#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:53:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181307 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/85/2238515.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2238515_Fobs loop_ _publ_author_name 'Fontenot, Krystal R.' 'Easson, Michael W.' 'Fronczek, Frank R.' 'Condon, Brian D.' _publ_section_title ; 1,1',4,5-Tetrahydrotrispiro[1,3,2-diazaphosphole-2,2'-[1,3,5,2,4,6]triazatriphosphinine-4',6''-dibenzo[d,f][1,3,2]dioxaphosphepine-6',6'''-dibenzo[d,f][1,3,2]dioxaphosphepine] acetone monosolvate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1491 _journal_page_last o1492 _journal_volume 69 _journal_year 2013 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.978 _cell_angle_gamma 90.000 _cell_length_a 9.4901 _cell_length_b 22.9466 _cell_length_c 13.1776 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.8274 _cod_data_source_file jj2173Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Krystal2Twin4 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 227.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2854.86 2923.56 48.49 o 2 0 0 28.89 14.44 6.19 o 3 0 0 31348.05 30501.56 521.05 o 4 0 0 132.22 89.77 10.83 o 5 0 0 1132.74 989.48 30.95 o 6 0 0 2.53 6.19 10.32 o 7 0 0 48.23 52.62 18.06 o 8 0 0 66.60 71.19 20.64 o 9 0 0 679.65 691.29 42.30 o 10 0 0 1639.67 1612.16 59.33 o 11 0 0 5.39 20.12 15.99 o 1 1 0 99.98 86.67 3.61 o 2 1 0 1703.69 1697.80 22.70 o 3 1 0 865.82 890.43 16.51 o 4 1 0 1100.39 1075.12 19.09 o 5 1 0 4204.18 4464.01 60.88 o 6 1 0 1035.46 1189.65 36.11 o 7 1 0 145.90 124.33 14.44 o 8 1 0 262.94 253.30 18.57 o 9 1 0 48.88 37.66 12.90 o 10 1 0 68.40 61.91 17.02 o 11 1 0 118.42 94.92 18.57 o 0 2 0 29620.60 28445.74 695.42 o 1 2 0 543.49 569.54 9.80 o 2 2 0 19338.48 19192.71 218.22 o 3 2 0 1003.76 976.07 15.99 o 4 2 0 161.36 187.78 8.25 o 5 2 0 1015.21 1075.12 29.92 o 6 2 0 150.03 129.49 19.09 o 7 2 0 846.26 836.78 36.63 o 8 2 0 215.36 201.71 17.54 o 9 2 0 171.75 156.83 15.48 o 10 2 0 1231.73 1278.38 35.60 o 11 2 0 933.83 971.42 39.21 o 1 3 0 4628.51 4484.64 60.36 o 2 3 0 2047.50 1820.58 30.95 o 3 3 0 100.63 101.11 7.22 o 4 3 0 170.73 110.40 10.32 o 5 3 0 3522.41 3544.69 68.61 o 6 3 0 119.33 103.69 18.57 o 7 3 0 1484.61 1349.57 38.18 o 8 3 0 364.59 360.61 25.79 o 9 3 0 63.77 68.61 13.93 o 10 3 0 1777.57 1888.68 41.27 o 11 3 0 184.26 171.79 17.54 o 0 4 0 10951.01 11376.95 338.42 o 1 4 0 4871.01 4814.81 62.42 o 2 4 0 1284.86 1309.85 15.99 o 3 4 0 5524.02 5401.38 66.03 o 4 4 0 41.72 34.05 8.77 o 5 4 0 1881.22 2002.17 50.56 o 6 4 0 209.19 182.11 23.22 o 7 4 0 609.31 581.93 27.86 o 8 4 0 438.05 510.22 24.25 o 9 4 0 97.07 94.41 13.41 o 10 4 0 269.56 336.88 32.50 o 11 4 0 10.09 25.79 18.57 o 1 5 0 3261.02 3294.48 42.30 o 2 5 0 13504.96 13249.12 136.71 o 3 5 0 20.68 17.02 5.16 o 4 5 0 2578.62 2416.44 38.18 o 5 5 0 477.16 440.57 22.70 o 6 5 0 40.66 57.78 17.02 o 7 5 0 1218.70 1217.50 51.59 o 8 5 0 255.73 231.64 19.60 o 9 5 0 24.89 23.22 11.87 o 10 5 0 569.71 637.13 37.14 o 11 5 0 0.53 0.00 17.54 o 0 6 0 3164.43 3034.47 98.02 o 1 6 0 11197.53 11709.70 142.90 o 2 6 0 0.80 3.61 3.61 o 3 6 0 1355.30 1240.20 20.12 o 4 6 0 3372.38 3474.01 51.07 o 5 6 0 879.02 864.63 34.56 o 6 6 0 136.48 117.11 27.86 o 7 6 0 353.31 369.89 26.83 o 8 6 0 558.71 597.92 26.83 o 9 6 0 5.77 3.61 13.93 o 10 6 0 356.51 402.40 32.50 o 11 6 0 496.71 549.42 39.21 o 1 7 0 3.70 4.64 4.64 o 2 7 0 1258.49 1293.34 19.09 o 3 7 0 1585.70 1657.56 28.89 o 4 7 0 3874.86 3655.61 57.26 o 5 7 0 524.25 538.07 46.95 o 6 7 0 1097.86 1062.74 67.58 o 7 7 0 98.08 92.34 19.60 o 8 7 0 1642.78 1544.58 58.30 o 9 7 0 124.15 95.96 16.51 o 10 7 0 21.27 24.76 12.90 o 0 8 0 4665.12 4715.76 150.12 o 1 8 0 4524.09 4583.70 86.67 o 2 8 0 6281.56 6926.36 109.37 o 3 8 0 3411.88 3293.97 46.43 o 4 8 0 1124.22 1287.66 29.92 o 5 8 0 1745.01 1739.07 83.57 o 6 8 0 23.65 25.79 15.99 o 7 8 0 203.13 186.75 22.70 o 8 8 0 2429.61 2344.73 73.77 o 9 8 0 1349.51 1353.18 43.85 o 10 8 0 18.63 23.22 12.38 o 1 9 0 2354.89 2448.94 50.04 o 2 9 0 15.49 12.90 7.22 o 3 9 0 5271.81 5834.73 72.22 o 4 9 0 1492.03 1499.70 32.50 o 5 9 0 697.75 676.33 26.83 o 6 9 0 17074.57 16400.71 297.67 o 7 9 0 114.71 98.54 15.48 o 8 9 0 182.34 164.57 21.67 o 9 9 0 15.51 0.00 13.41 o 10 9 0 242.29 258.98 21.15 o 0 10 0 2394.66 2316.87 83.57 o 1 10 0 855.26 821.82 26.31 o 2 10 0 2115.85 2736.29 101.63 o 3 10 0 8270.58 8543.16 185.72 o 4 10 0 872.94 959.04 25.28 o 5 10 0 966.23 1007.02 36.11 o 6 10 0 9.16 9.80 8.25 o 7 10 0 502.48 491.64 27.86 o 8 10 0 60.52 59.33 13.93 o 9 10 0 42.32 29.41 12.90 o 10 10 0 110.70 53.65 11.87 o 1 11 0 1526.80 1314.49 55.72 o 2 11 0 433.30 529.30 33.53 o 3 11 0 748.55 909.00 49.53 o 4 11 0 572.03 626.81 29.41 o 5 11 0 50.91 44.37 8.25 o 6 11 0 10091.35 9514.58 150.64 o 7 11 0 506.40 449.34 24.25 o 8 11 0 351.23 350.81 25.79 o 9 11 0 184.35 133.10 19.09 o 10 11 0 104.93 86.15 15.99 o 0 12 0 107.09 106.27 20.64 o 1 12 0 0.60 6.19 14.96 o 2 12 0 963.21 971.42 44.37 o 3 12 0 1914.77 2113.61 86.67 o 5 12 0 1971.91 1937.69 51.59 o 6 12 0 139.18 151.67 14.44 o 7 12 0 48.04 46.95 15.99 o 8 12 0 1915.75 1895.90 61.39 o 9 12 0 166.78 167.15 30.44 o 2 13 0 1610.47 1619.90 62.42 o 3 13 0 2993.42 2976.69 75.32 o 4 13 0 211.96 215.13 33.53 o 5 13 0 1544.83 1550.77 49.53 o 6 13 0 151.88 142.39 18.57 o 7 13 0 8.46 6.71 18.57 o 8 13 0 273.75 367.83 49.53 o 9 13 0 2453.51 2512.39 101.11 o 1 14 0 1500.72 1256.71 54.17 o 2 14 0 298.98 324.50 31.47 o 3 14 0 93.18 78.42 11.87 o 4 14 0 354.08 294.57 20.64 o 5 14 0 30.67 17.54 12.38 o 6 14 0 146.96 134.13 17.54 o 7 14 0 44.83 37.14 15.48 o 8 14 0 128.50 69.13 27.86 o 9 14 0 380.60 377.12 40.24 o 1 15 0 3381.25 3276.43 109.37 o 2 15 0 927.08 921.90 37.66 o 3 15 0 1026.94 956.46 25.28 o 4 15 0 0.15 4.13 6.71 o 5 15 0 453.08 460.69 21.15 o 6 15 0 2171.51 2038.80 60.36 o 7 15 0 496.06 489.07 52.62 o 8 15 0 142.90 164.05 29.41 o 9 15 0 1433.79 1502.79 42.30 o 0 16 0 41.81 54.17 14.44 o 1 16 0 1295.81 1334.10 26.83 o 2 16 0 77.60 74.29 10.32 o 3 16 0 1174.70 1246.39 26.83 o 4 16 0 484.66 472.04 20.64 o 5 16 0 816.93 723.80 31.47 o 6 16 0 325.45 245.05 42.30 o 7 16 0 285.52 279.10 45.40 o 8 16 0 1.31 21.15 11.87 o 1 17 0 840.89 852.25 21.15 o 2 17 0 1985.24 1820.58 33.02 o 3 17 0 1649.87 1657.56 26.31 o 4 17 0 617.34 548.39 21.67 o 5 17 0 2947.86 2802.32 52.11 o 6 17 0 314.11 326.56 19.60 o 7 17 0 1065.43 1134.45 37.14 o 8 17 0 30.92 14.44 20.12 o 0 18 0 268.68 264.65 19.60 o 1 18 0 11.33 14.96 5.67 o 2 18 0 65.14 64.49 7.74 o 3 18 0 78.51 73.77 8.77 o 4 18 0 456.00 447.79 21.15 o 5 18 0 2750.87 2630.01 76.87 o 6 18 0 510.15 515.38 33.53 o 7 18 0 6.76 4.13 14.96 o 8 18 0 166.47 139.29 22.70 o 1 19 0 1569.56 1601.33 22.18 o 2 19 0 2101.19 2056.86 31.99 o 3 19 0 1150.69 1201.00 22.70 o 4 19 0 2871.66 2904.47 51.07 o 5 19 0 15.20 9.29 10.83 o 6 19 0 119.48 85.64 24.25 o 7 19 0 236.73 218.74 22.70 o 0 20 0 3935.80 3898.08 65.52 o 1 20 0 103.09 107.31 9.80 o 2 20 0 425.04 469.98 14.44 o 3 20 0 24.58 15.99 8.25 o 4 20 0 62.98 34.56 11.35 o 5 20 0 2155.91 2123.92 43.85 o 6 20 0 0.54 0.52 12.38 o 7 20 0 496.23 376.08 33.53 o 1 21 0 63.91 60.88 9.80 o 2 21 0 1021.84 965.75 18.57 o 3 21 0 221.10 221.32 11.87 o 4 21 0 230.60 255.37 17.02 o 5 21 0 572.86 537.04 21.15 o 6 21 0 581.30 526.21 24.25 o 7 21 0 45.72 40.24 14.96 o 0 22 0 34.13 43.85 11.87 o 1 22 0 59.47 60.36 9.80 o 2 22 0 27.73 22.70 9.80 o 3 22 0 174.11 188.82 10.32 o 4 22 0 365.14 349.26 17.54 o 5 22 0 122.31 174.89 17.54 o 6 22 0 23.17 14.96 9.80 o 1 23 0 173.94 165.60 12.38 o 2 23 0 344.08 300.76 20.64 o 3 23 0 57.91 55.72 17.02 o 4 23 0 271.99 269.81 10.32 o 5 23 0 440.74 456.05 17.54 o 6 23 0 71.62 20.64 11.35 o 0 24 0 105.37 100.60 18.57 o 1 24 0 703.72 715.54 24.76 o 2 24 0 457.78 439.54 23.22 o 3 24 0 668.58 780.54 56.75 o 4 24 0 4.77 0.00 23.73 o 1 25 0 67.75 73.26 13.93 o 2 25 0 33.34 34.56 14.44 o 3 25 0 750.56 859.48 55.20 o 0 26 0 3.10 10.83 22.18 o 1 26 0 298.70 327.59 28.37 o 2 26 0 572.68 684.59 48.49 o 3 26 0 248.90 293.03 39.72 o 1 27 0 44.79 50.04 14.44 o 2 27 0 7.05 8.77 21.15 o -11 1 1 776.32 737.21 28.89 o -10 1 1 2387.19 2454.61 50.04 o -9 1 1 151.40 140.32 15.48 o -8 1 1 624.38 591.21 29.41 o -7 1 1 0.32 7.74 11.87 o -6 1 1 4496.27 4745.69 99.57 o -5 1 1 590.25 568.51 14.44 o -4 1 1 116.21 76.87 6.19 o -3 1 1 9495.11 9509.43 103.69 o -2 1 1 13274.13 13159.36 155.80 o -1 1 1 16098.94 16464.67 195.01 o 0 1 1 10124.13 10070.72 134.65 o 1 1 1 17381.67 17218.91 198.62 o 2 1 1 19020.12 18055.17 238.34 o 3 1 1 9419.31 9379.42 129.49 o 4 1 1 5818.13 6224.75 81.51 o 5 1 1 4.74 7.22 5.67 o 6 1 1 2667.21 2704.30 63.97 o 7 1 1 79.08 73.26 21.15 o 8 1 1 182.77 184.69 17.02 o 9 1 1 921.22 880.63 31.99 o 10 1 1 812.12 874.95 32.50 o 11 1 1 1036.14 1164.37 56.75 o -11 2 1 4.28 6.19 16.51 o -10 2 1 692.23 726.38 29.92 o -9 2 1 877.95 851.74 31.99 o -8 2 1 374.54 384.86 25.79 o -7 2 1 22.99 14.96 11.87 o -6 2 1 1868.28 2034.68 64.49 o -5 2 1 29.45 22.18 9.29 o -4 2 1 4631.91 4942.76 65.52 o -3 2 1 740.30 762.49 14.44 o -2 2 1 10960.85 11196.91 145.48 o -1 2 1 8764.80 9083.30 122.78 o 0 2 1 1897.69 1990.82 30.95 o 1 2 1 26508.86 25911.16 347.19 o 2 2 1 51665.30 51589.14 583.47 o 3 2 1 16.29 4.64 4.64 o 4 2 1 848.06 816.14 17.54 o 5 2 1 21.36 10.83 9.29 o 6 2 1 214.79 187.27 23.22 o 7 2 1 1187.09 1216.99 53.14 o 8 2 1 27.80 27.86 12.90 o 9 2 1 111.38 117.11 17.02 o 10 2 1 0.02 11.35 11.87 o 11 2 1 127.77 190.88 42.82 o -11 3 1 71.80 66.03 13.93 o -10 3 1 810.81 805.82 26.83 o -9 3 1 74.56 85.12 13.93 o -8 3 1 214.10 199.13 18.06 o -7 3 1 101.07 81.51 12.38 o -6 3 1 637.53 545.81 33.53 o -5 3 1 16.68 13.41 8.77 o -4 3 1 180.30 185.72 15.48 o -3 3 1 455.34 439.54 14.44 o -2 3 1 1661.42 1196.87 23.73 o -1 3 1 6066.10 5846.60 73.26 o 0 3 1 3100.65 3111.34 47.46 o 1 3 1 386.81 419.94 7.74 o 2 3 1 4570.05 4506.83 60.36 o 3 3 1 5732.02 6067.40 85.64 o 4 3 1 3897.51 3889.82 72.74 o 5 3 1 2633.10 2951.41 69.13 o 6 3 1 1461.16 1479.58 54.17 o 7 3 1 570.82 576.25 32.50 o 8 3 1 20.56 18.57 12.38 o 9 3 1 102.53 107.31 13.93 o 10 3 1 399.07 450.37 21.67 o 11 3 1 61.04 80.99 17.54 o -11 4 1 768.87 823.36 33.02 o -10 4 1 325.24 394.14 27.86 o -9 4 1 234.69 199.13 17.54 o -8 4 1 2167.44 2034.68 42.82 o -7 4 1 8.69 6.19 11.35 o -6 4 1 1086.55 1011.15 34.05 o -5 4 1 1475.30 1518.78 32.50 o -4 4 1 493.42 512.28 17.54 o -3 4 1 1339.61 1363.50 27.34 o -2 4 1 3192.18 3516.32 52.62 o -1 4 1 6008.04 6142.72 77.38 o 0 4 1 550.02 512.28 9.80 o 1 4 1 36416.12 37006.96 445.73 o 2 4 1 17394.08 17332.92 189.85 o 3 4 1 300.11 415.29 13.41 o 4 4 1 8073.08 7850.83 135.16 o 5 4 1 0.24 6.19 12.90 o 6 4 1 5.28 17.02 14.44 o 7 4 1 3.65 8.25 13.93 o 8 4 1 31.47 17.54 10.83 o 9 4 1 81.86 68.61 13.41 o 10 4 1 78.01 65.00 17.54 o 11 4 1 1.39 10.32 15.48 o -11 5 1 24.10 23.73 18.06 o -10 5 1 445.55 459.66 35.60 o -9 5 1 682.22 666.02 26.83 o -8 5 1 14.47 14.96 11.35 o -7 5 1 1351.92 1284.57 52.62 o -6 5 1 38.90 37.14 12.38 o -5 5 1 2246.64 2258.57 52.62 o -4 5 1 887.48 889.91 18.57 o -3 5 1 220.53 214.09 9.29 o -2 5 1 10159.16 10747.57 143.42 o -1 5 1 31.69 23.22 4.13 o 0 5 1 917.27 1041.07 13.93 o 1 5 1 7954.42 8387.36 88.73 o 2 5 1 9318.56 9147.79 89.77 o 3 5 1 14.08 6.71 4.64 o 4 5 1 502.84 517.44 19.09 o 5 5 1 1957.77 1967.09 61.39 o 6 5 1 391.23 387.43 47.46 o 7 5 1 1470.82 1352.67 41.79 o 8 5 1 1417.42 1399.61 37.66 o 9 5 1 23.37 28.89 11.35 o 10 5 1 26.67 7.22 14.96 o 11 5 1 0.19 9.80 15.99 o -11 6 1 1503.74 1490.93 62.42 o -10 6 1 31.77 21.15 16.51 o -9 6 1 147.68 116.08 17.02 o -8 6 1 4881.71 4714.73 83.57 o -7 6 1 44.49 41.79 17.54 o -6 6 1 625.60 600.50 33.53 o -5 6 1 3490.87 3394.57 71.19 o -4 6 1 386.02 387.95 13.41 o -3 6 1 352.62 388.47 11.35 o -2 6 1 23565.03 24482.14 270.84 o 0 6 1 2371.00 2209.05 27.34 o 1 6 1 12431.71 12504.69 120.72 o 2 6 1 576.73 498.35 10.32 o 3 6 1 55.44 37.14 6.19 o 4 6 1 1849.71 1681.81 35.60 o 5 6 1 0.83 2.58 10.83 o 6 6 1 1238.70 1174.17 43.33 o 7 6 1 143.73 123.81 15.48 o 8 6 1 1489.41 1434.69 38.18 o 9 6 1 45.32 13.41 14.96 o 10 6 1 18.29 7.74 14.44 o -11 7 1 250.36 234.73 31.47 o -10 7 1 870.68 913.13 34.56 o -9 7 1 2607.88 2663.03 65.00 o -8 7 1 0.19 6.19 15.99 o -7 7 1 2204.06 2269.41 71.19 o -6 7 1 730.05 704.71 56.75 o -5 7 1 0.03 21.67 13.41 o -4 7 1 4556.90 4734.34 71.71 o -3 7 1 9.21 7.74 5.67 o -2 7 1 2111.87 2280.76 30.95 o -1 7 1 3.98 7.74 5.16 o 0 7 1 1584.64 1636.41 23.73 o 1 7 1 2118.61 2535.61 33.53 o 2 7 1 6323.63 6310.90 76.87 o 3 7 1 2658.81 2666.64 48.49 o 4 7 1 37.26 19.60 7.74 o 5 7 1 3974.78 3934.70 150.12 o 6 7 1 64.22 63.97 14.44 o 7 7 1 8.65 24.76 17.02 o 8 7 1 997.84 861.54 44.88 o 9 7 1 154.57 155.28 18.57 o 10 7 1 922.73 883.21 31.99 o -10 8 1 201.97 195.52 18.57 o -9 8 1 148.97 132.07 17.54 o -8 8 1 1971.33 1893.32 64.49 o -7 8 1 1359.60 1341.32 52.62 o -6 8 1 774.12 745.46 40.76 o -5 8 1 1145.11 1108.13 34.56 o -4 8 1 4338.10 4405.20 67.07 o -3 8 1 3222.51 3310.48 50.56 o -2 8 1 104.16 139.81 8.77 o -1 8 1 15.34 16.51 7.74 o 0 8 1 1579.12 1526.52 31.99 o 1 8 1 1397.15 1408.90 38.69 o 2 8 1 981.45 913.13 15.99 o 3 8 1 290.71 353.39 12.38 o 4 8 1 743.66 939.95 24.76 o 5 8 1 1132.61 1040.55 63.45 o 6 8 1 46.65 21.67 12.90 o 7 8 1 3728.68 3531.79 96.99 o 8 8 1 906.64 812.53 43.33 o 9 8 1 1083.04 1125.16 39.72 o 10 8 1 5.50 21.67 11.87 o -10 9 1 26.78 18.06 11.87 o -9 9 1 285.21 312.63 26.83 o -8 9 1 2541.47 2482.47 75.32 o -7 9 1 4436.43 4325.23 90.80 o -6 9 1 403.20 338.94 26.31 o -5 9 1 1973.48 1992.37 62.42 o -4 9 1 257.63 266.20 12.90 o -3 9 1 270.76 257.43 10.83 o -2 9 1 3.63 0.00 9.29 o -1 9 1 201.31 171.79 12.90 o 0 9 1 232.96 248.14 26.83 o 1 9 1 2403.08 2801.81 69.13 o 2 9 1 159.93 127.43 9.29 o 3 9 1 10320.57 10918.33 144.45 o 4 9 1 1051.70 1052.93 23.22 o 5 9 1 1820.93 1771.57 45.91 o 6 9 1 1343.78 1349.06 42.82 o 7 9 1 120.76 113.50 19.09 o 8 9 1 1197.46 1226.27 51.07 o 9 9 1 21.04 29.92 13.41 o 10 9 1 24.03 30.95 11.87 o -10 10 1 351.97 342.04 26.31 o -9 10 1 20.97 9.29 11.35 o -8 10 1 282.48 276.52 22.70 o -7 10 1 1377.64 1338.74 41.27 o -6 10 1 651.55 617.01 26.83 o -5 10 1 4211.58 4372.18 104.73 o -4 10 1 1568.73 1761.77 39.21 o -3 10 1 4157.60 4720.41 87.19 o -2 10 1 974.37 1237.62 38.18 o -1 10 1 2378.11 2546.44 45.40 o 0 10 1 8234.02 8114.46 253.82 o 1 10 1 3473.14 3916.13 93.38 o 2 10 1 1131.36 1356.79 40.76 o 3 10 1 2113.96 2437.07 42.82 o 4 10 1 15.19 27.34 8.25 o 5 10 1 5318.71 5462.77 107.31 o 6 10 1 180.55 173.34 12.38 o 7 10 1 4285.66 4103.92 87.19 o 8 10 1 536.33 547.36 29.92 o 9 10 1 19.22 10.83 14.96 o 10 10 1 53.53 35.08 15.48 o -10 11 1 372.62 413.74 29.41 o -9 11 1 217.54 196.55 17.54 o -8 11 1 270.95 278.58 24.25 o -7 11 1 33.34 10.32 11.35 o -6 11 1 2137.65 2095.04 42.82 o -5 11 1 2634.02 2682.64 66.55 o -4 11 1 376.64 477.20 26.83 o -3 11 1 1883.22 1906.73 54.68 o -2 11 1 2528.34 2799.74 104.21 o -1 11 1 589.97 644.86 18.57 o 0 11 1 62.38 45.91 17.02 o 1 11 1 40.15 27.34 6.71 o 2 11 1 1157.55 1506.92 44.37 o 3 11 1 1.61 15.48 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