#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:52:48 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181306 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/84/2238476.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238476_Fobs loop_ _publ_author_name 'Elgazwy, Abdel-Sattar S. Hamad' 'Nassar, Ibrahim F.' 'Jones, Peter G.' _publ_section_title ; Ethyl 5-amino-1-[(4-methylphenyl)sulfonyl]-1H-pyrazole-4-carboxylate ; _journal_coeditor_code CV5421 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1376 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.263 _cell_angle_gamma 90.000 _cell_length_a 6.2787 _cell_length_b 15.4361 _cell_length_c 15.2714 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.7954 _cod_data_source_file cv5421Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rassan in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65.73 86.06 1.64 o 4 0 0 621.86 587.28 6.83 o 6 0 0 1352.15 1412.24 7.38 o 1 1 0 3457.29 3291.28 18.34 o 2 1 0 628.28 588.63 3.64 o 3 1 0 250.75 309.23 1.91 o 4 1 0 67.45 56.50 1.23 o 5 1 0 294.69 317.19 2.69 o 6 1 0 36.96 39.94 0.73 o 7 1 0 103.64 99.59 1.52 o 0 2 0 181.49 181.23 2.36 o 1 2 0 163.53 162.88 0.63 o 2 2 0 123.69 158.12 1.01 o 3 2 0 1591.28 1628.90 10.24 o 4 2 0 1404.41 1334.59 15.52 o 5 2 0 1605.06 1560.37 9.47 o 6 2 0 639.94 622.07 4.24 o 7 2 0 2.40 5.16 0.42 o 1 3 0 3.11 5.33 0.16 o 2 3 0 70.51 62.72 0.59 o 3 3 0 91.31 96.09 1.13 o 4 3 0 497.42 516.23 4.76 o 5 3 0 1860.12 1824.43 11.20 o 6 3 0 888.68 886.68 4.22 o 7 3 0 81.96 90.15 1.47 o 0 4 0 1496.45 1400.51 8.20 o 1 4 0 295.82 205.57 1.11 o 2 4 0 27.98 36.21 0.64 o 3 4 0 578.77 614.79 5.33 o 4 4 0 270.24 281.58 4.19 o 5 4 0 9.11 5.46 0.31 o 6 4 0 32.39 28.84 0.73 o 7 4 0 225.80 235.98 2.60 o 1 5 0 113.85 93.21 0.83 o 2 5 0 71.36 77.75 1.06 o 3 5 0 2.43 5.09 0.27 o 4 5 0 987.64 956.25 6.64 o 5 5 0 394.12 396.76 4.15 o 6 5 0 207.12 207.57 2.11 o 7 5 0 1.30 0.90 0.23 o 0 6 0 814.17 782.02 6.60 o 1 6 0 1284.84 1347.77 4.19 o 2 6 0 547.99 653.82 3.80 o 3 6 0 61.01 56.31 0.88 o 4 6 0 97.76 93.67 0.91 o 5 6 0 156.12 149.23 1.45 o 6 6 0 8.39 5.57 0.40 o 7 6 0 1.04 0.46 0.19 o 1 7 0 392.82 383.37 2.25 o 2 7 0 2.16 3.13 0.19 o 3 7 0 176.95 167.59 1.42 o 4 7 0 469.17 450.28 2.91 o 5 7 0 10.62 8.74 0.43 o 6 7 0 56.06 56.23 1.14 o 7 7 0 0.48 0.38 0.18 o 0 8 0 10861.96 10855.67 86.36 o 1 8 0 1044.66 1057.36 6.16 o 2 8 0 4.65 3.44 0.21 o 3 8 0 176.48 182.26 1.57 o 4 8 0 198.06 190.59 1.57 o 5 8 0 84.36 74.72 1.05 o 6 8 0 371.15 374.73 2.82 o 7 8 0 0.56 0.84 0.21 o 1 9 0 188.11 207.43 1.45 o 2 9 0 403.68 381.60 2.61 o 3 9 0 85.26 83.11 0.95 o 4 9 0 6.97 10.83 0.36 o 5 9 0 61.37 55.33 0.90 o 6 9 0 103.73 95.82 1.17 o 0 10 0 160.41 159.86 1.55 o 1 10 0 1423.89 1380.77 6.79 o 2 10 0 168.32 185.95 1.59 o 3 10 0 1197.46 1174.43 5.28 o 4 10 0 219.53 217.82 1.55 o 5 10 0 2568.09 2529.63 13.17 o 6 10 0 69.21 68.66 1.00 o 1 11 0 71.15 77.07 0.87 o 2 11 0 211.39 212.77 1.24 o 3 11 0 256.70 254.51 1.44 o 4 11 0 157.96 154.74 1.25 o 5 11 0 1126.21 1155.34 5.19 o 6 11 0 9.71 7.19 0.36 o 0 12 0 1593.39 1631.82 9.76 o 1 12 0 1100.44 1118.53 4.49 o 2 12 0 555.49 564.51 2.01 o 3 12 0 296.52 297.12 1.52 o 4 12 0 86.51 91.09 0.96 o 5 12 0 24.18 23.23 0.48 o 6 12 0 303.48 318.14 2.62 o 1 13 0 131.51 133.98 1.09 o 2 13 0 605.97 618.56 3.29 o 3 13 0 148.07 152.82 1.07 o 4 13 0 102.06 99.79 0.92 o 5 13 0 18.49 15.94 0.49 o 0 14 0 149.60 128.73 1.28 o 1 14 0 3.30 4.31 0.21 o 2 14 0 464.40 444.41 2.04 o 3 14 0 295.56 297.97 1.56 o 4 14 0 547.73 582.74 4.39 o 5 14 0 56.29 54.85 0.87 o 1 15 0 115.50 120.48 0.94 o 2 15 0 226.32 224.17 1.49 o 3 15 0 5.77 5.96 0.25 o 4 15 0 81.11 80.93 0.94 o 0 16 0 1714.32 1760.23 8.75 o 1 16 0 81.13 80.03 0.77 o 2 16 0 120.82 120.35 0.92 o 3 16 0 1.52 2.40 0.16 o 4 16 0 74.24 69.22 0.86 o 1 17 0 34.59 34.48 0.50 o 2 17 0 18.02 16.62 0.32 o 3 17 0 1.31 1.66 0.16 o 0 18 0 169.49 162.47 1.70 o 1 18 0 99.51 100.20 1.33 o 2 18 0 3.61 2.78 0.21 o 1 19 0 74.00 64.14 0.89 o -7 0 1 251.67 279.31 2.91 o -5 0 1 933.68 998.86 11.81 o -3 0 1 1224.08 1316.98 8.34 o -1 0 1 6053.37 6005.21 35.96 o 3 0 1 203.57 270.09 2.53 o 5 0 1 9126.27 9398.80 84.97 o 7 0 1 305.56 334.74 4.42 o -7 1 1 513.44 562.67 4.29 o -6 1 1 652.20 629.20 3.55 o -5 1 1 690.88 692.02 4.79 o -4 1 1 1362.63 1371.84 12.64 o -3 1 1 1.73 4.46 0.26 o -2 1 1 4430.06 4148.21 25.97 o -1 1 1 1342.64 1325.18 7.65 o 0 1 1 36.45 38.72 0.29 o 1 1 1 637.84 584.47 3.20 o 2 1 1 92.08 84.10 0.67 o 3 1 1 4.94 4.25 0.24 o 4 1 1 31.84 36.02 0.87 o 5 1 1 0.15 1.98 0.33 o 6 1 1 53.99 52.82 0.86 o 7 1 1 14.55 12.95 0.55 o -7 2 1 31.41 34.39 0.95 o -6 2 1 2.17 3.49 0.26 o -5 2 1 265.72 264.73 2.41 o -4 2 1 41.89 40.26 1.04 o -3 2 1 1183.05 1260.10 7.42 o -2 2 1 3396.44 3166.04 15.91 o -1 2 1 3430.13 3415.73 11.04 o 0 2 1 1446.75 1400.20 7.19 o 1 2 1 289.91 264.17 1.27 o 2 2 1 61.11 33.93 0.52 o 3 2 1 582.05 549.01 3.89 o 4 2 1 373.02 378.54 2.46 o 5 2 1 1076.53 1072.02 4.98 o 6 2 1 867.68 863.64 4.27 o 7 2 1 0.65 1.68 0.30 o -7 3 1 99.48 97.78 1.86 o -6 3 1 1021.45 1047.35 5.02 o -5 3 1 3.38 2.86 0.21 o -4 3 1 485.06 397.35 4.60 o -3 3 1 617.64 659.61 5.25 o -2 3 1 5.90 4.84 0.20 o -1 3 1 2444.14 2353.20 9.18 o 0 3 1 6809.02 6865.15 34.11 o 1 3 1 1680.96 1690.43 8.95 o 2 3 1 33.36 17.19 0.40 o 3 3 1 44.84 42.68 0.85 o 4 3 1 166.17 172.99 1.92 o 5 3 1 12.08 10.52 0.42 o 6 3 1 61.39 58.42 0.85 o 7 3 1 89.77 85.69 1.41 o -7 4 1 15.16 18.08 0.84 o -6 4 1 353.63 358.00 3.06 o -5 4 1 120.62 121.29 1.15 o -4 4 1 1100.28 1145.54 11.49 o -3 4 1 249.31 287.03 2.42 o -2 4 1 1161.39 1157.80 5.84 o -1 4 1 1606.27 1628.30 7.75 o 0 4 1 79.10 84.90 0.51 o 1 4 1 905.91 836.34 3.26 o 2 4 1 2105.09 2102.57 14.43 o 3 4 1 316.07 310.40 1.83 o 4 4 1 961.37 972.28 10.94 o 5 4 1 417.47 421.63 4.63 o 6 4 1 2.36 2.11 0.24 o 7 4 1 0.55 1.31 0.27 o -7 5 1 2.80 2.06 0.29 o -6 5 1 656.10 666.47 3.61 o -5 5 1 2.87 3.71 0.26 o -4 5 1 313.06 291.75 2.95 o -3 5 1 219.22 195.82 1.76 o -2 5 1 956.41 1071.26 4.27 o -1 5 1 349.92 330.98 1.60 o 0 5 1 1061.41 1048.32 4.20 o 1 5 1 4012.86 4025.86 20.01 o 2 5 1 43.89 40.63 0.87 o 3 5 1 29.47 26.62 0.54 o 4 5 1 22.30 17.53 0.57 o 5 5 1 0.04 0.86 0.22 o 6 5 1 12.76 14.69 0.54 o 7 5 1 7.58 8.81 0.45 o -7 6 1 1.66 4.14 0.31 o -6 6 1 0.04 0.33 0.25 o -5 6 1 588.46 525.38 3.39 o -4 6 1 237.95 239.08 1.82 o -3 6 1 47.47 27.34 0.56 o -2 6 1 8.97 12.31 0.47 o -1 6 1 1609.75 1533.95 6.07 o 0 6 1 1065.82 1051.37 6.06 o 1 6 1 698.22 640.50 2.79 o 2 6 1 1.33 1.12 0.21 o 3 6 1 323.20 398.67 2.37 o 4 6 1 42.73 36.22 0.64 o 5 6 1 103.33 107.18 1.15 o 6 6 1 233.44 242.81 2.36 o 7 6 1 20.42 24.47 0.66 o -7 7 1 34.28 31.22 0.72 o -6 7 1 145.02 137.81 1.48 o -5 7 1 2230.13 2158.59 6.96 o -4 7 1 52.94 65.20 0.69 o -3 7 1 186.58 196.35 1.65 o -2 7 1 267.98 257.55 2.65 o -1 7 1 674.54 650.37 3.61 o 0 7 1 6.56 5.39 0.29 o 1 7 1 121.14 121.62 1.20 o 2 7 1 90.97 86.89 0.95 o 3 7 1 8.37 12.62 0.42 o 4 7 1 118.47 125.38 0.89 o 5 7 1 164.79 164.77 1.41 o 6 7 1 1.73 1.61 0.28 o 7 7 1 0.62 0.84 0.21 o -7 8 1 9.31 7.31 0.43 o -6 8 1 10.84 8.48 0.37 o -5 8 1 389.76 384.15 2.89 o -4 8 1 17.40 25.95 0.47 o -3 8 1 306.70 314.27 2.54 o -2 8 1 107.11 105.39 1.03 o -1 8 1 6.98 14.60 0.68 o 0 8 1 460.74 457.27 2.89 o 1 8 1 18.55 11.80 0.35 o 2 8 1 49.73 48.45 0.61 o 3 8 1 23.28 11.96 0.44 o 4 8 1 42.99 45.48 0.61 o 5 8 1 2643.27 2652.59 11.43 o 6 8 1 188.56 199.89 1.56 o 7 8 1 23.81 20.41 0.65 o -6 9 1 275.20 275.88 3.48 o -5 9 1 614.97 594.69 4.20 o -4 9 1 167.69 150.26 1.10 o -3 9 1 167.04 170.77 1.28 o -2 9 1 562.46 558.85 2.93 o -1 9 1 962.48 946.21 5.31 o 0 9 1 936.57 903.64 5.02 o 1 9 1 948.83 928.37 4.07 o 2 9 1 393.92 400.67 2.03 o 3 9 1 46.42 44.08 0.60 o 4 9 1 63.39 56.23 0.80 o 5 9 1 14.51 19.77 0.88 o 6 9 1 0.25 0.73 0.19 o -6 10 1 112.74 102.73 1.13 o -5 10 1 31.65 30.88 0.58 o -4 10 1 258.43 243.18 1.46 o -3 10 1 2.38 3.11 0.18 o -2 10 1 454.90 419.95 2.33 o -1 10 1 768.68 803.53 3.66 o 0 10 1 4830.15 4817.06 14.30 o 1 10 1 295.30 294.05 1.53 o 2 10 1 3.94 5.51 0.34 o 3 10 1 201.94 213.65 1.24 o 4 10 1 2042.27 1975.81 7.20 o 5 10 1 451.81 448.50 2.21 o 6 10 1 1006.43 955.73 5.60 o -6 11 1 152.07 153.18 1.69 o -5 11 1 31.27 35.34 0.64 o -4 11 1 957.48 963.40 4.10 o -3 11 1 41.17 39.69 0.56 o -2 11 1 8.42 8.18 0.25 o -1 11 1 250.05 246.10 1.53 o 0 11 1 539.47 533.35 2.36 o 1 11 1 73.88 75.43 0.82 o 2 11 1 14.13 15.45 0.31 o 3 11 1 36.53 36.73 0.57 o 4 11 1 864.70 859.17 4.07 o 5 11 1 5.93 8.11 0.32 o 6 11 1 55.58 58.67 0.92 o -6 12 1 21.54 21.38 0.53 o -5 12 1 181.03 179.34 1.49 o -4 12 1 199.89 193.06 1.31 o -3 12 1 88.47 88.06 0.85 o -2 12 1 988.49 988.16 2.77 o -1 12 1 897.68 900.78 3.71 o 0 12 1 1433.81 1438.67 6.54 o 1 12 1 855.41 865.96 3.00 o 2 12 1 257.87 257.83 1.36 o 3 12 1 556.50 568.18 2.13 o 4 12 1 794.20 793.92 6.28 o 5 12 1 5.07 6.12 0.26 o 6 12 1 74.45 70.97 1.19 o -5 13 1 451.09 456.48 4.74 o -4 13 1 0.75 1.00 0.15 o -3 13 1 31.55 31.78 0.51 o -2 13 1 178.19 174.60 1.19 o -1 13 1 1925.11 1911.98 6.88 o 0 13 1 159.54 157.89 0.93 o 1 13 1 375.40 364.17 2.16 o 2 13 1 3.30 3.44 0.19 o 3 13 1 0.41 0.98 0.16 o 4 13 1 2.52 3.00 0.22 o 5 13 1 88.26 83.07 1.15 o -5 14 1 3.21 4.52 0.27 o -4 14 1 59.49 62.39 0.64 o -3 14 1 539.17 546.32 2.78 o -2 14 1 264.22 267.93 1.55 o -1 14 1 393.53 373.15 1.61 o 0 14 1 87.69 86.01 0.78 o 1 14 1 237.54 227.09 1.25 o 2 14 1 35.85 34.81 0.50 o 3 14 1 684.01 680.50 4.28 o 4 14 1 76.47 75.65 0.86 o 5 14 1 270.40 271.80 2.49 o -5 15 1 599.99 551.95 20.85 o -4 15 1 290.77 303.56 3.78 o -3 15 1 6.63 7.04 0.25 o -2 15 1 386.91 399.73 1.98 o -1 15 1 37.97 39.95 0.56 o 0 15 1 90.89 88.90 0.75 o 1 15 1 76.66 80.00 0.75 o 2 15 1 98.82 102.02 0.82 o 3 15 1 2.17 2.74 0.25 o 4 15 1 11.99 9.71 0.28 o -4 16 1 36.86 37.98 0.82 o -3 16 1 8.77 9.56 0.26 o -2 16 1 107.15 115.50 0.85 o -1 16 1 64.81 68.63 0.73 o 0 16 1 34.84 31.85 0.49 o 1 16 1 268.32 273.71 1.39 o 2 16 1 3.63 4.07 0.20 o 3 16 1 41.51 38.20 0.55 o 4 16 1 152.39 152.45 3.15 o -3 17 1 19.57 18.40 0.45 o -2 17 1 42.17 46.74 0.56 o -1 17 1 132.57 134.42 1.00 o 0 17 1 394.78 394.78 2.42 o 1 17 1 93.05 94.56 0.89 o 2 17 1 0.14 0.65 0.17 o 3 17 1 4.51 4.15 0.23 o -2 18 1 0.58 1.02 0.14 o -1 18 1 5.94 6.52 0.24 o 0 18 1 608.07 624.14 5.61 o 1 18 1 29.08 29.03 0.49 o 2 18 1 54.64 49.89 0.74 o -1 19 1 48.32 46.52 0.67 o 0 19 1 108.04 99.81 1.29 o 1 19 1 154.45 145.68 1.52 o -6 0 2 168.45 171.27 1.85 o -4 0 2 17.09 17.54 1.01 o -2 0 2 831.85 828.31 7.01 o 2 0 2 57.28 57.01 0.90 o 4 0 2 1754.06 1503.88 16.55 o 6 0 2 1109.40 1187.96 12.75 o -7 1 2 0.25 0.57 0.24 o -6 1 2 219.49 224.87 1.56 o -5 1 2 652.56 633.83 4.61 o -4 1 2 1381.37 1411.12 11.24 o -3 1 2 416.09 433.83 2.09 o -2 1 2 932.37 813.35 3.01 o -1 1 2 7079.47 7092.38 43.92 o 0 1 2 4397.22 4466.31 22.87 o 1 1 2 729.84 698.99 3.26 o 2 1 2 68.16 55.23 0.57 o 3 1 2 3537.57 3756.66 23.94 o 4 1 2 991.43 937.77 5.55 o 5 1 2 1318.03 1266.70 7.56 o 6 1 2 77.49 74.82 1.08 o 7 1 2 99.50 98.62 1.85 o -7 2 2 106.27 116.03 1.41 o -6 2 2 194.40 181.28 1.46 o -5 2 2 3.14 1.85 0.24 o -4 2 2 1.72 0.04 0.25 o -3 2 2 1654.37 1862.76 7.39 o -2 2 2 1204.05 1366.06 4.30 o -1 2 2 5691.93 5591.61 23.11 o 0 2 2 258.59 262.95 1.07 o 1 2 2 417.12 385.80 2.02 o 2 2 2 150.13 167.81 1.39 o 3 2 2 37.51 43.05 0.79 o 4 2 2 1869.52 1871.89 10.69 o 5 2 2 157.25 161.90 1.32 o 6 2 2 983.14 969.23 5.84 o 7 2 2 218.78 241.78 3.59 o -7 3 2 386.35 411.80 3.05 o -6 3 2 59.81 62.03 0.95 o -5 3 2 885.93 947.56 8.00 o -4 3 2 23.46 21.61 0.86 o -3 3 2 404.93 526.07 3.44 o -2 3 2 11.87 11.05 0.28 o -1 3 2 30850.09 30464.93 75.86 o 0 3 2 481.07 465.84 2.45 o 1 3 2 1189.96 1116.02 3.63 o 2 3 2 240.49 220.51 1.43 o 3 3 2 259.07 318.39 2.01 o 4 3 2 176.70 177.17 1.57 o 5 3 2 260.85 285.71 2.85 o 6 3 2 1.04 0.84 0.27 o 7 3 2 97.89 102.44 1.75 o -7 4 2 0.82 0.57 0.27 o -6 4 2 176.58 178.63 1.93 o -5 4 2 2813.31 2732.29 21.46 o -4 4 2 41.94 39.00 0.83 o -3 4 2 422.15 447.65 2.70 o -2 4 2 4.84 5.49 0.29 o -1 4 2 17102.73 18178.51 73.95 o 0 4 2 3476.03 3527.92 11.76 o 1 4 2 2038.80 1871.05 8.28 o 2 4 2 895.79 872.71 6.00 o 3 4 2 3617.94 3691.89 21.44 o 4 4 2 253.42 243.86 2.98 o 5 4 2 3.02 3.63 0.27 o 6 4 2 100.42 91.83 1.31 o 7 4 2 168.45 168.74 2.04 o -7 5 2 185.04 175.23 1.77 o -6 5 2 360.23 361.20 2.50 o -5 5 2 982.39 1013.91 5.93 o -4 5 2 118.83 116.45 1.51 o -3 5 2 41.50 69.32 0.89 o -2 5 2 96.81 114.96 1.39 o -1 5 2 732.00 644.40 3.03 o 0 5 2 390.07 433.17 1.78 o 1 5 2 792.65 739.92 3.17 o 2 5 2 206.31 185.57 1.56 o 3 5 2 859.77 916.26 5.56 o 4 5 2 88.18 76.33 0.95 o 5 5 2 149.96 142.13 1.24 o 6 5 2 5.92 7.09 0.35 o 7 5 2 97.64 93.95 1.47 o -7 6 2 275.40 267.36 2.73 o -6 6 2 1383.11 1300.63 6.13 o -5 6 2 19.31 20.14 0.59 o -4 6 2 610.35 574.76 5.12 o -3 6 2 35.56 28.72 0.58 o -2 6 2 932.12 889.10 7.14 o -1 6 2 391.73 389.98 2.13 o 0 6 2 915.16 936.68 4.84 o 1 6 2 154.80 161.83 1.29 o 2 6 2 622.05 669.43 3.63 o 3 6 2 67.43 66.79 0.90 o 4 6 2 54.07 53.42 0.75 o 5 6 2 53.76 50.27 0.71 o 6 6 2 314.37 327.51 3.22 o 7 6 2 1.98 3.67 0.32 o -7 7 2 0.45 2.23 0.21 o -6 7 2 31.11 26.81 0.68 o -5 7 2 378.73 370.47 2.37 o -4 7 2 2743.18 2744.52 16.64 o -3 7 2 138.39 144.21 1.43 o -2 7 2 110.51 95.24 1.07 o -1 7 2 27.97 25.12 0.60 o 0 7 2 4294.62 4376.96 18.87 o 1 7 2 620.61 661.12 5.73 o 2 7 2 50.57 46.35 0.62 o 3 7 2 282.39 272.05 1.79 o 4 7 2 1449.10 1431.76 9.27 o 5 7 2 75.15 75.72 0.89 o 6 7 2 56.76 55.56 1.07 o 7 7 2 48.77 41.38 0.83 o -7 8 2 29.31 32.05 0.63 o -6 8 2 13.25 11.89 0.45 o -5 8 2 1.29 0.31 0.18 o -4 8 2 21.19 19.06 0.42 o -3 8 2 135.54 151.19 1.42 o -2 8 2 2.29 1.20 0.16 o -1 8 2 0.65 1.71 0.16 o 0 8 2 357.16 319.35 2.31 o 1 8 2 111.20 101.09 0.93 o 2 8 2 501.08 589.58 2.53 o 3 8 2 68.71 55.25 0.85 o 4 8 2 679.52 669.35 3.36 o 5 8 2 60.36 58.78 0.85 o 6 8 2 80.48 77.27 1.13 o 7 8 2 5.00 6.06 0.34 o -6 9 2 251.25 243.85 2.08 o -5 9 2 7.27 7.79 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