 21.97 o 2 6 3 37.61 36.94 4.74 o 3 6 3 209.58 189.72 16.02 o 0 7 3 134.42 145.63 7.49 o 1 7 3 125.47 136.41 5.79 o 2 7 3 382.20 370.59 15.54 o 1 8 3 79.79 85.05 6.45 o 0 0 4 296.78 261.73 11.54 o 2 0 4 571.78 470.10 10.74 o 4 0 4 34.14 30.35 11.40 o 1 1 4 63.24 56.06 6.20 o 2 1 4 394.16 355.10 36.69 o 3 1 4 90.59 71.99 6.18 o 4 1 4 32.54 33.60 7.85 o 5 1 4 258.63 258.19 19.25 o 0 2 4 970.44 903.85 67.36 o 1 2 4 396.75 356.41 45.89 o 2 2 4 589.81 547.53 61.56 o 3 2 4 134.25 137.33 21.00 o 4 2 4 207.69 184.98 27.43 o 1 3 4 98.84 97.57 12.12 o 2 3 4 847.02 793.16 87.65 o 3 3 4 726.43 640.73 82.57 o 4 3 4 119.06 116.61 14.53 o 0 4 4 99.09 102.72 11.12 o 1 4 4 1355.50 1296.52 70.23 o 2 4 4 1083.03 1029.50 96.38 o 3 4 4 174.29 169.83 22.70 o 4 4 4 29.79 30.95 7.95 o 1 5 4 748.44 803.12 20.17 o 2 5 4 183.83 201.86 15.59 o 3 5 4 337.63 290.32 27.24 o 4 5 4 58.54 54.37 13.27 o 0 6 4 277.55 273.34 20.29 o 1 6 4 177.02 186.11 7.49 o 2 6 4 279.99 291.90 19.80 o 3 6 4 226.85 220.96 20.52 o 1 7 4 270.61 292.20 9.04 o 2 7 4 608.54 618.25 18.29 o 0 8 4 285.27 296.80 19.74 o 2 0 5 2005.74 1652.91 90.94 o 4 0 5 1315.21 1065.80 302.79 o 0 1 5 66.04 91.09 6.91 o 1 1 5 1564.11 1449.20 66.91 o 2 1 5 32.98 19.31 5.73 o 3 1 5 347.05 309.06 25.51 o 4 1 5 599.36 551.61 54.63 o 1 2 5 593.35 540.06 91.78 o 2 2 5 437.76 401.75 41.24 o 3 2 5 491.93 477.81 54.16 o 4 2 5 17.03 16.67 6.16 o 0 3 5 993.01 1084.75 14.95 o 1 3 5 415.94 456.71 38.94 o 2 3 5 377.63 370.56 38.21 o 3 3 5 118.69 118.32 17.78 o 4 3 5 94.56 113.53 18.75 o 1 4 5 19.82 23.39 5.81 o 2 4 5 416.06 423.57 41.88 o 3 4 5 12.12 4.25 6.69 o 4 4 5 11.77 13.54 7.64 o 0 5 5 1693.66 1946.94 21.67 o 1 5 5 984.20 1113.24 21.89 o 2 5 5 167.70 160.90 10.59 o 3 5 5 22.55 25.08 5.97 o 1 6 5 144.20 143.65 6.15 o 2 6 5 43.83 40.25 8.83 o 0 7 5 608.45 634.36 36.46 o 1 7 5 4.89 5.84 7.18 o 0 0 6 3084.50 3654.17 35.74 o 2 0 6 1567.23 1721.74 128.69 o 4 0 6 598.00 509.64 130.09 o 1 1 6 834.66 871.53 28.14 o 2 1 6 801.74 772.86 61.36 o 3 1 6 15.75 13.04 5.02 o 4 1 6 418.43 389.50 36.99 o 0 2 6 2945.24 2881.92 508.70 o 1 2 6 899.77 805.02 179.65 o 2 2 6 196.60 168.23 22.85 o 3 2 6 523.60 542.97 62.10 o 4 2 6 247.16 227.10 32.40 o 1 3 6 542.09 605.30 52.40 o 2 3 6 571.17 521.20 47.38 o 3 3 6 468.12 466.42 53.65 o 4 3 6 412.94 410.46 53.53 o 0 4 6 1429.73 1620.43 20.10 o 1 4 6 189.83 209.28 7.27 o 2 4 6 515.34 571.36 48.87 o 3 4 6 98.31 98.09 9.65 o 1 5 6 85.90 83.25 4.97 o 2 5 6 103.59 88.45 14.21 o 3 5 6 105.68 102.29 12.31 o 0 6 6 71.42 65.88 7.21 o 1 6 6 31.57 33.85 9.53 o 2 6 6 4.32 7.80 7.20 o 2 0 7 810.95 863.88 76.96 o 4 0 7 65.00 75.46 8.18 o 0 1 7 3700.31 4543.36 35.48 o 1 1 7 214.35 274.63 7.53 o 2 1 7 376.99 404.17 25.32 o 3 1 7 102.54 114.93 9.28 o 1 2 7 279.96 296.30 55.10 o 2 2 7 480.19 484.46 42.66 o 3 2 7 246.11 245.63 32.61 o 0 3 7 1296.61 1563.86 20.48 o 1 3 7 358.94 379.03 46.00 o 2 3 7 209.99 189.32 32.64 o 3 3 7 252.22 248.76 32.95 o 1 4 7 83.25 88.30 5.06 o 2 4 7 175.85 182.02 18.64 o 3 4 7 90.97 92.04 6.10 o 0 5 7 132.94 142.07 9.32 o 1 5 7 30.11 35.16 5.24 o 2 5 7 36.77 52.43 10.39 o 1 6 7 134.52 134.02 5.93 o 0 0 8 272.65 289.51 16.33 o 2 0 8 258.43 356.12 31.54 o 1 1 8 215.36 290.38 11.66 o 2 1 8 222.11 232.47 13.02 o 3 1 8 55.09 53.11 10.34 o 0 2 8 28.02 24.08 22.81 o 1 2 8 222.45 229.41 18.62 o 2 2 8 13.16 12.39 6.73 o 3 2 8 20.94 13.12 6.99 o 1 3 8 67.38 63.88 8.14 o 2 3 8 308.89 295.01 48.11 o 0 4 8 588.15 682.13 42.62 o 1 4 8 83.75 96.78 5.48 o 2 4 8 102.92 99.26 11.24 o 1 5 8 143.72 165.90 10.08 o 2 0 9 97.12 136.25 8.24 o 0 1 9 164.47 185.72 11.58 o 1 1 9 11.56 12.58 5.88 o 2 1 9 195.12 221.38 12.35 o 1 2 9 126.67 123.23 5.64 o 2 2 9 112.61 104.64 5.70 o 0 3 9 613.23 686.16 25.64 o 1 3 9 539.21 557.24 94.82 o 0 0 10 92.96 89.68 11.50 o