#------------------------------------------------------------------------------ #$Date: 2013-10-24 17:51:33 +0300 (Thu, 24 Oct 2013) $ #$Revision: 89414 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/85/2238502.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238502_Fobs loop_ _publ_author_name 'Damous, Maamar' 'D\'en\`es, George' 'Bouacida, Sofiane' 'Hamlaoui, Meriem' 'Merazig, Hocine' 'Daran, Jean-Claude' _publ_section_title ; 8-Hydroxyquinolin-1-ium hydrogen sulfate monohydrate ; _journal_coeditor_code HG5339 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1458 _journal_page_last o1459 _journal_volume 69 _journal_year 2013 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.068 _cell_angle_beta 106.344 _cell_angle_gamma 105.712 _cell_length_a 6.5536 _cell_length_b 8.0600 _cell_length_c 11.3369 _exptl_crystal_F_000 272.00 _reflns_d_resolution_high 0.8001 _[local]_cod_data_source_file hg5339Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' M12 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 117.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 40.25 39.55 0.57 o 2 0 0 2132.05 2013.65 10.39 o 3 0 0 969.42 952.94 6.36 o 4 0 0 16.61 15.81 0.46 o 5 0 0 312.72 308.02 7.92 o 6 0 0 29.96 31.38 1.32 o 7 0 0 1.53 1.37 0.52 o -7 1 0 20.67 18.89 3.04 o -6 1 0 82.49 78.70 1.62 o -5 1 0 66.74 61.83 1.21 o -4 1 0 10.52 9.42 0.31 o -3 1 0 55.77 48.96 0.53 o -2 1 0 1680.72 1637.03 9.95 o -1 1 0 1916.80 1775.43 16.76 o 1 1 0 216.33 205.46 1.91 o 2 1 0 316.30 289.30 2.50 o 3 1 0 28.62 28.79 0.68 o 4 1 0 667.38 684.67 13.94 o 5 1 0 240.93 254.39 3.83 o 6 1 0 209.43 201.88 3.95 o 7 1 0 12.79 11.16 1.31 o -7 2 0 19.77 16.94 1.32 o -6 2 0 14.53 12.53 0.69 o -5 2 0 17.08 17.77 0.67 o -4 2 0 1.54 0.91 0.16 o -3 2 0 281.33 289.33 2.35 o -2 2 0 67.52 45.92 1.17 o -1 2 0 1281.03 1320.86 11.70 o 0 2 0 1265.51 1236.36 6.83 o 1 2 0 365.95 334.26 3.38 o 2 2 0 7.89 7.55 0.51 o 3 2 0 1235.34 1260.07 9.18 o 4 2 0 88.76 83.27 1.73 o 5 2 0 194.58 195.63 3.71 o 6 2 0 6.02 5.26 0.71 o -7 3 0 9.64 9.66 0.75 o -6 3 0 2.73 1.97 0.33 o -5 3 0 57.13 53.85 1.12 o -4 3 0 64.01 67.10 0.95 o -3 3 0 132.01 133.12 1.18 o -2 3 0 73.19 67.13 2.29 o -1 3 0 1027.42 1074.66 6.63 o 0 3 0 225.39 211.92 2.83 o 1 3 0 16.34 14.63 0.61 o 2 3 0 32.14 37.92 0.67 o 3 3 0 145.93 145.82 1.79 o 4 3 0 0.82 0.86 0.35 o 5 3 0 26.73 25.14 1.18 o 6 3 0 0.26 0.44 0.55 o -7 4 0 39.29 39.04 1.59 o -6 4 0 15.30 14.59 0.80 o -5 4 0 23.88 23.61 0.70 o -4 4 0 123.31 126.55 1.47 o -3 4 0 376.07 383.33 2.73 o -2 4 0 25.23 32.00 0.74 o -1 4 0 405.57 424.93 3.15 o 0 4 0 0.02 0.31 0.38 o 1 4 0 0.58 1.30 0.26 o 2 4 0 0.48 0.59 0.19 o 3 4 0 2.70 2.50 0.47 o 4 4 0 0.17 0.27 0.35 o 5 4 0 51.15 50.33 2.15 o -7 5 0 22.94 21.65 1.15 o -6 5 0 192.33 196.88 2.81 o -5 5 0 91.06 94.69 1.60 o -4 5 0 280.06 279.22 4.02 o -3 5 0 13.78 23.74 0.80 o -2 5 0 593.04 571.55 5.01 o -1 5 0 1011.94 1005.69 6.06 o 0 5 0 1.44 1.33 0.35 o 1 5 0 26.59 26.44 1.39 o 2 5 0 1161.58 1185.78 17.25 o 3 5 0 180.58 181.61 2.33 o 4 5 0 260.65 263.50 6.40 o 5 5 0 2.26 1.01 0.94 o -7 6 0 144.86 152.11 3.08 o -6 6 0 25.71 25.27 1.19 o -5 6 0 0.17 0.36 0.31 o -4 6 0 42.93 43.94 1.06 o -3 6 0 130.02 122.63 1.94 o -2 6 0 427.34 431.81 3.80 o -1 6 0 19.56 19.29 0.75 o 0 6 0 568.29 561.40 7.34 o 1 6 0 0.02 0.45 0.26 o 2 6 0 744.22 743.00 6.47 o 3 6 0 39.63 41.11 1.56 o 4 6 0 0.46 -1.94 1.98 o -7 7 0 13.02 12.47 0.95 o -6 7 0 12.20 11.95 1.19 o -5 7 0 28.28 29.65 1.22 o -4 7 0 34.94 36.30 1.22 o -3 7 0 380.69 368.55 4.00 o -2 7 0 6.75 6.15 0.64 o -1 7 0 342.38 334.55 4.26 o 0 7 0 36.90 33.01 1.34 o 1 7 0 28.76 31.01 1.39 o 2 7 0 204.57 228.93 14.40 o 3 7 0 0.89 2.05 0.69 o -6 8 0 1.04 1.02 0.48 o -5 8 0 2.63 1.63 0.41 o -4 8 0 39.74 39.91 1.56 o -3 8 0 130.38 129.61 2.37 o -2 8 0 32.27 28.56 1.31 o -1 8 0 13.91 15.00 0.99 o 0 8 0 14.89 15.13 1.01 o 1 8 0 38.58 37.18 1.84 o 2 8 0 8.58 12.45 1.51 o -5 9 0 6.99 6.93 0.85 o -4 9 0 25.94 27.88 1.66 o -3 9 0 5.01 4.20 0.76 o -2 9 0 0.14 0.02 0.39 o -1 9 0 24.76 27.74 1.41 o 0 9 0 22.70 21.82 1.26 o -1 -9 1 44.35 46.57 2.68 o 0 -9 1 82.11 85.39 2.43 o 1 -9 1 9.97 10.48 0.89 o 2 -9 1 94.37 92.60 2.42 o 3 -9 1 59.39 61.65 2.07 o 4 -9 1 0.22 0.36 0.34 o 5 -9 1 41.48 39.15 1.85 o -2 -8 1 13.72 11.91 1.86 o -1 -8 1 53.51 56.76 2.22 o 0 -8 1 1.09 0.84 0.47 o 1 -8 1 24.74 22.62 1.17 o 2 -8 1 76.73 79.84 2.09 o 3 -8 1 13.81 12.05 0.91 o 4 -8 1 214.74 204.91 3.39 o 5 -8 1 45.43 46.08 1.91 o 6 -8 1 77.95 75.99 2.55 o -3 -7 1 64.10 63.44 3.11 o -2 -7 1 125.21 131.45 2.63 o -1 -7 1 117.11 123.96 2.20 o 0 -7 1 20.36 22.12 1.09 o 1 -7 1 299.50 292.86 3.90 o 2 -7 1 136.91 146.09 2.63 o 3 -7 1 292.39 291.69 5.43 o 4 -7 1 108.11 104.69 2.40 o 5 -7 1 40.37 38.68 1.64 o 6 -7 1 84.04 86.01 2.26 o -4 -6 1 2.24 1.70 0.64 o -3 -6 1 26.04 25.89 1.42 o -2 -6 1 29.44 26.56 0.95 o -1 -6 1 31.02 28.51 0.98 o 0 -6 1 16.47 15.27 0.84 o 1 -6 1 73.59 71.26 1.33 o 2 -6 1 95.95 95.19 1.58 o 3 -6 1 490.50 490.33 3.76 o 4 -6 1 59.18 58.74 1.60 o 5 -6 1 90.06 88.34 1.86 o 6 -6 1 19.76 18.33 1.03 o 7 -6 1 105.67 107.51 2.60 o -5 -5 1 13.62 14.55 2.56 o -4 -5 1 335.81 342.95 8.64 o -3 -5 1 71.47 76.47 1.37 o -2 -5 1 83.45 85.99 1.68 o -1 -5 1 0.07 0.66 0.30 o 0 -5 1 34.58 34.00 1.10 o 1 -5 1 196.08 214.84 2.20 o 2 -5 1 567.83 544.42 5.01 o 3 -5 1 231.87 245.00 2.38 o 4 -5 1 163.43 156.22 2.33 o 5 -5 1 47.53 48.45 1.06 o 6 -5 1 149.86 156.51 2.55 o 7 -5 1 190.97 203.70 3.42 o -5 -4 1 16.53 16.84 0.99 o -4 -4 1 423.55 438.70 6.75 o -3 -4 1 53.94 55.06 1.06 o -2 -4 1 4.82 5.92 0.36 o -1 -4 1 26.67 33.70 1.35 o 0 -4 1 21.48 23.66 0.84 o 1 -4 1 307.93 393.66 3.35 o 2 -4 1 579.28 592.49 3.47 o 3 -4 1 84.58 102.79 1.73 o 4 -4 1 9.87 8.84 0.37 o 5 -4 1 23.47 23.68 0.80 o 6 -4 1 25.83 27.83 1.04 o 7 -4 1 18.01 17.45 1.30 o -6 -3 1 1.01 0.48 0.43 o -5 -3 1 1.26 0.15 0.37 o -4 -3 1 147.48 151.29 2.58 o -3 -3 1 2.70 2.19 0.27 o -2 -3 1 218.53 228.46 2.72 o -1 -3 1 3.20 1.93 0.34 o 0 -3 1 0.03 0.22 0.14 o 1 -3 1 750.84 742.69 5.82 o 2 -3 1 387.54 386.23 3.37 o 3 -3 1 198.84 195.77 2.03 o 4 -3 1 202.06 195.23 2.05 o 5 -3 1 103.51 101.10 1.77 o 6 -3 1 200.00 193.67 3.84 o 7 -3 1 155.24 151.83 6.22 o -6 -2 1 20.77 20.65 1.28 o -5 -2 1 94.30 94.22 2.46 o -4 -2 1 77.89 72.73 1.69 o -3 -2 1 201.49 195.52 1.84 o -2 -2 1 54.60 42.00 0.63 o -1 -2 1 282.08 278.55 2.65 o 0 -2 1 1717.65 1764.03 16.99 o 1 -2 1 284.77 290.58 3.55 o 2 -2 1 9.83 11.03 0.48 o 3 -2 1 24.36 20.39 0.47 o 4 -2 1 3.97 4.27 0.30 o 5 -2 1 63.16 59.26 1.21 o 6 -2 1 2.67 1.62 0.43 o 7 -2 1 0.11 -0.71 0.71 o -7 -1 1 77.69 79.05 3.11 o -6 -1 1 54.89 48.38 1.87 o -5 -1 1 694.69 700.96 9.39 o -4 -1 1 73.43 74.09 1.53 o -3 -1 1 342.37 337.13 2.26 o -2 -1 1 2.07 3.52 0.17 o -1 -1 1 2418.09 2525.39 26.95 o 1 -1 1 88.66 97.42 0.92 o 2 -1 1 1.53 9.05 0.33 o 3 -1 1 293.47 278.62 2.58 o 4 -1 1 58.94 51.32 0.95 o 5 -1 1 7.94 9.64 0.55 o 6 -1 1 68.08 58.95 2.75 o 7 -1 1 0.38 1.09 0.61 o -7 0 1 111.79 108.58 2.63 o -6 0 1 133.90 130.04 2.14 o -5 0 1 5.36 6.06 0.53 o -4 0 1 646.52 648.49 7.25 o -3 0 1 325.09 355.64 2.60 o -2 0 1 1652.84 1717.60 16.12 o -1 0 1 1355.31 1333.98 23.48 o 1 0 1 1818.89 1652.59 14.73 o 2 0 1 1684.11 1603.62 6.89 o 3 0 1 267.65 247.11 2.23 o 4 0 1 18.05 16.68 0.57 o 5 0 1 425.50 420.26 5.38 o 6 0 1 23.73 23.23 1.34 o 7 0 1 14.52 18.25 2.29 o -7 1 1 44.22 41.76 1.65 o -6 1 1 3.42 3.17 0.37 o -5 1 1 541.78 524.79 4.68 o -4 1 1 725.71 699.58 3.67 o -3 1 1 7.30 4.69 0.37 o -2 1 1 13713.28 13094.87 180.34 o -1 1 1 158.67 143.56 1.08 o 0 1 1 3217.27 3123.29 17.90 o 1 1 1 313.14 300.78 3.72 o 2 1 1 35.63 23.65 0.52 o 3 1 1 156.40 167.20 1.82 o 4 1 1 6.81 7.08 0.40 o 5 1 1 3.72 3.00 0.53 o 6 1 1 14.33 13.67 1.38 o -7 2 1 6.72 5.08 0.74 o -6 2 1 2.03 2.16 0.31 o -5 2 1 147.95 137.39 1.67 o -4 2 1 78.44 92.15 1.50 o -3 2 1 251.13 271.99 1.50 o -2 2 1 5.06 5.89 0.19 o -1 2 1 423.13 412.78 2.46 o 0 2 1 202.60 220.37 2.31 o 1 2 1 10.54 17.13 0.39 o 2 2 1 0.21 0.09 0.18 o 3 2 1 46.23 52.59 1.04 o 4 2 1 532.98 546.48 6.50 o 5 2 1 0.01 0.29 0.39 o 6 2 1 44.39 53.18 2.83 o -8 3 1 0.33 -0.27 0.52 o -7 3 1 17.24 20.05 1.04 o -6 3 1 273.56 276.30 2.89 o -5 3 1 0.00 -0.08 0.19 o -4 3 1 64.18 59.41 0.96 o -3 3 1 34.55 33.23 0.80 o -2 3 1 59.07 52.31 0.86 o -1 3 1 2356.67 2300.56 16.64 o 0 3 1 364.03 381.51 4.23 o 1 3 1 126.30 117.69 1.30 o 2 3 1 19.38 16.31 0.51 o 3 3 1 65.21 69.76 1.28 o 4 3 1 70.23 64.40 1.73 o 5 3 1 0.81 0.80 0.48 o -7 4 1 160.14 169.14 3.32 o -6 4 1 6.43 5.65 0.52 o -5 4 1 7.19 6.74 0.42 o -4 4 1 0.04 0.37 0.24 o -3 4 1 390.53 428.73 3.64 o -2 4 1 910.76 919.25 6.23 o -1 4 1 453.45 467.08 3.81 o 0 4 1 34.82 44.57 1.18 o 1 4 1 58.17 58.97 0.99 o 2 4 1 38.49 39.36 0.82 o 3 4 1 90.44 86.91 1.98 o 4 4 1 6.05 6.15 0.76 o 5 4 1 11.82 10.60 1.07 o -7 5 1 72.65 69.22 2.00 o -6 5 1 30.76 32.84 1.14 o -5 5 1 346.65 366.28 7.37 o -4 5 1 100.61 97.76 1.41 o -3 5 1 578.44 574.95 5.42 o -2 5 1 237.20 243.58 2.35 o -1 5 1 401.44 389.99 4.96 o 0 5 1 65.31 60.31 1.90 o 1 5 1 9.24 8.45 0.45 o 2 5 1 0.46 0.39 0.28 o 3 5 1 141.81 145.56 4.39 o 4 5 1 74.69 73.88 2.55 o -7 6 1 109.71 107.45 2.58 o -6 6 1 218.47 222.50 3.52 o -5 6 1 57.01 60.58 1.51 o -4 6 1 324.55 325.19 4.37 o -3 6 1 421.79 427.62 3.58 o -2 6 1 41.73 41.07 1.02 o -1 6 1 104.56 111.03 3.39 o 0 6 1 578.49 575.26 8.14 o 1 6 1 260.82 265.36 5.80 o 2 6 1 110.34 106.96 3.60 o 3 6 1 4.28 3.20 0.61 o -7 7 1 22.98 22.79 1.36 o -6 7 1 0.02 -0.33 0.33 o -5 7 1 87.12 90.41 2.12 o -4 7 1 31.95 31.44 1.01 o -3 7 1 69.19 64.99 1.39 o -2 7 1 781.04 792.85 6.59 o -1 7 1 111.90 106.03 2.39 o 0 7 1 450.95 445.14 7.38 o 1 7 1 1.01 2.01 0.63 o 2 7 1 12.12 12.60 1.41 o 3 7 1 41.90 40.47 2.59 o -6 8 1 21.06 19.67 1.28 o -5 8 1 57.75 60.47 1.93 o -4 8 1 5.07 4.82 0.77 o -3 8 1 260.34 260.25 4.70 o -2 8 1 21.22 24.39 1.24 o -1 8 1 35.65 35.57 1.50 o 0 8 1 61.43 61.94 2.00 o 1 8 1 1.15 1.45 0.56 o -5 9 1 28.57 26.19 1.50 o -4 9 1 62.81 62.97 2.49 o -3 9 1 61.49 65.80 2.11 o -2 9 1 12.32 11.74 0.95 o -1 9 1 0.07 0.14 0.43 o 0 9 1 8.15 8.66 1.17 o 2 -10 2 5.72 6.55 0.82 o 3 -10 2 0.02 0.12 0.45 o -1 -9 2 5.58 4.40 0.75 o 0 -9 2 6.60 6.93 0.91 o 1 -9 2 71.27 68.50 2.10 o 2 -9 2 0.27 -0.30 0.49 o 3 -9 2 72.72 74.54 2.14 o 4 -9 2 0.01 0.56 0.39 o 5 -9 2 4.12 3.02 0.62 o -2 -8 2 276.76 293.49 5.18 o -1 -8 2 11.79 10.37 1.22 o 0 -8 2 168.65 166.61 3.07 o 1 -8 2 40.42 42.16 1.54 o 2 -8 2 7.82 11.21 0.80 o 3 -8 2 352.55 334.41 4.77 o 4 -8 2 4.84 2.92 0.50 o 5 -8 2 26.29 24.54 1.71 o 6 -8 2 1.41 0.91 0.44 o -3 -7 2 116.61 125.83 2.82 o -2 -7 2 12.04 12.73 0.74 o -1 -7 2 259.37 275.22 4.22 o 0 -7 2 23.75 22.31 1.07 o 1 -7 2 241.37 222.32 4.25 o 2 -7 2 916.90 918.48 9.05 o 3 -7 2 1.97 1.07 0.40 o 4 -7 2 339.55 328.92 4.87 o 5 -7 2 43.99 43.50 1.77 o 6 -7 2 70.98 69.93 2.37 o -4 -6 2 343.25 344.48 8.23 o -3 -6 2 77.49 80.39 1.64 o -2 -6 2 201.64 206.11 3.05 o -1 -6 2 211.01 218.46 4.46 o 0 -6 2 20.86 16.21 0.85 o 1 -6 2 705.40 714.02 9.34 o 2 -6 2 395.79 391.53 3.20 o 3 -6 2 311.70 298.02 3.03 o 4 -6 2 52.59 52.58 1.51 o 5 -6 2 86.04 88.06 1.88 o 6 -6 2 206.32 206.78 3.77 o 7 -6 2 20.39 20.84 1.35 o -5 -5 2 19.46 19.08 1.29 o -4 -5 2 121.35 125.10 2.59 o -3 -5 2 0.74 0.89 0.24 o -2 -5 2 19.22 21.82 0.69 o -1 -5 2 228.93 231.20 2.66 o 0 -5 2 106.58 100.00 1.32 o 1 -5 2 702.27 778.45 8.14 o 2 -5 2 321.20 330.21 3.82 o 3 -5 2 223.91 230.01 3.03 o 4 -5 2 69.51 66.96 1.42 o 5 -5 2 226.73 223.30 2.87 o 6 -5 2 22.69 20.26 0.93 o 7 -5 2 61.55 65.14 2.60 o -6 -4 2 140.98 138.08 3.68 o -5 -4 2 21.25 21.47 1.10 o -4 -4 2 19.70 19.79 0.85 o -3 -4 2 32.81 35.18 0.84 o -2 -4 2 37.10 34.31 0.79 o -1 -4 2 471.28 535.05 5.32 o 0 -4 2 74.99 62.31 1.16 o 1 -4 2 148.38 168.54 2.84 o 2 -4 2 375.39 344.11 3.72 o 3 -4 2 36.75 41.02 0.64 o 4 -4 2 188.19 175.77 2.07 o 5 -4 2 165.04 156.19 2.31 o 6 -4 2 37.47 33.73 1.26 o 7 -4 2 5.90 5.65 0.84 o -6 -3 2 68.55 69.01 2.31 o -5 -3 2 48.71 42.11 1.48 o -4 -3 2 16.47 18.00 0.78 o -3 -3 2 37.41 38.91 0.90 o -2 -3 2 6.12 6.58 0.35 o -1 -3 2 1228.42 1379.74 8.63 o 0 -3 2 1220.79 1300.96 8.77 o 1 -3 2 15.87 28.58 0.36 o 2 -3 2 173.69 161.83 2.35 o 3 -3 2 31.02 24.10 0.41 o 4 -3 2 20.49 22.73 0.58 o 5 -3 2 115.61 114.49 2.10 o 6 -3 2 1.15 0.56 0.40 o 7 -3 2 52.38 47.78 2.24 o -7 -2 2 22.00 21.64 1.25 o -6 -2 2 32.27 27.66 1.42 o -5 -2 2 79.01 86.70 2.31 o -4 -2 2 144.72 148.27 1.99 o -3 -2 2 48.76 45.71 0.68 o -2 -2 2 398.11 382.91 3.52 o -1 -2 2 0.15 1.58 0.14 o 0 -2 2 2569.59 2556.10 10.76 o 1 -2 2 1562.06 1557.97 16.95 o 2 -2 2 552.95 530.48 4.14 o 3 -2 2 286.38 274.38 2.27 o 4 -2 2 267.73 260.58 4.36 o 5 -2 2 385.59 387.64 6.78 o 6 -2 2 231.58 236.56 10.41 o 7 -2 2 0.01 -0.17 0.75 o -7 -1 2 2.47 2.53 0.50 o -6 -1 2 11.14 11.74 0.68 o -5 -1 2 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